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The degree of corrosion of stainless steel bar increased with increase of strain level.
The mechanical properties of stainless steel bar had an obvious degradation with increase of degree of corrosion.
The strain level ( 1.0 10 3) had no signiÞcant effect on mechanical properties of stainless steel bar within 15% corrosion degree.
Article history: This paper presents an experimental investigation into the corrosion of stainless steel bar in the stressed state. By performing
Received 13 April 2017 an electrochemical accelerated corrosion test on S11203 stainless steel bar under different strain levels and a tensile test on
Received in revised form 14 August 2017 corroded stainless steel bar, effect of strain level on corrosion of stainless steel bar was investigated. The experimental results
Accepted 18 November 2017 indicated that strain level affected the degree of corrosion of stainless steel bar. The higher the strain, the higher the degree of
3
corrosion. The degree of corrosion of stainless steel bar under a strain of 1.0 10 was 9 percent higher than that of under zero
strain. With increase of the degree of corrosion, the yield strength, ultimate strength and elon-gation of stainless steel bar
Keywords: gradually degenerated, and especially signiÞcant for the degradation of elon-gation. It was also found that the inßuence of
Corrosion of stainless steel bar
Strain level strain level ( 1.0 10 3) on corrosion morphology and mechanical properties of stainless steel bar within 15% corrosion degree
An electrochemical accelerated corrosion test was not signiÞcant.
https://doi.org/10.1016/j.conbuildmat.2017.11.102 0950-
0618/ 2017 Elsevier Ltd. All rights reserved.
190 X. Wu et al. / Construction and Building Materials 163 (2018) 189–199
of reinforcement. The stainless steel bar has more excellent corro-sion The purpose of this paper is to study the effect of different strain levels on
resistance because much denser passive Þlms can be formed on its surface corrosion of stainless steel bar. Test specimens were made of ferrite stainless
[16]. The salt-spray corrosion comparative tests of 2205 and 2304 stainless steel bar, which was due to the fact that the price of ferrite stainless steel bar
steel bar and ordinary reinforcement indi-cate that, the corrosion amount of was much cheaper than other stainless steel bars, and the ferrite stainless steel
ordinary reinforcement is greater than stainless steel bar at the same corrosion bar with high strength, low thermal expansion and high temperature resistance
condition, corrosion leads to the degradation of strengths and ductility of was widely applied in concrete structures. In this paper, an electro-chemical
ordinary reinforcement but without affecting mechanical proper-ties of accelerated corrosion test under different strain levels and a uniaxial tensile
stainless steel bar [18]. The study of Xu et al. [19] indicates that uniform test of corroded stainless steel bar were designed to study the impact of strain
pitting corrosion is main corrosion morphology of stainless steel bar in the on corrosion and mechanical properties of stainless steel bar.
coupling environment of chloride ion and current. In addition to the external
environmental factors, the composition, manufacturing processes and surface
appearance of stainless steel bar can also affect the corrosion behavior of
stain-less steel bar [20Ð23]. 2. Experimental study
Table 1
The chemical components and mechanical properties for the stainless steel bar.
thread thread
where m is initial mass of corroded section; r is the radius of the rebar (0.8 deformed. The constant tensile strain was applied by tightening Nut B. The
cm); q is the density of iron (7.8 g/cm3); l is the length of corroded section target value of the strain was realized by the control of strain gauges and
(50 cm). pressure sensor.
If the current intensity and the energizing time are known, the theoretical
corrosion degree of the stainless steel bar can be calcu-lated according to 2.3. Connections of circuit
FaradayÕs law. Assuming that 5 days, 10 days and 15 days of energizing time
correspond to 5%, 10%, and 15% the-oretical corrosion degree, the current 3.5% NaCl solution was prepared in each tank of the concrete reaction
intensity calculated by Fara-dayÕs law is 0.156 A. Under each speciÞc strain frame, as shown in Fig. 4. The closed circuit was formed by connecting
and energizing time, the electrochemical accelerated corrosion test was graphite rods to the negative pole of the power and rebars to the positive pole
conducted on 5 specimens to ensure the accuracy and comparability of exper- of the power. The DC power in the corrosion test had constant current output,
iment results. In addition, there are 5 non-corroded specimens as a and the energizing time was set to 10 days, 20 days and 30 days.
comparison group. The number and quantify of specimens are listed in Table
2.
2.4. Measurement of corrosion degree
2.2. Applying tensile strain Before applying strain, the mass of the specimen was measured and
recorded as M0. After the corrosion test was completed, the specimen was
In order to apply tensile strain to the stainless steel bar and carry out the cleaned in 12% hydrochloric acid solution and then washed in lime water and
corrosion test, a concrete reaction frame with solu-tion tanks was designed, as dried in the desicca-tor later. Meanwhile, the mass of the specimen was
shown in Fig. 2. weighed and recorded as M1.Finally, the specimen was cut into three sections
A constant tensile strain was applied to the specimen by the tensioning from the junction between non-corroded section and corroded section, as
shown in Fig. 1. Two sections at both ends of the spec-imen were weighed
device shown in Fig. 3. The tensioning device was mainly composed of a
jack, a connecting sleeve, backing plates and nuts. Before applying strain, the and recorded as M2. The average corrosion degree in the corroded section of
specimen was passed through the hole of concrete reaction frame, Þxed by the the specimen, gs, can be determined by Eq. (3).
backing plates and nuts. Strain gauges are pasted on the middle section of the
speci-men to gain the tensile strain of the specimen. When the jack was
tensioned, the screw arbor and the connecting sleeve moved outside, which
caused nut B to loosen and made the rebar M0 M1 100% 3
gs ¼
M0 M2 ðÞ
Table 2
Details of test specimens.
Note: Xd-Y = corrosion time of X days under a tensile strain of Y 10 3. For example, 10d-0.5 = corrosion time of 10 days under a tensile strain of 0.5 10 3.
gs can reßect the average loss of cross-sectional area of the corroded stainless steel 2.5. Uniaxial tension test
bar, but it canÕt directly reßect the inßuence of the local corrosion pits. If
signiÞcant corrosion pits on the surface of the stainless steel bar are found, the The uniaxial tensile test was carried out according to the spec-iÞcation
maximum loss ratio of sectional area is suggested to be used, instead of the loss (GB/T 228.1-2010, China). The test process involved plac-ing the corroded
ratio in weight, to express the mechanical properties of corroded stainless steel bar. section of the specimen in the testing machine, slowly extending it until it
The determination of the maximum loss ratio of sectional area usually involves fractured and observing the fracture pattern. During this process, the data
measuring the size of the corrosion pits by using the microm-eter, but it is difÞcult acquisition system automat-ically recorded the extensometer data and the
to accurately measure the size of the local corrosion pits in engineering practice. load- deformation curve.
The results of the paper show that corrosion morphology of the ferrite stainless
steel bar is relatively uniform and pitting corrosion isnÕt signif-icant. In view of
the above-mentioned facts, it is reasonable to use the mass loss rate to indicate the 3. Results
corrosion degree of the specimen in the test.
3.1. Corrosion morphology
Þrst occurred on the surface of the stainless steel bar. With increase of the with increase of strain level, which indicated that strain level affected the
corrosion time from 10 days to 30 days, the depth of the corrosion pits corrosion degree of stainless steel bar. The evaluation of the impact of strain
slightly increased, the areas of corrosion expanded little by little, and on corrosion degree of the stainless steel bar will be discussed more
transverse and longitudinal ribs grad-ually disappeared. Overall, the depth of speciÞcally in the section below.
local corrosion pits was rel-atively shallow, and the corrosion morphology
was relatively uniform. The experimental results also indicated that there was 3.3. Efficiency of current
no obvious difference in the corrosion morphology of the specimen during the
same corrosion time under different strain levels. In order to compare the deviance between experimental corro-sion degree
and theoretical corrosion degree calculated by Fara-dayÕs law, one
parameter, the efÞciency of current, can be deÞned by Eq. (4).
3.2. Degree of corrosion
Efficiency ¼ WG 100% 4
Corrosion degrees of specimens under each speciÞc strain and corrosion
period were obtained, and the mean values are shown in Table 3. WF ðÞ
where WG is the experimental mass loss of the specimen and WF is the
The experimental results of corrosion degrees under different strain levels theoretical mass loss of the specimen.
are shown in Fig. 6. It can be seen that corrosion degree increased as The results of efÞciency of current are listed in Table 4.
corrosion time increased under the same strain level, but corrosion rate It can be seen that the efÞciency of current varied from 86.8% to
gradually decreased with time. During the same corrosion period, corrosion 98.4%. The results indicated the efÞciency of current lower than
degree of the specimen increased 100%, which was extremely normal. The phenomenon can be
Table 3
Corrosion degrees of specimens.
Strain level 10 d
0 10 3
0.5 10 3 4.52%
1.0 10 3 4.73%
(%) load
degr
eecorrosion
4
time (d)
3.4. Mechanical properties of corroded stainless steel bar corrosion degree ηs(%)
Fig. 8. Ultimate load of the specimen.
The mechanical properties of the corroded specimen, such as yield
strength, ultimate strength and elongation, were obtained by the uniaxial
tensile test. The experimental results of corroded specimens are shown in f Fuc au Fu0 ð1 bugsÞ Fu0 1 1:775gs f 6
Figs. 7Ð9.
The mathematical relationships between mechanical properties and ¼
uc Ac ¼ ð1 gsÞ A0 ¼ ð1 gsÞ A0 ¼ ð1 gsÞ u0 ðÞ
corrosion degree of stainless steel bar were established to determine the dc
impact of corrosion on mechanical properties of stainless steel bar. The
mathematical formulas (Eqs. (5)Ð(7)) were given by Þtting the test data.
ae ¼ d0 ¼ 1 begs ¼ 1 3:714gs ð7Þ
where f yc , f uc denote effective yield strength and effective ultimate strength
of corroded stainless steel bar, respectively; f y0, f u0 denote yield strength and
f Fyc ay Fy0 ð1 bygsÞ Fy0 1 1:625gs f 5 ultimate strength of non-corroded stainless steel bar, respectively; Fyc , Fuc
¼ and dc denote yield load, ultimate load and elongation of corroded stainless
yc Ac ¼ ð1 gsÞ A0 ¼ ð1 gsÞ A0 ¼ ð1 gsÞ y0 ð Þ steel bar, respectively; Fy0, Fu0 and
Table 4
The efÞciency of current.
Strain level Energizing time (days) Theoretical corrosion (%) Experimental corrosion (%) Current efÞciency (%)
0 10 5 4.34 86.8
20 10 9.13 91.3
30 15 13.10 87.3
0.5 10 3 10 5 4.52 90.4
20 10 9.45 94.5
30 15 13.67 91.1
1.0 10 3 10 5 4.73 94.6
20 10 9.84 98.4
30 15 14.42 96.1
X. Wu et al. / Construction and Building Materials 163 (2018) 189–199 195
24
elongation data
22 elongation line
20
(%)
18
on
ga
tio
el
12
n
10
8
6 (a) ηs =8.58%.
0 2 4 6 8 8.6 10 12 14 16
corrosion degree ηs(%)
4. Discussion change with the cor-rosion time. Therefore, the mean of Kgs under different
corrosion time in Table 5 can be used for Þtting the relationship between Kg s
4.1. Effect of strain level on corrosion degree and strain level e, obtaining Eq. (9).
The strain inßuence coefÞcient of gs, Kgs, is deÞned by Eq. (8), which g
K s ¼ 1 þ 70e þ 2:0 104e2 ð9Þ
can be used for evaluating the extent of the impact on gs by the strain.
The value of Kgs calculated by Eq. (9) under a strain of 0.5 10 3 was 4
g percent higher than that of under zero strain, and the value of Kgs under a
sx
g
strain of 1 10 3 was 9 percent higher than that of under zero strain, which
g indicated that higher strain level can accelerate the corrosion of stainless steel
Ks ¼ s0 ð8Þ bar. The theory about rupture and repair of the passive Þlm can be used to
where gsx, gs0 denote the corrosion degree of the specimen under a nonzero explain the phenomenon. The tensile strain can cause the passive Þlm on the
strain and zero strain in the same period, respectively. metal surface to rupture at the weak site and then make the metal substrate
The values of Kg are listed in the Table 5. Fig. 11 shows the Þtted curves
s exposed. Since the potential of the metal substrate is lower than that of the
passive Þlm, a galvanic cell is formed
for describing the relationship between Kgs and strain level e.
196 X. Wu et al. / Construction and Building Materials 163 (2018) 189–199
Table 5
g
Strain inßuence coefÞcient of corrosion degree K s .
Strain level 10 d 20 d 30 d Mean Variation coefÞcient
0 10 3 1.000 1.000 1.000 1.000 0.000
0.5 10 3 1.041 1.035 1.044 1.040 0.004
1.0 10 3 1.090 1.078 1.101 1.090 0.011
0.98
1.10 corrosion time of 10 days
corrosion time of 20 days 0.97
corrosion time of 30 days
1.08 averange level corrosion 0.96
corrosion time of 10 days
0.95
corrosion time of 20 days
1.06
corrosion time of 30 days
S
η
0.94
ys
K
1.04
K
0.93
KηS=1+74ε+1.6×103ε2
0.92
1.02 KηS=1+62ε+1.6×103ε2
KηS=1+75ε+2.6×103ε2 0.91
η 3 2
1.00 K S=1+70ε+2.0×10 ε 0.90
0.89
0.0 2.0x10-4 4.0x10-4 6.0x10-4 8.0x10-4 1.0x10-3
-4 -4 -4 -4 -3
ε 0.0 2.0x10 4.0x10 6.0x10 8.0x10 1.0x10
strain level ε
g
Fig. 11. The relationship between K s and e.
Fig. 12. Variation of Ksy .
between the metal substrate and the passive Þlm. The electro-chemical
reaction can accelerate the dissolution of the anode metal and make more
metal substrateÕs areas exposed, meanwhile, a new passive Þlm will be
formed on the surface of the exposed metal substrate in the corrosive solution
due to passivation actions. Newly formed passive Þlm is ruptured again under
0.96
tensile strain and the cycle continues, accelerating the corrosion process [31Ð
34]. corrosion time of 10 days
corrosion time of 20 days
0.94
corrosion time of 30 days
4.2. Effect of strain level on mechanics properties of corroded stainless steel
0.92
bar
s
Ku
The strain inßuence coefÞcients of mechanics properties, such as Ksy, Kus 0.90
and Kes, are deÞned by Eqs. (10)Ð(12), which can be used for evaluating the
extent of the impact on mechanics properties by the strain. 0.88
f
y yx
0.86
f 0.0 2.0x10-4 4.0x10-4 6.0x10-4 8.0x10-4 1.0x10-3
Ks ¼ y0 ð10Þ
f strain level ε
u ux
f
Ks ¼ u0 ð11Þ Fig. 13. Variation of Ksu .
Table 6
Strain inßuence coefÞcients of Ksy , Ksu and Kse :.
0.9 steel bar by the strain. It is generally considered that the degree of corrosion is
directly correlated to mechanical perfor-mances. In consideration of the above
mentioned factors, an indirect method to predict the effect of strain level on
0.8 the mechanical performances of stainless steel bar was proposed. When strain
corrosion time of 10 days
corrosion time of 20 days level was known, the real degree of corrosion can be obtained by Eq. (9), and
corrosion time of 30 days then the yield strength, ultimate strength and elongation can be assessed and
0.7
predicted based on the relationship between mechanical performances of
e
Ks
corroded stainless steel bar and degree of corrosion (Eqs. (5)-(7)).
0.6
0.5
Table 7
Comparison of authorsÕ results with those of other researchers.
Researcher Bar type Corrosion condition Number Diameter (mm) Yield strength Ultimate strength Elongation
ay ¼ 1 by gs au ¼ 1 bu gs ae ¼ 1 be gs
Authors Bare bars Accelerated D16-S 16 1.625 1.775 3.714
Zhang et al. [35] Bars in concrete Natural D6.5-A 6.5 1.12 1.36 Ð
Lee HS and Cho YS [36] Bars in concrete Accelerated D13-295 13 1.20 1.11 2.11
D13-345 13 1.28 1.03 1.76
AA Almusallam [37] Bars in concrete Accelerated D6 6 Ð 1.28 Ð
D12 12 Ð 1.08 Ð
Yuan et al. [38] Bare bars Accelerated D12-B 12 1.07 Ð Ð
AHC Chan et al. [39] Bare bars Accelerated R08 16 Ð Ð 3.40
R16 32 Ð Ð 2.40
900 1. The strain level affected the degree of corrosion of stainless steel bar. The
D16-S higher the strain, the higher the degree of corro-
800 D6.5-A sion. The degree of corrosion of the specimen under a strain of 1.0 10 3
D13-295
700 was 9 percent higher than that of under zero strain. The degree of
D13-345
strength(
αy=1-1.625ηs corrosion of the stainless steel bar under service load can be predicted and
MPa)
D12-B
600 αy=1-1.28ηs
modiÞed by Eq. (9).
2. The yield strength, ultimate strength and elongation of cor-roded stainless
500
steel bar had an obvious degradation with increase of degree of corrosion,
αy=1-1.20ηs
400 especially the degradation of the elongation. When the degree of corrosion
yield
D13-295
700 αu=1-1.28ηs D13-345 were higher than those of ordinary steel bar. However, even if the degree
a)
400
D6 of corrosion reached 25%, nominal strength of stainless steel bar were
600
D12 generally higher than most ordinary steel bar.
500
ultimate
αu=1-1.08ηs
200 αu=1-1.11ηs Due to time and budget constraints, the corrosion test was only conducted
300 αu=1-1.03ηs on the S11203 stainless steel bar with a diameter of 16 mm, and the
deformations of the specimens in the test are all elas-tic deformations. In later
research, different types and sizes of stainless steel bars can be selected to
αu=1-1.36ηs
100 prove the suitability of the conclusion, and the impact of the plastic
deformation on corrosion of stainless steel bar should also be considered.
0
0 10 20 30 40 50 60
corrosion degree ηs(%)
(b) The degradation coefficient of ultimate strength. Acknowledgments
αe=1-2.11ηs R12
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