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ANALYTICAL REPORT

March 13, 2019

Terracon - Austin, TX
Sample Delivery Group: L1075168
Samples Received: 03/04/2019
Project Number: 96187C01
Description: Boundary Ventures, Inc.

Report To: Brian Mann


5307 Industrial Oaks, Suite 160
Austin, TX 78735

Entire Report Reviewed By:


[Preliminary Report]
Chris McCord
Jason Romer
Project Manager

Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.

12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com


TABLE OF CONTENTS ONE LAB. NATIONWIDE.

Cp: Cover Page 1 1


Cp
Tc: Table of Contents 2
2
Ss: Sample Summary 4 Tc
Cn: Case Narrative 11
3
Tr: TRRP Summary 12 Ss
TRRP form R 13 4
Cn
TRRP form S 15
5
TRRP Exception Reports 16 Tr
Sr: Sample Results 17
6
MW-1 L1075168-01 17 Sr
MW-2 L1075168-02 19 7
Qc
MW-3 L1075168-03 21
8
MW-4 L1075168-04 25 Gl
MW-5 L1075168-05 27
9
MW-6 L1075168-06 29 Al
MW-7 L1075168-07 31 10
Sc
MW-8 L1075168-08 33
MW-9 L1075168-09 35
MW-10 L1075168-10 37
MW-11 L1075168-11 39
MW-12 L1075168-12 41
MW-13 L1075168-13 45
PSW-1 L1075168-14 49
PSW-2 L1075168-15 53
PSW-3 L1075168-16 57
PSW-4 L1075168-17 61
SK-1 L1075168-18 65
DUPLICATE 1 L1075168-19 69
PS-1 L1075168-20 73
PS-2 L1075168-21 77
PS-3 L1075168-22 81
PS-4 L1075168-23 85
PS-5 L1075168-24 89
Qc: Quality Control Summary 93
Gravimetric Analysis by Method 2540 C-2011 93
Total Solids by Method 2540 G-2011 96
Wet Chemistry by Method 2320 B-2011 98
Wet Chemistry by Method 300.0 99
Wet Chemistry by Method 9040C 101
Wet Chemistry by Method 9050A 103

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 2 of 161
ONE LAB. NATIONWIDE.

Wet Chemistry by Method 9050AMod 104 1


Cp
Wet Chemistry by Method 9056A 105
2
Mercury by Method 7470A 106 Tc
Mercury by Method 7471A 107
3
Metals (ICP) by Method 6010B 108 Ss
Metals (ICPMS) by Method 6020 109 4
Cn
Volatile Organic Compounds (GC) by Method 8021B 111
5
Volatile Organic Compounds (GC/MS) by Method 8260B 114 Tr
Volatile Organic Compounds (GC/MS) by Method 8260C 126
6
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 134 Sr
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 138 7
Qc
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 145
8
Gl: Glossary of Terms 155 Gl
Al: Accreditations & Locations 157
9
Sc: Sample Chain of Custody 158 Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 3 of 161
SAMPLE SUMMARY ONE LAB. NATIONWIDE.

Collected by Collected date/time Received date/time


MW-1 L1075168-01 GW Cody 03/01/19 14:45 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Gravimetric Analysis by Method 2540 C-2011 WG1246056 1 03/07/19 19:53 03/07/19 23:39 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 14:32 03/07/19 14:32 GB Mt. Juliet, TN 3
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 09:41 03/06/19 09:41 ELN Mt. Juliet, TN Ss
Wet Chemistry by Method 300.0 WG1245159 50 03/06/19 02:30 03/06/19 02:30 ELN Mt. Juliet, TN
4
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Cn
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 09:41 ABL Mt. Juliet, TN 5
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 20:39 LD Mt. Juliet, TN Tr
Volatile Organic Compounds (GC) by Method 8021B WG1245228 1 03/05/19 18:46 03/05/19 18:46 BMB Mt. Juliet, TN
6
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246143 1 03/06/19 23:14 03/07/19 18:03 FM Mt. Juliet, TN
Sr

Collected by Collected date/time Received date/time 7

Cody 03/01/19 15:15 03/04/19 09:00


Qc
MW-2 L1075168-02 GW
Method Batch Dilution Preparation Analysis Analyst Location 8

date/time date/time
Gl
Gravimetric Analysis by Method 2540 C-2011 WG1246056 1 03/07/19 19:53 03/07/19 23:39 AEC Mt. Juliet, TN 9
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 14:44 03/07/19 14:44 GB Mt. Juliet, TN Al
Wet Chemistry by Method 300.0 WG1245159 10 03/06/19 02:45 03/06/19 02:45 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN 10
Sc
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 09:48 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 20:43 LD Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8021B WG1245228 1 03/05/19 19:07 03/05/19 19:07 BMB Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 06:05 DMW Mt. Juliet, TN

Collected by Collected date/time Received date/time


MW-3 L1075168-03 GW Cody 03/01/19 15:45 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246056 1 03/07/19 19:53 03/07/19 23:39 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 14:51 03/07/19 14:51 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 10 03/06/19 09:57 03/06/19 09:57 ELN Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 50 03/06/19 03:32 03/06/19 03:32 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 09:56 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 20:48 LD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245356 1 03/05/19 20:32 03/05/19 20:32 GLN Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 06:21 DMW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1246279 1 03/07/19 07:27 03/07/19 16:39 JF Mt. Juliet, TN

Collected by Collected date/time Received date/time


MW-4 L1075168-04 GW Cody 03/01/19 16:30 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246056 1 03/07/19 19:53 03/07/19 23:39 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 14:58 03/07/19 14:58 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 10:12 03/06/19 10:12 ELN Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 20 03/06/19 03:47 03/06/19 03:47 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 09:58 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 20:20 LD Mt. Juliet, TN

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 4 of 161
SAMPLE SUMMARY ONE LAB. NATIONWIDE.

Collected by Collected date/time Received date/time


MW-4 L1075168-04 GW Cody 03/01/19 16:30 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Volatile Organic Compounds (GC) by Method 8021B WG1245228 1 03/05/19 19:28 03/05/19 19:28 BMB Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 06:37 DMW Mt. Juliet, TN 3
Ss
Collected by Collected date/time Received date/time
4
MW-5 L1075168-05 GW Cody 03/01/19 16:15 03/04/19 09:00 Cn
Method Batch Dilution Preparation Analysis Analyst Location
5
date/time date/time Tr
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 15:05 03/07/19 15:05 GB Mt. Juliet, TN 6
Sr
Wet Chemistry by Method 300.0 WG1245159 50 03/06/19 04:02 03/06/19 04:02 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN 7
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN Qc
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:00 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:07 LD Mt. Juliet, TN 8
Gl
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 04:13 03/06/19 04:13 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246143 1 03/06/19 23:14 03/07/19 18:20 FM Mt. Juliet, TN 9
Al
Collected by Collected date/time Received date/time
10
MW-6 L1075168-06 GW Cody 03/01/19 16:00 03/04/19 09:00 Sc
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 15:12 03/07/19 15:12 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 5 03/06/19 04:18 03/06/19 04:18 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:03 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:11 LD Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 04:34 03/06/19 04:34 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 07:10 DMW Mt. Juliet, TN

Collected by Collected date/time Received date/time


MW-7 L1075168-07 GW Cody 03/01/19 12:45 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 15:19 03/07/19 15:19 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 20 03/06/19 04:33 03/06/19 04:33 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:05 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:16 LD Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 04:55 03/06/19 04:55 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 07:26 DMW Mt. Juliet, TN

Collected by Collected date/time Received date/time


MW-8 L1075168-08 GW Cody 03/01/19 11:35 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 15:26 03/07/19 15:26 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 04:49 03/06/19 04:49 ELN Mt. Juliet, TN

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 5 of 161
SAMPLE SUMMARY ONE LAB. NATIONWIDE.

Collected by Collected date/time Received date/time


MW-8 L1075168-08 GW Cody 03/01/19 11:35 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN 3
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:08 ABL Mt. Juliet, TN Ss
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:21 LD Mt. Juliet, TN
4
Volatile Organic Compounds (GC) by Method 8021B WG1248019 1 03/11/19 13:24 03/11/19 13:24 ACG Mt. Juliet, TN
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 07:43 DMW Mt. Juliet, TN
5

Collected by Collected date/time Received date/time


Tr
MW-9 L1075168-09 GW Cody 03/01/19 11:15 03/04/19 09:00
6

Method Batch Dilution Preparation Analysis Analyst Location


Sr
date/time date/time
7
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN Qc
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 15:42 03/07/19 15:42 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 05:35 03/06/19 05:35 ELN Mt. Juliet, TN 8
Gl
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN 9
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:10 ABL Mt. Juliet, TN Al
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:25 LD Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 05:38 03/06/19 05:38 DWR Mt. Juliet, TN 10
Sc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 08:00 DMW Mt. Juliet, TN

Collected by Collected date/time Received date/time


MW-10 L1075168-10 GW Cody 03/01/19 12:15 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 15:50 03/07/19 15:50 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 05:50 03/06/19 05:50 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:13 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:30 LD Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 05:59 03/06/19 05:59 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 17:54 DMW Mt. Juliet, TN

Collected by Collected date/time Received date/time


MW-11 L1075168-11 GW Cody 03/01/19 13:15 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 15:58 03/07/19 15:58 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 10:28 03/06/19 10:28 ELN Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 20 03/06/19 06:37 03/06/19 06:37 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:15 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:35 LD Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 06:20 03/06/19 06:20 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 18:10 DMW Mt. Juliet, TN

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 6 of 161
SAMPLE SUMMARY ONE LAB. NATIONWIDE.

Collected by Collected date/time Received date/time


MW-12 L1075168-12 GW Cody 03/01/19 13:45 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:05 03/07/19 16:05 GB Mt. Juliet, TN 3
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 10:43 03/06/19 10:43 ELN Mt. Juliet, TN Ss
Wet Chemistry by Method 300.0 WG1245159 20 03/06/19 06:52 03/06/19 06:52 ELN Mt. Juliet, TN
4
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Cn
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:17 ABL Mt. Juliet, TN 5
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:39 LD Mt. Juliet, TN Tr
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245356 1 03/05/19 20:52 03/05/19 20:52 GLN Mt. Juliet, TN
6
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 18:26 DMW Mt. Juliet, TN
Sr
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1246279 1 03/07/19 07:27 03/07/19 17:03 JF Mt. Juliet, TN
7

Collected by Collected date/time Received date/time


Qc
MW-13 L1075168-13 GW Cody 03/01/19 14:15 03/04/19 09:00
8

Method Batch Dilution Preparation Analysis Analyst Location


Gl
date/time date/time
9
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN Al
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:12 03/07/19 16:12 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 10:59 03/06/19 10:59 ELN Mt. Juliet, TN 10
Sc
Wet Chemistry by Method 300.0 WG1245159 100 03/06/19 07:23 03/06/19 07:23 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:25 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:44 LD Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 5 03/05/19 17:13 03/06/19 22:44 LD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245356 1 03/05/19 21:13 03/05/19 21:13 GLN Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 18:42 DMW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1246279 1 03/07/19 07:27 03/07/19 22:11 JF Mt. Juliet, TN

Collected by Collected date/time Received date/time


PSW-1 L1075168-14 GW Cody 03/01/19 17:10 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:18 03/07/19 16:18 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 10 03/06/19 07:38 03/06/19 07:38 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:27 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:49 LD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245356 1 03/05/19 21:33 03/05/19 21:33 GLN Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 18:59 DMW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1245476 10 03/06/19 16:44 03/07/19 07:37 JF Mt. Juliet, TN

Collected by Collected date/time Received date/time


PSW-2 L1075168-15 GW Cody 03/01/19 17:15 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246059 1 03/07/19 20:03 03/08/19 01:53 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:26 03/07/19 16:26 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 10 03/06/19 07:54 03/06/19 07:54 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 7 of 161
SAMPLE SUMMARY ONE LAB. NATIONWIDE.

Collected by Collected date/time Received date/time


PSW-2 L1075168-15 GW Cody 03/01/19 17:15 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:30 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 22:20 LD Mt. Juliet, TN 3
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245979 1 03/06/19 16:03 03/06/19 16:03 GLN Mt. Juliet, TN Ss
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 19:15 DMW Mt. Juliet, TN
4
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1245476 10 03/06/19 16:44 03/07/19 08:00 JF Mt. Juliet, TN
Cn

Collected by Collected date/time Received date/time 5

Cody 03/01/19 17:20 03/04/19 09:00


Tr
PSW-3 L1075168-16 GW
Method Batch Dilution Preparation Analysis Analyst Location 6

date/time date/time
Sr
Gravimetric Analysis by Method 2540 C-2011 WG1246059 1 03/07/19 20:03 03/08/19 01:53 AEC Mt. Juliet, TN 7
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:34 03/07/19 16:34 GB Mt. Juliet, TN Qc
Wet Chemistry by Method 300.0 WG1245159 10 03/06/19 08:09 03/06/19 08:09 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN 8
Gl
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:32 ABL Mt. Juliet, TN 9
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 22:25 LD Mt. Juliet, TN Al
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245979 1 03/06/19 16:22 03/06/19 16:22 GLN Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 19:31 DMW Mt. Juliet, TN 10
Sc
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1245476 10 03/06/19 16:44 03/07/19 08:24 JF Mt. Juliet, TN

Collected by Collected date/time Received date/time


PSW-4 L1075168-17 GW Cody 03/01/19 17:25 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246059 1 03/07/19 20:03 03/08/19 01:53 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:42 03/07/19 16:42 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 10 03/06/19 08:24 03/06/19 08:24 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245737 1 03/06/19 09:50 03/06/19 09:50 SJM Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:35 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 22:30 LD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245979 1 03/06/19 16:42 03/06/19 16:42 GLN Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 19:48 DMW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1245476 10 03/06/19 16:44 03/07/19 08:48 JF Mt. Juliet, TN

Collected by Collected date/time Received date/time


SK-1 L1075168-18 GW Cody 03/01/19 17:50 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG1246059 1 03/07/19 20:03 03/08/19 01:53 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:49 03/07/19 16:49 GB Mt. Juliet, TN
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 11:14 03/06/19 11:14 ELN Mt. Juliet, TN
Wet Chemistry by Method 9040C WG1245737 1 03/06/19 09:50 03/06/19 09:50 SJM Mt. Juliet, TN
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:37 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 22:34 LD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245979 1 03/06/19 17:01 03/06/19 17:01 GLN Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 20:04 DMW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1245476 1 03/06/19 16:44 03/07/19 04:26 JF Mt. Juliet, TN

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 8 of 161
SAMPLE SUMMARY ONE LAB. NATIONWIDE.

Collected by Collected date/time Received date/time


DUPLICATE 1 L1075168-19 GW Cody 03/01/19 00:00 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Gravimetric Analysis by Method 2540 C-2011 WG1246059 1 03/07/19 20:03 03/08/19 01:53 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 17:04 03/07/19 17:04 GB Mt. Juliet, TN 3
Wet Chemistry by Method 300.0 WG1245159 10 03/06/19 08:55 03/06/19 08:55 ELN Mt. Juliet, TN Ss
Wet Chemistry by Method 9040C WG1245737 1 03/06/19 09:50 03/06/19 09:50 SJM Mt. Juliet, TN
4
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Cn
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:39 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 22:39 LD Mt. Juliet, TN 5
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245979 1 03/06/19 17:21 03/06/19 17:21 GLN Mt. Juliet, TN Tr
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 20:21 DMW Mt. Juliet, TN
6
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1245476 10 03/06/19 16:44 03/07/19 09:13 JF Mt. Juliet, TN
Sr

Collected by Collected date/time Received date/time 7

Cody 03/01/19 09:15 03/04/19 09:00


Qc
PS-1 L1075168-20 Solid
Method Batch Dilution Preparation Analysis Analyst Location 8

date/time date/time
Gl
Total Solids by Method 2540 G-2011 WG1245367 1 03/06/19 13:46 03/06/19 14:08 JD Mt. Juliet, TN 9
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN Al
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 18:51 ST Mt. Juliet, TN
Mercury by Method 7471A WG1245047 1 03/04/19 17:18 03/05/19 09:02 ABL Mt. Juliet, TN 10
Sc
Metals (ICP) by Method 6010B WG1245191 1 03/05/19 10:59 03/07/19 20:41 TRB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG1245191 5 03/05/19 10:59 03/08/19 10:03 CCE Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245869 1 03/05/19 23:41 03/06/19 19:43 BMB Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 1 03/06/19 19:07 03/10/19 16:33 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1244658 2 03/04/19 21:24 03/05/19 05:28 JNJ Mt. Juliet, TN

Collected by Collected date/time Received date/time


PS-2 L1075168-21 Solid Cody 03/01/19 09:30 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Total Solids by Method 2540 G-2011 WG1245367 1 03/06/19 13:46 03/06/19 14:08 JD Mt. Juliet, TN
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 19:17 ST Mt. Juliet, TN
Mercury by Method 7471A WG1245047 1 03/04/19 17:18 03/05/19 09:04 ABL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG1245191 1 03/05/19 10:59 03/07/19 20:44 TRB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG1245191 5 03/05/19 10:59 03/08/19 10:06 CCE Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245896 1 03/05/19 23:41 03/06/19 12:03 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 10 03/06/19 19:07 03/09/19 03:57 DMW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1244658 20 03/04/19 21:24 03/05/19 06:27 JNJ Mt. Juliet, TN

Collected by Collected date/time Received date/time


PS-3 L1075168-22 Solid Cody 03/01/19 09:45 03/04/19 09:00

Method Batch Dilution Preparation Analysis Analyst Location


date/time date/time
Total Solids by Method 2540 G-2011 WG1245670 1 03/06/19 10:44 03/06/19 10:56 JD Mt. Juliet, TN
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 19:25 ST Mt. Juliet, TN
Mercury by Method 7471A WG1245047 1 03/04/19 17:18 03/05/19 09:07 ABL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG1245191 1 03/05/19 10:59 03/07/19 20:47 TRB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG1245191 5 03/05/19 10:59 03/08/19 10:09 CCE Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245896 1 03/05/19 23:41 03/06/19 12:22 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 1 03/06/19 19:07 03/09/19 23:30 KME Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1244658 2 03/04/19 21:24 03/05/19 05:48 JNJ Mt. Juliet, TN

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 9 of 161
SAMPLE SUMMARY ONE LAB. NATIONWIDE.

Collected by Collected date/time Received date/time


PS-4 L1075168-23 Solid Cody 03/01/19 10:00 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Total Solids by Method 2540 G-2011 WG1245670 1 03/06/19 10:44 03/06/19 10:56 JD Mt. Juliet, TN
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN 3
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 19:34 ST Mt. Juliet, TN Ss
Mercury by Method 7471A WG1245047 1 03/04/19 17:18 03/05/19 09:14 ABL Mt. Juliet, TN
4
Metals (ICP) by Method 6010B WG1245191 1 03/05/19 10:59 03/07/19 20:50 TRB Mt. Juliet, TN
Cn
Metals (ICP) by Method 6010B WG1245191 5 03/05/19 10:59 03/08/19 10:12 CCE Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245896 1 03/05/19 23:41 03/06/19 14:30 DWR Mt. Juliet, TN 5
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 1 03/06/19 19:07 03/09/19 01:11 DMW Mt. Juliet, TN Tr
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1244658 10 03/04/19 21:24 03/05/19 06:46 JNJ Mt. Juliet, TN
6
Sr
Collected by Collected date/time Received date/time
PS-5 L1075168-24 Solid Cody 03/01/19 17:00 03/04/19 09:00 7
Qc
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 8
Gl
Total Solids by Method 2540 G-2011 WG1245670 1 03/06/19 10:44 03/06/19 10:56 JD Mt. Juliet, TN
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN 9
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 19:59 ST Mt. Juliet, TN Al
Mercury by Method 7471A WG1245047 1 03/04/19 17:18 03/05/19 09:17 ABL Mt. Juliet, TN
Metals (ICP) by Method 6010B WG1245191 1 03/05/19 10:59 03/07/19 20:53 TRB Mt. Juliet, TN 10
Sc
Metals (ICP) by Method 6010B WG1245191 5 03/05/19 10:59 03/08/19 10:14 CCE Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245896 1 03/05/19 23:41 03/06/19 14:49 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 1 03/06/19 19:07 03/09/19 02:20 DMW Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 5 03/06/19 19:07 03/09/19 23:58 KME Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1244658 100 03/04/19 21:24 03/05/19 12:37 JNJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1244658 2 03/04/19 21:24 03/05/19 06:07 JNJ Mt. Juliet, TN

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 10 of 161
CASE NARRATIVE ONE LAB. NATIONWIDE.

1
Cp
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within 2
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form 3
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been 4
knowingly withheld that would affect the quality of the data. Cn

5
Tr

6
Sr
[Preliminary Report]
7
Qc

Chris McCord
Jason Romer 8
Project Manager Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 11 of 161
RG-366/TRRP-13
Revised May 2010 Laboratory Data Package Cover Page ONE LAB. NATIONWIDE.

This data package consists of this signature page, the laboratory review checklist, and the following
reportable data as applicable:
R1 - Field chain-of-custody documentation;
R2 - Sample identification cross-reference;
R3 - Test reports (analytical data sheets) for each environmental sample that includes:
a. Items consistent with NELAC Chapter 5,
b. dilution factors,
c. preparation methods,
d. cleanup methods, and
e. if required for the project, tentatively identified compounds (TICs).
R4 - Surrogate recovery data including:
a. Calculated recovery (%R), and
b. The laboratory’s surrogate QC limits.
R5 - Test reports/summary forms for blank samples;
R6 - Test reports/summary forms for laboratory control samples (LCSs) including:
a. LCS spiking amounts,
b. Calculated %R for each analyte, and
c. The laboratory’s LCS QC limits.
R7 - Test reports for project matrix spike/matrix spike duplicates (MS/MSDs) including:
a. Samples associated with the MS/MSD clearly identified,
b. MS/MSD spiking amounts,
c. Concentration of each MS/MSD analyte measured in the parent and spiked samples,
d. Calculated %Rs and relative percent differences (RPDs), and
e. The laboratory’s MS/MSD QC limits
R8 - Laboratory analytical duplicate (if applicable) recovery and precision:
a. The amount of analyte measured in the duplicate,
b. The calculated RPD, and
c. The laboratory’s QC limits for analytical duplicates.
R9 - List of method quantitation limits (MQLs) and detectability check sample results for each analyte
for each method and matrix.
R10 - Other problems or anomalies.
Release Statement: I am responsible for the release of this laboratory data package. This laboratory is
NELAC accredited under the Texas Laboratory Accreditation Program for all the methods, analytes, and
matrices reported in this data package except as noted in the Exception Reports. The data have been
reviewed and are technically compliant with the requirements of the methods used, except where
noted by the laboratory in the Exception Reports. By my signature below, I affirm to the best of my
knowledge all problems/anomalies observed by the laboratory have been identified in the Laboratory
Review Checklist, and no information affecting the quality of the data has been knowingly withheld.

[Preliminary Report]

Chris McCord
Jason Romer
Project Manager

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 12 of 161
RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Reportable Data ONE LAB. NATIONWIDE.

Laboratory Name: Pace Analytical National LRC Date: 03/13/2019 16:10


15:42
Laboratory Job Number: L1075168-01, 02, 03, 04, 05, 06, 07, 08, 09, 10, 11, 12, 13, 14,
Project Name: Boundary Ventures, Inc. 15, 16, 17, 18, 19, 20, 21, 22, 23 and 24
Prep Batch Number(s): WG1244658, WG1245047, WG1245002, WG1245130,
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Reviewer Name: Jason
Chris McCord
Romer WG1245367, WG1245670, WG1245979, WG1245735, WG1246279, WG1245955,
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
#¹ A² Description Yes No NA³ NR⁴ ER#⁵
R1 OI Chain-of-custody (C-O-C)
Did samples meet the laboratory’s standard conditions of sample acceptability upon receipt? X
Were all departures from standard conditions described in an exception report? X
R2 OI Sample and quality control (QC) identification
Are all field sample ID numbers cross-referenced to the laboratory ID numbers? X
Are all laboratory ID numbers cross-referenced to the corresponding QC data? X
R3 OI Test reports
Were all samples prepared and analyzed within holding times? X 1
Other than those results < MQL, were all other raw values bracketed by calibration standards? X
Were calculations checked by a peer or supervisor? X
Were all analyte identifications checked by a peer or supervisor? X
Were sample detection limits reported for all analytes not detected? X
Were all results for soil and sediment samples reported on a dry weight basis? X
Were % moisture (or solids) reported for all soil and sediment samples? X
Were bulk soils/solids samples for volatile analysis extracted with methanol per SW846 Method 5035? X
If required for the project, are TICs reported? X
R4 O Surrogate recovery data
Were surrogates added prior to extraction? X
Were surrogate percent recoveries in all samples within the laboratory QC limits? X 2
R5 OI Test reports/summary forms for blank samples
Were appropriate type(s) of blanks analyzed? X
Were blanks analyzed at the appropriate frequency? X
Were method blanks taken through the entire analytical process, including preparation and, if applicable, X
cleanup procedures?
Were blank concentrations < MQL? X
R6 OI Laboratory control samples (LCS):
Were all COCs included in the LCS? X
Was each LCS taken through the entire analytical procedure, including prep and cleanup steps? X
Were LCSs analyzed at the required frequency? X
Were LCS (and LCSD, if applicable) %Rs within the laboratory QC limits? X 3
Does the detectability check sample data document the laboratory’s capability to detect the COCs at the MDL X
used to calculate the SDLs?
Was the LCSD RPD within QC limits? X 4
R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data
Were the project/method specified analytes included in the MS and MSD? X
Were MS/MSD analyzed at the appropriate frequency? X
Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X 5
Were MS/MSD RPDs within laboratory QC limits? X 6
R8 OI Analytical duplicate data
Were appropriate analytical duplicates analyzed for each matrix? X
Were analytical duplicates analyzed at the appropriate frequency? X
Were RPDs or relative standard deviations within the laboratory QC limits? X 7
R9 OI Method quantitation limits (MQLs):
Are the MQLs for each method analyte included in the laboratory data package? X
Do the MQLs correspond to the concentration of the lowest non-zero calibration standard? X
Are unadjusted MQLs and DCSs included in the laboratory data package? X
R10 OI Other problems/anomalies
Are all known problems/anomalies/special conditions noted in this LRC and ER? X
Was applicable and available technology used to lower the SDL to minimize the matrix interference effects on X
the sample results?
Is the laboratory NELAC-accredited under the Texas Laboratory Accreditation Program for the analytes, matrices X
and methods associated with this laboratory data package?

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
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16:10 13 of 161
RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Reportable Data ONE LAB. NATIONWIDE.

Laboratory Name: Pace Analytical National LRC Date: 03/13/2019 16:10


15:42
Laboratory Job Number: L1075168-01, 02, 03, 04, 05, 06, 07, 08, 09, 10, 11, 12, 13, 14,
Project Name: Boundary Ventures, Inc. 15, 16, 17, 18, 19, 20, 21, 22, 23 and 24
Prep Batch Number(s): WG1244658, WG1245047, WG1245002, WG1245130,
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Reviewer Name: Jason
Chris McCord
Romer WG1245367, WG1245670, WG1245979, WG1245735, WG1246279, WG1245955,
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
#¹ A² Description Yes No NA³ NR⁴ ER#⁵
1. Items identified by the letter “R” must be included in the laboratory data package submitted in the TRRP-required report(s). Items identified by the letter “S”
should be retained and made available upon request for the appropriate retention period.
2. O = organic analyses; I = inorganic analyses (and general chemistry, when applicable);
3. NA = Not applicable;
4. NR = Not reviewed;
5. ER# = Exception Report identification number (an Exception Report should be completed for an item if “NR” or “No” is checked).

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 14 of 161
RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Supporting Data ONE LAB. NATIONWIDE.

Laboratory Name: Pace Analytical National LRC Date: 03/13/2019 16:10


15:42
Laboratory Job Number: L1075168-01, 02, 03, 04, 05, 06, 07, 08, 09, 10, 11, 12, 13, 14,
Project Name: Boundary Ventures, Inc. 15, 16, 17, 18, 19, 20, 21, 22, 23 and 24
Prep Batch Number(s): WG1244658, WG1245047, WG1245002, WG1245130,
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Reviewer Name: Jason
Chris McCord
Romer WG1245367, WG1245670, WG1245979, WG1245735, WG1246279, WG1245955,
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
#¹ A² Description Yes No NA³ NR⁴ ER#⁵
S1 OI Initial calibration (ICAL)
Were response factors and/or relative response factors for each analyte within QC limits? X
Were percent RSDs or correlation coefficient criteria met? X
Was the number of standards recommended in the method used for all analytes? X
Were all points generated between the lowest and highest standard used to calculate the curve? X
Are ICAL data available for all instruments used? X
Has the initial calibration curve been verified using an appropriate second source standard? X
S2 OI Initial and continuing calibration verification (ICCV and CCV) and continuing calibration blank (CCB):
Was the CCV analyzed at the method-required frequency? X
Were percent differences for each analyte within the method-required QC limits? X
Was the ICAL curve verified for each analyte? X
Was the absolute value of the analyte concentration in the inorganic CCB < MDL? X
S3 O Mass spectral tuning
Was the appropriate compound for the method used for tuning? X
Were ion abundance data within the method-required QC limits? X
S4 O Internal standards (IS)
Were IS area counts and retention times within the method-required QC limits? X
S5 OI Raw data (NELAC Section 5.5.10)
Were the raw data (for example, chromatograms, spectral data) reviewed by an analyst? X
Were data associated with manual integrations flagged on the raw data? X
S6 O Dual column confirmation
Did dual column confirmation results meet the method-required QC? X
S7 O Tentatively identified compounds (TICs)
If TICs were requested, were the mass spectra and TIC data subject to appropriate checks? X
S8 I Interference Check Sample (ICS) results
Were percent recoveries within method QC limits? X
S9 I Serial dilutions, post digestion spikes, and method of standard additions
Were percent differences, recoveries, and the linearity within the QC limits specified in the method? X 8
S10 OI Method detection limit (MDL) studies
Was a MDL study performed for each reported analyte? X
Is the MDL either adjusted or supported by the analysis of DCSs? X
S11 OI Proficiency test reports
Was the laboratory's performance acceptable on the applicable proficiency tests or evaluation studies? X
S12 OI Standards documentation
Are all standards used in the analyses NIST-traceable or obtained from other appropriate sources? X
S13 OI Compound/analyte identification procedures
Are the procedures for compound/analyte identification documented? X
S14 OI Demonstration of analyst competency (DOC)
Was DOC conducted consistent with NELAC Chapter 5? X
Is documentation of the analyst’s competency up-to-date and on file? X
S15 OI Verification/validation documentation for methods (NELAC Chapter 5)
Are all the methods used to generate the data documented, verified, and validated, where applicable? X
S16 OI Laboratory standard operating procedures (SOPs)
Are laboratory SOPs current and on file for each method performed X
1. Items identified by the letter “R” must be included in the laboratory data package submitted in the TRRP-required report(s). Items identified by the letter “S”
should be retained and made available upon request for the appropriate retention period.
2. O = organic analyses; I = inorganic analyses (and general chemistry, when applicable);
3. NA = Not applicable;
4. NR = Not reviewed;
5. ER# = Exception Report identification number (an Exception Report should be completed for an item if “NR” or “No” is checked).

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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03/13/19 15:42
16:10 15 of 161
RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Exception Reports ONE LAB. NATIONWIDE.

Laboratory Name: Pace Analytical National LRC Date: 03/13/2019 16:10


15:42
Laboratory Job Number: L1075168-01, 02, 03, 04, 05, 06, 07, 08, 09, 10, 11, 12, 13, 14,
Project Name: Boundary Ventures, Inc. 15, 16, 17, 18, 19, 20, 21, 22, 23 and 24
Prep Batch Number(s): WG1244658, WG1245047, WG1245002, WG1245130,
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Reviewer Name: Jason
Chris McCord
Romer WG1245367, WG1245670, WG1245979, WG1245735, WG1246279, WG1245955,
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
ER #¹ Description
9040C WG1245130 L1075168-15, 06, 10, 01, 03, 02, 04, 05, 07, 12, 08, 16, 13, 09, 11 and 14: Prepared and/or analyzed
past recommended holding time. Concentrations should be considered minimum values.
1 9040C WG1245737 L1075168-18, 17 and 19: Prepared and/or analyzed past recommended holding time. Concentrations
should be considered minimum values.
TCEQ Method 1005 WG1246136 o-Terphenyl L1075168-24 and 21: Percent Recovery is outside of established control
limits.
2 8270C WG1244658 2,4,6-Tribromophenol, 2-Fluorophenol, Phenol-d5, Nitrobenzene-d5, p-Terphenyl-d14,
2-Fluorobiphenyl L1075168-21, 24 and 23: Percent Recovery is outside of established control limits.
8260C WG1245979 4-Bromofluorobenzene L1075168-16: Percent Recovery is outside of established control limits.
8260B WG1245869 Dibromomethane, 1,1,2,2-Tetrachloroethane: Percent Recovery is outside of established control
3 limits.
8270C WG1244658 Benzidine: Percent Recovery is outside of established control limits.
8021B WG1245643 Ethylbenzene, Total Xylene: Relative Percent Difference is outside of established control limits.
4 8270D WG1245476 Benzidine: Relative Percent Difference is outside of established control limits.
8270D WG1246279 Pentachlorophenol: Relative Percent Difference is outside of established control limits.
8260B WG1245869 1,2,4-Trimethylbenzene: Percent Recovery is outside of established control limits.
6020 WG1245245 Barium, Calcium, Sodium: Percent Recovery is outside of established control limits.
TCEQ Method 1005 WG1246136 TPH C12 - C28, TPH C6 - C35: Percent Recovery is outside of established control limits.
8260B WG1245869 Ethylbenzene, p-Isopropyltoluene, Naphthalene, Toluene, 1,2,3-Trimethylbenzene,
1,3,5-Trimethylbenzene, Xylenes, Total: Percent Recovery is outside of established control limits.
8260B WG1245896 Chloroethane, Tetrachloroethene, 1,1,1-Trichloroethane: Percent Recovery is outside of established
5 control limits.
8021B WG1245643 Total Xylene: Percent Recovery is outside of established control limits.
8270D WG1246279 Benzidine: Percent Recovery is outside of established control limits.
8270C WG1244658 Benzidine, 3,3-Dichlorobenzidine, Hexachlorocyclopentadiene, n-Nitrosodimethylamine,
n-Nitrosodiphenylamine, Diethyl phthalate, 4,6-Dinitro-2-methylphenol, 2,4-Dinitrophenol, Pentachlorophenol: Percent
Recovery is outside of established control limits.
7470A WG1245002 Mercury: Percent Recovery is outside of established control limits.
TCEQ Method 1005 WG1246136 TPH C12 - C28: Relative Percent Difference is outside of established control limits.
8260B WG1245896 Bromomethane, sec-Butylbenzene, tert-Butylbenzene, Chloroethane, p-Isopropyltoluene,
n-Propylbenzene, 1,1,2-Trichlorotrifluoroethane, Trichlorofluoromethane, Vinyl chloride: Relative Percent Difference is
outside of established control limits.
8021B WG1245228 Benzene, Toluene, Ethylbenzene, Total Xylene: Relative Percent Difference is outside of established
6 control limits.
8270D WG1246279 3,3-Dichlorobenzidine, 2,4-Dimethylphenol: Relative Percent Difference is outside of established
control limits.
8270C WG1244658 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, Hexachlorobenzene, Hexachloro-1,3-butadiene,
Hexachloroethane, 2-Nitrophenol, Pentachlorophenol: Relative Percent Difference is outside of established control
limits.
9056A WG1245719 Chloride: Relative Percent Difference is outside of established control limits.
7 2540 C-2011 WG1246058 Dissolved Solids: Relative Percent Difference is outside of established control limits.
2540 C-2011 WG1246059 Dissolved Solids: Relative Percent Difference is outside of established control limits.
6010B WG1245191 Barium, Chromium, Lead: Post Spike Percent Recovery and/or Serial Dilution Relative Percent
8 Difference was outside of established control limits.
1. Items identified by the letter “R” must be included in the laboratory data package submitted in the TRRP-required report(s). Items identified by the letter “S”
should be retained and made available upon request for the appropriate retention period.
2. O = organic analyses; I = inorganic analyses (and general chemistry, when applicable);
3. NA = Not applicable;
4. NR = Not reviewed;
5. ER# = Exception Report identification number (an Exception Report should be completed for an item if “NR” or “No” is checked).

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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03/13/19 15:42
16:10 16 of 161
MW-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 14:45 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 2960 14.1 50.0 50.0 1 03/07/2019 23:39 WG1246056 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 157 2.71 20.0 20.0 1 03/07/2019 14:32 WG1245955
5
Sample Narrative: Tr
L1075168-01 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 1510 2.60 1.00 50.0 50 03/06/2019 02:30 WG1245159 8
Sulfate 2.85 J 0.0774 5.00 5.00 1 03/06/2019 09:41 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.54 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-01 WG1245130: 6.54 at 11.6C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 4510 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U J6 0.0000490 0.000200 0.000200 1 03/05/2019 09:41 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.104 0.000250 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Barium 0.812 0.000360 0.00500 0.00500 1 03/06/2019 20:39 WG1245245
Cadmium 0.000204 J 0.000160 0.00100 0.00100 1 03/06/2019 20:39 WG1245245
Calcium 252 0.0460 1.00 1.00 1 03/06/2019 20:39 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Magnesium 43.7 0.100 1.00 1.00 1 03/06/2019 20:39 WG1245245
Potassium 6.10 0.0370 1.00 1.00 1 03/06/2019 20:39 WG1245245
Selenium 0.000561 J 0.000380 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Sodium 496 0.110 1.00 1.00 1 03/06/2019 20:39 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 17 of 161
MW-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 14:45 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/05/2019 18:46 WG1245228
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 18:46 WG1245228
Ethylbenzene U 0.000160 0.000500 0.000500 1 03/05/2019 18:46 WG1245228 3
Total Xylene U 0.000510 0.00150 0.00150 1 03/05/2019 18:46 WG1245228 Ss
(S) a,a,a-Trifluorotoluene(PID) 99.8 79.0-125 03/05/2019 18:46 WG1245228
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143
Qc
(S) o-Terphenyl 85.2 70.0-130 03/07/2019 18:03 WG1246143
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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03/13/19 15:42
16:10 18 of 161
MW-2 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 15:15 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1300 7.05 25.0 25.0 1 03/07/2019 23:39 WG1246056 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 285 2.71 20.0 20.0 1 03/07/2019 14:44 WG1245955
5
Sample Narrative: Tr
L1075168-02 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 487 0.519 1.00 10.0 10 03/06/2019 02:45 WG1245159 8
Sulfate 99.3 0.774 5.00 50.0 10 03/06/2019 02:45 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.67 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-02 WG1245130: 6.67 at 11.2C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 2180 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 09:48 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00617 0.000250 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Barium 0.755 0.000360 0.00500 0.00500 1 03/06/2019 20:43 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 20:43 WG1245245
Calcium 160 0.0460 1.00 1.00 1 03/06/2019 20:43 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Magnesium 43.0 0.100 1.00 1.00 1 03/06/2019 20:43 WG1245245
Potassium 6.16 0.0370 1.00 1.00 1 03/06/2019 20:43 WG1245245
Selenium 0.000593 J 0.000380 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Sodium 176 0.110 1.00 1.00 1 03/06/2019 20:43 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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03/13/19 15:42
16:10 19 of 161
MW-2 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 15:15 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/05/2019 19:07 WG1245228
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 19:07 WG1245228
Ethylbenzene U 0.000160 0.000500 0.000500 1 03/05/2019 19:07 WG1245228 3
Total Xylene U 0.000510 0.00150 0.00150 1 03/05/2019 19:07 WG1245228 Ss
(S) a,a,a-Trifluorotoluene(PID) 99.4 79.0-125 03/05/2019 19:07 WG1245228
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479
Qc
(S) o-Terphenyl 89.0 70.0-130 03/06/2019 06:05 WG1245479
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 20 of 161
MW-3 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 15:45 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 3640 14.1 50.0 50.0 1 03/07/2019 23:39 WG1246056 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 214 2.71 20.0 20.0 1 03/07/2019 14:51 WG1245955
5
Sample Narrative: Tr
L1075168-03 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 1630 2.60 1.00 50.0 50 03/06/2019 03:32 WG1245159 8
Sulfate 200 0.774 5.00 50.0 10 03/06/2019 09:57 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.57 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-03 WG1245130: 6.57 at 12C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 4730 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 09:56 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00412 0.000250 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Barium 0.478 0.000360 0.00500 0.00500 1 03/06/2019 20:48 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 20:48 WG1245245
Calcium 436 0.0460 1.00 1.00 1 03/06/2019 20:48 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Magnesium 49.7 0.100 1.00 1.00 1 03/06/2019 20:48 WG1245245
Potassium 8.67 0.0370 1.00 1.00 1 03/06/2019 20:48 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Sodium 367 0.110 1.00 1.00 1 03/06/2019 20:48 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 21 of 161
MW-3 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 15:45 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone U 0.0100 0.0500 0.0500 1 03/05/2019 20:32 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 20:32 WG1245356
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/05/2019 20:32 WG1245356 3
Benzene U 0.000331 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Bromomethane U 0.000866 0.00500 0.00500 1 03/05/2019 20:32 WG1245356 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/05/2019 20:32 WG1245356
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Ethylbenzene U 0.000384 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
2-Butanone (MEK) U 0.00393 0.0100 0.0100 1 03/05/2019 20:32 WG1245356
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/05/2019 20:32 WG1245356
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Naphthalene U 0.00100 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
n-Propylbenzene U 0.000349 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/05/2019 20:32 WG1245356

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 22 of 161
MW-3 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 15:45 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Trichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/05/2019 20:32 WG1245356 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/05/2019 20:32 WG1245356
4
1,2,4-Trimethylbenzene U 0.000373 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Cn
1,2,3-Trimethylbenzene U 0.000321 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,3,5-Trimethylbenzene U 0.000387 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Tr
Xylenes, Total U 0.00106 0.00300 0.00300 1 03/05/2019 20:32 WG1245356
6
(S) Toluene-d8 106 80.0-120 03/05/2019 20:32 WG1245356
Sr
(S) 4-Bromofluorobenzene 104 77.0-126 03/05/2019 20:32 WG1245356
(S) 1,2-Dichloroethane-d4 105 70.0-130 03/05/2019 20:32 WG1245356 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479
Al
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479 10
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479 Sc
(S) o-Terphenyl 86.9 70.0-130 03/06/2019 06:21 WG1245479

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.000316 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Acenaphthylene U 0.000309 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzidine U 0.00432 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Benzo(a)anthracene U 0.0000975 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(b)fluoranthene U 0.0000896 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(k)fluoranthene U 0.000355 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(g,h,i)perylene U 0.000161 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(a)pyrene U 0.000340 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Bis(2-chlorethoxy)methane U 0.000329 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Bis(2-chloroethyl)ether U 0.00162 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Bis(2-chloroisopropyl)ether U 0.000445 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
4-Bromophenyl-phenylether U 0.000335 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
2-Chloronaphthalene U 0.000330 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
4-Chlorophenyl-phenylether U 0.000303 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Dibenz(a,h)anthracene U 0.000279 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
3,3-Dichlorobenzidine U 0.00202 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
2,4-Dinitrotoluene U 0.00165 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
2,6-Dinitrotoluene U 0.000279 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Fluoranthene U 0.000310 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Fluorene U 0.000323 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Hexachlorobenzene U 0.000341 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Hexachloro-1,3-butadiene U 0.000329 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Hexachlorocyclopentadiene U 0.00233 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Hexachloroethane U 0.000365 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Naphthalene U 0.000372 0.00100 0.00100 1 03/07/2019 16:39 WG1246279

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 23 of 161
MW-3 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 15:45 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.000367 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Tc
n-Nitrosodimethylamine U 0.00126 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
n-Nitrosodiphenylamine U 0.00119 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 3
n-Nitrosodi-n-propylamine U 0.000403 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 Ss
Phenanthrene U 0.000366 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
4
Benzylbutyl phthalate U 0.000275 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
Cn
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
Di-n-butyl phthalate U 0.000266 0.00300 0.00300 1 03/07/2019 16:39 WG1246279 5
Diethyl phthalate 0.000716 J 0.000282 0.00300 0.00300 1 03/07/2019 16:39 WG1246279 Tr
Dimethyl phthalate U 0.000283 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
6
Di-n-octyl phthalate U 0.000278 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
1,2,4-Trichlorobenzene U 0.000355 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 7
4-Chloro-3-methylphenol U 0.000263 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 Qc
2-Chlorophenol U 0.000283 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
8
2,4-Dichlorophenol U 0.000284 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Gl
2,4-Dimethylphenol U 0.000264 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 9
2,4-Dinitrophenol U 0.00325 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 Al
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Sc
Pentachlorophenol U J3 0.000313 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Phenol 0.00266 J 0.000334 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
2,4,6-Trichlorophenol U 0.000297 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
(S) 2-Fluorophenol 38.4 10.0-120 03/07/2019 16:39 WG1246279
(S) Phenol-d5 22.9 10.0-120 03/07/2019 16:39 WG1246279
(S) Nitrobenzene-d5 53.5 10.0-127 03/07/2019 16:39 WG1246279
(S) 2-Fluorobiphenyl 61.5 10.0-130 03/07/2019 16:39 WG1246279
(S) 2,4,6-Tribromophenol 77.5 10.0-155 03/07/2019 16:39 WG1246279
(S) p-Terphenyl-d14 76.2 10.0-128 03/07/2019 16:39 WG1246279

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 24 of 161
MW-4 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 16:30 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1700 14.1 50.0 50.0 1 03/07/2019 23:39 WG1246056 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 382 2.71 20.0 20.0 1 03/07/2019 14:58 WG1245955
5
Sample Narrative: Tr
L1075168-04 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 682 1.04 1.00 20.0 20 03/06/2019 03:47 WG1245159 8
Sulfate 16.3 0.0774 5.00 5.00 1 03/06/2019 10:12 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.78 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-04 WG1245130: 6.78 at 11.8C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 2730 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 09:58 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00198 J 0.000250 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Barium 2.43 V 0.000360 0.00500 0.00500 1 03/06/2019 20:20 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 20:20 WG1245245
Calcium 211 V 0.0460 1.00 1.00 1 03/06/2019 20:20 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Magnesium 22.8 0.100 1.00 1.00 1 03/06/2019 20:20 WG1245245
Potassium 1.78 0.0370 1.00 1.00 1 03/06/2019 20:20 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Sodium 279 V 0.110 1.00 1.00 1 03/06/2019 20:20 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 25 of 161
MW-4 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 16:30 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/05/2019 19:28 WG1245228
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 19:28 WG1245228
Ethylbenzene U 0.000160 0.000500 0.000500 1 03/05/2019 19:28 WG1245228 3
Total Xylene U 0.000510 0.00150 0.00150 1 03/05/2019 19:28 WG1245228 Ss
(S) a,a,a-Trifluorotoluene(PID) 98.4 79.0-125 03/05/2019 19:28 WG1245228
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479
Qc
(S) o-Terphenyl 83.6 70.0-130 03/06/2019 06:37 WG1245479
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 26 of 161
MW-5 SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 16:15 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 5200 28.2 100 100 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 295 2.71 20.0 20.0 1 03/07/2019 15:05 WG1245955
5
Sample Narrative: Tr
L1075168-05 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 2360 2.60 1.00 50.0 50 03/06/2019 04:02 WG1245159 8
Sulfate 443 3.87 5.00 250 50 03/06/2019 04:02 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.62 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-05 WG1245130: 6.62 at 11.9C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 7010 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury 0.0000675 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:00 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00189 J 0.000250 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Barium 0.156 0.000360 0.00500 0.00500 1 03/06/2019 21:07 WG1245245
Cadmium 0.000194 J 0.000160 0.00100 0.00100 1 03/06/2019 21:07 WG1245245
Calcium 628 0.0460 1.00 1.00 1 03/06/2019 21:07 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Magnesium 75.1 0.100 1.00 1.00 1 03/06/2019 21:07 WG1245245
Potassium 29.2 0.0370 1.00 1.00 1 03/06/2019 21:07 WG1245245
Selenium 0.00199 J 0.000380 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Sodium 688 0.110 1.00 1.00 1 03/06/2019 21:07 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 27 of 161
MW-5 SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 16:15 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene 0.000248 J 0.000190 0.000500 0.000500 1 03/06/2019 04:13 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 04:13 WG1245643
Ethylbenzene U J3 0.000160 0.000500 0.000500 1 03/06/2019 04:13 WG1245643 3
Total Xylene U J3 0.000510 0.00150 0.00150 1 03/06/2019 04:13 WG1245643 Ss
(S) a,a,a-Trifluorotoluene(PID) 100 79.0-125 03/06/2019 04:13 WG1245643
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143 6
TPH C12 - C28 0.674 J 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143
7
TPH C6 - C35 0.674 J 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143
Qc
(S) o-Terphenyl 89.8 70.0-130 03/07/2019 18:20 WG1246143
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 28 of 161
MW-6 SAMPLE RESULTS - 06 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 16:00 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1120 J3 5.64 20.0 20.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 416 2.71 20.0 20.0 1 03/07/2019 15:12 WG1245955
5
Sample Narrative: Tr
L1075168-06 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 267 0.260 1.00 5.00 5 03/06/2019 04:18 WG1245159 8
Sulfate 135 0.387 5.00 25.0 5 03/06/2019 04:18 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.90 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-06 WG1245130: 6.9 at 11.4C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 1830 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:03 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00161 J 0.000250 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Barium 0.125 0.000360 0.00500 0.00500 1 03/06/2019 21:11 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:11 WG1245245
Calcium 144 0.0460 1.00 1.00 1 03/06/2019 21:11 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Magnesium 19.4 0.100 1.00 1.00 1 03/06/2019 21:11 WG1245245
Potassium 4.00 0.0370 1.00 1.00 1 03/06/2019 21:11 WG1245245
Selenium 0.00186 J 0.000380 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Sodium 212 0.110 1.00 1.00 1 03/06/2019 21:11 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 29 of 161
MW-6 SAMPLE RESULTS - 06 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 16:00 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 04:34 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 04:34 WG1245643
Ethylbenzene U J3 0.000160 0.000500 0.000500 1 03/06/2019 04:34 WG1245643 3
Total Xylene U J3 0.000510 0.00150 0.00150 1 03/06/2019 04:34 WG1245643 Ss
(S) a,a,a-Trifluorotoluene(PID) 101 79.0-125 03/06/2019 04:34 WG1245643
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479
Qc
(S) o-Terphenyl 86.9 70.0-130 03/06/2019 07:10 WG1245479
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 30 of 161
MW-7 SAMPLE RESULTS - 07 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 12:45 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 2030 14.1 50.0 50.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 432 2.71 20.0 20.0 1 03/07/2019 15:19 WG1245955
5
Sample Narrative: Tr
L1075168-07 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 804 1.04 1.00 20.0 20 03/06/2019 04:33 WG1245159 8
Sulfate 127 1.55 5.00 100 20 03/06/2019 04:33 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.76 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-07 WG1245130: 6.76 at 11C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 3300 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:05 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0174 0.000250 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Barium 0.692 0.000360 0.00500 0.00500 1 03/06/2019 21:16 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:16 WG1245245
Calcium 277 0.0460 1.00 1.00 1 03/06/2019 21:16 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Magnesium 28.7 0.100 1.00 1.00 1 03/06/2019 21:16 WG1245245
Potassium 3.59 0.0370 1.00 1.00 1 03/06/2019 21:16 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Sodium 319 0.110 1.00 1.00 1 03/06/2019 21:16 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 31 of 161
MW-7 SAMPLE RESULTS - 07 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 12:45 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 04:55 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 04:55 WG1245643
Ethylbenzene U J3 0.000160 0.000500 0.000500 1 03/06/2019 04:55 WG1245643 3
Total Xylene U J3 0.000510 0.00150 0.00150 1 03/06/2019 04:55 WG1245643 Ss
(S) a,a,a-Trifluorotoluene(PID) 100 79.0-125 03/06/2019 04:55 WG1245643
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479
Qc
(S) o-Terphenyl 79.2 70.0-130 03/06/2019 07:26 WG1245479
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 32 of 161
MW-8 SAMPLE RESULTS - 08 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 11:35 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 287 2.82 10.0 10.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 176 2.71 20.0 20.0 1 03/07/2019 15:26 WG1245955
5
Sample Narrative: Tr
L1075168-08 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 13.3 0.0519 1.00 1.00 1 03/06/2019 04:49 WG1245159 8
Sulfate 10.7 0.0774 5.00 5.00 1 03/06/2019 04:49 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.23 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-08 WG1245130: 7.23 at 11.1C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 405 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:08 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00720 0.000250 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Barium 0.472 0.000360 0.00500 0.00500 1 03/06/2019 21:21 WG1245245
Cadmium 0.000219 J 0.000160 0.00100 0.00100 1 03/06/2019 21:21 WG1245245
Calcium 39.8 0.0460 1.00 1.00 1 03/06/2019 21:21 WG1245245
Chromium 0.0137 0.000540 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Lead 0.00947 0.000240 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Magnesium 8.83 0.100 1.00 1.00 1 03/06/2019 21:21 WG1245245
Potassium 2.54 0.0370 1.00 1.00 1 03/06/2019 21:21 WG1245245
Selenium 0.00155 J 0.000380 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Sodium 39.8 0.110 1.00 1.00 1 03/06/2019 21:21 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 33 of 161
MW-8 SAMPLE RESULTS - 08 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 11:35 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/11/2019 13:24 WG1248019
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/11/2019 13:24 WG1248019
Ethylbenzene U 0.000160 0.000500 0.000500 1 03/11/2019 13:24 WG1248019 3
Total Xylene U 0.000510 0.00150 0.00150 1 03/11/2019 13:24 WG1248019 Ss
(S) a,a,a-Trifluorotoluene(PID) 96.7 79.0-125 03/11/2019 13:24 WG1248019
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479
Qc
(S) o-Terphenyl 91.3 70.0-130 03/06/2019 07:43 WG1245479
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 34 of 161
MW-9 SAMPLE RESULTS - 09 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 11:15 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 301 2.82 10.0 10.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 231 2.71 20.0 20.0 1 03/07/2019 15:42 WG1245955
5
Sample Narrative: Tr
L1075168-09 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 13.0 0.0519 1.00 1.00 1 03/06/2019 05:35 WG1245159 8
Sulfate 19.9 0.0774 5.00 5.00 1 03/06/2019 05:35 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.12 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-09 WG1245130: 7.12 at 13.3C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 524 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:10 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00114 J 0.000250 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Barium 0.142 0.000360 0.00500 0.00500 1 03/06/2019 21:25 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:25 WG1245245
Calcium 14.8 0.0460 1.00 1.00 1 03/06/2019 21:25 WG1245245
Chromium 0.000997 BJ 0.000540 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Lead 0.000395 J 0.000240 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Magnesium 4.26 0.100 1.00 1.00 1 03/06/2019 21:25 WG1245245
Potassium 0.423 J 0.0370 1.00 1.00 1 03/06/2019 21:25 WG1245245
Selenium 0.000484 J 0.000380 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Sodium 95.9 0.110 1.00 1.00 1 03/06/2019 21:25 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 35 of 161
MW-9 SAMPLE RESULTS - 09 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 11:15 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 05:38 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 05:38 WG1245643
Ethylbenzene U J3 0.000160 0.000500 0.000500 1 03/06/2019 05:38 WG1245643 3
Total Xylene U J3 0.000510 0.00150 0.00150 1 03/06/2019 05:38 WG1245643 Ss
(S) a,a,a-Trifluorotoluene(PID) 99.0 79.0-125 03/06/2019 05:38 WG1245643
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479
Qc
(S) o-Terphenyl 82.9 70.0-130 03/06/2019 08:00 WG1245479
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 36 of 161
MW-10 SAMPLE RESULTS - 10 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 12:15 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 331 2.82 10.0 10.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 277 2.71 20.0 20.0 1 03/07/2019 15:50 WG1245955
5
Sample Narrative: Tr
L1075168-10 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 10.9 0.0519 1.00 1.00 1 03/06/2019 05:50 WG1245159 8
Sulfate 5.99 0.0774 5.00 5.00 1 03/06/2019 05:50 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.46 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-10 WG1245130: 7.46 at 13.7C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 564 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:13 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00397 0.000250 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Barium 0.546 0.000360 0.00500 0.00500 1 03/06/2019 21:30 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:30 WG1245245
Calcium 58.4 0.0460 1.00 1.00 1 03/06/2019 21:30 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Magnesium 11.1 0.100 1.00 1.00 1 03/06/2019 21:30 WG1245245
Potassium 0.277 J 0.0370 1.00 1.00 1 03/06/2019 21:30 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Sodium 46.8 0.110 1.00 1.00 1 03/06/2019 21:30 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 37 of 161
MW-10 SAMPLE RESULTS - 10 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 12:15 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 05:59 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 05:59 WG1245643
Ethylbenzene U J3 0.000160 0.000500 0.000500 1 03/06/2019 05:59 WG1245643 3
Total Xylene U J3 0.000510 0.00150 0.00150 1 03/06/2019 05:59 WG1245643 Ss
(S) a,a,a-Trifluorotoluene(PID) 97.1 79.0-125 03/06/2019 05:59 WG1245643
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678
Qc
(S) o-Terphenyl 89.2 70.0-130 03/06/2019 17:54 WG1245678
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 38 of 161
MW-11 SAMPLE RESULTS - 11 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 13:15 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 2110 14.1 50.0 50.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 298 2.71 20.0 20.0 1 03/07/2019 15:58 WG1245955
5
Sample Narrative: Tr
L1075168-11 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 858 1.04 1.00 20.0 20 03/06/2019 06:37 WG1245159 8
Sulfate 14.9 0.0774 5.00 5.00 1 03/06/2019 10:28 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.95 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-11 WG1245130: 6.95 at 12.9C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 3090 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:15 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0199 0.000250 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Barium 3.06 0.000360 0.00500 0.00500 1 03/06/2019 21:35 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:35 WG1245245
Calcium 265 0.0460 1.00 1.00 1 03/06/2019 21:35 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Magnesium 27.9 0.100 1.00 1.00 1 03/06/2019 21:35 WG1245245
Potassium 4.83 0.0370 1.00 1.00 1 03/06/2019 21:35 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Sodium 270 0.110 1.00 1.00 1 03/06/2019 21:35 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 39 of 161
MW-11 SAMPLE RESULTS - 11 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 13:15 L1075168

Volatile Organic Compounds (GC) by Method 8021B


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 06:20 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 06:20 WG1245643
Ethylbenzene U 0.000160 0.000500 0.000500 1 03/06/2019 06:20 WG1245643 3
Total Xylene 0.000570 J J6 0.000510 0.00150 0.00150 1 03/06/2019 06:20 WG1245643 Ss
(S) a,a,a-Trifluorotoluene(PID) 98.2 79.0-125 03/06/2019 06:20 WG1245643
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 5
Tr
Analyte mg/l mg/l mg/l mg/l date / time
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678
Qc
(S) o-Terphenyl 93.1 70.0-130 03/06/2019 18:10 WG1245678
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 40 of 161
MW-12 SAMPLE RESULTS - 12 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 13:45 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 2520 14.1 50.0 50.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 361 2.71 20.0 20.0 1 03/07/2019 16:05 WG1245955
5
Sample Narrative: Tr
L1075168-12 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 885 1.04 1.00 20.0 20 03/06/2019 06:52 WG1245159 8
Sulfate 18.5 0.0774 5.00 5.00 1 03/06/2019 10:43 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.88 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-12 WG1245130: 6.88 at 12.3C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 3250 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:17 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00129 J 0.000250 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Barium 3.57 0.000360 0.00500 0.00500 1 03/06/2019 21:39 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:39 WG1245245
Calcium 260 0.0460 1.00 1.00 1 03/06/2019 21:39 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Magnesium 27.0 0.100 1.00 1.00 1 03/06/2019 21:39 WG1245245
Potassium 3.88 0.0370 1.00 1.00 1 03/06/2019 21:39 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Sodium 307 0.110 1.00 1.00 1 03/06/2019 21:39 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 41 of 161
MW-12 SAMPLE RESULTS - 12 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 13:45 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone U 0.0100 0.0500 0.0500 1 03/05/2019 20:52 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 20:52 WG1245356
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/05/2019 20:52 WG1245356 3
Benzene U 0.000331 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Bromomethane U 0.000866 0.00500 0.00500 1 03/05/2019 20:52 WG1245356 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/05/2019 20:52 WG1245356
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Ethylbenzene U 0.000384 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
2-Butanone (MEK) U 0.00393 0.0100 0.0100 1 03/05/2019 20:52 WG1245356
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/05/2019 20:52 WG1245356
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Naphthalene U 0.00100 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
n-Propylbenzene U 0.000349 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/05/2019 20:52 WG1245356

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 42 of 161
MW-12 SAMPLE RESULTS - 12 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 13:45 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Trichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/05/2019 20:52 WG1245356 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/05/2019 20:52 WG1245356
4
1,2,4-Trimethylbenzene U 0.000373 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Cn
1,2,3-Trimethylbenzene U 0.000321 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
1,3,5-Trimethylbenzene U 0.000387 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 Tr
Xylenes, Total U 0.00106 0.00300 0.00300 1 03/05/2019 20:52 WG1245356
6
(S) Toluene-d8 108 80.0-120 03/05/2019 20:52 WG1245356
Sr
(S) 4-Bromofluorobenzene 105 77.0-126 03/05/2019 20:52 WG1245356
(S) 1,2-Dichloroethane-d4 104 70.0-130 03/05/2019 20:52 WG1245356 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678
Al
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678 10
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678 Sc
(S) o-Terphenyl 93.0 70.0-130 03/06/2019 18:26 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.000316 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Acenaphthylene U 0.000309 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Benzidine U 0.00432 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Benzo(a)anthracene U 0.0000975 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Benzo(b)fluoranthene U 0.0000896 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Benzo(k)fluoranthene U 0.000355 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Benzo(g,h,i)perylene U 0.000161 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Benzo(a)pyrene U 0.000340 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Bis(2-chlorethoxy)methane U 0.000329 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Bis(2-chloroethyl)ether U 0.00162 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Bis(2-chloroisopropyl)ether U 0.000445 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
4-Bromophenyl-phenylether U 0.000335 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
2-Chloronaphthalene U 0.000330 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
4-Chlorophenyl-phenylether U 0.000303 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Dibenz(a,h)anthracene U 0.000279 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
3,3-Dichlorobenzidine U 0.00202 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
2,4-Dinitrotoluene U 0.00165 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
2,6-Dinitrotoluene U 0.000279 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Fluoranthene U 0.000310 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Fluorene U 0.000323 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Hexachlorobenzene U 0.000341 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Hexachloro-1,3-butadiene U 0.000329 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Hexachlorocyclopentadiene U 0.00233 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Hexachloroethane U 0.000365 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Naphthalene U 0.000372 0.00100 0.00100 1 03/07/2019 17:03 WG1246279

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 43 of 161
MW-12 SAMPLE RESULTS - 12 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 13:45 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.000367 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Tc
n-Nitrosodimethylamine U 0.00126 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
n-Nitrosodiphenylamine U 0.00119 0.0100 0.0100 1 03/07/2019 17:03 WG1246279 3
n-Nitrosodi-n-propylamine U 0.000403 0.0100 0.0100 1 03/07/2019 17:03 WG1246279 Ss
Phenanthrene U 0.000366 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
4
Benzylbutyl phthalate U 0.000275 0.00300 0.00300 1 03/07/2019 17:03 WG1246279
Cn
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 0.00300 1 03/07/2019 17:03 WG1246279
Di-n-butyl phthalate U 0.000266 0.00300 0.00300 1 03/07/2019 17:03 WG1246279 5
Diethyl phthalate 0.000491 J 0.000282 0.00300 0.00300 1 03/07/2019 17:03 WG1246279 Tr
Dimethyl phthalate U 0.000283 0.00300 0.00300 1 03/07/2019 17:03 WG1246279
6
Di-n-octyl phthalate U 0.000278 0.00300 0.00300 1 03/07/2019 17:03 WG1246279
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
1,2,4-Trichlorobenzene U 0.000355 0.0100 0.0100 1 03/07/2019 17:03 WG1246279 7
4-Chloro-3-methylphenol U 0.000263 0.0100 0.0100 1 03/07/2019 17:03 WG1246279 Qc
2-Chlorophenol U 0.000283 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
8
2,4-Dichlorophenol U 0.000284 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Gl
2,4-Dimethylphenol U 0.000264 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 0.0100 1 03/07/2019 17:03 WG1246279 9
2,4-Dinitrophenol U 0.00325 0.0100 0.0100 1 03/07/2019 17:03 WG1246279 Al
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Sc
Pentachlorophenol U J3 0.000313 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Phenol 0.00127 J 0.000334 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
2,4,6-Trichlorophenol U 0.000297 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
(S) 2-Fluorophenol 34.6 10.0-120 03/07/2019 17:03 WG1246279
(S) Phenol-d5 21.1 10.0-120 03/07/2019 17:03 WG1246279
(S) Nitrobenzene-d5 49.1 10.0-127 03/07/2019 17:03 WG1246279
(S) 2-Fluorobiphenyl 54.7 10.0-130 03/07/2019 17:03 WG1246279
(S) 2,4,6-Tribromophenol 61.0 10.0-155 03/07/2019 17:03 WG1246279
(S) p-Terphenyl-d14 66.6 10.0-128 03/07/2019 17:03 WG1246279

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 44 of 161
MW-13 SAMPLE RESULTS - 13 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 14:15 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 15600 56.4 200 200 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 123 2.71 20.0 20.0 1 03/07/2019 16:12 WG1245955
5
Sample Narrative: Tr
L1075168-13 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 7610 5.19 1.00 100 100 03/06/2019 07:23 WG1245159 8
Sulfate 0.291 J 0.0774 5.00 5.00 1 03/06/2019 10:59 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.16 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-13 WG1245130: 6.16 at 12.4C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 21200 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury 0.0000566 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:25 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0582 0.000250 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Barium 28.9 0.00180 0.00500 0.0250 5 03/06/2019 22:44 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:44 WG1245245
Calcium 1480 0.230 1.00 5.00 5 03/06/2019 22:44 WG1245245
Chromium 0.00140 BJ 0.000540 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Lead 0.000647 J 0.000240 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Magnesium 4.00 0.100 1.00 1.00 1 03/06/2019 21:44 WG1245245
Potassium 156 0.0370 1.00 1.00 1 03/06/2019 21:44 WG1245245
Selenium 0.00172 J 0.000380 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Sodium 2670 0.550 1.00 5.00 5 03/06/2019 22:44 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 45 of 161
MW-13 SAMPLE RESULTS - 13 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 14:15 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone 0.0360 J 0.0100 0.0500 0.0500 1 03/05/2019 21:13 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 21:13 WG1245356
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/05/2019 21:13 WG1245356 3
Benzene 0.00547 0.000331 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Bromomethane U 0.000866 0.00500 0.00500 1 03/05/2019 21:13 WG1245356 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/05/2019 21:13 WG1245356
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Ethylbenzene 0.00434 0.000384 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Isopropylbenzene 0.000430 J 0.000326 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
2-Butanone (MEK) 0.00713 J 0.00393 0.0100 0.0100 1 03/05/2019 21:13 WG1245356
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
4-Methyl-2-pentanone (MIBK) 0.0656 0.00214 0.0100 0.0100 1 03/05/2019 21:13 WG1245356
Methyl tert-butyl ether 0.00101 0.000367 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Naphthalene 0.0249 0.00100 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
n-Propylbenzene 0.000559 J 0.000349 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Toluene 0.00360 0.000412 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/05/2019 21:13 WG1245356

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 46 of 161
MW-13 SAMPLE RESULTS - 13 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 14:15 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Trichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/05/2019 21:13 WG1245356 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/05/2019 21:13 WG1245356
4
1,2,4-Trimethylbenzene 0.00261 0.000373 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Cn
1,2,3-Trimethylbenzene 0.0187 0.000321 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
1,3,5-Trimethylbenzene 0.000880 J 0.000387 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 Tr
Xylenes, Total 0.0113 0.00106 0.00300 0.00300 1 03/05/2019 21:13 WG1245356
6
(S) Toluene-d8 105 80.0-120 03/05/2019 21:13 WG1245356
Sr
(S) 4-Bromofluorobenzene 105 77.0-126 03/05/2019 21:13 WG1245356
(S) 1,2-Dichloroethane-d4 103 70.0-130 03/05/2019 21:13 WG1245356 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 1.39 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678
Al
TPH C12 - C28 14.4 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678 10
TPH C6 - C35 15.8 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678 Sc
(S) o-Terphenyl 89.6 70.0-130 03/06/2019 18:42 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.000316 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Acenaphthylene U 0.000309 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Benzidine U 0.00432 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Benzo(a)anthracene U 0.0000975 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Benzo(b)fluoranthene U 0.0000896 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Benzo(k)fluoranthene U 0.000355 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Benzo(g,h,i)perylene U 0.000161 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Benzo(a)pyrene U 0.000340 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Bis(2-chlorethoxy)methane U 0.000329 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Bis(2-chloroethyl)ether U 0.00162 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Bis(2-chloroisopropyl)ether U 0.000445 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
4-Bromophenyl-phenylether U 0.000335 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
2-Chloronaphthalene U 0.000330 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
4-Chlorophenyl-phenylether U 0.000303 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Dibenz(a,h)anthracene U 0.000279 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
3,3-Dichlorobenzidine U 0.00202 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
2,4-Dinitrotoluene U 0.00165 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
2,6-Dinitrotoluene U 0.000279 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Fluoranthene U 0.000310 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Fluorene U 0.000323 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Hexachlorobenzene U 0.000341 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Hexachloro-1,3-butadiene U 0.000329 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Hexachlorocyclopentadiene U 0.00233 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Hexachloroethane U 0.000365 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Naphthalene 0.00168 0.000372 0.00100 0.00100 1 03/07/2019 22:11 WG1246279

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 47 of 161
MW-13 SAMPLE RESULTS - 13 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 14:15 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.000367 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Tc
n-Nitrosodimethylamine U 0.00126 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
n-Nitrosodiphenylamine U 0.00119 0.0100 0.0100 1 03/07/2019 22:11 WG1246279 3
n-Nitrosodi-n-propylamine U 0.000403 0.0100 0.0100 1 03/07/2019 22:11 WG1246279 Ss
Phenanthrene U 0.000366 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
4
Benzylbutyl phthalate U 0.000275 0.00300 0.00300 1 03/07/2019 22:11 WG1246279
Cn
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 0.00300 1 03/07/2019 22:11 WG1246279
Di-n-butyl phthalate U 0.000266 0.00300 0.00300 1 03/07/2019 22:11 WG1246279 5
Diethyl phthalate U 0.000282 0.00300 0.00300 1 03/07/2019 22:11 WG1246279 Tr
Dimethyl phthalate U 0.000283 0.00300 0.00300 1 03/07/2019 22:11 WG1246279
6
Di-n-octyl phthalate U 0.000278 0.00300 0.00300 1 03/07/2019 22:11 WG1246279
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
1,2,4-Trichlorobenzene U 0.000355 0.0100 0.0100 1 03/07/2019 22:11 WG1246279 7
4-Chloro-3-methylphenol U 0.000263 0.0100 0.0100 1 03/07/2019 22:11 WG1246279 Qc
2-Chlorophenol U 0.000283 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
8
2,4-Dichlorophenol U 0.000284 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Gl
2,4-Dimethylphenol 0.00584 J 0.000264 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 0.0100 1 03/07/2019 22:11 WG1246279 9
2,4-Dinitrophenol U 0.00325 0.0100 0.0100 1 03/07/2019 22:11 WG1246279 Al
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Sc
Pentachlorophenol U J3 0.000313 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Phenol 0.00244 J 0.000334 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
2,4,6-Trichlorophenol U 0.000297 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
(S) 2-Fluorophenol 37.4 10.0-120 03/07/2019 22:11 WG1246279
(S) Phenol-d5 23.5 10.0-120 03/07/2019 22:11 WG1246279
(S) Nitrobenzene-d5 50.3 10.0-127 03/07/2019 22:11 WG1246279
(S) 2-Fluorobiphenyl 37.5 10.0-130 03/07/2019 22:11 WG1246279
(S) 2,4,6-Tribromophenol 83.0 10.0-155 03/07/2019 22:11 WG1246279
(S) p-Terphenyl-d14 58.4 10.0-128 03/07/2019 22:11 WG1246279

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 48 of 161
PSW-1 SAMPLE RESULTS - 14 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:10 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1590 14.1 50.0 50.0 1 03/07/2019 23:09 WG1246058 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 346 2.71 20.0 20.0 1 03/07/2019 16:18 WG1245955
5
Sample Narrative: Tr
L1075168-14 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 584 0.519 1.00 10.0 10 03/06/2019 07:38 WG1245159 8
Sulfate 105 0.774 5.00 50.0 10 03/06/2019 07:38 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.77 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-14 WG1245130: 7.77 at 12.2C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 2690 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury 0.0000997 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:27 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0250 0.000250 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Barium 1.70 0.000360 0.00500 0.00500 1 03/06/2019 21:49 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:49 WG1245245
Calcium 102 0.0460 1.00 1.00 1 03/06/2019 21:49 WG1245245
Chromium 0.00374 B 0.000540 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Lead 0.00526 0.000240 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Magnesium 7.58 0.100 1.00 1.00 1 03/06/2019 21:49 WG1245245
Potassium 17.7 0.0370 1.00 1.00 1 03/06/2019 21:49 WG1245245
Selenium 0.00166 J 0.000380 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Sodium 433 0.110 1.00 1.00 1 03/06/2019 21:49 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 49 of 161
PSW-1 SAMPLE RESULTS - 14 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:10 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone 0.228 0.0100 0.0500 0.0500 1 03/05/2019 21:33 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 21:33 WG1245356
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/05/2019 21:33 WG1245356 3
Benzene 0.000375 J 0.000331 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Bromomethane U 0.000866 0.00500 0.00500 1 03/05/2019 21:33 WG1245356 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/05/2019 21:33 WG1245356
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Ethylbenzene 0.00254 0.000384 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
2-Butanone (MEK) 0.00707 J 0.00393 0.0100 0.0100 1 03/05/2019 21:33 WG1245356
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/05/2019 21:33 WG1245356
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Naphthalene 0.00147 J 0.00100 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
n-Propylbenzene 0.000442 J 0.000349 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Toluene 0.00750 0.000412 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/05/2019 21:33 WG1245356

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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03/13/19 15:42
16:10 50 of 161
PSW-1 SAMPLE RESULTS - 14 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:10 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Trichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/05/2019 21:33 WG1245356 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/05/2019 21:33 WG1245356
4
1,2,4-Trimethylbenzene 0.00266 0.000373 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Cn
1,2,3-Trimethylbenzene 0.00106 0.000321 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
1,3,5-Trimethylbenzene 0.000981 J 0.000387 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 Tr
Xylenes, Total 0.0214 0.00106 0.00300 0.00300 1 03/05/2019 21:33 WG1245356
6
(S) Toluene-d8 108 80.0-120 03/05/2019 21:33 WG1245356
Sr
(S) 4-Bromofluorobenzene 108 77.0-126 03/05/2019 21:33 WG1245356
(S) 1,2-Dichloroethane-d4 105 70.0-130 03/05/2019 21:33 WG1245356 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678
Al
TPH C12 - C28 9.56 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678
TPH C28 - C35 0.749 J 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678 10
TPH C6 - C35 10.3 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678 Sc
(S) o-Terphenyl 86.7 70.0-130 03/06/2019 18:59 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.00316 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Acenaphthylene U 0.00309 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Benzo(a)anthracene U 0.000975 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Benzo(b)fluoranthene U 0.000896 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Benzo(k)fluoranthene U 0.00355 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Benzo(g,h,i)perylene U 0.00161 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Benzo(a)pyrene U 0.00340 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Bis(2-chlorethoxy)methane U 0.00329 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Bis(2-chloroethyl)ether U 0.0162 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Bis(2-chloroisopropyl)ether U 0.00445 0.0100 0.100 10 03/07/2019 07:37 WG1245476
4-Bromophenyl-phenylether U 0.00335 0.0100 0.100 10 03/07/2019 07:37 WG1245476
2-Chloronaphthalene U 0.00330 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
4-Chlorophenyl-phenylether U 0.00303 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Dibenz(a,h)anthracene U 0.00279 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
3,3-Dichlorobenzidine U 0.0202 0.0100 0.100 10 03/07/2019 07:37 WG1245476
2,4-Dinitrotoluene U 0.0165 0.0100 0.100 10 03/07/2019 07:37 WG1245476
2,6-Dinitrotoluene U 0.00279 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Fluoranthene U 0.00310 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Hexachlorobenzene U 0.00341 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Hexachloro-1,3-butadiene U 0.00329 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Hexachlorocyclopentadiene U 0.0233 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Hexachloroethane U 0.00365 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Indeno(1,2,3-cd)pyrene U 0.00279 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 07:37 WG1245476

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 51 of 161
PSW-1 SAMPLE RESULTS - 14 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:10 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.00367 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Tc
n-Nitrosodimethylamine U 0.0126 0.0100 0.100 10 03/07/2019 07:37 WG1245476
n-Nitrosodiphenylamine U 0.0119 0.0100 0.100 10 03/07/2019 07:37 WG1245476 3
n-Nitrosodi-n-propylamine U 0.00403 0.0100 0.100 10 03/07/2019 07:37 WG1245476 Ss
Phenanthrene U 0.00366 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
4
Benzylbutyl phthalate U 0.00275 0.00300 0.0300 10 03/07/2019 07:37 WG1245476
Cn
Bis(2-ethylhexyl)phthalate U 0.00709 0.00300 0.0300 10 03/07/2019 07:37 WG1245476
Di-n-butyl phthalate U 0.00266 0.00300 0.0300 10 03/07/2019 07:37 WG1245476 5
Diethyl phthalate U 0.00282 0.00300 0.0300 10 03/07/2019 07:37 WG1245476 Tr
Dimethyl phthalate U 0.00283 0.00300 0.0300 10 03/07/2019 07:37 WG1245476
6
Di-n-octyl phthalate U 0.00278 0.00300 0.0300 10 03/07/2019 07:37 WG1245476
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
1,2,4-Trichlorobenzene U 0.00355 0.0100 0.100 10 03/07/2019 07:37 WG1245476 7
4-Chloro-3-methylphenol U 0.00263 0.0100 0.100 10 03/07/2019 07:37 WG1245476 Qc
2-Chlorophenol U 0.00283 0.0100 0.100 10 03/07/2019 07:37 WG1245476
8
2,4-Dichlorophenol U 0.00284 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Gl
2,4-Dimethylphenol 0.0160 J 0.00264 0.0100 0.100 10 03/07/2019 07:37 WG1245476
4,6-Dinitro-2-methylphenol U 0.0262 0.0100 0.100 10 03/07/2019 07:37 WG1245476 9
2,4-Dinitrophenol U 0.0325 0.0100 0.100 10 03/07/2019 07:37 WG1245476 Al
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 07:37 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Sc
Pentachlorophenol U 0.00313 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 07:37 WG1245476
2,4,6-Trichlorophenol U 0.00297 0.0100 0.100 10 03/07/2019 07:37 WG1245476
(S) 2-Fluorophenol 47.5 10.0-120 03/07/2019 07:37 WG1245476
(S) Phenol-d5 33.4 10.0-120 03/07/2019 07:37 WG1245476
(S) Nitrobenzene-d5 73.8 10.0-127 03/07/2019 07:37 WG1245476
(S) 2-Fluorobiphenyl 72.6 10.0-130 03/07/2019 07:37 WG1245476
(S) 2,4,6-Tribromophenol 95.6 10.0-155 03/07/2019 07:37 WG1245476
(S) p-Terphenyl-d14 87.1 10.0-128 03/07/2019 07:37 WG1245476

Sample Narrative:
L1075168-14 WG1245476: Dilution due to viscosity.

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 52 of 161
PSW-2 SAMPLE RESULTS - 15 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:15 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1650 14.1 50.0 50.0 1 03/08/2019 01:53 WG1246059 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 348 2.71 20.0 20.0 1 03/07/2019 16:26 WG1245955
5
Sample Narrative: Tr
L1075168-15 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 595 0.519 1.00 10.0 10 03/06/2019 07:54 WG1245159 8
Sulfate 107 0.774 5.00 50.0 10 03/06/2019 07:54 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.88 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-15 WG1245130: 7.88 at 12.5C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 2670 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury 0.0000997 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:30 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0249 0.000250 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Barium 1.40 0.000360 0.00500 0.00500 1 03/06/2019 22:20 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:20 WG1245245
Calcium 102 0.0460 1.00 1.00 1 03/06/2019 22:20 WG1245245
Chromium 0.00370 B 0.000540 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Lead 0.00392 0.000240 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Magnesium 7.70 0.100 1.00 1.00 1 03/06/2019 22:20 WG1245245
Potassium 17.8 0.0370 1.00 1.00 1 03/06/2019 22:20 WG1245245
Selenium 0.00153 J 0.000380 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Sodium 439 0.110 1.00 1.00 1 03/06/2019 22:20 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 53 of 161
PSW-2 SAMPLE RESULTS - 15 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:15 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone 0.244 0.0100 0.0500 0.0500 1 03/06/2019 16:03 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 16:03 WG1245979
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/06/2019 16:03 WG1245979 3
Benzene 0.000379 J 0.000331 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Bromomethane U 0.000866 0.00500 0.00500 1 03/06/2019 16:03 WG1245979 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/06/2019 16:03 WG1245979
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Ethylbenzene 0.00215 0.000384 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
2-Butanone (MEK) 0.0122 0.00393 0.0100 0.0100 1 03/06/2019 16:03 WG1245979
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/06/2019 16:03 WG1245979
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Naphthalene 0.00118 J 0.00100 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
n-Propylbenzene 0.000460 J 0.000349 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Toluene 0.00635 0.000412 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/06/2019 16:03 WG1245979

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 54 of 161
PSW-2 SAMPLE RESULTS - 15 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:15 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Trichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/06/2019 16:03 WG1245979 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/06/2019 16:03 WG1245979
4
1,2,4-Trimethylbenzene 0.00263 0.000373 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Cn
1,2,3-Trimethylbenzene 0.00101 0.000321 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
1,3,5-Trimethylbenzene 0.000993 J 0.000387 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 Tr
Xylenes, Total 0.0182 0.00106 0.00300 0.00300 1 03/06/2019 16:03 WG1245979
6
(S) Toluene-d8 98.9 80.0-120 03/06/2019 16:03 WG1245979
Sr
(S) 4-Bromofluorobenzene 113 77.0-126 03/06/2019 16:03 WG1245979
(S) 1,2-Dichloroethane-d4 122 70.0-130 03/06/2019 16:03 WG1245979 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678
Al
TPH C12 - C28 10.3 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678
TPH C28 - C35 0.817 J 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678 10
TPH C6 - C35 11.1 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678 Sc
(S) o-Terphenyl 93.3 70.0-130 03/06/2019 19:15 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.00316 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Acenaphthylene U 0.00309 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Benzo(a)anthracene U 0.000975 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Benzo(b)fluoranthene U 0.000896 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Benzo(k)fluoranthene U 0.00355 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Benzo(g,h,i)perylene U 0.00161 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Benzo(a)pyrene U 0.00340 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Bis(2-chlorethoxy)methane U 0.00329 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Bis(2-chloroethyl)ether U 0.0162 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Bis(2-chloroisopropyl)ether U 0.00445 0.0100 0.100 10 03/07/2019 08:00 WG1245476
4-Bromophenyl-phenylether U 0.00335 0.0100 0.100 10 03/07/2019 08:00 WG1245476
2-Chloronaphthalene U 0.00330 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
4-Chlorophenyl-phenylether U 0.00303 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Dibenz(a,h)anthracene U 0.00279 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
3,3-Dichlorobenzidine U 0.0202 0.0100 0.100 10 03/07/2019 08:00 WG1245476
2,4-Dinitrotoluene U 0.0165 0.0100 0.100 10 03/07/2019 08:00 WG1245476
2,6-Dinitrotoluene U 0.00279 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Fluoranthene U 0.00310 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Hexachlorobenzene U 0.00341 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Hexachloro-1,3-butadiene U 0.00329 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Hexachlorocyclopentadiene U 0.0233 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Hexachloroethane U 0.00365 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Indeno(1,2,3-cd)pyrene U 0.00279 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 08:00 WG1245476

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 55 of 161
PSW-2 SAMPLE RESULTS - 15 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:15 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.00367 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Tc
n-Nitrosodimethylamine U 0.0126 0.0100 0.100 10 03/07/2019 08:00 WG1245476
n-Nitrosodiphenylamine U 0.0119 0.0100 0.100 10 03/07/2019 08:00 WG1245476 3
n-Nitrosodi-n-propylamine U 0.00403 0.0100 0.100 10 03/07/2019 08:00 WG1245476 Ss
Phenanthrene U 0.00366 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
4
Benzylbutyl phthalate U 0.00275 0.00300 0.0300 10 03/07/2019 08:00 WG1245476
Cn
Bis(2-ethylhexyl)phthalate U 0.00709 0.00300 0.0300 10 03/07/2019 08:00 WG1245476
Di-n-butyl phthalate U 0.00266 0.00300 0.0300 10 03/07/2019 08:00 WG1245476 5
Diethyl phthalate U 0.00282 0.00300 0.0300 10 03/07/2019 08:00 WG1245476 Tr
Dimethyl phthalate U 0.00283 0.00300 0.0300 10 03/07/2019 08:00 WG1245476
6
Di-n-octyl phthalate U 0.00278 0.00300 0.0300 10 03/07/2019 08:00 WG1245476
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
1,2,4-Trichlorobenzene U 0.00355 0.0100 0.100 10 03/07/2019 08:00 WG1245476 7
4-Chloro-3-methylphenol U 0.00263 0.0100 0.100 10 03/07/2019 08:00 WG1245476 Qc
2-Chlorophenol U 0.00283 0.0100 0.100 10 03/07/2019 08:00 WG1245476
8
2,4-Dichlorophenol U 0.00284 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Gl
2,4-Dimethylphenol 0.0274 J 0.00264 0.0100 0.100 10 03/07/2019 08:00 WG1245476
4,6-Dinitro-2-methylphenol U 0.0262 0.0100 0.100 10 03/07/2019 08:00 WG1245476 9
2,4-Dinitrophenol U 0.0325 0.0100 0.100 10 03/07/2019 08:00 WG1245476 Al
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 08:00 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Sc
Pentachlorophenol U 0.00313 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 08:00 WG1245476
2,4,6-Trichlorophenol U 0.00297 0.0100 0.100 10 03/07/2019 08:00 WG1245476
(S) 2-Fluorophenol 52.1 10.0-120 03/07/2019 08:00 WG1245476
(S) Phenol-d5 32.0 10.0-120 03/07/2019 08:00 WG1245476
(S) Nitrobenzene-d5 86.7 10.0-127 03/07/2019 08:00 WG1245476
(S) 2-Fluorobiphenyl 85.9 10.0-130 03/07/2019 08:00 WG1245476
(S) 2,4,6-Tribromophenol 111 10.0-155 03/07/2019 08:00 WG1245476
(S) p-Terphenyl-d14 95.5 10.0-128 03/07/2019 08:00 WG1245476

Sample Narrative:
L1075168-15 WG1245476: Dilution due to viscosity.

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 56 of 161
PSW-3 SAMPLE RESULTS - 16 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:20 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1610 14.1 50.0 50.0 1 03/08/2019 01:53 WG1246059 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 347 2.71 20.0 20.0 1 03/07/2019 16:34 WG1245955
5
Sample Narrative: Tr
L1075168-16 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 601 0.519 1.00 10.0 10 03/06/2019 08:09 WG1245159 8
Sulfate 107 0.774 5.00 50.0 10 03/06/2019 08:09 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.91 T8 1 03/05/2019 11:55 WG1245130

Sample Narrative:
L1075168-16 WG1245130: 7.91 at 13.3C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 2700 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury 0.000104 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:32 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0258 0.000250 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Barium 2.82 0.000360 0.00500 0.00500 1 03/06/2019 22:25 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:25 WG1245245
Calcium 108 0.0460 1.00 1.00 1 03/06/2019 22:25 WG1245245
Chromium 0.00475 B 0.000540 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Lead 0.00803 0.000240 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Magnesium 7.87 0.100 1.00 1.00 1 03/06/2019 22:25 WG1245245
Potassium 17.7 0.0370 1.00 1.00 1 03/06/2019 22:25 WG1245245
Selenium 0.00167 J 0.000380 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Sodium 438 0.110 1.00 1.00 1 03/06/2019 22:25 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 57 of 161
PSW-3 SAMPLE RESULTS - 16 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:20 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone 0.266 0.0100 0.0500 0.0500 1 03/06/2019 16:22 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 16:22 WG1245979
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/06/2019 16:22 WG1245979 3
Benzene 0.000338 J 0.000331 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Bromomethane U 0.000866 0.00500 0.00500 1 03/06/2019 16:22 WG1245979 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/06/2019 16:22 WG1245979
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Ethylbenzene 0.00222 0.000384 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
2-Butanone (MEK) 0.0123 0.00393 0.0100 0.0100 1 03/06/2019 16:22 WG1245979
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/06/2019 16:22 WG1245979
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Naphthalene 0.00124 J 0.00100 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
n-Propylbenzene 0.000371 J 0.000349 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Toluene 0.00691 0.000412 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/06/2019 16:22 WG1245979

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 58 of 161
PSW-3 SAMPLE RESULTS - 16 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:20 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Trichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/06/2019 16:22 WG1245979 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/06/2019 16:22 WG1245979
4
1,2,4-Trimethylbenzene 0.00256 0.000373 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Cn
1,2,3-Trimethylbenzene 0.000975 J 0.000321 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
1,3,5-Trimethylbenzene 0.000917 J 0.000387 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 Tr
Xylenes, Total 0.0200 0.00106 0.00300 0.00300 1 03/06/2019 16:22 WG1245979
6
(S) Toluene-d8 96.2 80.0-120 03/06/2019 16:22 WG1245979
Sr
(S) 4-Bromofluorobenzene 129 J1 77.0-126 03/06/2019 16:22 WG1245979
(S) 1,2-Dichloroethane-d4 123 70.0-130 03/06/2019 16:22 WG1245979 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 0.641 J 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678
Al
TPH C12 - C28 9.26 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678
TPH C28 - C35 0.762 J 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678 10
TPH C6 - C35 10.7 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678 Sc
(S) o-Terphenyl 85.1 70.0-130 03/06/2019 19:31 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.00316 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Acenaphthylene U 0.00309 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Benzo(a)anthracene U 0.000975 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Benzo(b)fluoranthene U 0.000896 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Benzo(k)fluoranthene U 0.00355 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Benzo(g,h,i)perylene U 0.00161 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Benzo(a)pyrene U 0.00340 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Bis(2-chlorethoxy)methane U 0.00329 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Bis(2-chloroethyl)ether U 0.0162 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Bis(2-chloroisopropyl)ether U 0.00445 0.0100 0.100 10 03/07/2019 08:24 WG1245476
4-Bromophenyl-phenylether U 0.00335 0.0100 0.100 10 03/07/2019 08:24 WG1245476
2-Chloronaphthalene U 0.00330 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
4-Chlorophenyl-phenylether U 0.00303 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Dibenz(a,h)anthracene U 0.00279 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
3,3-Dichlorobenzidine U 0.0202 0.0100 0.100 10 03/07/2019 08:24 WG1245476
2,4-Dinitrotoluene U 0.0165 0.0100 0.100 10 03/07/2019 08:24 WG1245476
2,6-Dinitrotoluene U 0.00279 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Fluoranthene U 0.00310 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Hexachlorobenzene U 0.00341 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Hexachloro-1,3-butadiene U 0.00329 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Hexachlorocyclopentadiene U 0.0233 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Hexachloroethane U 0.00365 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Indeno(1,2,3-cd)pyrene U 0.00279 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 08:24 WG1245476

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 59 of 161
PSW-3 SAMPLE RESULTS - 16 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:20 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.00367 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Tc
n-Nitrosodimethylamine U 0.0126 0.0100 0.100 10 03/07/2019 08:24 WG1245476
n-Nitrosodiphenylamine U 0.0119 0.0100 0.100 10 03/07/2019 08:24 WG1245476 3
n-Nitrosodi-n-propylamine U 0.00403 0.0100 0.100 10 03/07/2019 08:24 WG1245476 Ss
Phenanthrene U 0.00366 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
4
Benzylbutyl phthalate U 0.00275 0.00300 0.0300 10 03/07/2019 08:24 WG1245476
Cn
Bis(2-ethylhexyl)phthalate U 0.00709 0.00300 0.0300 10 03/07/2019 08:24 WG1245476
Di-n-butyl phthalate U 0.00266 0.00300 0.0300 10 03/07/2019 08:24 WG1245476 5
Diethyl phthalate U 0.00282 0.00300 0.0300 10 03/07/2019 08:24 WG1245476 Tr
Dimethyl phthalate U 0.00283 0.00300 0.0300 10 03/07/2019 08:24 WG1245476
6
Di-n-octyl phthalate U 0.00278 0.00300 0.0300 10 03/07/2019 08:24 WG1245476
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
1,2,4-Trichlorobenzene U 0.00355 0.0100 0.100 10 03/07/2019 08:24 WG1245476 7
4-Chloro-3-methylphenol U 0.00263 0.0100 0.100 10 03/07/2019 08:24 WG1245476 Qc
2-Chlorophenol U 0.00283 0.0100 0.100 10 03/07/2019 08:24 WG1245476
8
2,4-Dichlorophenol U 0.00284 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Gl
2,4-Dimethylphenol 0.0174 J 0.00264 0.0100 0.100 10 03/07/2019 08:24 WG1245476
4,6-Dinitro-2-methylphenol U 0.0262 0.0100 0.100 10 03/07/2019 08:24 WG1245476 9
2,4-Dinitrophenol U 0.0325 0.0100 0.100 10 03/07/2019 08:24 WG1245476 Al
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 08:24 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Sc
Pentachlorophenol U 0.00313 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 08:24 WG1245476
2,4,6-Trichlorophenol U 0.00297 0.0100 0.100 10 03/07/2019 08:24 WG1245476
(S) 2-Fluorophenol 45.1 10.0-120 03/07/2019 08:24 WG1245476
(S) Phenol-d5 29.5 10.0-120 03/07/2019 08:24 WG1245476
(S) Nitrobenzene-d5 78.0 10.0-127 03/07/2019 08:24 WG1245476
(S) 2-Fluorobiphenyl 71.9 10.0-130 03/07/2019 08:24 WG1245476
(S) 2,4,6-Tribromophenol 92.3 10.0-155 03/07/2019 08:24 WG1245476
(S) p-Terphenyl-d14 76.0 10.0-128 03/07/2019 08:24 WG1245476

Sample Narrative:
L1075168-16 WG1245476: Dilution due to viscosity.

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 60 of 161
PSW-4 SAMPLE RESULTS - 17 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:25 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1640 14.1 50.0 50.0 1 03/08/2019 01:53 WG1246059 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 348 2.71 20.0 20.0 1 03/07/2019 16:42 WG1245955
5
Sample Narrative: Tr
L1075168-17 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 601 0.519 1.00 10.0 10 03/06/2019 08:24 WG1245159 8
Sulfate 111 0.774 5.00 50.0 10 03/06/2019 08:24 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.86 T8 1 03/06/2019 09:50 WG1245737

Sample Narrative:
L1075168-17 WG1245737: 7.86 at 17.6C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 2700 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury 0.000109 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:35 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0260 0.000250 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Barium 3.17 0.000360 0.00500 0.00500 1 03/06/2019 22:30 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:30 WG1245245
Calcium 110 0.0460 1.00 1.00 1 03/06/2019 22:30 WG1245245
Chromium 0.00612 0.000540 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Lead 0.00902 0.000240 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Magnesium 8.27 0.100 1.00 1.00 1 03/06/2019 22:30 WG1245245
Potassium 18.0 0.0370 1.00 1.00 1 03/06/2019 22:30 WG1245245
Selenium 0.00225 0.000380 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Sodium 442 0.110 1.00 1.00 1 03/06/2019 22:30 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 61 of 161
PSW-4 SAMPLE RESULTS - 17 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:25 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone 0.0999 0.0100 0.0500 0.0500 1 03/06/2019 16:42 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 16:42 WG1245979
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/06/2019 16:42 WG1245979 3
Benzene 0.000368 J 0.000331 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Bromomethane U 0.000866 0.00500 0.00500 1 03/06/2019 16:42 WG1245979 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/06/2019 16:42 WG1245979
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Ethylbenzene 0.00222 0.000384 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
2-Butanone (MEK) 0.00894 J 0.00393 0.0100 0.0100 1 03/06/2019 16:42 WG1245979
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/06/2019 16:42 WG1245979
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Naphthalene 0.00116 J 0.00100 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
n-Propylbenzene 0.000528 J 0.000349 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Toluene 0.00697 0.000412 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/06/2019 16:42 WG1245979

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 62 of 161
PSW-4 SAMPLE RESULTS - 17 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:25 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Trichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/06/2019 16:42 WG1245979 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/06/2019 16:42 WG1245979
4
1,2,4-Trimethylbenzene 0.00260 0.000373 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Cn
1,2,3-Trimethylbenzene 0.00102 0.000321 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
1,3,5-Trimethylbenzene 0.00103 0.000387 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 Tr
Xylenes, Total 0.0186 0.00106 0.00300 0.00300 1 03/06/2019 16:42 WG1245979
6
(S) Toluene-d8 103 80.0-120 03/06/2019 16:42 WG1245979
Sr
(S) 4-Bromofluorobenzene 94.6 77.0-126 03/06/2019 16:42 WG1245979
(S) 1,2-Dichloroethane-d4 122 70.0-130 03/06/2019 16:42 WG1245979 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678
Al
TPH C12 - C28 9.96 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678
TPH C28 - C35 0.754 J 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678 10
TPH C6 - C35 10.7 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678 Sc
(S) o-Terphenyl 90.7 70.0-130 03/06/2019 19:48 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.00316 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Acenaphthylene U 0.00309 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Benzo(a)anthracene U 0.000975 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Benzo(b)fluoranthene U 0.000896 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Benzo(k)fluoranthene U 0.00355 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Benzo(g,h,i)perylene U 0.00161 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Benzo(a)pyrene U 0.00340 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Bis(2-chlorethoxy)methane U 0.00329 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Bis(2-chloroethyl)ether U 0.0162 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Bis(2-chloroisopropyl)ether U 0.00445 0.0100 0.100 10 03/07/2019 08:48 WG1245476
4-Bromophenyl-phenylether U 0.00335 0.0100 0.100 10 03/07/2019 08:48 WG1245476
2-Chloronaphthalene U 0.00330 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
4-Chlorophenyl-phenylether U 0.00303 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Dibenz(a,h)anthracene U 0.00279 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
3,3-Dichlorobenzidine U 0.0202 0.0100 0.100 10 03/07/2019 08:48 WG1245476
2,4-Dinitrotoluene U 0.0165 0.0100 0.100 10 03/07/2019 08:48 WG1245476
2,6-Dinitrotoluene U 0.00279 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Fluoranthene U 0.00310 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Hexachlorobenzene U 0.00341 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Hexachloro-1,3-butadiene U 0.00329 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Hexachlorocyclopentadiene U 0.0233 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Hexachloroethane U 0.00365 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Indeno(1,2,3-cd)pyrene U 0.00279 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 08:48 WG1245476

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 63 of 161
PSW-4 SAMPLE RESULTS - 17 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:25 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.00367 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Tc
n-Nitrosodimethylamine U 0.0126 0.0100 0.100 10 03/07/2019 08:48 WG1245476
n-Nitrosodiphenylamine U 0.0119 0.0100 0.100 10 03/07/2019 08:48 WG1245476 3
n-Nitrosodi-n-propylamine U 0.00403 0.0100 0.100 10 03/07/2019 08:48 WG1245476 Ss
Phenanthrene U 0.00366 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
4
Benzylbutyl phthalate U 0.00275 0.00300 0.0300 10 03/07/2019 08:48 WG1245476
Cn
Bis(2-ethylhexyl)phthalate U 0.00709 0.00300 0.0300 10 03/07/2019 08:48 WG1245476
Di-n-butyl phthalate U 0.00266 0.00300 0.0300 10 03/07/2019 08:48 WG1245476 5
Diethyl phthalate U 0.00282 0.00300 0.0300 10 03/07/2019 08:48 WG1245476 Tr
Dimethyl phthalate U 0.00283 0.00300 0.0300 10 03/07/2019 08:48 WG1245476
6
Di-n-octyl phthalate U 0.00278 0.00300 0.0300 10 03/07/2019 08:48 WG1245476
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
1,2,4-Trichlorobenzene U 0.00355 0.0100 0.100 10 03/07/2019 08:48 WG1245476 7
4-Chloro-3-methylphenol U 0.00263 0.0100 0.100 10 03/07/2019 08:48 WG1245476 Qc
2-Chlorophenol U 0.00283 0.0100 0.100 10 03/07/2019 08:48 WG1245476
8
2,4-Dichlorophenol U 0.00284 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Gl
2,4-Dimethylphenol 0.0191 J 0.00264 0.0100 0.100 10 03/07/2019 08:48 WG1245476
4,6-Dinitro-2-methylphenol U 0.0262 0.0100 0.100 10 03/07/2019 08:48 WG1245476 9
2,4-Dinitrophenol U 0.0325 0.0100 0.100 10 03/07/2019 08:48 WG1245476 Al
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 08:48 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Sc
Pentachlorophenol U 0.00313 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Phenol 0.00646 J 0.00334 0.0100 0.100 10 03/07/2019 08:48 WG1245476
2,4,6-Trichlorophenol U 0.00297 0.0100 0.100 10 03/07/2019 08:48 WG1245476
(S) 2-Fluorophenol 42.4 10.0-120 03/07/2019 08:48 WG1245476
(S) Phenol-d5 26.8 10.0-120 03/07/2019 08:48 WG1245476
(S) Nitrobenzene-d5 75.2 10.0-127 03/07/2019 08:48 WG1245476
(S) 2-Fluorobiphenyl 75.3 10.0-130 03/07/2019 08:48 WG1245476
(S) 2,4,6-Tribromophenol 89.6 10.0-155 03/07/2019 08:48 WG1245476
(S) p-Terphenyl-d14 78.6 10.0-128 03/07/2019 08:48 WG1245476

Sample Narrative:
L1075168-17 WG1245476: Dilution due to viscosity.

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 64 of 161
SK-1 SAMPLE RESULTS - 18 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:50 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 116 J3 2.82 10.0 10.0 1 03/08/2019 01:53 WG1246059 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 34.0 2.71 20.0 20.0 1 03/07/2019 16:49 WG1245955
5
Sample Narrative: Tr
L1075168-18 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 15.7 0.0519 1.00 1.00 1 03/06/2019 11:14 WG1245159 8
Sulfate 4.61 J 0.0774 5.00 5.00 1 03/06/2019 11:14 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.89 T8 1 03/06/2019 09:50 WG1245737

Sample Narrative:
L1075168-18 WG1245737: 6.89 at 17.6C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 138 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:37 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.00178 J 0.000250 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Barium 0.282 0.000360 0.00500 0.00500 1 03/06/2019 22:34 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:34 WG1245245
Calcium 10.8 0.0460 1.00 1.00 1 03/06/2019 22:34 WG1245245
Chromium 0.00337 B 0.000540 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Lead 0.00231 0.000240 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Magnesium 2.55 0.100 1.00 1.00 1 03/06/2019 22:34 WG1245245
Potassium 3.00 0.0370 1.00 1.00 1 03/06/2019 22:34 WG1245245
Selenium 0.000734 J 0.000380 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Sodium 12.1 0.110 1.00 1.00 1 03/06/2019 22:34 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 65 of 161
SK-1 SAMPLE RESULTS - 18 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:50 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone U 0.0100 0.0500 0.0500 1 03/06/2019 17:01 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 17:01 WG1245979
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/06/2019 17:01 WG1245979 3
Benzene 0.00382 0.000331 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Cn
Bromoform 0.00345 0.000469 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Bromomethane U 0.000866 0.00500 0.00500 1 03/06/2019 17:01 WG1245979 5
n-Butylbenzene 0.000593 J 0.000361 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 Tr
sec-Butylbenzene 0.000517 J 0.000365 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/06/2019 17:01 WG1245979
2-Chlorotoluene 0.000869 J 0.000375 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Sc
Dibromomethane 0.000372 J 0.000346 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Ethylbenzene 0.0281 0.000384 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Isopropylbenzene 0.00155 0.000326 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
2-Butanone (MEK) U 0.00393 0.0100 0.0100 1 03/06/2019 17:01 WG1245979
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/06/2019 17:01 WG1245979
Methyl tert-butyl ether 0.000432 J 0.000367 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Naphthalene 0.00525 0.00100 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
n-Propylbenzene 0.00394 0.000349 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Styrene 0.000574 J 0.000307 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Toluene 0.0605 0.000412 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/06/2019 17:01 WG1245979

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 66 of 161
SK-1 SAMPLE RESULTS - 18 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:50 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Trichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/06/2019 17:01 WG1245979 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/06/2019 17:01 WG1245979
4
1,2,4-Trimethylbenzene 0.0128 0.000373 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Cn
1,2,3-Trimethylbenzene 0.00396 0.000321 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
1,3,5-Trimethylbenzene 0.00712 0.000387 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 Tr
Xylenes, Total 0.213 0.00106 0.00300 0.00300 1 03/06/2019 17:01 WG1245979
6
(S) Toluene-d8 104 80.0-120 03/06/2019 17:01 WG1245979
Sr
(S) 4-Bromofluorobenzene 104 77.0-126 03/06/2019 17:01 WG1245979
(S) 1,2-Dichloroethane-d4 106 70.0-130 03/06/2019 17:01 WG1245979 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 0.622 J 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678
Al
TPH C12 - C28 0.816 J 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678 10
TPH C6 - C35 1.44 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678 Sc
(S) o-Terphenyl 86.8 70.0-130 03/06/2019 20:04 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.000316 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Acenaphthylene U 0.000309 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Benzidine U J3 0.00432 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Benzo(a)anthracene U 0.0000975 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Benzo(b)fluoranthene U 0.0000896 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Benzo(k)fluoranthene U 0.000355 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Benzo(g,h,i)perylene U 0.000161 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Benzo(a)pyrene U 0.000340 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Bis(2-chlorethoxy)methane U 0.000329 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Bis(2-chloroethyl)ether U 0.00162 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Bis(2-chloroisopropyl)ether U 0.000445 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
4-Bromophenyl-phenylether U 0.000335 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
2-Chloronaphthalene U 0.000330 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
4-Chlorophenyl-phenylether U 0.000303 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Dibenz(a,h)anthracene U 0.000279 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
3,3-Dichlorobenzidine U 0.00202 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
2,4-Dinitrotoluene U 0.00165 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
2,6-Dinitrotoluene U 0.000279 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Fluoranthene 0.000367 J 0.000310 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Fluorene 0.000370 J 0.000323 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Hexachlorobenzene U 0.000341 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Hexachloro-1,3-butadiene U 0.000329 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Hexachlorocyclopentadiene U 0.00233 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Hexachloroethane U 0.000365 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Naphthalene U 0.000372 0.00100 0.00100 1 03/07/2019 04:26 WG1245476

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 67 of 161
SK-1 SAMPLE RESULTS - 18 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:50 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.000367 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Tc
n-Nitrosodimethylamine U 0.00126 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
n-Nitrosodiphenylamine U 0.00119 0.0100 0.0100 1 03/07/2019 04:26 WG1245476 3
n-Nitrosodi-n-propylamine U 0.000403 0.0100 0.0100 1 03/07/2019 04:26 WG1245476 Ss
Phenanthrene U 0.000366 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
4
Benzylbutyl phthalate U 0.000275 0.00300 0.00300 1 03/07/2019 04:26 WG1245476
Cn
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 0.00300 1 03/07/2019 04:26 WG1245476
Di-n-butyl phthalate U 0.000266 0.00300 0.00300 1 03/07/2019 04:26 WG1245476 5
Diethyl phthalate U 0.000282 0.00300 0.00300 1 03/07/2019 04:26 WG1245476 Tr
Dimethyl phthalate U 0.000283 0.00300 0.00300 1 03/07/2019 04:26 WG1245476
6
Di-n-octyl phthalate U 0.000278 0.00300 0.00300 1 03/07/2019 04:26 WG1245476
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
1,2,4-Trichlorobenzene U 0.000355 0.0100 0.0100 1 03/07/2019 04:26 WG1245476 7
4-Chloro-3-methylphenol U 0.000263 0.0100 0.0100 1 03/07/2019 04:26 WG1245476 Qc
2-Chlorophenol U 0.000283 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
8
2,4-Dichlorophenol U 0.000284 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Gl
2,4-Dimethylphenol U 0.000264 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 0.0100 1 03/07/2019 04:26 WG1245476 9
2,4-Dinitrophenol U 0.00325 0.0100 0.0100 1 03/07/2019 04:26 WG1245476 Al
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Sc
Pentachlorophenol U 0.000313 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Phenol 0.00140 J 0.000334 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
2,4,6-Trichlorophenol U 0.000297 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
(S) 2-Fluorophenol 39.2 10.0-120 03/07/2019 04:26 WG1245476
(S) Phenol-d5 23.8 10.0-120 03/07/2019 04:26 WG1245476
(S) Nitrobenzene-d5 50.0 10.0-127 03/07/2019 04:26 WG1245476
(S) 2-Fluorobiphenyl 53.4 10.0-130 03/07/2019 04:26 WG1245476
(S) 2,4,6-Tribromophenol 66.5 10.0-155 03/07/2019 04:26 WG1245476
(S) p-Terphenyl-d14 59.3 10.0-128 03/07/2019 04:26 WG1245476

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 68 of 161
DUPLICATE 1 SAMPLE RESULTS - 19 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 00:00 L1075168

Gravimetric Analysis by Method 2540 C-2011 1

Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch


Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 1620 14.1 50.0 50.0 1 03/08/2019 01:53 WG1246059 Tc

3
Wet Chemistry by Method 2320 B-2011 Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 339 2.71 20.0 20.0 1 03/07/2019 17:04 WG1245955
5
Sample Narrative: Tr
L1075168-19 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Analyte mg/l mg/l mg/l mg/l date / time


Qc
Chloride 606 0.519 1.00 10.0 10 03/06/2019 08:55 WG1245159 8
Sulfate 118 0.774 5.00 50.0 10 03/06/2019 08:55 WG1245159 Gl

9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 7.70 T8 1 03/06/2019 09:50 WG1245737

Sample Narrative:
L1075168-19 WG1245737: 7.7 at 17.8C

Wet Chemistry by Method 9050A


Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 2690 10.0 10.0 1 03/07/2019 13:22 WG1245735

Mercury by Method 7470A


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Mercury 0.0000943 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:39 WG1245002

Metals (ICPMS) by Method 6020


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Arsenic 0.0257 0.000250 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Barium 1.52 0.000360 0.00500 0.00500 1 03/06/2019 22:39 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:39 WG1245245
Calcium 102 0.0460 1.00 1.00 1 03/06/2019 22:39 WG1245245
Chromium 0.00390 B 0.000540 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Lead 0.00436 0.000240 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Magnesium 7.74 0.100 1.00 1.00 1 03/06/2019 22:39 WG1245245
Potassium 17.9 0.0370 1.00 1.00 1 03/06/2019 22:39 WG1245245
Selenium 0.00153 J 0.000380 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Sodium 436 0.110 1.00 1.00 1 03/06/2019 22:39 WG1245245

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 69 of 161
DUPLICATE 1 SAMPLE RESULTS - 19 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 00:00 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Acetone 0.118 0.0100 0.0500 0.0500 1 03/06/2019 17:21 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 17:21 WG1245979
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/06/2019 17:21 WG1245979 3
Benzene U 0.000331 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Bromomethane U 0.000866 0.00500 0.00500 1 03/06/2019 17:21 WG1245979 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/06/2019 17:21 WG1245979
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,3-Dichlorobenzene U 0.000220 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,4-Dichlorobenzene U 0.000274 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,2-Dichloroethane U 0.000361 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,3-Dichloropropane U 0.000366 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
2,2-Dichloropropane U 0.000321 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Ethylbenzene 0.00193 0.000384 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
2-Butanone (MEK) 0.00701 J 0.00393 0.0100 0.0100 1 03/06/2019 17:21 WG1245979
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/06/2019 17:21 WG1245979
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Naphthalene 0.00110 J 0.00100 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
n-Propylbenzene U 0.000349 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Toluene 0.00576 0.000412 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,2,4-Trichlorobenzene U 0.000355 0.00100 0.00100 1 03/06/2019 17:21 WG1245979

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 70 of 161
DUPLICATE 1 SAMPLE RESULTS - 19 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 00:00 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260C


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Tc
1,1,2-Trichloroethane U 0.000383 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Trichloroethene U 0.000398 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/06/2019 17:21 WG1245979 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/06/2019 17:21 WG1245979
4
1,2,4-Trimethylbenzene 0.00192 0.000373 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Cn
1,2,3-Trimethylbenzene 0.000762 J 0.000321 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
1,3,5-Trimethylbenzene 0.000715 J 0.000387 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 Tr
Xylenes, Total 0.0162 0.00106 0.00300 0.00300 1 03/06/2019 17:21 WG1245979
6
(S) Toluene-d8 105 80.0-120 03/06/2019 17:21 WG1245979
Sr
(S) 4-Bromofluorobenzene 108 77.0-126 03/06/2019 17:21 WG1245979
(S) 1,2-Dichloroethane-d4 112 70.0-130 03/06/2019 17:21 WG1245979 7
Qc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
Analyte mg/l mg/l mg/l mg/l date / time
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678
Al
TPH C12 - C28 8.96 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678
TPH C28 - C35 0.683 J 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678 10
TPH C6 - C35 9.64 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678 Sc
(S) o-Terphenyl 91.1 70.0-130 03/06/2019 20:21 WG1245678

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte mg/l mg/l mg/l mg/l date / time
Acenaphthene U 0.00316 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Acenaphthylene U 0.00309 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Benzo(a)anthracene U 0.000975 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Benzo(b)fluoranthene U 0.000896 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Benzo(k)fluoranthene U 0.00355 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Benzo(g,h,i)perylene U 0.00161 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Benzo(a)pyrene U 0.00340 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Bis(2-chlorethoxy)methane U 0.00329 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Bis(2-chloroethyl)ether U 0.0162 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Bis(2-chloroisopropyl)ether U 0.00445 0.0100 0.100 10 03/07/2019 09:13 WG1245476
4-Bromophenyl-phenylether U 0.00335 0.0100 0.100 10 03/07/2019 09:13 WG1245476
2-Chloronaphthalene U 0.00330 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
4-Chlorophenyl-phenylether U 0.00303 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Dibenz(a,h)anthracene U 0.00279 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
3,3-Dichlorobenzidine U 0.0202 0.0100 0.100 10 03/07/2019 09:13 WG1245476
2,4-Dinitrotoluene U 0.0165 0.0100 0.100 10 03/07/2019 09:13 WG1245476
2,6-Dinitrotoluene U 0.00279 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Fluoranthene U 0.00310 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Hexachlorobenzene U 0.00341 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Hexachloro-1,3-butadiene U 0.00329 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Hexachlorocyclopentadiene U 0.0233 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Hexachloroethane U 0.00365 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Indeno(1,2,3-cd)pyrene U 0.00279 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 09:13 WG1245476

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 71 of 161
DUPLICATE 1 SAMPLE RESULTS - 19 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 00:00 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270D


1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Nitrobenzene U 0.00367 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Tc
n-Nitrosodimethylamine U 0.0126 0.0100 0.100 10 03/07/2019 09:13 WG1245476
n-Nitrosodiphenylamine U 0.0119 0.0100 0.100 10 03/07/2019 09:13 WG1245476 3
n-Nitrosodi-n-propylamine U 0.00403 0.0100 0.100 10 03/07/2019 09:13 WG1245476 Ss
Phenanthrene U 0.00366 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
4
Benzylbutyl phthalate U 0.00275 0.00300 0.0300 10 03/07/2019 09:13 WG1245476
Cn
Bis(2-ethylhexyl)phthalate U 0.00709 0.00300 0.0300 10 03/07/2019 09:13 WG1245476
Di-n-butyl phthalate U 0.00266 0.00300 0.0300 10 03/07/2019 09:13 WG1245476 5
Diethyl phthalate U 0.00282 0.00300 0.0300 10 03/07/2019 09:13 WG1245476 Tr
Dimethyl phthalate U 0.00283 0.00300 0.0300 10 03/07/2019 09:13 WG1245476
6
Di-n-octyl phthalate U 0.00278 0.00300 0.0300 10 03/07/2019 09:13 WG1245476
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
1,2,4-Trichlorobenzene U 0.00355 0.0100 0.100 10 03/07/2019 09:13 WG1245476 7
4-Chloro-3-methylphenol U 0.00263 0.0100 0.100 10 03/07/2019 09:13 WG1245476 Qc
2-Chlorophenol U 0.00283 0.0100 0.100 10 03/07/2019 09:13 WG1245476
8
2,4-Dichlorophenol U 0.00284 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Gl
2,4-Dimethylphenol 0.0122 J 0.00264 0.0100 0.100 10 03/07/2019 09:13 WG1245476
4,6-Dinitro-2-methylphenol U 0.0262 0.0100 0.100 10 03/07/2019 09:13 WG1245476 9
2,4-Dinitrophenol U 0.0325 0.0100 0.100 10 03/07/2019 09:13 WG1245476 Al
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 09:13 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Sc
Pentachlorophenol U 0.00313 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 09:13 WG1245476
2,4,6-Trichlorophenol U 0.00297 0.0100 0.100 10 03/07/2019 09:13 WG1245476
(S) 2-Fluorophenol 44.5 10.0-120 03/07/2019 09:13 WG1245476
(S) Phenol-d5 25.7 10.0-120 03/07/2019 09:13 WG1245476
(S) Nitrobenzene-d5 67.8 10.0-127 03/07/2019 09:13 WG1245476
(S) 2-Fluorobiphenyl 67.4 10.0-130 03/07/2019 09:13 WG1245476
(S) 2,4,6-Tribromophenol 94.0 10.0-155 03/07/2019 09:13 WG1245476
(S) p-Terphenyl-d14 76.7 10.0-128 03/07/2019 09:13 WG1245476

Sample Narrative:
L1075168-19 WG1245476: Dilution due to viscosity.

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 72 of 161
PS-1 SAMPLE RESULTS - 20 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:15 L1075168

Total Solids by Method 2540 G-2011 1

Result Qualifier Dilution Analysis Batch


Cp
Analyte % date / time
2
Total Solids 63.3 1 03/06/2019 14:08 WG1245367 Tc

3
Wet Chemistry by Method 9050AMod Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm umhos/cm date / time 4
Cn
Specific Conductance 933 10.0 10.0 10.0 1 03/06/2019 21:03 WG1245948
5
Wet Chemistry by Method 9056A Tr
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
6
Analyte mg/kg mg/kg mg/kg mg/kg date / time Sr
Chloride 265 1.26 10.0 15.8 1 03/06/2019 18:51 WG1245719
7
Qc
Mercury by Method 7471A
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 8

Analyte mg/kg mg/kg mg/kg mg/kg date / time


Gl
Mercury 0.748 0.00442 0.0200 0.0316 1 03/05/2019 09:02 WG1245047 9
Al
Metals (ICP) by Method 6010B
10
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Sc
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Arsenic 17.2 0.726 2.00 3.16 1 03/07/2019 20:41 WG1245191
Barium 23500 1.34 0.500 3.95 5 03/08/2019 10:03 WG1245191
Cadmium U 0.553 0.500 3.95 5 03/08/2019 10:03 WG1245191
Chromium 28.0 0.221 1.00 1.58 1 03/07/2019 20:41 WG1245191
Lead 61.3 0.300 0.500 0.790 1 03/07/2019 20:41 WG1245191
Selenium 1.10 J 0.979 2.00 3.16 1 03/07/2019 20:41 WG1245191
Silver U 0.190 1.00 1.58 1 03/07/2019 20:41 WG1245191

Volatile Organic Compounds (GC/MS) by Method 8260B


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Acetone 0.120 0.0216 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
Acrylonitrile U 0.00300 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
Benzene 0.00171 0.000632 0.00100 0.00158 1 03/06/2019 19:43 WG1245869
Bromobenzene U 0.00166 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
Bromodichloromethane U 0.00124 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Bromoform U 0.00944 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
Bromomethane U 0.00584 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
n-Butylbenzene U 0.00606 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
sec-Butylbenzene U 0.00400 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
tert-Butylbenzene U 0.00245 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Carbon tetrachloride U 0.00171 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Chlorobenzene U 0.000905 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Chlorodibromomethane U 0.000711 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Chloroethane U 0.00171 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Chloroform U 0.000655 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Chloromethane U 0.00220 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
2-Chlorotoluene U 0.00145 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
4-Chlorotoluene U 0.00178 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
1,2-Dibromo-3-Chloropropane U 0.00805 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
1,2-Dibromoethane U 0.000829 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Dibromomethane U J4 0.00158 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
1,2-Dichlorobenzene U 0.00229 0.00500 0.00790 1 03/06/2019 19:43 WG1245869

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 73 of 161
PS-1 SAMPLE RESULTS - 20 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:15 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260B


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
1,3-Dichlorobenzene U 0.00268 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Tc
1,4-Dichlorobenzene U 0.00311 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Dichlorodifluoromethane U 0.00129 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 3
1,1-Dichloroethane U 0.000908 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 Ss
1,2-Dichloroethane U 0.000750 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
4
1,1-Dichloroethene U 0.000790 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Cn
cis-1,2-Dichloroethene U 0.00109 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
trans-1,2-Dichloroethene U 0.00226 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 5
1,2-Dichloropropane U 0.00201 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 Tr
1,1-Dichloropropene U 0.00111 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
6
1,3-Dichloropropane U 0.00276 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Sr
cis-1,3-Dichloropropene U 0.00107 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
trans-1,3-Dichloropropene U 0.00242 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 7
2,2-Dichloropropane U 0.00125 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 Qc
Di-isopropyl ether U 0.000553 0.00100 0.00158 1 03/06/2019 19:43 WG1245869
8
Ethylbenzene 0.148 0.000837 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Gl
Hexachloro-1,3-butadiene U 0.0201 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
Isopropylbenzene 0.00499 0.00136 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 9
p-Isopropyltoluene U 0.00368 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 Al
2-Butanone (MEK) U 0.0197 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
10
Methylene Chloride U 0.0105 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
Sc
4-Methyl-2-pentanone (MIBK) U 0.0158 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
Methyl tert-butyl ether U 0.000466 0.00100 0.00158 1 03/06/2019 19:43 WG1245869
Naphthalene 0.0524 0.00493 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
n-Propylbenzene 0.00940 0.00186 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Styrene U 0.00431 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
1,1,1,2-Tetrachloroethane U 0.000790 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
1,1,2,2-Tetrachloroethane U J4 0.000616 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
1,1,2-Trichlorotrifluoroethane U 0.00107 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Tetrachloroethene U 0.00111 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Toluene 0.294 0.00197 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
1,2,3-Trichlorobenzene U 0.000987 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
1,2,4-Trichlorobenzene U 0.00761 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
1,1,1-Trichloroethane U 0.000434 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
1,1,2-Trichloroethane U 0.00139 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Trichloroethene U 0.000632 0.00100 0.00158 1 03/06/2019 19:43 WG1245869
Trichlorofluoromethane U 0.000790 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
1,2,3-Trichloropropane U 0.00805 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
1,2,4-Trimethylbenzene 0.0648 0.00183 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
1,2,3-Trimethylbenzene 0.0237 0.00182 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
1,3,5-Trimethylbenzene 0.0172 0.00171 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Vinyl chloride U 0.00108 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Xylenes, Total 1.05 0.00755 0.00650 0.0103 1 03/06/2019 19:43 WG1245869
(S) Toluene-d8 112 75.0-131 03/06/2019 19:43 WG1245869
(S) 4-Bromofluorobenzene 97.6 67.0-138 03/06/2019 19:43 WG1245869
(S) 1,2-Dichloroethane-d4 77.1 70.0-130 03/06/2019 19:43 WG1245869

Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
TPH C6 - C12 U 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
TPH C12 - C28 349 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
TPH C28 - C35 59.7 J 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
TPH C6 - C35 409 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
(S) o-Terphenyl 111 70.0-130 03/10/2019 16:33 WG1246136

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 74 of 161
PS-1 SAMPLE RESULTS - 20 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:15 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270C


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
Acenaphthene U 0.0203 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Tc
Acenaphthylene U 0.0212 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Anthracene U 0.0200 0.0333 0.105 2 03/05/2019 05:28 WG1244658 3
Benzidine U J4 0.201 0.333 1.05 2 03/05/2019 05:28 WG1244658 Ss
Benzo(a)anthracene 0.0336 J 0.0135 0.0333 0.105 2 03/05/2019 05:28 WG1244658
4
Benzo(b)fluoranthene 0.132 0.0220 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Cn
Benzo(k)fluoranthene U 0.0184 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Benzo(g,h,i)perylene 0.0613 J 0.0228 0.0333 0.105 2 03/05/2019 05:28 WG1244658 5
Benzo(a)pyrene U 0.0173 0.0333 0.105 2 03/05/2019 05:28 WG1244658 Tr
Bis(2-chlorethoxy)methane U 0.0243 0.333 1.05 2 03/05/2019 05:28 WG1244658
6
Bis(2-chloroethyl)ether U 0.0283 0.333 1.05 2 03/05/2019 05:28 WG1244658
Sr
Bis(2-chloroisopropyl)ether U 0.0240 0.333 1.05 2 03/05/2019 05:28 WG1244658
4-Bromophenyl-phenylether U 0.0360 0.333 1.05 2 03/05/2019 05:28 WG1244658 7
2-Chloronaphthalene U 0.0202 0.0333 0.105 2 03/05/2019 05:28 WG1244658 Qc
4-Chlorophenyl-phenylether U 0.0198 0.333 1.05 2 03/05/2019 05:28 WG1244658
8
Chrysene 0.0461 J 0.0175 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Gl
Dibenz(a,h)anthracene U 0.0259 0.0333 0.105 2 03/05/2019 05:28 WG1244658
3,3-Dichlorobenzidine U 0.251 0.333 1.05 2 03/05/2019 05:28 WG1244658 9
2,4-Dinitrotoluene U 0.0192 0.333 1.05 2 03/05/2019 05:28 WG1244658 Al
2,6-Dinitrotoluene U 0.0233 0.333 1.05 2 03/05/2019 05:28 WG1244658
10
Fluoranthene 0.362 0.0157 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Sc
Fluorene 0.154 0.0215 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Hexachlorobenzene U 0.0270 0.333 1.05 2 03/05/2019 05:28 WG1244658
Hexachloro-1,3-butadiene U 0.0316 0.333 1.05 2 03/05/2019 05:28 WG1244658
Hexachlorocyclopentadiene U 0.185 0.333 1.05 2 03/05/2019 05:28 WG1244658
Hexachloroethane U 0.0423 0.333 1.05 2 03/05/2019 05:28 WG1244658
Indeno(1,2,3-cd)pyrene 0.0499 J 0.0244 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Isophorone U 0.0165 0.333 1.05 2 03/05/2019 05:28 WG1244658
Naphthalene 0.136 0.0281 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Nitrobenzene U 0.0220 0.333 1.05 2 03/05/2019 05:28 WG1244658
n-Nitrosodimethylamine U 0.204 0.333 1.05 2 03/05/2019 05:28 WG1244658
n-Nitrosodiphenylamine U 0.284 0.333 1.05 2 03/05/2019 05:28 WG1244658
n-Nitrosodi-n-propylamine U 0.0286 0.333 1.05 2 03/05/2019 05:28 WG1244658
Phenanthrene 0.245 0.0167 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Benzylbutyl phthalate U 0.0325 0.333 1.05 2 03/05/2019 05:28 WG1244658
Bis(2-ethylhexyl)phthalate 0.193 J 0.0379 0.333 1.05 2 03/05/2019 05:28 WG1244658
Di-n-butyl phthalate U 0.0344 0.333 1.05 2 03/05/2019 05:28 WG1244658
Diethyl phthalate U 0.0218 0.333 1.05 2 03/05/2019 05:28 WG1244658
Dimethyl phthalate U 0.0171 0.333 1.05 2 03/05/2019 05:28 WG1244658
Di-n-octyl phthalate U 0.0286 0.333 1.05 2 03/05/2019 05:28 WG1244658
Pyrene 0.449 0.0388 0.0333 0.105 2 03/05/2019 05:28 WG1244658
1,2,4-Trichlorobenzene U 0.0277 0.333 1.05 2 03/05/2019 05:28 WG1244658
4-Chloro-3-methylphenol U 0.0151 0.333 1.05 2 03/05/2019 05:28 WG1244658
2-Chlorophenol U 0.0262 0.333 1.05 2 03/05/2019 05:28 WG1244658
2,4-Dichlorophenol U 0.0236 0.333 1.05 2 03/05/2019 05:28 WG1244658
2,4-Dimethylphenol 0.218 J 0.149 0.333 1.05 2 03/05/2019 05:28 WG1244658
4,6-Dinitro-2-methylphenol U 0.392 0.333 1.05 2 03/05/2019 05:28 WG1244658
2,4-Dinitrophenol U 0.310 0.333 1.05 2 03/05/2019 05:28 WG1244658
2-Nitrophenol U 0.0411 0.333 1.05 2 03/05/2019 05:28 WG1244658
4-Nitrophenol U 0.166 0.333 1.05 2 03/05/2019 05:28 WG1244658
Pentachlorophenol U 0.152 0.333 1.05 2 03/05/2019 05:28 WG1244658
Phenol 0.0428 J 0.0220 0.333 1.05 2 03/05/2019 05:28 WG1244658
2,4,6-Trichlorophenol U 0.0246 0.333 1.05 2 03/05/2019 05:28 WG1244658
(S) 2-Fluorophenol 83.9 12.0-120 03/05/2019 05:28 WG1244658
(S) Phenol-d5 71.6 10.0-120 03/05/2019 05:28 WG1244658
(S) Nitrobenzene-d5 65.9 10.0-122 03/05/2019 05:28 WG1244658

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 75 of 161
PS-1 SAMPLE RESULTS - 20 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:15 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270C


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
(S) 2-Fluorobiphenyl 67.8 15.0-120 03/05/2019 05:28 WG1244658
Tc
(S) 2,4,6-Tribromophenol 68.3 10.0-127 03/05/2019 05:28 WG1244658
(S) p-Terphenyl-d14 72.5 10.0-120 03/05/2019 05:28 WG1244658 3
Ss
Sample Narrative:
4
L1075168-20 WG1244658: Dilution due to matrix impact during extract concentration procedure
Cn

5
Tr

6
Sr

7
Qc

8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 76 of 161
PS-2 SAMPLE RESULTS - 21 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:30 L1075168

Total Solids by Method 2540 G-2011 1

Result Qualifier Dilution Analysis Batch


Cp
Analyte % date / time
2
Total Solids 57.8 1 03/06/2019 14:08 WG1245367 Tc

3
Wet Chemistry by Method 9050AMod Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm umhos/cm date / time 4
Cn
Specific Conductance 964 10.0 10.0 10.0 1 03/06/2019 21:03 WG1245948
5
Wet Chemistry by Method 9056A Tr
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
6
Analyte mg/kg mg/kg mg/kg mg/kg date / time Sr
Chloride 444 1.38 10.0 17.3 1 03/06/2019 19:17 WG1245719
7
Qc
Mercury by Method 7471A
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 8

Analyte mg/kg mg/kg mg/kg mg/kg date / time


Gl
Mercury 1.74 0.00484 0.0200 0.0346 1 03/05/2019 09:04 WG1245047 9
Al
Metals (ICP) by Method 6010B
10
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Sc
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Arsenic 20.8 0.796 2.00 3.46 1 03/07/2019 20:44 WG1245191
Barium 24400 1.47 0.500 4.32 5 03/08/2019 10:06 WG1245191
Cadmium U 0.605 0.500 4.32 5 03/08/2019 10:06 WG1245191
Chromium 28.5 0.242 1.00 1.73 1 03/07/2019 20:44 WG1245191
Lead 68.2 0.329 0.500 0.865 1 03/07/2019 20:44 WG1245191
Selenium 1.25 J 1.07 2.00 3.46 1 03/07/2019 20:44 WG1245191
Silver U 0.208 1.00 1.73 1 03/07/2019 20:44 WG1245191

Volatile Organic Compounds (GC/MS) by Method 8260B


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Acetone U 0.0237 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
Acrylonitrile U 0.00329 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
Benzene 0.00225 0.000692 0.00100 0.00173 1 03/06/2019 12:03 WG1245896
Bromobenzene U 0.00182 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
Bromodichloromethane U 0.00136 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Bromoform U 0.0103 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
Bromomethane U 0.00640 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
n-Butylbenzene U 0.00664 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
sec-Butylbenzene U 0.00438 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
tert-Butylbenzene U 0.00268 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Carbon tetrachloride U 0.00187 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Chlorobenzene U 0.000991 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Chlorodibromomethane U 0.000778 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Chloroethane U 0.00187 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Chloroform U 0.000718 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Chloromethane U 0.00240 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
2-Chlorotoluene U 0.00159 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
4-Chlorotoluene U 0.00195 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
1,2-Dibromo-3-Chloropropane U 0.00882 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
1,2-Dibromoethane U 0.000908 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Dibromomethane U 0.00173 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
1,2-Dichlorobenzene U 0.00251 0.00500 0.00865 1 03/06/2019 12:03 WG1245896

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 77 of 161
PS-2 SAMPLE RESULTS - 21 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:30 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260B


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
1,3-Dichlorobenzene U 0.00294 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Tc
1,4-Dichlorobenzene U 0.00341 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Dichlorodifluoromethane U 0.00141 0.00250 0.00432 1 03/06/2019 12:03 WG1245896 3
1,1-Dichloroethane U 0.000995 0.00250 0.00432 1 03/06/2019 12:03 WG1245896 Ss
1,2-Dichloroethane U 0.000822 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
4
1,1-Dichloroethene U 0.000865 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Cn
cis-1,2-Dichloroethene U 0.00119 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
trans-1,2-Dichloroethene U 0.00247 0.00500 0.00865 1 03/06/2019 12:03 WG1245896 5
1,2-Dichloropropane U 0.00220 0.00500 0.00865 1 03/06/2019 12:03 WG1245896 Tr
1,1-Dichloropropene U 0.00121 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
6
1,3-Dichloropropane U 0.00303 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Sr
cis-1,3-Dichloropropene U 0.00117 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
trans-1,3-Dichloropropene U 0.00265 0.00500 0.00865 1 03/06/2019 12:03 WG1245896 7
2,2-Dichloropropane U 0.00137 0.00250 0.00432 1 03/06/2019 12:03 WG1245896 Qc
Di-isopropyl ether U 0.000605 0.00100 0.00173 1 03/06/2019 12:03 WG1245896
8
Ethylbenzene 0.0612 0.000917 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Gl
Hexachloro-1,3-butadiene U 0.0220 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
Isopropylbenzene 0.00210 J 0.00149 0.00250 0.00432 1 03/06/2019 12:03 WG1245896 9
p-Isopropyltoluene U 0.00403 0.00500 0.00865 1 03/06/2019 12:03 WG1245896 Al
2-Butanone (MEK) 0.0242 J 0.0216 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
10
Methylene Chloride U 0.0115 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
Sc
4-Methyl-2-pentanone (MIBK) U 0.0173 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
Methyl tert-butyl ether U 0.000510 0.00100 0.00173 1 03/06/2019 12:03 WG1245896
Naphthalene 0.0587 B 0.00540 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
n-Propylbenzene 0.00433 J 0.00204 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Styrene U 0.00472 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
1,1,1,2-Tetrachloroethane U 0.000865 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
1,1,2,2-Tetrachloroethane U 0.000675 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
1,1,2-Trichlorotrifluoroethane U 0.00117 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Tetrachloroethene U 0.00121 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Toluene 0.116 0.00216 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
1,2,3-Trichlorobenzene U 0.00108 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
1,2,4-Trichlorobenzene U 0.00834 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
1,1,1-Trichloroethane U 0.000476 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
1,1,2-Trichloroethane U 0.00153 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Trichloroethene U 0.000692 0.00100 0.00173 1 03/06/2019 12:03 WG1245896
Trichlorofluoromethane U 0.000865 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
1,2,3-Trichloropropane U 0.00882 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
1,2,4-Trimethylbenzene 0.0272 0.00201 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
1,2,3-Trimethylbenzene 0.0104 0.00199 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
1,3,5-Trimethylbenzene 0.00825 J 0.00187 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Vinyl chloride U 0.00118 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Xylenes, Total 0.477 0.00827 0.00650 0.0112 1 03/06/2019 12:03 WG1245896
(S) Toluene-d8 94.0 75.0-131 03/06/2019 12:03 WG1245896
(S) 4-Bromofluorobenzene 91.7 67.0-138 03/06/2019 12:03 WG1245896
(S) 1,2-Dichloroethane-d4 118 70.0-130 03/06/2019 12:03 WG1245896

Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
TPH C6 - C12 332 J 259 50.0 865 10 03/09/2019 03:57 WG1246136
TPH C12 - C28 12800 259 50.0 865 10 03/09/2019 03:57 WG1246136
TPH C28 - C35 6420 259 50.0 865 10 03/09/2019 03:57 WG1246136
TPH C6 - C35 19500 259 50.0 865 10 03/09/2019 03:57 WG1246136
(S) o-Terphenyl 133 J1 70.0-130 03/09/2019 03:57 WG1246136

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 78 of 161
PS-2 SAMPLE RESULTS - 21 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:30 L1075168

Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
Sample Narrative:
Tc
L1075168-21 WG1246136: Surrogate failure due to matrix interference
3
Semi Volatile Organic Compounds (GC/MS) by Method 8270C Ss
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 4
Analyte mg/kg mg/kg mg/kg mg/kg date / time Cn
Acenaphthene U 0.222 0.0333 1.15 20 03/05/2019 06:27 WG1244658
5
Acenaphthylene U 0.232 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Tr
Anthracene 0.391 J 0.219 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Benzidine U J4 2.20 0.333 11.5 20 03/05/2019 06:27 WG1244658 6
Benzo(a)anthracene 0.531 J 0.148 0.0333 1.15 20 03/05/2019 06:27 WG1244658 Sr
Benzo(b)fluoranthene 1.85 0.240 0.0333 1.15 20 03/05/2019 06:27 WG1244658
7
Benzo(k)fluoranthene U 0.201 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Qc
Benzo(g,h,i)perylene 0.893 J 0.249 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Benzo(a)pyrene U 0.190 0.0333 1.15 20 03/05/2019 06:27 WG1244658 8
Bis(2-chlorethoxy)methane U 0.266 0.333 11.5 20 03/05/2019 06:27 WG1244658 Gl
Bis(2-chloroethyl)ether U 0.310 0.333 11.5 20 03/05/2019 06:27 WG1244658
9
Bis(2-chloroisopropyl)ether U 0.263 0.333 11.5 20 03/05/2019 06:27 WG1244658
Al
4-Bromophenyl-phenylether U 0.394 0.333 11.5 20 03/05/2019 06:27 WG1244658
2-Chloronaphthalene U 0.221 0.0333 1.15 20 03/05/2019 06:27 WG1244658 10
4-Chlorophenyl-phenylether U 0.217 0.333 11.5 20 03/05/2019 06:27 WG1244658 Sc
Chrysene 0.699 J 0.192 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Dibenz(a,h)anthracene U 0.284 0.0333 1.15 20 03/05/2019 06:27 WG1244658
3,3-Dichlorobenzidine U 2.75 0.333 11.5 20 03/05/2019 06:27 WG1244658
2,4-Dinitrotoluene U 0.210 0.333 11.5 20 03/05/2019 06:27 WG1244658
2,6-Dinitrotoluene U 0.255 0.333 11.5 20 03/05/2019 06:27 WG1244658
Fluoranthene 6.75 0.172 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Fluorene 1.85 0.236 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Hexachlorobenzene U 0.296 0.333 11.5 20 03/05/2019 06:27 WG1244658
Hexachloro-1,3-butadiene U 0.346 0.333 11.5 20 03/05/2019 06:27 WG1244658
Hexachlorocyclopentadiene U 2.03 0.333 11.5 20 03/05/2019 06:27 WG1244658
Hexachloroethane U 0.464 0.333 11.5 20 03/05/2019 06:27 WG1244658
Indeno(1,2,3-cd)pyrene 0.777 J 0.267 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Isophorone U 0.181 0.333 11.5 20 03/05/2019 06:27 WG1244658
Naphthalene U 0.308 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Nitrobenzene U 0.240 0.333 11.5 20 03/05/2019 06:27 WG1244658
n-Nitrosodimethylamine U 2.24 0.333 11.5 20 03/05/2019 06:27 WG1244658
n-Nitrosodiphenylamine U 3.11 0.333 11.5 20 03/05/2019 06:27 WG1244658
n-Nitrosodi-n-propylamine U 0.313 0.333 11.5 20 03/05/2019 06:27 WG1244658
Phenanthrene 3.27 0.183 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Benzylbutyl phthalate U 0.356 0.333 11.5 20 03/05/2019 06:27 WG1244658
Bis(2-ethylhexyl)phthalate 0.560 J 0.415 0.333 11.5 20 03/05/2019 06:27 WG1244658
Di-n-butyl phthalate U 0.377 0.333 11.5 20 03/05/2019 06:27 WG1244658
Diethyl phthalate U 0.239 0.333 11.5 20 03/05/2019 06:27 WG1244658
Dimethyl phthalate U 0.187 0.333 11.5 20 03/05/2019 06:27 WG1244658
Di-n-octyl phthalate U 0.314 0.333 11.5 20 03/05/2019 06:27 WG1244658
Pyrene 3.55 0.426 0.0333 1.15 20 03/05/2019 06:27 WG1244658
1,2,4-Trichlorobenzene U 0.303 0.333 11.5 20 03/05/2019 06:27 WG1244658
4-Chloro-3-methylphenol U 0.165 0.333 11.5 20 03/05/2019 06:27 WG1244658
2-Chlorophenol U 0.287 0.333 11.5 20 03/05/2019 06:27 WG1244658
2,4-Dichlorophenol U 0.258 0.333 11.5 20 03/05/2019 06:27 WG1244658
2,4-Dimethylphenol U 1.63 0.333 11.5 20 03/05/2019 06:27 WG1244658
4,6-Dinitro-2-methylphenol U 4.29 0.333 11.5 20 03/05/2019 06:27 WG1244658
2,4-Dinitrophenol U 3.39 0.333 11.5 20 03/05/2019 06:27 WG1244658
2-Nitrophenol U 0.450 0.333 11.5 20 03/05/2019 06:27 WG1244658
4-Nitrophenol U 1.82 0.333 11.5 20 03/05/2019 06:27 WG1244658

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 79 of 161
PS-2 SAMPLE RESULTS - 21 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:30 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270C


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
Pentachlorophenol U 1.66 0.333 11.5 20 03/05/2019 06:27 WG1244658
Tc
Phenol U 0.240 0.333 11.5 20 03/05/2019 06:27 WG1244658
2,4,6-Trichlorophenol U 0.269 0.333 11.5 20 03/05/2019 06:27 WG1244658 3
(S) 2-Fluorophenol 69.0 J7 12.0-120 03/05/2019 06:27 WG1244658 Ss
(S) Phenol-d5 68.4 J7 10.0-120 03/05/2019 06:27 WG1244658
4
(S) Nitrobenzene-d5 92.0 J7 10.0-122 03/05/2019 06:27 WG1244658
Cn
(S) 2-Fluorobiphenyl 55.2 J7 15.0-120 03/05/2019 06:27 WG1244658
(S) 2,4,6-Tribromophenol 51.0 J7 10.0-127 03/05/2019 06:27 WG1244658 5
(S) p-Terphenyl-d14 83.4 J7 10.0-120 03/05/2019 06:27 WG1244658 Tr

6
Sample Narrative:
Sr
L1075168-21 WG1244658: Dilution due to matrix.
7
Qc

8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 80 of 161
PS-3 SAMPLE RESULTS - 22 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:45 L1075168

Total Solids by Method 2540 G-2011 1

Result Qualifier Dilution Analysis Batch


Cp
Analyte % date / time
2
Total Solids 60.1 1 03/06/2019 10:56 WG1245670 Tc

3
Wet Chemistry by Method 9050AMod Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm umhos/cm date / time 4
Cn
Specific Conductance 1100 10.0 10.0 10.0 1 03/06/2019 21:03 WG1245948
5
Wet Chemistry by Method 9056A Tr
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
6
Analyte mg/kg mg/kg mg/kg mg/kg date / time Sr
Chloride 664 1.32 10.0 16.6 1 03/06/2019 19:25 WG1245719
7
Qc
Mercury by Method 7471A
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 8

Analyte mg/kg mg/kg mg/kg mg/kg date / time


Gl
Mercury 0.641 0.00466 0.0200 0.0333 1 03/05/2019 09:07 WG1245047 9
Al
Metals (ICP) by Method 6010B
10
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Sc
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Arsenic 18.9 0.766 2.00 3.33 1 03/07/2019 20:47 WG1245191
Barium 26300 1.41 0.500 4.16 5 03/08/2019 10:09 WG1245191
Cadmium U 0.583 0.500 4.16 5 03/08/2019 10:09 WG1245191
Chromium 30.1 0.233 1.00 1.66 1 03/07/2019 20:47 WG1245191
Lead 68.9 0.316 0.500 0.832 1 03/07/2019 20:47 WG1245191
Selenium 1.88 J 1.03 2.00 3.33 1 03/07/2019 20:47 WG1245191
Silver U 0.200 1.00 1.66 1 03/07/2019 20:47 WG1245191

Volatile Organic Compounds (GC/MS) by Method 8260B


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Acetone 0.135 0.0228 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
Acrylonitrile U 0.00316 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
Benzene 0.0156 0.000666 0.00100 0.00166 1 03/06/2019 12:22 WG1245896
Bromobenzene U 0.00175 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
Bromodichloromethane U 0.00131 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Bromoform U 0.00995 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
Bromomethane U 0.00616 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
n-Butylbenzene U 0.00639 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
sec-Butylbenzene U 0.00421 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
tert-Butylbenzene U 0.00258 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Carbon tetrachloride U 0.00180 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Chlorobenzene U 0.000954 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Chlorodibromomethane U 0.000749 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Chloroethane U 0.00180 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Chloroform U 0.000691 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Chloromethane U 0.00231 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
2-Chlorotoluene U 0.00153 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
4-Chlorotoluene U 0.00188 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
1,2-Dibromo-3-Chloropropane U 0.00849 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
1,2-Dibromoethane U 0.000874 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Dibromomethane U 0.00166 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
1,2-Dichlorobenzene U 0.00241 0.00500 0.00832 1 03/06/2019 12:22 WG1245896

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 81 of 161
PS-3 SAMPLE RESULTS - 22 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:45 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260B


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
1,3-Dichlorobenzene U 0.00283 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Tc
1,4-Dichlorobenzene U 0.00328 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Dichlorodifluoromethane U 0.00136 0.00250 0.00416 1 03/06/2019 12:22 WG1245896 3
1,1-Dichloroethane U 0.000957 0.00250 0.00416 1 03/06/2019 12:22 WG1245896 Ss
1,2-Dichloroethane U 0.000791 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
4
1,1-Dichloroethene U 0.000832 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Cn
cis-1,2-Dichloroethene U 0.00115 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
trans-1,2-Dichloroethene U 0.00238 0.00500 0.00832 1 03/06/2019 12:22 WG1245896 5
1,2-Dichloropropane U 0.00211 0.00500 0.00832 1 03/06/2019 12:22 WG1245896 Tr
1,1-Dichloropropene U 0.00117 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
6
1,3-Dichloropropane U 0.00291 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Sr
cis-1,3-Dichloropropene U 0.00113 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
trans-1,3-Dichloropropene U 0.00255 0.00500 0.00832 1 03/06/2019 12:22 WG1245896 7
2,2-Dichloropropane U 0.00132 0.00250 0.00416 1 03/06/2019 12:22 WG1245896 Qc
Di-isopropyl ether U 0.000583 0.00100 0.00166 1 03/06/2019 12:22 WG1245896
8
Ethylbenzene 0.107 0.000882 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Gl
Hexachloro-1,3-butadiene U 0.0211 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
Isopropylbenzene 0.00217 J 0.00144 0.00250 0.00416 1 03/06/2019 12:22 WG1245896 9
p-Isopropyltoluene U 0.00388 0.00500 0.00832 1 03/06/2019 12:22 WG1245896 Al
2-Butanone (MEK) 0.0400 J 0.0208 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
10
Methylene Chloride U 0.0111 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
Sc
4-Methyl-2-pentanone (MIBK) U 0.0166 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
Methyl tert-butyl ether U 0.000491 0.00100 0.00166 1 03/06/2019 12:22 WG1245896
Naphthalene 0.0458 B 0.00519 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
n-Propylbenzene 0.00464 J 0.00196 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Styrene U 0.00454 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
1,1,1,2-Tetrachloroethane U 0.000832 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
1,1,2,2-Tetrachloroethane U 0.000649 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
1,1,2-Trichlorotrifluoroethane U 0.00112 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Tetrachloroethene U 0.00117 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Toluene 0.619 0.00208 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
1,2,3-Trichlorobenzene U 0.00104 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
1,2,4-Trichlorobenzene U 0.00802 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
1,1,1-Trichloroethane U 0.000458 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
1,1,2-Trichloroethane U 0.00147 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Trichloroethene U 0.000666 0.00100 0.00166 1 03/06/2019 12:22 WG1245896
Trichlorofluoromethane U 0.000832 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
1,2,3-Trichloropropane U 0.00849 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
1,2,4-Trimethylbenzene 0.0265 0.00193 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
1,2,3-Trimethylbenzene U 0.00191 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
1,3,5-Trimethylbenzene 0.00787 J 0.00180 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Vinyl chloride U 0.00114 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Xylenes, Total 0.726 0.00796 0.00650 0.0108 1 03/06/2019 12:22 WG1245896
(S) Toluene-d8 96.5 75.0-131 03/06/2019 12:22 WG1245896
(S) 4-Bromofluorobenzene 87.8 67.0-138 03/06/2019 12:22 WG1245896
(S) 1,2-Dichloroethane-d4 117 70.0-130 03/06/2019 12:22 WG1245896

Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
TPH C6 - C12 U 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
TPH C12 - C28 225 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
TPH C28 - C35 39.6 J 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
TPH C6 - C35 265 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
(S) o-Terphenyl 119 70.0-130 03/09/2019 23:30 WG1246136

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 82 of 161
PS-3 SAMPLE RESULTS - 22 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:45 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270C


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
Acenaphthene U 0.0214 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Tc
Acenaphthylene U 0.0223 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Anthracene U 0.0210 0.0333 0.111 2 03/05/2019 05:48 WG1244658 3
Benzidine U J4 0.212 0.333 1.11 2 03/05/2019 05:48 WG1244658 Ss
Benzo(a)anthracene U 0.0142 0.0333 0.111 2 03/05/2019 05:48 WG1244658
4
Benzo(b)fluoranthene U 0.0231 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Cn
Benzo(k)fluoranthene U 0.0194 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Benzo(g,h,i)perylene U 0.0240 0.0333 0.111 2 03/05/2019 05:48 WG1244658 5
Benzo(a)pyrene U 0.0182 0.0333 0.111 2 03/05/2019 05:48 WG1244658 Tr
Bis(2-chlorethoxy)methane U 0.0256 0.333 1.11 2 03/05/2019 05:48 WG1244658
6
Bis(2-chloroethyl)ether U 0.0298 0.333 1.11 2 03/05/2019 05:48 WG1244658
Sr
Bis(2-chloroisopropyl)ether U 0.0253 0.333 1.11 2 03/05/2019 05:48 WG1244658
4-Bromophenyl-phenylether U 0.0380 0.333 1.11 2 03/05/2019 05:48 WG1244658 7
2-Chloronaphthalene U 0.0213 0.0333 0.111 2 03/05/2019 05:48 WG1244658 Qc
4-Chlorophenyl-phenylether U 0.0209 0.333 1.11 2 03/05/2019 05:48 WG1244658
8
Chrysene U 0.0185 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Gl
Dibenz(a,h)anthracene U 0.0273 0.0333 0.111 2 03/05/2019 05:48 WG1244658
3,3-Dichlorobenzidine U 0.264 0.333 1.11 2 03/05/2019 05:48 WG1244658 9
2,4-Dinitrotoluene U 0.0202 0.333 1.11 2 03/05/2019 05:48 WG1244658 Al
2,6-Dinitrotoluene U 0.0245 0.333 1.11 2 03/05/2019 05:48 WG1244658
10
Fluoranthene U 0.0165 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Sc
Fluorene U 0.0227 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Hexachlorobenzene U 0.0285 0.333 1.11 2 03/05/2019 05:48 WG1244658
Hexachloro-1,3-butadiene U 0.0333 0.333 1.11 2 03/05/2019 05:48 WG1244658
Hexachlorocyclopentadiene U 0.195 0.333 1.11 2 03/05/2019 05:48 WG1244658
Hexachloroethane U 0.0446 0.333 1.11 2 03/05/2019 05:48 WG1244658
Indeno(1,2,3-cd)pyrene U 0.0257 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Isophorone U 0.0174 0.333 1.11 2 03/05/2019 05:48 WG1244658
Naphthalene 0.0296 J 0.0296 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Nitrobenzene U 0.0231 0.333 1.11 2 03/05/2019 05:48 WG1244658
n-Nitrosodimethylamine U 0.215 0.333 1.11 2 03/05/2019 05:48 WG1244658
n-Nitrosodiphenylamine U 0.300 0.333 1.11 2 03/05/2019 05:48 WG1244658
n-Nitrosodi-n-propylamine U 0.0302 0.333 1.11 2 03/05/2019 05:48 WG1244658
Phenanthrene U 0.0176 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Benzylbutyl phthalate U 0.0343 0.333 1.11 2 03/05/2019 05:48 WG1244658
Bis(2-ethylhexyl)phthalate 0.113 J 0.0399 0.333 1.11 2 03/05/2019 05:48 WG1244658
Di-n-butyl phthalate U 0.0363 0.333 1.11 2 03/05/2019 05:48 WG1244658
Diethyl phthalate U 0.0230 0.333 1.11 2 03/05/2019 05:48 WG1244658
Dimethyl phthalate U 0.0180 0.333 1.11 2 03/05/2019 05:48 WG1244658
Di-n-octyl phthalate U 0.0302 0.333 1.11 2 03/05/2019 05:48 WG1244658
Pyrene 0.143 0.0409 0.0333 0.111 2 03/05/2019 05:48 WG1244658
1,2,4-Trichlorobenzene U 0.0292 0.333 1.11 2 03/05/2019 05:48 WG1244658
4-Chloro-3-methylphenol U 0.0159 0.333 1.11 2 03/05/2019 05:48 WG1244658
2-Chlorophenol U 0.0277 0.333 1.11 2 03/05/2019 05:48 WG1244658
2,4-Dichlorophenol U 0.0248 0.333 1.11 2 03/05/2019 05:48 WG1244658
2,4-Dimethylphenol U 0.157 0.333 1.11 2 03/05/2019 05:48 WG1244658
4,6-Dinitro-2-methylphenol U 0.413 0.333 1.11 2 03/05/2019 05:48 WG1244658
2,4-Dinitrophenol U 0.326 0.333 1.11 2 03/05/2019 05:48 WG1244658
2-Nitrophenol U 0.0433 0.333 1.11 2 03/05/2019 05:48 WG1244658
4-Nitrophenol U 0.175 0.333 1.11 2 03/05/2019 05:48 WG1244658
Pentachlorophenol U 0.160 0.333 1.11 2 03/05/2019 05:48 WG1244658
Phenol 0.0355 J 0.0231 0.333 1.11 2 03/05/2019 05:48 WG1244658
2,4,6-Trichlorophenol U 0.0259 0.333 1.11 2 03/05/2019 05:48 WG1244658
(S) 2-Fluorophenol 70.7 12.0-120 03/05/2019 05:48 WG1244658
(S) Phenol-d5 62.1 10.0-120 03/05/2019 05:48 WG1244658
(S) Nitrobenzene-d5 55.6 10.0-122 03/05/2019 05:48 WG1244658

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 83 of 161
PS-3 SAMPLE RESULTS - 22 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 09:45 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270C


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
(S) 2-Fluorobiphenyl 60.2 15.0-120 03/05/2019 05:48 WG1244658
Tc
(S) 2,4,6-Tribromophenol 64.4 10.0-127 03/05/2019 05:48 WG1244658
(S) p-Terphenyl-d14 62.4 10.0-120 03/05/2019 05:48 WG1244658 3
Ss
Sample Narrative:
4
L1075168-22 WG1244658: Dilution due to matrix impact during extract concentration procedure
Cn

5
Tr

6
Sr

7
Qc

8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 84 of 161
PS-4 SAMPLE RESULTS - 23 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 10:00 L1075168

Total Solids by Method 2540 G-2011 1

Result Qualifier Dilution Analysis Batch


Cp
Analyte % date / time
2
Total Solids 62.9 1 03/06/2019 10:56 WG1245670 Tc

3
Wet Chemistry by Method 9050AMod Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm umhos/cm date / time 4
Cn
Specific Conductance 2630 10.0 10.0 10.0 1 03/06/2019 21:03 WG1245948
5
Wet Chemistry by Method 9056A Tr
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
6
Analyte mg/kg mg/kg mg/kg mg/kg date / time Sr
Chloride 909 1.26 10.0 15.9 1 03/06/2019 19:34 WG1245719
7
Qc
Mercury by Method 7471A
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 8

Analyte mg/kg mg/kg mg/kg mg/kg date / time


Gl
Mercury 0.872 0.00445 0.0200 0.0318 1 03/05/2019 09:14 WG1245047 9
Al
Metals (ICP) by Method 6010B
10
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Sc
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Arsenic 21.0 0.731 2.00 3.18 1 03/07/2019 20:50 WG1245191
Barium 23300 1.35 0.500 3.97 5 03/08/2019 10:12 WG1245191
Cadmium U 0.556 0.500 3.97 5 03/08/2019 10:12 WG1245191
Chromium 36.9 0.223 1.00 1.59 1 03/07/2019 20:50 WG1245191
Lead 77.9 0.302 0.500 0.795 1 03/07/2019 20:50 WG1245191
Selenium U 0.985 2.00 3.18 1 03/07/2019 20:50 WG1245191
Silver U 0.191 1.00 1.59 1 03/07/2019 20:50 WG1245191

Volatile Organic Compounds (GC/MS) by Method 8260B


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Acetone U 0.0218 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
Acrylonitrile U 0.00302 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
Benzene 0.00214 0.000636 0.00100 0.00159 1 03/06/2019 14:30 WG1245896
Bromobenzene U 0.00167 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
Bromodichloromethane U 0.00125 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Bromoform U 0.00951 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
Bromomethane U 0.00588 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
n-Butylbenzene 0.0198 J 0.00610 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
sec-Butylbenzene 0.0155 J 0.00402 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
tert-Butylbenzene U 0.00246 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Carbon tetrachloride U 0.00172 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Chlorobenzene U 0.000911 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Chlorodibromomethane U 0.000715 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Chloroethane U 0.00172 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Chloroform U 0.000660 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Chloromethane U 0.00221 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
2-Chlorotoluene U 0.00146 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
4-Chlorotoluene U 0.00180 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
1,2-Dibromo-3-Chloropropane U 0.00811 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
1,2-Dibromoethane U 0.000834 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Dibromomethane U 0.00159 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
1,2-Dichlorobenzene U 0.00230 0.00500 0.00795 1 03/06/2019 14:30 WG1245896

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 85 of 161
PS-4 SAMPLE RESULTS - 23 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 10:00 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260B


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
1,3-Dichlorobenzene U 0.00270 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Tc
1,4-Dichlorobenzene U 0.00313 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Dichlorodifluoromethane U 0.00130 0.00250 0.00397 1 03/06/2019 14:30 WG1245896 3
1,1-Dichloroethane U 0.000914 0.00250 0.00397 1 03/06/2019 14:30 WG1245896 Ss
1,2-Dichloroethane U 0.000755 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
4
1,1-Dichloroethene U 0.000795 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Cn
cis-1,2-Dichloroethene U 0.00110 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
trans-1,2-Dichloroethene U 0.00227 0.00500 0.00795 1 03/06/2019 14:30 WG1245896 5
1,2-Dichloropropane U 0.00202 0.00500 0.00795 1 03/06/2019 14:30 WG1245896 Tr
1,1-Dichloropropene U 0.00111 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
6
1,3-Dichloropropane U 0.00278 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Sr
cis-1,3-Dichloropropene U 0.00108 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
trans-1,3-Dichloropropene U 0.00243 0.00500 0.00795 1 03/06/2019 14:30 WG1245896 7
2,2-Dichloropropane U 0.00126 0.00250 0.00397 1 03/06/2019 14:30 WG1245896 Qc
Di-isopropyl ether U 0.000556 0.00100 0.00159 1 03/06/2019 14:30 WG1245896
8
Ethylbenzene 0.527 0.000842 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Gl
Hexachloro-1,3-butadiene U 0.0202 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
Isopropylbenzene 0.0242 0.00137 0.00250 0.00397 1 03/06/2019 14:30 WG1245896 9
p-Isopropyltoluene 0.0127 0.00370 0.00500 0.00795 1 03/06/2019 14:30 WG1245896 Al
2-Butanone (MEK) U 0.0199 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
10
Methylene Chloride U 0.0106 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
Sc
4-Methyl-2-pentanone (MIBK) U 0.0159 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
Methyl tert-butyl ether U 0.000469 0.00100 0.00159 1 03/06/2019 14:30 WG1245896
Naphthalene 0.324 0.00496 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
n-Propylbenzene 0.0705 0.00188 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Styrene U 0.00434 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
1,1,1,2-Tetrachloroethane U 0.000795 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
1,1,2,2-Tetrachloroethane U 0.000620 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
1,1,2-Trichlorotrifluoroethane U 0.00107 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Tetrachloroethene U 0.00111 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Toluene 1.24 0.00199 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
1,2,3-Trichlorobenzene U 0.000993 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
1,2,4-Trichlorobenzene U 0.00766 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
1,1,1-Trichloroethane U 0.000437 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
1,1,2-Trichloroethane U 0.00140 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Trichloroethene U 0.000636 0.00100 0.00159 1 03/06/2019 14:30 WG1245896
Trichlorofluoromethane U 0.000795 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
1,2,3-Trichloropropane U 0.00811 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
1,2,4-Trimethylbenzene 0.424 0.00184 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
1,2,3-Trimethylbenzene 0.171 0.00183 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
1,3,5-Trimethylbenzene 0.138 0.00172 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Vinyl chloride U 0.00109 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Xylenes, Total 3.51 0.00760 0.00650 0.0103 1 03/06/2019 14:30 WG1245896
(S) Toluene-d8 95.6 75.0-131 03/06/2019 14:30 WG1245896
(S) 4-Bromofluorobenzene 94.3 67.0-138 03/06/2019 14:30 WG1245896
(S) 1,2-Dichloroethane-d4 110 70.0-130 03/06/2019 14:30 WG1245896

Sample Narrative:
L1075168-23 WG1245896: Lowest possible dilution due to sample foaming.

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 86 of 161
PS-4 SAMPLE RESULTS - 23 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 10:00 L1075168

Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
TPH C6 - C12 99.5 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136
Tc
TPH C12 - C28 1720 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136
TPH C28 - C35 197 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136 3
TPH C6 - C35 2020 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136 Ss
(S) o-Terphenyl 129 70.0-130 03/09/2019 01:11 WG1246136
4
Cn
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 5
Tr
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.102 0.0333 0.529 10 03/05/2019 06:46 WG1244658 6
Acenaphthylene U 0.107 0.0333 0.529 10 03/05/2019 06:46 WG1244658 Sr
Anthracene 0.315 J 0.100 0.0333 0.529 10 03/05/2019 06:46 WG1244658
7
Benzidine U J4 1.01 0.333 5.29 10 03/05/2019 06:46 WG1244658
Qc
Benzo(a)anthracene 0.696 0.0680 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Benzo(b)fluoranthene 2.03 0.110 0.0333 0.529 10 03/05/2019 06:46 WG1244658 8
Benzo(k)fluoranthene 0.184 J 0.0925 0.0333 0.529 10 03/05/2019 06:46 WG1244658 Gl
Benzo(g,h,i)perylene 0.855 0.115 0.0333 0.529 10 03/05/2019 06:46 WG1244658
9
Benzo(a)pyrene 0.474 J 0.0871 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Al
Bis(2-chlorethoxy)methane U 0.122 0.333 5.29 10 03/05/2019 06:46 WG1244658
Bis(2-chloroethyl)ether U 0.142 0.333 5.29 10 03/05/2019 06:46 WG1244658 10
Bis(2-chloroisopropyl)ether U 0.121 0.333 5.29 10 03/05/2019 06:46 WG1244658 Sc
4-Bromophenyl-phenylether U 0.181 0.333 5.29 10 03/05/2019 06:46 WG1244658
2-Chloronaphthalene U 0.102 0.0333 0.529 10 03/05/2019 06:46 WG1244658
4-Chlorophenyl-phenylether U 0.0997 0.333 5.29 10 03/05/2019 06:46 WG1244658
Chrysene 0.647 0.0882 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Dibenz(a,h)anthracene U 0.130 0.0333 0.529 10 03/05/2019 06:46 WG1244658
3,3-Dichlorobenzidine U 1.26 0.333 5.29 10 03/05/2019 06:46 WG1244658
2,4-Dinitrotoluene U 0.0965 0.333 5.29 10 03/05/2019 06:46 WG1244658
2,6-Dinitrotoluene U 0.117 0.333 5.29 10 03/05/2019 06:46 WG1244658
Fluoranthene 7.09 0.0788 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Fluorene 2.02 0.108 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Hexachlorobenzene U 0.136 0.333 5.29 10 03/05/2019 06:46 WG1244658
Hexachloro-1,3-butadiene U 0.159 0.333 5.29 10 03/05/2019 06:46 WG1244658
Hexachlorocyclopentadiene U 0.933 0.333 5.29 10 03/05/2019 06:46 WG1244658
Hexachloroethane U 0.213 0.333 5.29 10 03/05/2019 06:46 WG1244658
Indeno(1,2,3-cd)pyrene 0.612 0.123 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Isophorone U 0.0830 0.333 5.29 10 03/05/2019 06:46 WG1244658
Naphthalene 1.30 0.141 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Nitrobenzene U 0.110 0.333 5.29 10 03/05/2019 06:46 WG1244658
n-Nitrosodimethylamine U 1.03 0.333 5.29 10 03/05/2019 06:46 WG1244658
n-Nitrosodiphenylamine 2.56 J 1.43 0.333 5.29 10 03/05/2019 06:46 WG1244658
n-Nitrosodi-n-propylamine U 0.144 0.333 5.29 10 03/05/2019 06:46 WG1244658
Phenanthrene 2.99 0.0839 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Benzylbutyl phthalate U 0.164 0.333 5.29 10 03/05/2019 06:46 WG1244658
Bis(2-ethylhexyl)phthalate 1.59 J 0.191 0.333 5.29 10 03/05/2019 06:46 WG1244658
Di-n-butyl phthalate U 0.173 0.333 5.29 10 03/05/2019 06:46 WG1244658
Diethyl phthalate U 0.110 0.333 5.29 10 03/05/2019 06:46 WG1244658
Dimethyl phthalate U 0.0858 0.333 5.29 10 03/05/2019 06:46 WG1244658
Di-n-octyl phthalate U 0.144 0.333 5.29 10 03/05/2019 06:46 WG1244658
Pyrene 4.67 0.196 0.0333 0.529 10 03/05/2019 06:46 WG1244658
1,2,4-Trichlorobenzene U 0.139 0.333 5.29 10 03/05/2019 06:46 WG1244658
4-Chloro-3-methylphenol U 0.0758 0.333 5.29 10 03/05/2019 06:46 WG1244658
2-Chlorophenol U 0.132 0.333 5.29 10 03/05/2019 06:46 WG1244658
2,4-Dichlorophenol U 0.119 0.333 5.29 10 03/05/2019 06:46 WG1244658
2,4-Dimethylphenol U 0.749 0.333 5.29 10 03/05/2019 06:46 WG1244658
4,6-Dinitro-2-methylphenol U 1.97 0.333 5.29 10 03/05/2019 06:46 WG1244658

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 87 of 161
PS-4 SAMPLE RESULTS - 23 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 10:00 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270C


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
2,4-Dinitrophenol U 1.56 0.333 5.29 10 03/05/2019 06:46 WG1244658
Tc
2-Nitrophenol U 0.207 0.333 5.29 10 03/05/2019 06:46 WG1244658
4-Nitrophenol U 0.834 0.333 5.29 10 03/05/2019 06:46 WG1244658 3
Pentachlorophenol U 0.763 0.333 5.29 10 03/05/2019 06:46 WG1244658 Ss
Phenol U 0.110 0.333 5.29 10 03/05/2019 06:46 WG1244658
4
2,4,6-Trichlorophenol U 0.124 0.333 5.29 10 03/05/2019 06:46 WG1244658
Cn
(S) 2-Fluorophenol 65.8 12.0-120 03/05/2019 06:46 WG1244658
(S) Phenol-d5 56.0 10.0-120 03/05/2019 06:46 WG1244658 5
(S) Nitrobenzene-d5 142 J1 10.0-122 03/05/2019 06:46 WG1244658 Tr
(S) 2-Fluorobiphenyl 53.9 15.0-120 03/05/2019 06:46 WG1244658
6
(S) 2,4,6-Tribromophenol 47.9 10.0-127 03/05/2019 06:46 WG1244658
Sr
(S) p-Terphenyl-d14 79.8 10.0-120 03/05/2019 06:46 WG1244658
7
Sample Narrative: Qc
L1075168-23 WG1244658: Dilution due to matrix.
8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 88 of 161
PS-5 SAMPLE RESULTS - 24 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:00 L1075168

Total Solids by Method 2540 G-2011 1

Result Qualifier Dilution Analysis Batch


Cp
Analyte % date / time
2
Total Solids 56.0 1 03/06/2019 10:56 WG1245670 Tc

3
Wet Chemistry by Method 9050AMod Ss
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm umhos/cm date / time 4
Cn
Specific Conductance 1020 10.0 10.0 10.0 1 03/06/2019 21:03 WG1245948
5
Wet Chemistry by Method 9056A Tr
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
6
Analyte mg/kg mg/kg mg/kg mg/kg date / time Sr
Chloride 498 1.42 10.0 17.9 1 03/06/2019 19:59 WG1245719
7
Qc
Mercury by Method 7471A
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 8

Analyte mg/kg mg/kg mg/kg mg/kg date / time


Gl
Mercury 0.758 0.00500 0.0200 0.0357 1 03/05/2019 09:17 WG1245047 9
Al
Metals (ICP) by Method 6010B
10
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Sc
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Arsenic 20.2 0.822 2.00 3.57 1 03/07/2019 20:53 WG1245191
Barium 25200 1.52 0.500 4.47 5 03/08/2019 10:14 WG1245191
Cadmium U 0.625 0.500 4.47 5 03/08/2019 10:14 WG1245191
Chromium 47.0 0.250 1.00 1.79 1 03/07/2019 20:53 WG1245191
Lead 78.9 0.339 0.500 0.893 1 03/07/2019 20:53 WG1245191
Selenium U 1.11 2.00 3.57 1 03/07/2019 20:53 WG1245191
Silver U 0.214 1.00 1.79 1 03/07/2019 20:53 WG1245191

Volatile Organic Compounds (GC/MS) by Method 8260B


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
Acetone U 0.0245 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
Acrylonitrile U 0.00339 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
Benzene 0.0152 0.000715 0.00100 0.00179 1 03/06/2019 14:49 WG1245896
Bromobenzene U 0.00188 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
Bromodichloromethane U 0.00141 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Bromoform U 0.0107 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
Bromomethane U 0.00661 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
n-Butylbenzene 0.00715 J 0.00686 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
sec-Butylbenzene 0.00539 J 0.00452 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
tert-Butylbenzene U 0.00277 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Carbon tetrachloride 0.00544 J 0.00193 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Chlorobenzene U 0.00102 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Chlorodibromomethane U 0.000804 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Chloroethane U 0.00193 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Chloroform U 0.000741 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Chloromethane U 0.00248 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
2-Chlorotoluene U 0.00164 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
4-Chlorotoluene U 0.00202 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
1,2-Dibromo-3-Chloropropane U 0.00911 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
1,2-Dibromoethane U 0.000938 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Dibromomethane U 0.00179 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
1,2-Dichlorobenzene U 0.00259 0.00500 0.00893 1 03/06/2019 14:49 WG1245896

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 89 of 161
PS-5 SAMPLE RESULTS - 24 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:00 L1075168

Volatile Organic Compounds (GC/MS) by Method 8260B


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
1,3-Dichlorobenzene U 0.00304 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Tc
1,4-Dichlorobenzene U 0.00352 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Dichlorodifluoromethane U 0.00146 0.00250 0.00447 1 03/06/2019 14:49 WG1245896 3
1,1-Dichloroethane U 0.00103 0.00250 0.00447 1 03/06/2019 14:49 WG1245896 Ss
1,2-Dichloroethane U 0.000849 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
4
1,1-Dichloroethene U 0.000893 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Cn
cis-1,2-Dichloroethene U 0.00123 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
trans-1,2-Dichloroethene U 0.00255 0.00500 0.00893 1 03/06/2019 14:49 WG1245896 5
1,2-Dichloropropane U 0.00227 0.00500 0.00893 1 03/06/2019 14:49 WG1245896 Tr
1,1-Dichloropropene U 0.00125 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
6
1,3-Dichloropropane U 0.00313 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Sr
cis-1,3-Dichloropropene U 0.00121 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
trans-1,3-Dichloropropene U 0.00273 0.00500 0.00893 1 03/06/2019 14:49 WG1245896 7
2,2-Dichloropropane U 0.00142 0.00250 0.00447 1 03/06/2019 14:49 WG1245896 Qc
Di-isopropyl ether U 0.000625 0.00100 0.00179 1 03/06/2019 14:49 WG1245896
8
Ethylbenzene 0.0888 0.000947 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Gl
Hexachloro-1,3-butadiene U 0.0227 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
Isopropylbenzene U 0.00154 0.00250 0.00447 1 03/06/2019 14:49 WG1245896 9
p-Isopropyltoluene 0.00783 J 0.00416 0.00500 0.00893 1 03/06/2019 14:49 WG1245896 Al
2-Butanone (MEK) U 0.0223 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
10
Methylene Chloride U 0.0119 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
Sc
4-Methyl-2-pentanone (MIBK) U 0.0179 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
Methyl tert-butyl ether U 0.000527 0.00100 0.00179 1 03/06/2019 14:49 WG1245896
Naphthalene 0.0641 B 0.00557 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
n-Propylbenzene 0.0147 0.00211 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Styrene U 0.00488 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
1,1,1,2-Tetrachloroethane U 0.000893 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
1,1,2,2-Tetrachloroethane U 0.000697 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
1,1,2-Trichlorotrifluoroethane U 0.00121 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Tetrachloroethene U 0.00125 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Toluene 0.526 0.00223 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
1,2,3-Trichlorobenzene U 0.00112 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
1,2,4-Trichlorobenzene U 0.00861 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
1,1,1-Trichloroethane U 0.000491 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
1,1,2-Trichloroethane U 0.00158 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Trichloroethene U 0.000715 0.00100 0.00179 1 03/06/2019 14:49 WG1245896
Trichlorofluoromethane U 0.000893 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
1,2,3-Trichloropropane U 0.00911 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
1,2,4-Trimethylbenzene 0.102 0.00207 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
1,2,3-Trimethylbenzene 0.0802 0.00205 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
1,3,5-Trimethylbenzene 0.0486 0.00193 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Vinyl chloride U 0.00122 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Xylenes, Total 0.654 0.00854 0.00650 0.0116 1 03/06/2019 14:49 WG1245896
(S) Toluene-d8 99.0 75.0-131 03/06/2019 14:49 WG1245896
(S) 4-Bromofluorobenzene 102 67.0-138 03/06/2019 14:49 WG1245896
(S) 1,2-Dichloroethane-d4 109 70.0-130 03/06/2019 14:49 WG1245896

Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005


Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg mg/kg date / time
TPH C6 - C12 142 26.8 50.0 89.3 1 03/09/2019 02:20 WG1246136
TPH C12 - C28 4650 134 50.0 447 5 03/09/2019 23:58 WG1246136
TPH C28 - C35 153 26.8 50.0 89.3 1 03/09/2019 02:20 WG1246136
TPH C6 - C35 4950 134 50.0 447 5 03/09/2019 23:58 WG1246136
(S) o-Terphenyl 139 J1 70.0-130 03/09/2019 02:20 WG1246136
(S) o-Terphenyl 157 J1 70.0-130 03/09/2019 23:58 WG1246136

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 90 of 161
PS-5 SAMPLE RESULTS - 24 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:00 L1075168

Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
Tc
Sample Narrative:
L1075168-24 WG1246136: Surrogate failure due to matrix interference 3
Ss
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
4
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cn
Analyte mg/kg mg/kg mg/kg mg/kg date / time
5
Acenaphthene U 1.15 0.0333 5.95 100 03/05/2019 12:37 WG1244658
Tr
Acenaphthylene U 1.20 0.0333 5.95 100 03/05/2019 12:37 WG1244658
Anthracene U 1.13 0.0333 5.95 100 03/05/2019 12:37 WG1244658 6
Benzidine U J4 0.228 0.333 1.19 2 03/05/2019 06:07 WG1244658 Sr
Benzo(a)anthracene 0.168 0.0153 0.0333 0.119 2 03/05/2019 06:07 WG1244658
7
Benzo(b)fluoranthene U 0.0248 0.0333 0.119 2 03/05/2019 06:07 WG1244658
Qc
Benzo(k)fluoranthene U 0.0208 0.0333 0.119 2 03/05/2019 06:07 WG1244658
Benzo(g,h,i)perylene 0.0806 J 0.0258 0.0333 0.119 2 03/05/2019 06:07 WG1244658 8
Benzo(a)pyrene 0.0893 J 0.0196 0.0333 0.119 2 03/05/2019 06:07 WG1244658 Gl
Bis(2-chlorethoxy)methane U 0.0275 0.333 1.19 2 03/05/2019 06:07 WG1244658
9
Bis(2-chloroethyl)ether U 0.0320 0.333 1.19 2 03/05/2019 06:07 WG1244658
Al
Bis(2-chloroisopropyl)ether U 0.0272 0.333 1.19 2 03/05/2019 06:07 WG1244658
4-Bromophenyl-phenylether U 2.04 0.333 59.5 100 03/05/2019 12:37 WG1244658 10
2-Chloronaphthalene U 1.14 0.0333 5.95 100 03/05/2019 12:37 WG1244658 Sc
4-Chlorophenyl-phenylether U 1.12 0.333 59.5 100 03/05/2019 12:37 WG1244658
Chrysene 0.243 0.0198 0.0333 0.119 2 03/05/2019 06:07 WG1244658
Dibenz(a,h)anthracene U 0.0293 0.0333 0.119 2 03/05/2019 06:07 WG1244658
3,3-Dichlorobenzidine U 0.284 0.333 1.19 2 03/05/2019 06:07 WG1244658
2,4-Dinitrotoluene U 1.08 0.333 59.5 100 03/05/2019 12:37 WG1244658
2,6-Dinitrotoluene U 1.32 0.333 59.5 100 03/05/2019 12:37 WG1244658
Fluoranthene U 0.886 0.0333 5.95 100 03/05/2019 12:37 WG1244658
Fluorene U 1.22 0.0333 5.95 100 03/05/2019 12:37 WG1244658
Hexachlorobenzene U 1.53 0.333 59.5 100 03/05/2019 12:37 WG1244658
Hexachloro-1,3-butadiene U 0.0357 0.333 1.19 2 03/05/2019 06:07 WG1244658
Hexachlorocyclopentadiene U 10.5 0.333 59.5 100 03/05/2019 12:37 WG1244658
Hexachloroethane U 0.0479 0.333 1.19 2 03/05/2019 06:07 WG1244658
Indeno(1,2,3-cd)pyrene U 0.0276 0.0333 0.119 2 03/05/2019 06:07 WG1244658
Isophorone U 0.0187 0.333 1.19 2 03/05/2019 06:07 WG1244658
Naphthalene U 0.0318 0.0333 0.119 2 03/05/2019 06:07 WG1244658
Nitrobenzene U 0.0248 0.333 1.19 2 03/05/2019 06:07 WG1244658
n-Nitrosodimethylamine U 0.231 0.333 1.19 2 03/05/2019 06:07 WG1244658
n-Nitrosodiphenylamine U 16.1 0.333 59.5 100 03/05/2019 12:37 WG1244658
n-Nitrosodi-n-propylamine U 0.0324 0.333 1.19 2 03/05/2019 06:07 WG1244658
Phenanthrene 2.20 J 0.943 0.0333 5.95 100 03/05/2019 12:37 WG1244658
Benzylbutyl phthalate U 0.0368 0.333 1.19 2 03/05/2019 06:07 WG1244658
Bis(2-ethylhexyl)phthalate 0.498 J 0.0429 0.333 1.19 2 03/05/2019 06:07 WG1244658
Di-n-butyl phthalate U 1.95 0.333 59.5 100 03/05/2019 12:37 WG1244658
Diethyl phthalate U 1.23 0.333 59.5 100 03/05/2019 12:37 WG1244658
Dimethyl phthalate U 0.965 0.333 59.5 100 03/05/2019 12:37 WG1244658
Di-n-octyl phthalate U 0.0324 0.333 1.19 2 03/05/2019 06:07 WG1244658
Pyrene 1.61 0.0440 0.0333 0.119 2 03/05/2019 06:07 WG1244658
1,2,4-Trichlorobenzene U 0.0313 0.333 1.19 2 03/05/2019 06:07 WG1244658
4-Chloro-3-methylphenol U 0.0170 0.333 1.19 2 03/05/2019 06:07 WG1244658
2-Chlorophenol U 0.0297 0.333 1.19 2 03/05/2019 06:07 WG1244658
2,4-Dichlorophenol U 0.0267 0.333 1.19 2 03/05/2019 06:07 WG1244658
2,4-Dimethylphenol U 0.168 0.333 1.19 2 03/05/2019 06:07 WG1244658
4,6-Dinitro-2-methylphenol U 22.2 0.333 59.5 100 03/05/2019 12:37 WG1244658
2,4-Dinitrophenol U 17.5 0.333 59.5 100 03/05/2019 12:37 WG1244658
2-Nitrophenol U 0.0465 0.333 1.19 2 03/05/2019 06:07 WG1244658

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 91 of 161
PS-5 SAMPLE RESULTS - 24 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 17:00 L1075168

Semi Volatile Organic Compounds (GC/MS) by Method 8270C


1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
Analyte mg/kg mg/kg mg/kg mg/kg date / time
2
4-Nitrophenol U 9.38 0.333 59.5 100 03/05/2019 12:37 WG1244658
Tc
Pentachlorophenol U 8.58 0.333 59.5 100 03/05/2019 12:37 WG1244658
Phenol U 0.0248 0.333 1.19 2 03/05/2019 06:07 WG1244658 3
2,4,6-Trichlorophenol U 1.39 0.333 59.5 100 03/05/2019 12:37 WG1244658 Ss
(S) 2-Fluorophenol 73.0 12.0-120 03/05/2019 06:07 WG1244658
4
(S) 2-Fluorophenol 74.5 J7 12.0-120 03/05/2019 12:37 WG1244658
Cn
(S) Phenol-d5 60.2 J7 10.0-120 03/05/2019 12:37 WG1244658
(S) Phenol-d5 67.1 10.0-120 03/05/2019 06:07 WG1244658 5
(S) Nitrobenzene-d5 169 J1 10.0-122 03/05/2019 06:07 WG1244658 Tr
(S) Nitrobenzene-d5 111 J7 10.0-122 03/05/2019 12:37 WG1244658
6
(S) 2-Fluorobiphenyl 47.6 15.0-120 03/05/2019 06:07 WG1244658
Sr
(S) 2-Fluorobiphenyl 79.9 J7 15.0-120 03/05/2019 12:37 WG1244658
(S) 2,4,6-Tribromophenol 70.7 10.0-127 03/05/2019 06:07 WG1244658 7
(S) 2,4,6-Tribromophenol 74.8 J7 10.0-127 03/05/2019 12:37 WG1244658 Qc
(S) p-Terphenyl-d14 87.8 10.0-120 03/05/2019 06:07 WG1244658
8
(S) p-Terphenyl-d14 84.1 J7 10.0-120 03/05/2019 12:37 WG1244658
Gl
Sample Narrative: 9
L1075168-24 WG1244658: IS/SURR failed on lower dilution. Al
L1075168-24 WG1244658: Dilution due to matrix impact during extract concentration procedure
10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 92 of 161
WG1246056 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Gravimetric Analysis by Method 2540 C-2011 L1075168-01,02,03,04

Method Blank (MB) 1


Cp
(MB) R3390172-1 03/07/19 23:39
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/l mg/l mg/l Tc
Dissolved Solids U 2.82 10.0
3
Ss
L1075168-04 Original Sample (OS) • Duplicate (DUP) 4

(OS) L1075168-04 03/07/19 23:39 • (DUP) R3390172-3 03/07/19 23:39


Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte mg/l mg/l % %
Dissolved Solids 1700 1720 1 0.878 5 6
Sr

Laboratory Control Sample (LCS) 7


Qc
(LCS) R3390172-2 03/07/19 23:39
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 8

Analyte mg/l mg/l % %


Gl
Dissolved Solids 8800 8720 99.1 85.0-115
9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 93 of 161
WG1246058 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Gravimetric Analysis by Method 2540 C-2011 L1075168-05,06,07,08,09,10,11,12,13,14

Method Blank (MB) 1


Cp
(MB) R3390170-1 03/07/19 23:09
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/l mg/l mg/l Tc
Dissolved Solids U 2.82 10.0
3
Ss
L1075168-06 Original Sample (OS) • Duplicate (DUP) 4

(OS) L1075168-06 03/07/19 23:09 • (DUP) R3390170-3 03/07/19 23:09


Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte mg/l mg/l % %
Dissolved Solids 1120 1020 1 8.79 J3 5 6
Sr

Laboratory Control Sample (LCS) 7


Qc
(LCS) R3390170-2 03/07/19 23:09
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 8

Analyte mg/l mg/l % %


Gl
Dissolved Solids 8800 8210 93.3 85.0-115
9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 94 of 161
WG1246059 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Gravimetric Analysis by Method 2540 C-2011 L1075168-15,16,17,18,19

Method Blank (MB) 1


Cp
(MB) R3390171-1 03/08/19 01:53
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/l mg/l mg/l Tc
Dissolved Solids U 2.82 10.0
3
Ss
L1075168-18 Original Sample (OS) • Duplicate (DUP) 4

(OS) L1075168-18 03/08/19 01:53 • (DUP) R3390171-3 03/08/19 01:53


Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte mg/l mg/l % %
Dissolved Solids 116 127 1 9.05 J3 5 6
Sr

Laboratory Control Sample (LCS) 7


Qc
(LCS) R3390171-2 03/08/19 01:53
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 8

Analyte mg/l mg/l % %


Gl
Dissolved Solids 8800 8610 97.8 85.0-115
9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 95 of 161
WG1245367 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Total Solids by Method 2540 G-2011 L1075168-20,21

Method Blank (MB) 1


Cp
(MB) R3389442-1 03/06/19 14:08
MB Result MB Qualifier MB MDL MB RDL 2
Analyte % % % Tc
Total Solids 0.00100
3
Ss
L1075104-02 Original Sample (OS) • Duplicate (DUP) 4

(OS) L1075104-02 03/06/19 14:08 • (DUP) R3389442-3 03/06/19 14:08


Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte % % % %
Total Solids 87.5 91.8 1 4.82 10 6
Sr

Laboratory Control Sample (LCS) 7


Qc
(LCS) R3389442-2 03/06/19 14:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 8

Analyte % % % %
Gl
Total Solids 50.0 50.0 100 85.0-115
9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 96 of 161
WG1245670 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Total Solids by Method 2540 G-2011 L1075168-22,23,24

Method Blank (MB) 1


Cp
(MB) R3389479-1 03/06/19 10:56
MB Result MB Qualifier MB MDL MB RDL 2
Analyte % % % Tc
Total Solids 0.00100
3
Ss
L1075101-12 Original Sample (OS) • Duplicate (DUP) 4

(OS) L1075101-12 03/06/19 10:56 • (DUP) R3389479-3 03/06/19 10:56


Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte % % % %
Total Solids 81.0 80.6 1 0.407 10 6
Sr

Laboratory Control Sample (LCS) 7


Qc
(LCS) R3389479-2 03/06/19 10:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 8

Analyte % % % %
Gl
Total Solids 50.0 50.0 100 85.0-115
9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 97 of 161
WG1245955 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 2320 B-2011 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19

Method Blank (MB) 1


Cp
(MB) R3389725-1 03/07/19 14:26
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/l mg/l mg/l Tc
Alkalinity U 2.71 20.0
3
Ss
Sample Narrative:
BLANK: Endpoint pH 4.5 4
Cn

L1075168-01 Original Sample (OS) • Duplicate (DUP) 5


Tr
(OS) L1075168-01 03/07/19 14:32 • (DUP) R3389725-2 03/07/19 14:38
DUP RPD 6
Original Result DUP Result Dilution DUP RPD DUP Qualifier Sr
Limits
Analyte mg/l mg/l % %
7
Alkalinity 157 157 1 0.0644 20
Qc
Sample Narrative: 8
OS: Endpoint pH 4.5 headspace Gl
DUP: Endpoint pH 4.5
9
Al
L1075168-19 Original Sample (OS) • Duplicate (DUP) 10

(OS) L1075168-19 03/07/19 17:04 • (DUP) R3389725-4 03/07/19 17:11


Sc
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier Limits
Analyte mg/l mg/l % %
Alkalinity 339 335 1 1.26 20

Sample Narrative:
OS: Endpoint pH 4.5 headspace
DUP: Endpoint pH 4.5

Laboratory Control Sample (LCS)


(LCS) R3389725-3 03/07/19 15:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l % %
Alkalinity 100 93.4 93.4 85.0-115

Sample Narrative:
LCS: Endpoint pH 4.5

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 98 of 161
WG1245159 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 300.0 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19

Method Blank (MB) 1


Cp
(MB) R3389142-1 03/06/19 00:32
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/l mg/l mg/l Tc
Chloride U 0.0519 1.00
3
Sulfate U 0.0774 5.00
Ss

4
L1075175-01 Original Sample (OS) • Duplicate (DUP) Cn
(OS) L1075175-01 03/06/19 01:29 • (DUP) R3389142-3 03/06/19 01:44
5
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Tr
Limits
Analyte mg/l mg/l % % 6
Chloride 21.8 21.7 1 0.349 20 Sr
Sulfate 51.2 51.1 1 0.281 20
7
Qc
L1075168-08 Original Sample (OS) • Duplicate (DUP) 8

(OS) L1075168-08 03/06/19 04:49 • (DUP) R3389142-6 03/06/19 05:04


Gl
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 9
Limits
Al
Analyte mg/l mg/l % %
Chloride 13.3 13.2 1 0.777 20 10
Sulfate 10.7 10.6 1 0.786 20 Sc

Laboratory Control Sample (LCS)


(LCS) R3389142-2 03/06/19 00:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/l mg/l % %
Chloride 40.0 40.3 101 90.0-110
Sulfate 40.0 41.0 103 90.0-110

L1075175-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1075175-01 03/06/19 01:29 • (MS) R3389142-4 03/06/19 01:59 • (MSD) R3389142-5 03/06/19 02:15
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Chloride 50.0 21.8 71.2 71.5 98.7 99.3 1 80.0-120 0.414 20
Sulfate 50.0 51.2 98.4 99.0 94.4 95.5 1 80.0-120 0.537 20

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


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16:10 99 of 161
WG1245159 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 300.0 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19

L1075168-08 Original Sample (OS) • Matrix Spike (MS) 1


Cp
(OS) L1075168-08 03/06/19 04:49 • (MS) R3389142-7 03/06/19 05:19
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier 2
Analyte mg/l mg/l mg/l % % Tc
Chloride 50.0 13.3 62.5 98.5 1 80.0-120
3
Sulfate 50.0 10.7 60.2 99.0 1 80.0-120
Ss

4
Cn

5
Tr

6
Sr

7
Qc

8
Gl

9
Al

10
Sc

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 100 of 161
WG1245130 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9040C L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16

L1075088-06 Original Sample (OS) • Duplicate (DUP) 1


Cp
(OS) L1075088-06 03/05/19 11:55 • (DUP) R3388776-2 03/05/19 11:55
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 2
Limits Tc
Analyte su su % %
pH 8.28 8.30 1 0.241 1 3
Ss
Sample Narrative:
4
OS: 8.28 at 16.3C Cn
DUP: 8.3 at 16.3C
5
Tr
L1075168-16 Original Sample (OS) • Duplicate (DUP)
6
(OS) L1075168-16 03/05/19 11:55 • (DUP) R3388776-3 03/05/19 11:55 Sr
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier Limits 7
Analyte su su % % Qc
pH 7.91 7.90 1 0.127 1
8
Gl
Sample Narrative:
OS: 7.91 at 13.3C 9
DUP: 7.9 at 13.3C Al

10
Sc
Laboratory Control Sample (LCS)
(LCS) R3388776-1 03/05/19 11:55
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su % %
pH 10.0 10.0 100 99.0-101

Sample Narrative:
LCS: 10.01 at 16.9C

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 101 of 161
WG1245737 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9040C L1075168-17,18,19

L1075431-04 Original Sample (OS) • Duplicate (DUP) 1


Cp
(OS) L1075431-04 03/06/19 09:50 • (DUP) R3389133-2 03/06/19 09:50
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 2
Limits Tc
Analyte su su % %
pH 12.7 12.7 1 0.0786 1 3
Ss
Sample Narrative:
4
OS: 12.71 at 18.1C Cn
DUP: 12.72 at 18.1C
5
Tr
L1075510-10 Original Sample (OS) • Duplicate (DUP)
6
(OS) L1075510-10 03/06/19 09:50 • (DUP) R3389133-3 03/06/19 09:50 Sr
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier Limits 7
Analyte su su % % Qc
pH 11.7 11.7 1 0.000 1
8
Gl
Sample Narrative:
OS: 11.71 at 15.5C 9
DUP: 11.71 at 15.5C Al

10
Sc
Laboratory Control Sample (LCS)
(LCS) R3389133-1 03/06/19 09:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su % %
pH 10.0 10.0 100 99.0-101

Sample Narrative:
LCS: 10 at 15.7C

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 102 of 161
WG1245735 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9050A L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19

Method Blank (MB) 1


Cp
(MB) R3389563-1 03/07/19 13:22
MB Result MB Qualifier MB MDL MB RDL 2
Analyte umhos/cm umhos/cm umhos/cm Tc
Specific Conductance U 10.0 10.0
3
Ss
L1075168-01 Original Sample (OS) • Duplicate (DUP) 4

(OS) L1075168-01 03/07/19 13:22 • (DUP) R3389563-3 03/07/19 13:22


Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte umhos/cm umhos/cm % %
Specific Conductance 4510 4500 1 0.222 20 6
Sr

L1075285-01 Original Sample (OS) • Duplicate (DUP) 7


Qc
(OS) L1075285-01 03/07/19 13:22 • (DUP) R3389563-4 03/07/19 13:22
DUP RPD 8
Original Result DUP Result Dilution DUP RPD DUP Qualifier Gl
Limits
Analyte umhos/cm umhos/cm % %
9
Specific Conductance 239 239 1 0.0838 20
Al

10
Laboratory Control Sample (LCS) Sc
(LCS) R3389563-2 03/07/19 13:22
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte umhos/cm umhos/cm % %
Specific Conductance 877 861 98.2 90.0-110

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 103 of 161
WG1245948 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9050AMod L1075168-20,21,22,23,24

Method Blank (MB) 1


Cp
(MB) R3389320-1 03/06/19 21:03
MB Result MB Qualifier MB MDL MB RDL 2
Analyte umhos/cm umhos/cm umhos/cm Tc
Specific Conductance U 10.0 10.0
3
Ss
L1075168-20 Original Sample (OS) • Duplicate (DUP) 4

(OS) L1075168-20 03/06/19 21:03 • (DUP) R3389320-3 03/06/19 21:03


Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte umhos/cm umhos/cm % %
Specific Conductance 933 936 1 0.321 20 6
Sr

L1075732-04 Original Sample (OS) • Duplicate (DUP) 7


Qc
(OS) L1075732-04 03/06/19 21:03 • (DUP) R3389320-4 03/06/19 21:03
DUP RPD 8
Original Result DUP Result Dilution DUP RPD DUP Qualifier Gl
Limits
Analyte umhos/cm umhos/cm % %
9
Specific Conductance 122 122 1 0.164 20
Al

10
Laboratory Control Sample (LCS) Sc
(LCS) R3389320-2 03/06/19 21:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte umhos/cm umhos/cm % %
Specific Conductance 877 876 99.9 90.0-110

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:


Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 104 of 161
WG1245719 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9056A L1075168-20,21,22,23,24

Method Blank (MB) 1