Fluid Phase Equilibria 288 (2010) 1–54

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Fluid Phase Equilibria

journal homepage: www.elsevier.com/locate/fluid

High-pressure fluid-phase equilibria: Experimental methods and systems

investigated (2000–2004)
Ralf Dohrn a,∗ , Stephanie Peper b , José M.S. Fonseca c
a
Bayer Technology Services GmbH, Fluid Properties & Thermodynamics, Geb. B310, D 51368 Leverkusen, Germany
b
Helmut-Schmidt-University/University of the Federal Armed Forces Hamburg, Institute of Thermodynamics, D 22043 Hamburg, Germany
c
Technical University of Denmark, Department of Chemical and Biochemical Engineering, DK-2800 Kgs. Lyngby, Denmark

a r t i c l e i n f o a b s t r a c t

Article history: As a part of a series of reviews, a compilation of systems for which high-pressure phase-equilibrium
Received 26 June 2009 data were published between 2000 and 2004 is given. Vapor–liquid equilibria, liquid–liquid equilibria,
Received in revised form 12 August 2009 vapor–liquid–liquid equilibria, solid–liquid equilibria, solid–vapor equilibria, solid–vapor–liquid equilib-
Accepted 13 August 2009
ria, critical points, the solubility of high-boiling substances in supercritical fluids, the solubility of gases
Available online 20 August 2009
in liquids and the solubility (sorption) of volatile components in polymers are included. For the systems
investigated, the reference, the temperature and pressure range of the data, and the experimental method
Keywords:
used for the measurements are given in 54 tables. Most of experimental data in the literature have been
Experiment
Data
given for binary systems. Of the 1204 binary systems, 681 (57%) have carbon dioxide as one of the com-
Method ponents. Information on 156 pure components, 451 ternary systems of which 267 (62%) contain carbon
VLE high pressure dioxide, 150 multicomponent and complex systems, and 129 systems with hydrates is given. Experimen-
Hydrocarbons tal methods for the investigation of high-pressure phase equilibria are classified and described. Work on
Non-hydrocarbons the continuation of the review series is under way, covering the period between 2005 and 2008, and will
be published in 2010.
© 2009 Elsevier B.V. All rights reserved.

1. Introduction sive to use imprecise data or to estimate data a couple of times

For the design and optimization of high-pressure chemical pro-
cesses and separation operations, information on high-pressure
phase equilibria and solubilities is essential. The simulation of
petroleum reservoirs, enhanced oil recovery, carbon capture and
storage, the transportation and storage of natural gas, refrigeration
and heat-pump cycles, and the study of geological processes are
other examples for the need of high-pressure phase-equilibrium
data. The interest in old and new applications of supercritical fluids
[1–3], like extraction, particle formation, impregnation and dyeing,
cleaning, reaction, chromatography, injection molding and extru-
sion, and electronic chip manufacturing, as well as the interest
in ionic liquids and “green solvents”, led to a continuation of the
increase in the number of publications concerning high-pressure
phase-equilibrium data.
There are many ways to obtain information about the phase
behavior of fluid mixtures, but the direct measurement of phase-
equilibrium data remains an important source of information,
though it is difficult and expensive to take precise experimental
data. On the other hand, for a company, it is very often more expen-
∗ Corresponding author. Fax: +49 214 30 81554.
E-mail address: ralf.dohrn@bayertechnology.com (R. Dohrn).
over the years, if experimental data are not available. There are
several review articles about techniques for experimental investi-
gations [4–14]. Information about experimental equilibrium data
is important, even when thermodynamic models are used to calcu-
late the phase behavior of a mixture. Thermodynamic models can
help to reduce the number of experimental data points needed for
a special design problem, but very often, at least some experimen-
tal data points are needed to adjust interaction parameters of the
model [15].
Reviews of high-pressure phase-equilibrium data in the litera-
ture have been published by several authors [8,10,13,14,16–24].
Some reviews cover a specific topic, like the solubility of cer-
tain substances in supercritical carbon dioxide, e.g., Bartle et al.
[14] for solids and liquids, Gücli-Üstündag and Temelli [19,23,24]
for lipids, and Higashi et al. [21] for high-boiling compounds,
or for a specific binary system, like Diamond and Akenfiev [22]
on carbon dioxide + water. Other reviews cover high-pressure
fluid-phase-equilibria data that have been published in a spe-
cific periods, e.g., Knapp et al. [17] covering 1900–1980, Fornari
et al. [8] covering 1978–1987, Dohrn and Brunner [10] covering
1988–1993, and Christov and Dohrn [13] covering 1994–1999. This
work gives an overview about systems for which high-pressure
phase-equilibrium data have been published from 2000 to 2004,
including vapor–liquid equilibria (VLE), liquid–liquid equilibria

0378-3812/$ – see front matter © 2009 Elsevier B.V. All rights reserved.
doi:10.1016/j.fluid.2009.08.008
2 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

(LLE), vapor–liquid–liquid equilibria (VLLE), the solubility of high-

boiling substances in supercritical fluids, and the solubility of gases
in liquids (GLE). Work on the continuation of the review series is
under way, covering the period between 2005 and 2008, and will
be published in 2010.

2. Literature search and evaluation

This survey covers the most important journals in the field of

high-pressure phase equilibria, as listed in Table 1; abbreviation
of journal titles were used according to ISO 4 [25]. To find can-
didates for articles that are of interest for this review we used a
three-stage search strategy. In Stage 1 we systematically searched
the table of contents of all volumes that appeared between 2000
and 2004 of the journals of Table 1, checked in cases of doubt the
abstracts and downloaded the article. Stage 1 yielded more than
95% of the articles of interest. In Stage 2 we used the online search
function of the journals to search for certain keywords, like “high-
pressure”, “phase equilibrium” or “gas solubility”. Stage 3 was only
started after the evaluation process of the articles of interest was
almost finished. We identified important authors in the field of
high-pressure phase-equilibrium measurements and searched for
other papers of these authors that might have been overlooked in
Stages 1 and 2. During the evaluation process of more than 700
articles of interest, about 10% of the papers were found to be irrel-
evant for this review, since they contain neither new experimental
data nor the description of a new experimental apparatus, or the
measured data were not “high pressure”. Of course, the expression
“high pressure” is relative; we chose 1 MPa as the lower limit: a
paper was considered to contain high-pressure data if at least one
data point was measured at a pressure of 1 MPa or higher.
The increase of interest in high-pressure phase equilibria con-
tinues. Fig. 1 shows an almost linear increase of articles published
per year during the last 25 years. While in the early 1980s about
20 articles on high-pressure phase equilibria were published each
year, this number increases by 6–7 each year, so that in 2004 more
than 7 times as many articles appeared as in 1982. In Table 1, the
Table 1
Bibliographic information.
Journal Number of articles
Fig. 1. Increase in the number of articles published per year during the last 25 years.
number of papers published in different journals from 1978 to 1987
[8] is compared with the number published from 1988 to 1993
[10], from 1994 to 1999 [13], and from 2000 to 2004 (this work).
Authors tend to submit their publications on high-pressure phase-
equilibrium data to a rather limited number of mostly specialized
journals. More than 80% of the information was published in the
three major journals of high-pressure phase equilibria: the Journal
of Chemical Engineering Data, Fluid-Phase Equilibria, and The Journal
of Supercritical Fluids. As compared to our previous reviews [10,13],
we no longer cover Zeitschrift für Physikalische Chemie since no rele-
vant articles were found in this journal for the period between 2000
and 2004, and ELDATA (International Electronic Journal of Physico-
Chemical Data), which had 13 relevant articles in the previous
period (1994–1999), but ceased to appear in 1999. We included
International Journal of Thermophysics as a new journal. And we also
included Green Chemistry, which first appeared in 1999 and shows
rising coverage of high-pressure phase equilibria due to increas-
ing interest in the solubility of volatile components in ionic liquids,
particularly in the period of the coming review that will cover 2005
and 2008.

1978–1987a 1988–1993b 1994–1999c 2000–2004d

3. Experimental methods
J. Chem. Eng. Data 92 115 214 231
Fluid Phase Equilibr. 69 158 182 206
J. Supercrit. Fluidse 0 43 73 115 Particularly at high pressures, the measurement of phase equi-
Ind. Eng. Chem. Res. 15 18 30 58 libria is the most suitable method to determine the phase behavior,
J. Chem. Thermodyn. – – 30 26 which often is far more complex than at ambient and moderate
Int. J. Thermophys. – – – 23
pressures. Due to large deviations from ideal behavior, the pre-
Phys. Chem. Chem. 10 8 6 13
Phys.f diction of high-pressure phase equilibria is less accurate than at
AIChE J. 5 5 1 10 lower pressures. Another difficulty of using predictive methods is
J. Phys. Chem. B 3 5 1 4 the fact that molecules of interest for high-pressure applications,
Chem. Eng. Sci. 2 1 4 4
particularly supercritical fluid extraction, can be large and contain
Can. J. Chem. Eng. 3 13 8 1
Green Chemistryg 0 0 0 1
several functional groups. Many different methods are used to mea-
J. Chem. Eng. Jpn. – 14 4 0 sure high-pressure phase equilibria. The reason is that not a single
Other journals – – 16 5 method is suitable to determine all different phenomena. To the
Total 199 380 569 697 reader the variety of experimental methods is even more confusing
since different authors use different names for the same experi-
Abbreviation of journal titles according to ISO 4 [25]. (–): not covered in the review
of the period.
mental method. Expressions like ‘static’ or ‘dynamic’ are used in
a
Fornari et al. [8]. connection with many different methods.
b
Dohrn and Brunner [10]. Therefore, an overview and a classification of experimental
c
Christov and Dohrn [13]. methods for the determination of high-pressure phase equilibria
d
This work.
e
are given in this chapter. The classification includes a unique name
The first issue of The Journal of Supercritical Fluids appeared in 1988.
f
Before 1999: Berichte der Bunsengesellschaft für Physikalische Chemie and J. and an abbreviation of the name for each method. In Tables 3–56,
Chem./Faraday Trans. listing the investigated systems, information on the experimental
g
The first issue of The Green Chemistry appeared in 1999. method used to determine the data is included.
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54
Fig. 2. Classification of experimental methods for high-pressure phase equilibria.
The classification of experimental methods for the investiga-
tion of high-pressure phase equilibria that has been used in the
previous reviews [10,13] has been further refined for this work
(Fig. 2). There are two main classes, depending on how the com-
positions of the equilibrium phases are determined (analytically or
not) and whether the mixture to be investigated has been prepared
(synthesized) with precisely known composition or not: analytical
methods and synthetic methods.
3.1. Analytical methods (An)
Analytical methods (designated with An) involve the analytical
determination of the compositions of the coexisting phases. When
the equilibrium cell is filled with the components at the beginning
of the experiment, the overall composition of the mixture is not
precisely known, only so far that the mixture under desired con-
ditions (P and T) separates into two or more phases that are to
be investigated, e.g., into a liquid and a vapor phase when VLE is
to be measured. The composition of the phases is analyzed either
with sampling and analysis under ambient pressure or without
sampling by using physicochemical methods of analysis inside the
equilibrium cell under pressure.
Analytical methods with sampling can be classified, depend-
ing on the attainment of equilibrium, into isothermal methods
(AnT), isobaric–isothermal methods (AnPT) and isobaric methods
(AnP). Withdrawing a large sample from an autoclave causes a
considerable pressure drop, which disturbs the phase equilibrium
significantly. This pressure drop can be avoided by a variable-
volume cell (Var) [26], by using a buffer autoclave in combination
with a syringe pump [27], or by blocking off (Blo) the sampling
volume from the remaining content of the equilibrium cell before
pressure reduction [28–30]. Sane et al. [31] use an electronic
syringe pump to keep the pressure in a variable-volume cell con-
stant during sampling. If only a small sample is withdrawn or if
a relatively large equilibrium cell is used, the slight pressure drop
does not affect the phase compositions significantly. The largest
equilibrium cell (volume of 9 dm3 ) used in the articles of this review
was used by the late Danesh and co-workers [32] to measure phase
equilibria in gas condensate systems.
3
Small samples can be withdrawn using capillaries (Cap) [33] or
special sampling valves (Val), e.g., using HPLC-valves [34] or fast-
acting pneumatic valves, like the rapid on-line sampler-injector of
Richon [35]. Often sampling valves are directly coupled to analytical
equipment, e.g., to a gas chromatograph [36], a high-performance
liquid chromatograph [37], or a supercritical fluid chromatograph
[34]. For sampling from multiphase systems (e.g., VLLE) a movable
sampling needle [38] can be used.
The smallest equilibrium cell of all articles from this review
using an analytical method with sampling was used by Bahramifar
et al. [39]: only 0.5 cm3 volume with a sampling loop of 23 mm3 .
The largest relative sample (14%) from a constant volume cell was
taken by Garmroodi et al. [40]: a 143 mm3 sample from a 1 cm3
equilibrium cell.
Sometimes, equilibrium cells used for analytical methods are
equipped with one or more windows for visual observation of the
cell content (Vis). Secuianu et al. [41] use a variable-volume cell
with two sapphire windows where one of the windows acts as a
piston.
Analytical methods without sampling use a physicochemical
method of analysis inside the equilibrium cell under pressure.
These are mainly spectroscopic methods (AnSpec), e.g., Andersen
et al. [42], gravimetric methods (AnGrav), e.g., Sato et al. [43], or
other methods (AnOth), e.g., Boudouris et al. [44]. These methods
avoid the problems related to sampling from a high-pressure cell.
The main advantage of analytical methods is that they can be
used for systems with more than 2 components without significant
complications. When the compositions of all phases are analyzed,
each experiment yields complete information on the tie-line(s).
3.1.1. Analytical isothermal methods (AnT)
Characteristic for isothermal methods is that the temperature
of the system stays constant during the equilibration process, e.g.,
when the system is in contact with a heat reservoir. The other equi-
librium properties, like the pressure and the composition of the
phases, reach equilibrium values, depending on other variables,
like mole numbers and volume. At the beginning of an experiment,
an equilibrium cell is charged with the substances of interest. The
pressure is adjusted above or below the desired equilibrium value,
depending on how equilibration will change the pressure. After
4 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54
the desired temperature has been reached, the mixture is kept at
a constant temperature. By stirring the mixture or by rocking the
autoclave or by recirculating one or more phases, time for equilibra-
tion of the phases is reduced. After some time, the pressure reaches
a plateau. The pressure can be readjusted, by adding or withdrawing
material or by changing the volume of the equilibrium cell. Usually,
the equilibration is continued for at least 30 min after the pressure
plateau is sufficiently close to the desired value. Before taking sam-
ples from the coexisting phases, the mixture is given sufficient time
without stirring, rocking or recirculation for the separation of the
phases [41]. Otherwise the sample might not be homogeneous but
contain material from another phase, e.g., droplets, bubbles or solid
particles.
For the measurement of solid–liquid equilibria in wax systems,
Pauly et al. [45] used an isobaric and isothermal filtration step
to ensure that the liquid phase to be sampled is free of solid
particles. This was performed in an equilibrium cell with two
variable-volume chambers connected via a filtration system (a disc
of sintered steel with 3 ␮m of porosity).
Isothermal methods that use stirring or rocking to ensure a rapid
approach to equilibrium are often called analytical-static methods.
As opposed to recirculating methods, the mixture does not leave the
equilibrium cell during the experiment. But, since the expressions
“static cell” and “static method” are used by some authors for other
experimental methods (e.g., for a synthetic method in a view cell
or for a synthetic method using the material balance to determine
solubilities of gases in liquids), we avoid the expression “static” in
our classification.
Sampling through capillaries can lead to differential vaporiza-
tion and scattering results, especially for mixtures containing light
and heavy components when no precautions have been taken to
prevent a pressure drop all along the capillary [46]. Differential
vaporization can be avoided with an experimental design that
ensures that most of the pressure drop occurs at the end of the
capillary close to the chromatographic circuit, e.g., Richon and co-
workers [47] used a micro-stem ending with a nose entering inside
the capillary to reduce the cross-sectional area at the end of the
capillary. Another possibility to reduce sampling problems is the
recirculation of one or more phases, having the advantage that
the sampling volume (e.g., the loop of a six-port valve) is filled
isobarically. Disadvantages of a recirculation are the need for a well-
working pump with only little pressure drop and the need for a
uniform temperature field to avoid partial condensation or vapor-
ization in the recirculation line. Therefore, recirculation methods
are not suitable in the region close to the critical point where small
changes in temperature and pressure have a strong influence on
the phase behavior [11].
When only the vapor phase is recirculated (Vcir), it is withdrawn
continually and passed back into the equilibrium cell through the
liquid phase by the action of a pump, e.g., Mather and co-worker
[48]. Samples can be withdrawn by placing a sampling valve in the
recirculation loop [37] or by blocking off a volume between two
valves in the recirculation loop [49]. The liquid phase is usually
analyzed by taking samples through capillaries. Laursen et al. [50]
proposed a simple VLE equipment with vapor-phase recirculation
that allows liquid phase sampling to measure the gas solubility in
substances with high stickiness and viscosity, like wood resins.
Recirculation of both the vapor and the liquid phase (VLcir) has
the advantage that sampling from both phases is possible without
using capillaries [51,52]. If a vibrating-tube densimeter is installed
in a recirculation loop, the density of the circulated phase can be
determined easily. The pump should be turned off during density
measurement to avoid errors due to pulsation [52]. Sometimes only
the liquid phase is circulated (Lcir), e.g., for mixing, for blocking
off a large liquid phase volume from the equilibrium cell before
pressure reduction [53], for the measurement of liquid–liquid equi-
libria or for the measurement of solubilities of gases in liquids
[54].
In a special kind of blocking off a part of the equilibrium cell
the sampling volume is within the equilibrium cell. We call this
method “in situ sampling” (AnTIns). It can be used for the mea-
surement of the solubility of solids in supercritical fluids. Sherman
et al. [55] put an excess amount of solute in a glass vial, capped
with coarse filter paper, in the equilibrium cell. After equilibration
and careful depressurization, the vial is removed and weighed. The
solubility can be calculated from the difference of the initial and
final mass of the solute in the vial and the difference of the volume
of the equilibrium cell and the vial. As modification, Galia et al.
[56] used three vials, of which only one was initially filled with the
solute.
Nikitin et al. [57,58] used an alternative technique which avoids
sampling from a high-pressure cell, for sorption measurements
of carbon dioxide in polystyrene. Equilibration, the absorption of
volatile component in the polymer, might take several hours. Then,
a fast depressurization procedure (<10 s) followed by a quick trans-
port of the sample to an analytical balance (<5 s) is performed. The
mass decrease of the polymer sample due to desorption of car-
bon dioxide is recorded and analyzed. The initial value of sorbate
mass can be determined by extrapolation of the desorption curve
to the beginning of depressurization. We designate this sampling
and analytical method with “material loss analysis” (AnTMla).
As compared to analytical isobaric–isothermal methods,
isothermal methods have the advantage that time for equilibration
can be easily extended. If carried out carefully they can produce
very reliable results.
27.6% of all systems investigated of this review have been mea-
sured with an analytical isothermal method.
3.1.2. Analytical isobaric–isothermal methods (AnPT)
In isobaric–isothermal methods, often called dynamic methods,
one or more fluid streams are pumped continuously into a ther-
mostated equilibrium cell. The pressure is kept constant during the
experiment by controlling an effluent stream, usually of the vapor
phase.
3.1.2.1. Continuous-flow methods (AnPTCon). In a typical design of a
continuous-flow method, high-pressure metering pumps feed the
preheated components into a mixer, where the desired temper-
ature and phase equilibrium is attained. Often, static mixers are
used [59,60]. The feed stream from the mixer is separated in an
equilibrium cell into a vapor and a liquid phase. To facilitate phase
separation, a cyclone separator was used by Fonseca et al. [59].
Effluents from both phases are withdrawn continually, depressur-
ized, accumulated and analyzed, usually after the experiment. The
pressure is adjusted by controlling the effluent stream of the top
phase. The interface level between the fluid phases in the equilib-
rium cell can be adjusted with the bottom-phase expansion valve,
whereby the interface level is usually determined visually [61].
Continuous-flow methods have the advantage that sampling
does not disturb the equilibrium. If larger samples are needed for
analyses, the run time of the experiment can be extended to accu-
mulate more material. Measurements at higher temperatures are
possible without thermal decomposition or polymerization reac-
tions due to the short residence time of the components in the
apparatus [62]. Using a continuous-flow method, Haruki et al. [63]
measured phase equilibria for water + hydrocarbon systems near
the critical point of water.
Hurst et al. [64] describe a continuous-flow cell with large
diameter optical ports suitable for visual observation and Raman
spectroscopic studies of aqueous solutions at temperatures up to
500 ◦ C. The cell was instrumented with a heated cylindrical insert
(‘hot finger’) that was employed for salt solubility, salt deposition
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54
and salt nucleation studies in near-critical aqueous solutions. The
crystalline phases were observed using Raman spectroscopy.
Continuous-flow methods can be used only for systems where
the time needed to attain phase equilibrium is sufficiently short.
3.1.2.2. Semi-flow methods (AnPTSem). In semi-flow methods, only
one phase is flowing while the other phase stays in an equilib-
rium cell. Semi-flow methods are sometimes called “single-pass
flow methods”, “gas-saturation methods” or “pure-gas circulation
methods”. A gas stream from a high-pressure cylinder is passed
through two cells in series containing the liquid. The first cell serves
as a presaturator and the second cell as equilibrium cell. Upon
equilibration, the effluent of the vapor phase is reduced in pres-
sure and directed to a trap where the condensed liquid is collected.
The quantity of the gas coming out of the trap can be determined
volumetrically, e.g., with a wet test meter.
Most often, only the composition of the vapor phase is ana-
lyzed (AnPTSemY), for example to determine the solubility of a
low-boiling (liquid or solid) substance in a supercritical gas [65].
The composition of the vapor-phase effluent can be determined in
many different ways, e.g., by using a spectroscopic method [66],
by using a multi-port sampling valve and subsequent HPLC anal-
ysis or after expansion to atmospheric pressure using cold traps,
an absorption bath, or a chromatography column filled with an
appropriate adsorbent for the solute studied [67]. For these kinds of
measurements (AnPTSemY), no samples from the condensed phase
are taken.
When a semi-flow method is used for the measurement of
vapor–liquid equilibria AnPTSemXY, the composition of the liquid
phase needs to be determined. Therefore, a sample from the liquid
phase is withdrawn through tubing, depressurized, and analyzed
[68]. Semi-flow methods can also be used to measure the solubility
of a gas in a liquid, e.g., Tan et al. [69]. The experimental proce-
dure (AnPTSemX) is similar to the one for measuring vapor–liquid
equilibria, but there is no need to determine the composition of the
effluent from the vapor phase.
Tuma et al. [70] used a modified supercritical fluid chromato-
graph (SFC) to measure the solubility of dyes in carbon dioxide. The
column was filled with finely pulverized dyestuff. Analysis of the
vapor-phase stream is done by VIS-spectroscopy (AnPTSemYSpec).
The major uncertainty of all flow methods is the possible lack of
attainment of equilibrium. Sauceau et al. [71] used an equilibrium
cell with three compartments, which is equivalent to three cells in
series. Another difficulty is the partial condensation of the solute
from the saturated vapor stream in the tubing, particularly in and
after the expansion valve. This undesired variable hold-up of the
solute can lead to scattering results in the order of 10% [72]. To
collect precipitated solute at the end of an experiment from the
tubing and from the expansion valve, Takeshita and Sato [73] use a
stream of carbon dioxide after having blocked off the equilibrium
cell.
Ferri et al. [74] describe an experimental technique that allows
to measure high concentrations of dyestuff in a supercritical fluid.
They use a second pump to stabilize the flow rate of the fluid in the
extractor, damping the pulses of the first pump. Glass wool before
and after the packed bed guarantees a uniform flow distribution
and prevents particle entrainment. A line by-passing the extractor
allows solubility measurements at high concentrations. It dilutes
the saturated fluid stream with clean carbon dioxide and reduces
the risk of valve clogging and flow rate instability.
To overcome the problems connected to depressurization,
Pauchon et al. [75] developed a semi-flow method that works
without pressure reduction. The effluent vapor-phase flows into
the top part of an autoclave which is filled with mercury. The
use of mercury, acting as a piston, allows obtaining a precise
adjustment of the vapor flow and avoids pressure changes that
5
produce solute precipitation. Sampling at isobaric conditions is per-
formed with a six-port valve. Special attention must be taken into
account during the regeneration of mercury and cleaning of the
apparatus.
3.1.2.3. Chromatographic methods (AnPTChro). Chromatographic
methods measure solute retention in a chromatographic column
and connect it with the Gibbs energy of solute transfer between
the stationary and the mobile phase. Roth [76] gives a review on
applications of SFC for the determination of the relative values of
solute solubilities in supercritical fluids, and on the determination
of solute partition coefficients between a supercritical fluid and
the stationary phase. In SFC, the thermodynamic analysis of solute
retention is more difficult than in GC because the uptake of the
mobile phase fluid by the stationary phase is no longer negligi-
ble. Chromatographic methods have as advantage the possibility
to determine equilibrium properties and diffusion coefficients in
one experiment [77].
Sato et al. [78] used a chromatographic method (AnPTChro) to
measure the vapor–liquid equilibrium ratio of n-hexane at infinite
dilution in propylene + impact polypropylene copolymer, while to
determine the solubility of propylene in the polymer they used the
synthetic isothermal method (SynT).
Chester [79] reviewed a chromatographic technique, which he
calls “flow injection peak-shape method” that allows to deter-
mine the pT coordinates of the vapor–liquid critical locus of binary
systems. It can be implemented using open-tubular SFC instru-
mentation by replacing the SFC column with several meters of
fused-silica tube. This tube may be deactivated but is not coated
with a stationary phase. The procedure to map a critical locus
involves selecting a temperature, then making injections at various
pressures while looking for the pressure where the peaks change
from their rectangular appearance ( = liquid + vapor phase in the
column) to distorted Gaussian (= homogeneous phase in the col-
umn). This transition pressure provides an estimate of the mixture
critical pressure corresponding to the oven temperature.
3.1.3. Analytical isobaric methods (AnP)
The boiling temperature of a mixture is measured at isobaric
conditions and phase compositions are determined after sampling
and analysis. Typically, isobaric experiments are performed in an
ebulliometer (from latin ebullio “to boil, to bubble up”), which is
a one-stage total-reflux boiler equipped with a vapor-lift pump to
spray slugs of equilibrated liquid and vapor onto a thermometer
well. As opposed to the more frequently used synthetic isobaric
method (SynP), vapor and liquid streams are separated, collected
and can be sampled and analyzed. The compositions of the liquid
and the vapor phase change with time and reach a steady state
which should differ insignificantly from the true equilibrium value.
Usually, the analytical isobaric method is used to measure low-
pressure data. Then, it is often called the “dynamic” VLE method.
3.1.4. Analytical spectroscopic methods (AnSpec)
Spectroscopic methods allow analyzing the composition
of the phases at high pressures without having to take sam-
ples, e.g., by using near infrared spectroscopy [42]. Cruz
Francisco et al. [80] investigated the phase behavior of
lecithin + water + hydrocarbon + carbon dioxide mixtures using
a 2 H NMR technique in combination with light microscopy.
Aizawa et al. [81] developed a high-pressure optical cell for the
investigation of absorption and fluorescence phenomena using a
“totsu” (denoting the shape) type window. The protruding part of
the window acts as a light-guide and enhances the laser power
imparted onto the sample in the monitoring light.
Shieh et al. [82] studied the effect of carbon dioxide on the mor-
phological structure of compatible crystalline/amorphous polymer
6 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54
blends by means of small angle X-ray scattering (SAXS) with the
measurement of absolute scattering intensity.
The advantage of avoiding the trouble with taking samples is
often overcompensated by the need of time consuming calibrations
at high pressures. Only 1.5% of all systems covered in this review
have been investigated with a spectroscopic method.
3.1.5. Analytical gravimetric methods (AnGrav)
With gravimetric methods the mass of a condensed phase (e.g.,
a polymer [43] or an ionic liquid [83]) in phase equilibrium with
a fluid phase is measured. Using additional information, like the
phase densities, the phase compositions can be determined. Pala-
mara et al. [84] placed the entire high-pressure cell on a balance
and performed the equilibration under isobaric conditions. The
weight of the cell and attached valve is critical because commer-
cially available analytical balances sensitive enough to perform
these measurements have low maximum load capacities. In the
study of Palamara et al. [84] the cell and attached valve weighed
approximately 190 g.
Cutugno et al. [85] placed a quartz spring balance and Moore
and Wanke [86] placed an electro microbalance within a high-
pressure cell to measure sorption of gases in polymers. Kleinrahm
and Wagner [87] developed a unique balance, so-called a magnetic
suspension balance, for accurate measurements of fluid densities.
It has the main advantage that the sample and the balance are iso-
lated. An electronically controlled magnetic suspension coupling is
used to transmit the measured force from the sample enclosed in a
pressure vessel to a microbalance. The suspension magnet, which
is used for transmitting the force, consists of a permanent mag-
net, a sensor core and a device for decoupling the measuring-load.
An electromagnet, which is attached at the underfloor weighing
hook of a balance, maintains the freely suspended state of the sus-
pension magnet via an electronic control unit. Using this magnetic
suspension coupling, the measuring force is transmitted contact-
lessly from the measuring chamber to the microbalance, which
is located outside the chamber under ambient atmospheric con-
ditions. Several investigators used a magnetic suspension balance
to measure the solubility and diffusivity of volatile components in
polymers, e.g., Sato et al. [88].
Gravimetric methods need corrections for buoyancy. Therefore,
particularly at high pressures, exact information on the density of
the fluid phase and on the density and volume of the condensed
phase is essential.
3.1.6. Other analytical methods (AnOth)
Like in gravimetric methods, quartz crystal microbalances can
be used to determine the solubility of a gas in a polymer by measur-
ing the mass of the polymer in equilibrium with the gas. From the
basic principle, it is not a gravimetric measurement, so that buoy-
ancy effects play a different role. Quartz crystal microbalances are
based on the piezoelectric effect observed in a AT-cut quartz crys-
tal. The crystal under the influence of an applied alternating electric
voltage undergoes a shear deformation which becomes maximum
at a certain frequency called the resonance frequency [44]. This res-
onance frequency depends on the mass, and thus any mass change
will result in a respective frequency shift. The sorption experi-
ment involves measurement of the resonance frequency of the bare
(clean) crystal, of the same crystal coated with polymer, and of the
coated crystal after the polymer reaches equilibrium with a gas, all
at the same controlled temperature. Concurrently, the resonance
frequency of a reference crystal is also measured under the same
conditions in order to compensate any temperature or pressure
effects. Park et al. [89] examined the effect of temperature deviation
and pressure change on the frequency shift by measuring the fre-
quency change of an uncoated crystal under high-pressure carbon
dioxide.
Guigard et al. [90] further developed the quartz crystal tech-
nique to measure low solubilities of metal chelates in supercritical
fluids. A small mass of solute was deposited on the crystal and sol-
ubility was measured by observing the crystal’s frequency change
as this solute dissolves in the supercritical fluid.
Mohammadi et al. [91] used a quartz crystal balance as an
extremely sensitive detector for the appearance of hydrates. 1 ng
mass change results in a 1 Hz frequency change. Concerning the
classification of methods this is not an analytical method (AnOth),
but a non-visual synthetic method (SynNon).
As compared to conventional methods, such as gravimetric
(AnGrav) or pressure decay (SynT), a much higher sensitivity for
the determination of mass changes can be achieved with a quartz
microbalance. Therefore, smaller samples are needed and phase
equilibrium is attained much faster [92], since equilibration time
is inversely proportional to the square of the film thickness. Errors
rise with temperature and pressure, due to dampening and viscous
dissipation [89].
Another analytical method was used by Morris et al. [93] to
measure low gas solubilities, e.g., of hydrogen in water. A palla-
dium/hydrogen electrical resistance sensor was used to determine
the hydrogen content in the liquid phase.
Abbott et al. [94] proposed a capacitative method (dielectric
constant method) to measure the solubility of low-volatile sub-
stances in supercritical gases. They used a 25 cm3 high-pressure
cell, lined with a layer of Teflon. A capacitor consisting of two par-
allel rectangular stainless steel plates (area of 6.6 cm2 , held 1 mm
apart by Teflon spacers) was placed in the vapor phase. The dielec-
tric constant of the saturated vapor phase was measured at different
pressures. To calculate the concentration of the solute in the vapor
phase from the dielectric constant, information on the permanent
dipole moments and the molecular polarizabilites of the compo-
nents of the mixture needs to be known.
3.2. Synthetic methods (Syn)
The idea of synthetic methods is to prepare a mixture of pre-
cisely known composition and then observe the phase behavior
in an equilibrium cell and measure properties in the equilibrium
state, like pressure and temperature. No sampling is necessary. The
problem of analyzing fluid mixtures is replaced by the problem of
“synthesizing” them [7]. Synthetic methods can be applied with or
without a phase transition. In both cases, first a mixture of precisely
known composition is prepared.
In synthetic methods with a phase transition values of tempera-
ture and pressure are adjusted so that the mixture is homogeneous,
a single phase exists. Then the temperature or pressure is varied
until the beginning of the formation of a new, a second phase is
observed. The composition of the first, large phase can be set to the
known overall composition. The composition of the second, small
phase is not known. Each experiment yields one point of the pTx
phase envelope.
Instead of a variation of temperature or pressure to cause a phase
transition the overall concentration can be changed. Wubbolts et al.
[95] use this approach, designated with “vanishing-point method”
or “clear-point method”, for SLE measurements. A clear solution of
a given solute concentration is added to a known amount of anti-
solvent until the last crystal disappears. The composition of the
mixture at this vanishing point equals the solubility of the mix-
ture. When the procedure is repeated with a solution of a different
concentration another point of the curve is found.
Depending on how the phase transition is detected, synthetic
methods with a phase transitions can be divided into visual (SynVis)
and non-visual synthetic methods (SynNon).
In synthetic methods without a phase transition, equilibrium
properties like pressure, temperature, phase volumes and densi-
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54
ties are measured and phase compositions are calculated using the
material balance. Synthetic methods without a phase transition can
be divided into isothermal (SynT), isobaric (SynP) and other (Syn-
Oth) synthetic methods. During the period covered in this review
(2000–2004) synthetic methods with a phase transition have been
used about 5 times more often than synthetic methods without a
phase transition.
Synthetic methods can be used where analytical methods fail,
i.e., when phase separation is difficult due to similar densities
of the coexisting phases, e.g., near or even at critical points and
in barotropic systems, where at certain conditions the coexisting
phases have the same density. Often, the experimental procedure
is easy and quick [5]. Because no sampling is necessary the experi-
mental equipment can concentrate on few components and the vol-
ume of the equilibrium cell can be small. Therefore, the apparatus
can be rather inexpensive. On the other hand, it can be designed for
extreme conditions concerning temperatures and pressures [96].
Cohen-Adad [97] describes a diamond anvil cell that can be used
for pressures up to 135 GPa. The experimental data at the highest
pressures of all articles covered in this review were taken by Fang
et al. [98], also with a diamond anvil cell, at pressures up to 2.6 GPa.
For multicomponent systems, experiments with synthetic
methods yield less information than with analytical methods,
because the tie-lines cannot be determined without additional
experiments. Therefore, synthetic methods are less often used for
systems containing more than 2 components.
3.2.1. Visual synthetic methods (SynVis)
The appearance of a new phase is usually detected by visual
observation of the resulting turbidity or meniscus in a view cell.
For isooptic systems where the coexisting phases have approxi-
mately the same refractive index, visual observation is impossible.
The visual synthetic method can be used not only for the determina-
tion of simple vapor–liquid equilibria, but also to study complicated
phase behavior, e.g., multiphase equilibria [99], solid–liquid equi-
libria [100], critical curves of mixtures [101], gas hydrate formation
[102], cloud-point determination [103] and phase equilibria in
polymer–solvent systems [104].
The Cailletet apparatus of TU Delft [105] is the most frequently
used type of apparatus according to the synthetic visual method. It
consists of a thick-walled Pyrex glass tube (50 cm long, 3 mm inner
diameter) with the open end placed in an autoclave and immersed
in mercury. The mercury confines the sample in the Cailletet tube. A
stainless steel ball driven by reciprocating magnets stirs the sample.
Daridon et al. [106] used a very small cell with a volume of
0.03 cm3 for the visual observation of synthetic waxes at high
pressures. The cell is placed within a polarizing microscope. The
apparatus allows the visual observation of crystals of 2 ␮m.
When only small quantities of a sample shall be used in the
experiment, e.g., to observe solid–liquid–gas equilibria, a glass cap-
illary can be placed inside the high-pressure view cell [107,108].
To improve the detection of phase transitions, some authors use
laser light scattering techniques [103,109]. Jager and Sloan [110]
use Raman spectroscopy to detect hydrates. Dong et al. [111] use
additional SAXS measurements to determine the median micelle
size of the water-in-carbon dioxide microemulsions.
Veiga et al. [112] used glass capillary helixes not only to inves-
tigate the high pressure behavior of pure compounds but also at
negative pressures as far down as −20.8 MPa.
With 36.4% of all systems investigated in this review, synthetic
visual methods were the most frequently used type of method.
3.2.2. Non-visual synthetic methods (SynNon)
As an alternative to visual observation, other physical proper-
ties can be monitored to detect phase transitions. Minicucci et al.
[113] made use of transmitted X-rays instead of visible light, as
7
the basis of phase detection, while Drozd-Rzoska et al. [114] used
measurements of the relative dielectric permittivity for LLE mea-
surements at high, low and negative pressures. If the total volume
of a variable-volume cell can be measured accurately, the appear-
ance of a new phase can be obtained from the abrupt change in
slope on the pressure–volume plot more accurately than by visual
observation [115,116]. As an alternative pVT measurements can be
performed and the intersection of isochors can be used to deter-
mine points on the coexistence curve. A sharp change in the slope
(dp/dT), occurs at the phase boundary.
May et al. [117] used a microwave re-entrant resonator to detect
the appearance of dew and bubble points in hydrocarbon sys-
tems. Takagi et al. [118] measured bubble point pressures using an
ultrasonic speed apparatus. Since the acoustic wave excited in the
sample for the speed of sound measurement was strongly absorbed
in the gas phase as compared to the absorption in the liquid phase,
the appearance of the gas phase was detected by the change of
the acoustic echo signal. For searching critical points of pure fluids,
acoustic methods have the advantage that even for temperatures
several degrees above the critical point, the sound velocity exhibits
a minimum when measured isothermally as a function of pressure
[119].
To measure the critical temperature of thermally unstable sub-
stance, the pulse-heating method, as described by Nikitin et al.
[120], can be used. It is based on measuring the pressure depen-
dence of the temperature of the attainable superheat (spontaneous
boiling-up) of a liquid with the help of a thin wire probe heated
by pulses of electric current. When the pressure in the liquid
approaches the critical pressure, the temperature of the attainable
superheat approaches the critical temperature.
A synthetic non-visual method that looks at first sight like
an analytical continuous-flow method (AnPTCon) was used by
VonNiederhausern et al. [121] to determine the critical points of
thermally unstable or reactive components. To achieve very short
residence times, a sample of precisely known composition is con-
tinuously displaced and heated in a capillary tube. No analysis of the
samples takes place. To determine the critical point, several tem-
perature scans must be made in the vicinity of the critical point.
Below the critical point, the temperature scan will show a flat, hor-
izontal region indicative of isothermal boiling. Above the critical
point, the transition region is no longer flat and horizontal. The
critical point is inferred by the temperature and pressure where
isothermal boiling is no longer observed.
Valyashko et al. [122] used jumps of the isochoric heat capacity
to detect the appearance of a vapor phase or a second liquid phase.
Wurflinger and Urban [123] studied the phase behavior of liquid
crystals with high-pressure differential thermal analysis (DTA).
The experiments at the highest temperatures of all articles cov-
ered in this review were performed by Manara et al. [96]. They
investigated the melting point of uranium dioxide at high pres-
sures. Temperatures of almost 3200 K were needed. Such high
temperatures can be measured optically by pyrometry. Two pulsed
Nd–YAG laser beams were mixed through a suitable optical sys-
tem in the same fiber and then focused onto the sample surface.
The pulse with the higher power peak was used to heat the sample
above the melting point; the other one, less powerful, but of longer
duration, was used to control the cooling rate on the sample sur-
face. This lead to a much better definition of the freezing plateau.
Pressure was applied by using helium.
Diamond anvil cells are particularly suitable for non-visual mea-
surements at very high pressures [97]. The selective transparency
of diamond for IR to X-ray and gamma-ray radiations permits in
situ measurements during experiments.
Ngo et al. [124] used the synthetic non-visual method to mea-
sure the solubility of solids in carbon dioxide. First the cell was
charged with the solid. Then it was pressurized with carbon diox-
8 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54
ide and stirred constantly. Equilibrium of the mixture was observed
in situ by periodically taking spectra (UV absorbance) of the solu-
tion. The pressure was raised stepwise until no further significant
increase in the peak absorbance was observed. This meant that all
solids had been dissolved in the fluid phase.
Randzio [125] used a new transitiometric method for investi-
gation of the solid phase behavior in asymmetric binary systems.
Transitiometry is based on a simultaneous recording of both
mechanical and thermal variables of a thermodynamic transition
induced by scanning one independent variable (p, T or V) while
the other independent variable is being kept constant. Taking
the (tetracosane + methane) binary system as a test example, the
three-phase curve (solid + liquid + vapor) has been determined. The
apparatus (“transitiometer”) consists of a calorimeter equipped
with high-pressure vessels, and a pVT system. During the isobaric
temperature scans both the heat flux and the volume variations
were recorded.
For measurements of solid–liquid equilibria at high pressures,
the dead-volume of the apparatus can have a very negative influ-
ence [97]. The volatility of constituents changes the nominal
composition of a sample and can induce an incorrect apparent
retrograde solubility curve.
To investigate the phase behavior in porous media, non-visual
methods are particularly advantageous. Zatsepina and Buffett [126]
used electrical resistance measurements to monitor the appear-
ance and growth of CO2 –hydrate crystals in the pore fluid. Omi et
al. [127] used a high-pressure NMR probe to investigate the pres-
sure and pore size dependence of the critical behavior of xenon in
mesopores.
Ivanic et al. [128] monitored the pressure and temperature in
a hydrate-bearing system and identified equilibrium at the condi-
tions where the last hydrate crystal in the system dissociates at the
cross-point of the pT curves from cooling and from heating.
Oag et al. [119] describe an apparatus where the determina-
tion of phase transitions and critical points can be carried out with
different methods: visually, by measuring the laser reflectance of
the fluid, which is at its maximum at the critical point, the sound
velocity and by using vibrating shear mode sensors.
3.2.3. Synthetic isothermal methods (SynT)
Synthetic isothermal methods are performed without a phase
transition, where the pressure of a synthesized multiphase mix-
ture is measured at isothermal conditions and phase compositions
are calculated using the material balance. At the beginning of an
experiment, an equilibrium cell is charged with a known amount
of the first component, evacuated and thermostated to a given
temperature. Then a known amount of the second component is
added whereby the pressure increases. The second component
dissolves into the liquid phase, which leads to a decay of the pres-
sure in the equilibrium cell. Therefore, this method is also called
pressure-decay method, especially when a polymer is used as the
first component. After equilibration pressure and temperature are
registered. No samples are taken. The composition of the vapor
phase is calculated using a phase equilibrium model or assumed
as just containing the pure gas, if we consider solubility in poly-
mers for example, or other compounds with negligible volatility.
The composition of the liquid phase is calculated using the mate-
rial balance from the known total composition, the composition
of the vapor phase and the phase densities and volumes [129].
By repeating the addition of the second component into the cell,
several points along the boiling point line can be measured.
At lower pressures, were they are often designated as “static
method” or “isothermal pTx method”, synthetic isothermal meth-
ods are very commonly used [130,131]. Examples for the use of
the synthetic isothermal methods at high pressures are the deter-
mination of the solubility of low-boiling substances in polymers
[132] or the solubility of gases in ionic liquids [133] or in electrolyte
solutions, e.g., by Gmehling and co-workers [134].
When used for a pure component, the synthetic isothermal
method delivers the vapor pressure, e.g., Funke et al. [135]. Then, it
is often called the “static” vapor-pressure method.
Often in synthetic isothermal methods, a view cell is used as
equilibrium cell. This has the advantages that unusual behavior,
like foaming, can be seen, that the volumes of the liquid and the
vapor phase can be determined visually and that the cell can be used
also according to the synthetic visual method. For example, Fukné-
Kokot et al. [107] measured solid–liquid–gas equilibria using the
synthetic isothermal method to determine the CO2 content in the
liquid phase and the synthetic visual method to detect solid forma-
tion.
Krüger et al. [136] compared results of the isothermal method
for VLE of the n-pentane + poly(dimethylsiloxane) system with
results of the gravimetric sorption method (AnGrav) and with
inverse gas chromatography. These methods differ in the under-
lying experimental principles as well as in the complexity of data
analysis. Despite of these differences, the agreement of the mea-
sured VLE data is excellent.
3.2.4. Synthetic isobaric methods (SynP)
The boiling temperature of a synthesized mixture is measured at
isobaric conditions and phase compositions are calculated using the
material balance. As opposed to analytical isobaric methods (AnP),
no sampling or analysis is performed. Just as synthetic isothermal
methods (SynT), synthetic isobaric methods (SynP) are performed
without a phase transition. When used for a pure component –
the composition is given anyway – the synthetic isobaric method
delivers the vapor pressure, e.g., Weber et al. [137]. Then, it is often
called the “dynamic” vapor-pressure method. Typically, isobaric
experiments are performed in an ebulliometer as described in Sec-
tion 3.1.3 (AnP). An ebulliometer was first used to determine the
molecular weights of substances, by measuring the changes of the
boiling point of water caused by the presence of the unknown sub-
stance. Twin ebulliometry can be used to determine the activity
coefficient at infinite dilution. The temperature difference between
an ebulliometer filled with the first (pure) component and a sec-
ond ebulliometer (under the same pressure) filled with the first
component and with a small amount of a second component
(diluted solution) is measured. From the difference of the boiling
temperatures, the activity coefficient at infinite dilution can be cal-
culated. Usually synthetic isobaric methods are used to measure
low-pressure data.
Ewing and Ochoa [138] used comparative ebulliometry to pre-
cisely determine the vapor pressure of pure components at high
pressures. The sample and a reference fluid are boiled in separate
ebulliometers under a common pressure of gas such as helium or
nitrogen, and the condensation temperatures of the sample and of
the reference fluid are measured. The common pressure is calcu-
lated from the known vapor pressure of the reference fluid. The
method has many advantages: direct measurement of pressure is
avoided, the fluids are degassed by boiling, and the ebulliome-
ters act as heat pipes to provide high-performance thermostats.
The corresponding disadvantages are the considerable demands on
thermometry, the solubility of the buffer gas at high pressures, and
thermal gradients due to pressure heads. But the greatest advan-
tage is speed of measurement; typically, a pressure–temperature
point can be obtained in an hour.
3.2.5. Other synthetic methods (SynOth)
Properties measured in the homogenous or heterogeneous
region are used to calculate the phase boundaries.
Abdulagatov et al. [139] used two-phase isochoric heat capacity
measurements to determine the values of the critical pressure and
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 9

slope of the vapor-pressure curve at the critical point of 18 pure
components.
For systems with two degrees of freedom (e.g., binary two-phase
equilibria or ternary three-phase equilibria), the compositions
are fixed when temperature and pressure are given. Luks and
co-worker [140] took phase volume and overall composition raw
data for a set of three experimental runs at the same temperature
and pressure; in each run a different phase is caused to be volu-
metrically dominant relative to the other two phases. With the use
of mass balance, the compositions and molar volumes of the three
phases were determined from the three conjugate measurements
[141].
Di Nicola et al. [142] used isochoric pvTx measurements in the
single phase region (remark: otherwise it would be SynT) to fit
the binary interaction parameters of an equation of state. Then,
the compositions of the coexisting phases are calculated using the
equation of state model.
4. Systems investigated
Almost 700 articles with experimental data on high-pressure
phase equilibria were found [143–745]. More than 2000 sys-
tems have been investigated, from pure components, binary
systems up to complex mixtures with many components. In
Tables 3–56, the following information about the systems inves-
tigated is given: the reference, the temperature and pressure
range of the data and the experimental method used for the mea-
surements. The abbreviations used to designate the experimental
method have been explained in the text above or are explained
in Table 2.
Because the size of the equilibrium cell can be of importance,
e.g., for the pressure drop during sampling or for the amount of
substances needed, the volume of the equilibrium cell is also given
in the tables.
Information on pure-component systems is given in Table 3.
Most of experimental phase equilibrium data were on binary sys-
tems: 1204 systems investigated have been divided into 28 tables
(Tables 4–31), with Table 4 (carbon dioxide + X) containing 681
binary system being by far the largest one. Many data have been
measured for binary systems containing water, propane, difluo-
romethane (HFC-32), and methane. Information on the tables and
their order can be found in the list of tables.
The additional components X are listed in alphabetic sequence.
The results of 434 ternary systems are given in 17 tables
(Tables 32–48), e.g., 76 ternary systems of the type CO2 + water + X.
The order of the tables is analog to the order of the binary systems.
Information on 134 multicomponent systems (4–10 components)
is listed in Tables 49–52. Results for complex systems with many
components, like gas condensate reservoirs, are listed in Table 53.
Special tables have been generated for systems containing
hydrates (Tables 54–56). Overall, 129 systems with hydrates were
found.
To provide the reader with information on articles with cor-
rections and discussions on published experimental high-pressure
data, we prepared a compilation (Table 57). We give the original
article and the articles with corrigenda, comments or rebuttals to
comments when at least one of them falls in the period of the
review.
Work on the continuation of the review series is under way,
covering the period between 2005 and 2008, and will be published
in 2010.

Table 2
Experimental methods: abbreviations and frequency of use in review period.

46.7% Analytical methods, total composition is not exactly known, analysis of phases in equilibrium
Analytical methods with sampling:
27.6% AnT Analytical method: isothermal method
Blo Blocking off a large sampling volume from the equilibrium cell
Cap Sampling through capillaries
Ins In situ sampling: a sampling vial is in the equilibrium cell, careful depressurization, removal of vial
Lcir Liquid-phase recirculation
Mla Material loss analysis: sampling after depressurization, weight loss of sample due to desorption is
investigated
Val Sampling using a special valve
Var Variable-volume cell
Vcir Vapor-phase recirculation
VLcir Recirculation of the vapor and the liquid phase
0.0% AnP Analytical isobaric method, ebulliometry with phase analysis
15.4% AnPT Analytical isobaric-isothermal method
Con Continuous-flow method
SemX Semi-flow method used to measure the solubility of a gas in a liquid
SemY Semi-flow method used to measure the solubility of substance in a gas (or supercritical fluid)
Chro Chromatographic method, e.g. inverse SFC, inverse HPLC
Analytical methods without sampling:
1.5% AnSpec Spectroscopic analysis
1.1% AnGrav Gravimetric determination of phase composition: suspension balance or microbalance or quartz
spring balance
1.1% AnOth Other determination of phase composition, e.g. by resonance in a Quartz Crystal Microbalance

53.3% Synthetic methods, total composition is exactly known, no analysis of phases in equilibrium
Synthetic methods with a phase transition:
36.4% SynVis Visual detection of phase transitions
8.4% SynNon Non-visual detection of phase transitions
Synthetic methods without a phase transition:
6.1% SynT Isothermal, at least 2 phases, total pressure measured, often for pure-component vapor pressures;
mixtures: y calculated
0.2% SynP Isobaric, at least two phases, ebulliometry, often for pure-component vapor pressures, mixtures:
differential ebulliometry
2.2% SynOth Measured properties in the homogenous or heterogenous region are used to calculate the phase
boundaries

Additional remarks for all methods: Var, variable-volume cell; Vis, view cell, visual observation; Spec, spectroscopic method to get information; Pc, the critical pressure has
been measured; Tc, the critical temperature has been measured; X, only the composition of the liquid phase is determined; Y, only the composition of the vapor phase is
determined.
10 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 3
Pure-component systems: X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,2,3,3,4,4-Nonafluorohexan-5-one Otake et al. [553] 332–498 0–2.2 16 SynVisVarPcTc

1,1,1,2,2,3,3-Heptafluoropentan-4-one Otake et al. [553] 302–476 0–2.5 16 SynVisVarPcTc
1,1,1,2,2-Pentafluoro-3-(1,1,2,2-tetrafluoroethoxy)-propane Yasumoto et al. [731] 299–473 0–2.2 16 SynVisVarPcTc
1,1,1,2,2-Pentafluoro-3-butanone Sako et al. [596] 453–453 2.9–2.9 5.3 SynVisPcTc
Sako et al. [597] 453–453 2.9–2.9 5.3 SynVisPcTc
1,1,1,2,2-Pentafluoroethane (HFC-125) Lee et al. [439] 293–313 1.2–2 80 SynT
Lim et al. [463] 283–293 0.9–1.2 85 SynVis
Pitschmann and Straub [564] 303–339 1.5–3.6 n.a. SynVisPcTc
1,1,1,2,2-Pentafluoropentan-3-one Otake et al. [553] 299–475 0–2.6 16 SynVisVarPcTc
1,1,1,2,3,3,3-Heptafluoropropane (HFC-227ea) Di Nicola [264] 235–365 0–2.4 254.8 SynT
Gruzdev et al. [342] 272–373 0.1–2.8 439 SynT
Hu et al. [363] 233–375 0–2.9 13 SynVis
Lee et al. [439] 303–323 0.5–0.9 80 SynT
Park et al. [555] 283–323 0.2–0.9 85 SynVis
Valtz et al. [685] 293–353 0.3–1.8 n.a. SynVis
Valtz et al. [689] 276–375 0.2–2.9 n.a. SynVis
Wang and Duan [701] 253–373 0–2.8 200 SynT
1,1,1,2,3,3-Hexafluoro-3-(2,2,2-trifluoroethoxy)propane Yasumoto et al. [731] 302–475 0–2.2 16 SynVisVarPcTc
1,1,1,2,3,3-Hexafluoro-3-(2,2,3,3,3-pentafluoropropoxy)-propane Yasumoto et al. [731] 312–486 0–1.9 16 SynVisVarPcTc
1,1,1,2,3,3-Hexafluoro-3-(2,2,3,3-tetrafluoropropoxy)-propane Yasumoto et al. [731] 285–516 0–2.1 16 SynVisVarPcTc
1,1,1,2,3,3-Hexafluoropropane (HFC-236ea) Di Nicola and Giuliani [260] 255–363 0–1.2 254.8 SynT
1,1,1,2,4,4,4-Heptafluoroisobutyl Sako et al. [596] 447–447 2.1–2.1 5.3 SynVisPcTc
trifluoromethyl ether Sako et al. [597] 447–447 2.1–2.1 5.3 SynVisPcTc
1,1,1,2-Tetrafluoro-2-difluoro-methoxyethyl Sako et al. [596] 449–449 2.4–2.4 5.3 SynVisPcTc
difluoromethyl ether Sako et al. [597] 449–449 2.4–2.4 5.3 SynVisPcTc
1,1,1,2-Tetrafluoro-2-trifluoromethyl-3- Sako et al. [596] 467–467 2.5–2.5 5.3 SynVisPcTc
butanone Sako et al. [597] 467–467 2.5–2.5 5.3 SynVisPcTc
1,1,1,2-Tetrafluoroethane (HFC-134a) Ho et al. [353] 273–313 0.2–1 85 SynVis
Lim et al. [466] 273–313 0.6–1.8 85 SynVis
Park et al. [555] 303–323 0.7–1.3 85 SynVis
Yasumoto et al. [731] 374–374 4–4 16 SynVisVarPcTc
1,1,1,3,3,3-Hexafluoropropane (HFC-236fa) Duan et al. [274] 253–396 0–3 200 SynT
1,1,1,3,3-Pentafluoropropane (HFC-245fa) Wang and Duan [701] 255–393 0–1.9 200 SynT
1,1,1-Trifluoro-2-(2,2,2-trifluoroethoxy)ethane Yasumoto et al. [731] 293–476 0–2.7 16 SynVisVarPcTc
1,1,1-Trifluoroethane (HFC-143a) Duan et al. [274] 251–343 0.2–3.5 200 SynT
Lim et al. [462] 323–333 2.3–2.8 85 SynT
Lim et al. [465] 283–293 0.8–1.1 85 SynT
Lim et al. [466] 273–313 0.2–1 85 SynVis
Pitschmann and Straub [564] 316–345 2–3.7 n.a. SynVisPcTc
Widiatmo et al. [705] 300–345 1.3–3.7 139 SynT
1,1,2,2-Tetrafluoro-1-(2,2,2-trifluoroethoxy)ethane Yasumoto et al. [731] 297–463 0–2.7 16 SynVisVarPcTc
1,1,2,2-Tetrafluoro-2-(2,2-difluoroethoxy)ethane Yasumoto et al. [731] 300–501 0–3.1 16 SynVisVarPcTc
1,1,2,2-Tetrafluoro-3-(1,1,2,2-tetrafluoroethoxy)propane Yasumoto et al. [731] 322–510 0–2.5 16 SynVisVarPcTc
1,1,2,2-Tetrafluorobutan-3-one Otake et al. [553] 297–500 0–3.6 16 SynVisVarPcTc
1,1-Difluoroethane (HFC-152a) Lim et al. [463] 293–293 0.5–0.5 85 SynVis
Lim et al. [465] 283–293 0.3–0.5 85 SynT
Lim et al. [466] 273–313 0.2–0.9 85 SynVis
Park et al. [555] 283–303 0.3–0.6 85 SynVis
Takagi et al. [661] 243–333 0–1.4 60 SynNon
1,2-Ethanediol VonNiederhausern et al. [693] 719–719 8.2–8.2 n.a. SynNonConPcTc
1,2-Propanediol VonNiederhausern et al. [693] 676–676 5.9–5.9 n.a. SynNonConPcTc
1,3-Propanediol VonNiederhausern et al. [693] 722–722 6.3–6.3 n.a. SynNonConPcTc
Wilson et al. [708] 718–718 6.5–6.5 n.a. SynNonConPcTc
1,4-Butanediol Wilson et al. [708] 723–723 5.5–5.5 n.a. SynNonConPcTc
1-Butanol Abdulagatov et al. [139] 530–563 4.8–4.8 n.a. SynOthPcTc
1-Chloro-1,1-difluoroethane Yasumoto et al. [731] 410–410 4–4 16 SynVisVarPcTc
1-Docosanol Nikitin et al. [537] 827–827 1–1 n.a. SynNonPcTc
Nikitin et al. [538] 827–827 1–1 n.a. SynNonPcTc
1-Eicosanol Nikitin et al. [537] 808–808 1.1–1.1 n.a. SynNonPcTc
Nikitin et al. [538] 808–808 1.1–1.1 n.a. SynNonPcTc
1-Heptadecanol Nikitin et al. [537] 780–780 1.3–1.3 n.a. SynNonPcTc
Nikitin et al. [538] 780–780 1.3–1.3 n.a. SynNonPcTc
1-Hexadecanol Nikitin et al. [537] 770–770 1.4–1.4 n.a. SynNonPcTc
Nikitin et al. [538] 770–770 1.4–1.4 n.a. SynNonPcTc
1-n-Butoxy-2-propanol VonNiederhausern et al. [693] 624–624 2.7–2.7 n.a. SynNonConPcTc
1-n-Propoxy-2-propanol VonNiederhausern et al. [693] 605–605 3–3 n.a. SynNonConPcTc
1-Octadecanol Nikitin et al. [537] 790–790 1.2–1.2 n.a. SynNonPcTc
Nikitin et al. [538] 790–790 1.2–1.2 n.a. SynNonPcTc
1-Octanol Yang et al. [100] 263–293 24.8–183.6 n.a. SynVis
Yang et al. [728] 263–293 24.8–183.6 n.a. SynVis
1-Pentadecanol Nikitin et al. [537] 757–757 1.6–1.6 n.a. SynNonPcTc
Nikitin et al. [538] 757–757 1.6–1.6 n.a. SynNonPcTc
1-Phenylethanol VonNiederhausern et al. [693] 699–699 3.7–3.7 n.a. SynNonConPcTc
1-Propanol Abdulagatov et al. [139] 403–536 10.1–10.1 n.a. SynOthPcTc
1-Tetradecanol Nikitin et al. [537] 743–743 1.6–1.6 n.a. SynNonPcTc
Nikitin et al. [538] 743–743 1.6–1.6 n.a. SynNonPcTc
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 11

Table 3 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

1-Tridecanol Nikitin et al. [537] 732–732 1.7–1.7 n.a. SynNonPcTc

Nikitin et al. [538] 732–732 1.7–1.7 n.a. SynNonPcTc
2-(2-Aminoethylamino)ethanol Wilson et al. [708] 739–739 4.6–4.6 n.a. SynNonConPcTc
2-(2-Butoxyethoxy)ethyl acetate Wilson et al. [708] 693–693 2.1–2.1 n.a. SynNonConPcTc
2-(2-Ethoxyethoxy)ethyl acetate Wilson et al. [708] 673–673 2.5–2.5 n.a. SynNonConPcTc
2,2-Difluoroethylbis(trifluoromethyl)amine Otake et al. [553] 293–460 0–2.6 16 SynVisVarPcTc
2,3,3,5,5,6,6-Heptafluoro-1,4-dioxane Sako et al. [596] 452–452 2.8–2.8 5.3 SynVisPcTc
Sako et al. [597] 452–452 2.8–2.8 5.3 SynVisPcTc
2-Butanol Abdulagatov et al. [139] 519–546 4.6–4.6 n.a. SynOthPcTc
2-Difluoromethoxy-1,1,1-trifluoroethane Yasumoto et al. [731] 294–444 0–3.4 16 SynVisVarPcTc
2-Methyl-1,3-propanediol Wilson et al. [708] 708–708 5.3–5.3 n.a. SynNonConPcTc
2-Methylpropane (isobutane) Galicia-Luna et al. [47] 317–406 0.5–3.5 40 SynT
Glos et al. [331] 115–340 0–1 n.a. SynT
Glos et al. [332] 115–340 0–1 n.a. SynT
Lee et al. [439] 293–323 0.3–0.6 80 SynT
Miyamoto et al. [517] 310–407 0.5–3.6 11–25 SynTVar
2-Propanol (isopropanol) Abdulagatov et al. [139] 473–508 5.1–5.1 n.a. SynOthPcTc
2-Trifluoromethyl-4,4,5,5-tetrafluoro-1,3- Sako et al. [596] 435–435 2.6–2.6 5.3 SynVisPcTc
dioxolane Sako et al. [597] 435–435 2.6–2.6 5.3 SynVisPcTc
3-Difluoromethoxy-1,1,1,2,2-pentafluoropropane Yasumoto et al. [731] 298–455 0–2.7 16 SynVisVarPcTc
3-Methoxy-1,1,2,2,3,3-hexafluoropropane Yasumoto et al. [731] 301–487 0–3.1 16 SynVisVarPcTc
3-Methoxy-1,1,2,2-tetrafluoropropane Yasumoto et al. [731] 342–505 0–3.2 16 SynVisVarPcTc
4-Ethoxy-1,1,1,2,2,3,3,4,4-nonafluorobutane Yasumoto et al. [731] 309–482 0–1.9 16 SynVisVarPcTc
Yasumoto et al. [731] 473–482 1.7–1.9 16 SynVisVarPcTc
4-Methoxy-1,1,1,2,2,3,3-heptafluorobutane Yasumoto et al. [731] 291–481 0–2.3 16 SynVisVarPcTc
5-Methoxy-1,1,2,2,3,3,4,4-octafluoropentane Yasumoto et al. [731] 301–546 0–2.5 16 SynVisVarPcTc
5-n-Decyl-2-(4 -isothiocyanato-phenyl)-1,3-dioxane Wuerflinger and Urban [123] 317–395 0.1–200 n.a. SynNon
5-n-Hexyl-2-(4 -isothiocyanato-phenyl)-1,3-dioxane Wuerflinger and Urban [123] 308–395 0.1–200 n.a. SynNon
5-n-Octyl-2-(4 -isothiocyanato-phenyl)-1,3-dioxane Wuerflinger and Urban [123] 319–395 0.1–200 n.a. SynNon
Acetonitrile (ethanenitrile) Ewing and Ochoa [138] 277–535 0–4.1 605 SynPVcir
VonNiederhausern et al. [693] 545–545 4.8–4.8 n.a. SynNonConPcTc
Adamantane Poot et al. [565] 546–639 3.4–67.2 n.a. SynVis
Ammonia Brandt et al. [187] 342–405 3.2–11.3 n.a. SynVisVar
Argon Abdulagatov et al. [139] 83–149 4.8–4.8 n.a. SynOthPcTc
Benzene Wang et al. [698] 562–562 4.8–4.8 18 SynVisPcTc
Bis(2-aminoethyl)amine VonNiederhausern et al. [693] 709–709 4.3–4.3 n.a. SynNonConPcTc
Wilson et al. [708] 709–709 4.3–4.3 n.a. SynNonConPcTc
Butanedioic acid Nikitin et al. [541] 851–851 6.4–6.4 n.a. SynNonPcTc
Butylbenzene Nikitin et al. [120] 660–660 2.9–2.9 n.a. SynNonPcTc
Butylcyclohexane Nikitin et al. [540] 650–650 2.5–2.5 n.a. SynNonPcTc
Carbon dioxide Abdulagatov et al. [139] 278–304 7.3–7.3 n.a. SynOthPcTc
Horstmann et al. [358] 304–304 7.3–7.3 10 SynVisTc
May et al. [117] 295–295 6–6 185 SynNonVcirVar
Stuart et al. [654] 299–300 6.6–7 28 SynVisVar
Chlorodifluoromethane (HCFC-22) He et al. [351] 310–345 1.4–3.1 25 SynT
Chlorotrifluoromethane (CFC-13) Magee et al. [491] 250–301 1–3.8 28.8 SynT
Cumene Wang et al. [698] 631–631 3.3–3.3 18 SynVisPcTc
Cyclohexane Domanska and Morawski [269] 293–353 23.3–153.1 n.a. SynNonVar
Ewing and Ochoa [287] 281–552 0–4 605 SynPVcir
Nikitin et al. [540] 551–551 4–4 n.a. SynNonPcTc
Decanedioic acid Nikitin et al. [541] 845–845 2.5–2.5 n.a. SynNonPcTc
Deuterium oxide Abdulagatov et al. [139] 605–643 21.6–21.6 n.a. SynOthPcTc
Veiga et al. [112] 258–333 -20.8–8.2 0.004 SynVis
Diamantane Poot et al. [565] 523–655 4.1–115.2 n.a. SynVis
Diethyl sulfide VonNiederhausern et al. [693] 557–557 3.8–3.8 n.a. SynNonConPcTc
Difluoromethane (HFC-32) Coquelet et al. [26] 283–343 1.1–4.8 n.a. SynVis
Lee et al. [440] 268–318 0.6–2.7 85 SynVis
Lim et al. [463] 283–293 1.1–1.4 85 SynVis
Park et al. [555] 283–303 1.1–1.9 85 SynVis
Pitschmann and Straub [564] 318–351 2.8–5.7 n.a. SynVisPcTc
Dimethyl ether Wu et al. [710] 233–400 0–5.3 11.3 SynTVis
Docosanoic acid Nikitin et al. [539] 837–837 1.1–1.1 n.a. SynNonPcTc
Dodecanedioic acid Nikitin et al. [541] 859–859 2.1–2.1 n.a. SynNonPcTc
Dodecanoic acid Nikitin et al. [539] 743–743 1.9–1.9 n.a. SynNonPcTc
Eicosane Domanska and Morawski [269] 313–353 16.2–225 n.a. SynNonVar
Eicosanoic acid Nikitin et al. [539] 820–820 1.2–1.2 n.a. SynNonPcTc
Ethane Funke et al. [311] 91–305 0–4.8 n.a. SynTPcTc
Horstmann et al. [358] 305–305 4.8–4.8 10 SynVisTc
Ethanoic acid Nikitin et al. [539] 590–590 5.8–5.8 n.a. SynNonPcTc
Ethylbenzene Nikitin et al. [120] 614–614 3.6–3.6 n.a. SynNonPcTc
VonNiederhausern et al. [121] 492–618 0.6–3.6 0.1 SynNonConPcTc
Ethylcyclohexane Nikitin et al. [540] 604–604 3.2–3.2 n.a. SynNonPcTc
Gallium Veiga et al. [112] 302–303 -8–18 0.004 SynVis
Heptadecanoic acid Nikitin et al. [539] 792–792 1.3–1.3 n.a. SynNonPcTc
Heptanedioic acid Nikitin et al. [541] 842–842 3.2–3.2 n.a. SynNonPcTc
Hexadecanoic acid Nikitin et al. [539] 785–785 1.4–1.4 n.a. SynNonPcTc
Hexafluoroethane (pfc-116) Kao and Miller [405] 177–291 0–2.9 30 SynT
Hexanedioic acid Nikitin et al. [541] 841–841 3.8–3.8 n.a. SynNonPcTc
12 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 3 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Hexanoic acid Nikitin et al. [539] 652–652 3.3–3.3 n.a. SynNonPcTc

Hexylbenzene Nikitin et al. [120] 695–695 2.3–2.3 n.a. SynNonPcTc
Methane Abdulagatov et al. [139] 105–190 4.6–4.6 n.a. SynOthPcTc
Methanol Veiga et al. [112] 298–329 −3.8–23.8 0.004 SynVis
Methylbenzene Nikitin et al. [120] 588–588 4–4 n.a. SynNonPcTc
Methylcyclohexane Nikitin et al. [540] 569–569 3.4–3.4 n.a. SynNonPcTc
Mobil eal arctic 22 oil Skripov et al. [645] 825–825 0.6–0.6 n.a. SynNonPcTc
n-Butane Glos et al. [331] 135–340 0–0.7 n.a. SynT
Glos et al. [332] 135–340 0–0.7 n.a. SynT
n-Decane Abdulagatov et al. [139] 453–617 2.1–2.1 n.a. SynOthPcTc
n-Dodecane Yang et al. [728] 268–293 27.4–160.3 n.a. SynVis
n-Heptane Abdulagatov et al. [139] 373–540 2.7–2.7 n.a. SynOthPcTc
Weber [137] 335–479 0–1 n.a. SynPVcir
n-Hexadecane Domanska and Morawski [269] 293–353 9.2–309.7 n.a. SynNonVar
Skripov et al. [645] 720–720 1.4–1.4 n.a. SynNonPcTc
Yang et al. [100] 293–323 8.1–144.6 n.a. SynVis
n-Hexane Abdulagatov et al. [139] 343–507 3–3 n.a. SynOthPcTc
Nitrogen tetraoxide Abdulagatov et al. [139] 313–431 4.4–4.4 n.a. SynOthPcTc
Nitrous oxide Di Nicola et al. [265] 219–273 0.5–3.1 273.5 SynOth
n-Nonane Abdulagatov et al. [139] 383–594 2.2–2.2 n.a. SynOthPcTc
n-Octadecane Domanska and Morawski [269] 303–353 11.2–259.9 n.a. SynNonVar
n-Octane Abdulagatov et al. [139] 373–569 2.4–2.4 n.a. SynOthPcTc
Ewing and Ochoa [288] 323–563 0–2.3 605 SynPVcir
Nonanedioic acid Nikitin et al. [541] 844–844 2.7–2.7 n.a. SynNonPcTc
n-Pentane Abdulagatov et al. [139] 313–470 3.4–3.4 n.a. SynOthPcTc
Pfohl et al. [132] 308–423 0–1.5 345 SynTVis
n-Tetradecane Yang et al. [100] 283–318 16–183.1 n.a. SynVis
n-Tridecane Daridon et al. [106] 267–287 0.1–98.3 0.03 SynVis
Domanska and Morawski [269] 293–353 134.3–582 n.a. SynNonVar
Octadecanoic acid Nikitin et al. [539] 803–803 1.3–1.3 n.a. SynNonPcTc
Octafluorocyclobutane Kao and Miller [405] 234–387 0–2.6 85 SynT
Octanedioic acid Nikitin et al. [541] 843–843 2.9–2.9 n.a. SynNonPcTc
Octanoic acid Nikitin et al. [539] 690–690 2.8–2.8 n.a. SynNonPcTc
Pentadecanoic acid Nikitin et al. [539] 777–777 1.5–1.5 n.a. SynNonPcTc
Pentafluoroethyl methyl ether (HFC245mc) Kayukawa et al. [409] 240–380 0–1.7 n.a. SynT
Widiatmo et al. [705] 310–406 0.3–2.8 139 SynT
Pentanedioic acid Nikitin et al. [541] 840–840 4.2–4.2 n.a. SynNonPcTc
Pentylbenzene Nikitin et al. [120] 675–675 2.5–2.5 n.a. SynNonPcTc
Phenyl acetate Wilson et al. [708] 685–685 3.5–3.5 n.a. SynNonConPcTc
Phenyldecane Nikitin et al. [120] 752–752 1.7–1.7 n.a. SynNonPcTc
Phenylheptane Nikitin et al. [120] 708–708 2.1–2.1 n.a. SynNonPcTc
Phenyloctane Nikitin et al. [120] 725–725 1.9–1.9 n.a. SynNonPcTc
Phenyltridecane Nikitin et al. [120] 790–790 1.5–1.5 n.a. SynNonPcTc
Phenylundecane Nikitin et al. [120] 763–763 1.6–1.6 n.a. SynNonPcTc
Poly(ethylene) (MDPE) Grolier et al. [341] 380–460 50–200 36.3 SynNon
Propane Abdulagatov et al. [139] 292–369 4.2–4.2 n.a. SynOthPcTc
Coquelet et al. [26] 277–353 0.5–3.1 n.a. SynVis
Glos et al. [331] 90–340 0–2.4 n.a. SynT
Glos et al. [332] 90–340 0–2.4 n.a. SynT
Horstmann et al. [358] 369–369 4.2–4.2 10 SynVisTc
Lee et al. [440] 268–318 0.4–1.5 85 SynVis
Propene Glos et al. [331] 95–340 0–2.9 n.a. SynT
Glos et al. [332] 95–340 0–2.9 n.a. SynT
Ho et al. [353] 273–313 0.5–1.6 85 SynVis
Wang et al. [698] 364–364 4.6–4.6 18 SynVisPcTc
Propylcyclohexane Nikitin et al. [540] 624–624 2.8–2.8 n.a. SynNonPcTc
Propylene carbonate Wilson et al. [708] 762–762 4.1–4.1 n.a. SynNonConPcTc
Styrene VonNiederhausern et al. [121] 473–635 0.3–3.8 0.1 SynNonConPcTc
Sulfur dioxide Valtz et al. [35] 288–403 0.2–4.9 n.a. SynVis
Valtz et al. [689] 288–403 0.2–3.3 n.a. SynVis
Sulfur hexafluoride Horstmann et al. [358] 318–318 3.7–3.7 10 SynVisTc
Hurly et al. [368] 278–313 1.4–3.3 27 SynT
Sulphur hexafluoride Funke et al. [135] 224–318 0.2–3.7 n.a. SynTPcTc
Synthethic natural gas Jarne et al. [380] 213–261 0.1–8.1 n.a. SynVis
Tert-perfluorobutyl methyl ether Sako et al. [596] 462–462 2.3–2.3 5.3 SynVisPcTc
Sako et al. [597] 462–462 2.3–2.3 5.3 SynVisPcTc
Tetradecanedioic acid Nikitin et al. [541] 862–862 1.9–1.9 n.a. SynNonPcTc
Tetradecanoic acid Nikitin et al. [539] 763–763 1.6–1.6 n.a. SynNonPcTc
Toluene Abdulagatov et al. [139] 562–593 4.2–4.2 n.a. SynOthPcTc
Bazaev et al. [164] 591–673 4–35.5 n.a. SynOthPcTc
VonNiederhausern et al. [121] 586–591 3.9–4.1 0.1 SynNonConPcTc
Trifluoromethane (HFC-23) Lim et al. [462] 283–293 3.2–4.2 85 SynT
Lim et al. [463] 283–293 3.2–4.1 85 SynVis
Lim et al. [465] 283–293 3.2–4.2 85 SynT
Trifluoromethyl methyl ether Kayukawa et al. [409] 300–375 0.6–3.4 n.a. SynNon
Undecanoic acid Nikitin et al. [539] 728–728 2.1–2.1 n.a. SynNonPcTc
Uranium dioxide Manara et al. [96] 3135–3180 10–250 n.a. SynNonVis
Uranium dioxide (non-stoichiometric) Manara et al. [496] 2400–3150 100–100 n.a. SynNonVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 13

Table 3 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Water Abdulagatov et al. [139] 573–646 22–22 n.a. SynOthPcTc

Veiga et al. [112] 253–333 −15.5–19.5 0.004 SynVis
Xenon Omi et al. [127] 291–323 0–10 n.a. SynNonTc
XMPA refrigeration oil Skripov et al. [645] 890–890 2.5–2.5 n.a. SynNonPcTc

Table 4
Binary systems: carbon dioxide + X.

X Reference T (K) P (MPa) V (cm3 ) Method

(S)-Boc-piperazine Uchida et al. [679] 308–328 9–20.5 240 AnPTSemY

1-((4-Nitrophenyl)azo)-2-naphthalenol (Para Red) Fasihi et al. [290] 308–348 12.2–35.5 1 AnTValY
1,1,1,2,2-Pentafluoroethane (HFC-125) Di Nicola et al. [263] 284–304 1.6–3.3 254.8 SynT
1,1,1,2,3,3,3-heptafluoropropane (HFC-227ea) Valtz et al. [687] 276–367 0.2–7.1 n.a. AnTValVis
1,1,1,2,3,4,4,5,5,5-Decafluoropentane Kho et al. [413] 298–298 0.7–6.3 130 AnTVisVar
1,1,1,2-Tetrafluoroethane (HFC-134a) Duran-Valencia et al. [276] 252–292 0.1–2 50 AnTVal
Silva-Oliver et al. [641] 329–354 1.9–7.3 40 AnTValVis
1,10-Phenanthroline Shamsipur et al. [621] 308–348 10.1–35.5 1 AnTValY
1,2-Limoneneoxide Corazza et al. [236] 313–343 8.2–13.8 25 SynVisVar
1,4-Bis-(1-methylethylamino)-9,10-anthraquinone (AQiso03) Tuma et al. [70] 299–346 7–20 n.a. AnPTSemYSpec
1,4-Bis-(butylamino)-9,10-anthraquinone (AQ04) Tuma et al. [70] 299–346 7–20 n.a. AnPTSemYSpec
1,4-Bis-(ethylamino)-9,10-anthraquinone (AQ02) Tuma et al. [70] 299–346 7–20 n.a. AnPTSemYSpec
1,4-Bis-(methylamino)-9,10-anthraquinone (AQ01) Tuma et al. [70] 299–346 7–20 n.a. AnPTSemYSpec
1,4-Bis-(octadecylamino)-9,10-anthraquinone (AQ18) Tuma et al. [678] 330–400 17–180 n.a. SynVisSpec
1,4-Bis-(octylamino)-9,10-anthraquinone (AQ08) Kraska et al. [430] 310–340 9–19.9 n.a. AnPTSemYSpec
Tuma et al. [70] 299–346 7–20 n.a. AnPTSemYSpec
1,4-Bis-(pentylamino)-9,10-anthraquinone (AQ05) Tuma et al. [70] 299–346 7–20 n.a. AnPTSemYSpec
1,4-Bis-(propylamino)-9,10-anthraquinone (AQ03) Kraska et al. [430] 305–340 7.8–18.9 n.a. AnPTSemYSpec
Tuma et al. [70] 299–346 7–20 n.a. AnPTSemYSpec
1,4-Diamino-2-methoxy-9,10-anthraquinone (C.I. Disperse Red 11) Tuma et al. [678] 300–340 10–140 n.a. SynVisSpec
1,4-Dihydroxy-3-methylthioxanthone Shamsipur et al. [619] 308–348 12.1–35.4 1 AnTValY
1,4-Dimethoxybenzene Lee et al. [447] 313–328 20–28 50 AnPTSemY
1,4-Naphthoquinone Ngo et al. [124] 313–313 8.4–12.3 n.a. SynNonSpec
1,8-Cineole Cruz Francisco and Sivik [239] 313–333 8–25 30 AnPTSemY
1,8-Dihydroxy-2-(prop-2-enyl)-9-anthrone Karami et al. [406] 308–348 10.1–32.9 1 AnTValY
1,8-Dihydroxy-9-anthrone Karami et al. [406] 308–348 10.1–35.5 1 AnTValY
1,8-Dihydroxyanthraquinone Galia et al. [56] 327–357 6.9–20.1 85.3 AnTIns
1-Amino-2,3-dimethyl-9,10-anthraquinone Shamsipur et al. [618] 308–358 12.2–35.5 1 AnTValY
1-Amino-2,4-dimethyl-9,10-anthraquinone Shamsipur et al. [618] 308–358 12.2–35.5 1 AnTValY
1-Amino-2-ethyl-9,10-nthraquinone Shamsipur et al. [618] 308–358 12.2–35.5 1 AnTValY
1-Amino-2-methyl-9,10-anthraquinone Shamsipur et al. [618] 308–358 12.2–35.5 1 AnTValY
1-Amino-4-hydroxy-2-phenoxy-9,10-anthraquinone (C.I. Disperse Red 60) Kraska et al. [430] 303–322 7.2–97.6 n.a. AnSpecVis
Tuma et al. [678] 310–310 7–130 n.a. SynVisSpec
1-Butanol Chen et al. [224] 333–353 5–12 100 AnTVcirVis
Secuianu et al. [607] 293–324 0.5–10 25–60 AnTVisVar
Silva-Oliver and Galicia-Luna [640] 324–426 9.6–17 40 AnTValVisPc
Yeo et al. [732] 303–428 7–17.4 26.71 SynVisVar
1-Butyl-3-methylimidazolium hexafluorophosphate ([bmim][PF6]) Wu et al. [711] 313–313 15–15 55 AnPTSemYVis
1-Butyl-3-methylimidazolium tetrafluoroborate ([bmim][BF4]) Wu et al. [711] 313–313 15–15 55 AnPTSemYVis
1-Butyne Bardas et al. [163] 303–333 0.2–8.4 200 AnTVLcirVis
1-Decanol Scheidgen and Schneider [601] 393–393 0–1000 80 AnT
1-Ethyl-2-pyrrolidinone Lee et al. [441] 313–393 1.7–23.1 28 SynVisVarPc
1-Ethyl-3-methylimidazolium ethyl sulfate [emim][EtSO4] Blanchard et al. [133] 313–333 0–9.4 10 SynT
1-Ethyl-3-methylimidazolium hexafluorophosphate Shariati and Peters [624] 308–366 1.4–97.1 3.5 SynVisVar
1H,1H,9H,9H-perfluoro-1,9-nonanediol Mesiano et al. [512] 323–323 30–35 n.a. SynVisVar
1-Heptanol Elizalde-Solis et al. [283] 293–431 4–21.5 100 AnTValVisPc
Scheidgen and Schneider [601] 393–393 0–1000 80 AnT
Scheidgen and Schneider [601] 393–393 0–1000 80 AnT
1-Hexanol Beier et al. [168] 303–313 0.5–9.8 50 AnTVLcirVis
Elizalde-Solis et al. [283] 324–432 2.2–20.1 100 AnTValVisPc
1-Hexyl-3-methylimidazolium hexafluorophosphate Shariati and Peters [623] 298–363 0.6–94.6 3.5 SynVisVar
1-Hydroxy-2-(1-propoxymethyl)-9,10-anthraquinone Shamsipur et al. [620] 308–348 12.2–35.5 1 AnTValY
1-Hydroxy-2-(butoxymethyl)-9,10-anthraquinone Shamsipur et al. [620] 308–348 12.2–35.5 1 AnTValY
1-Hydroxy-2-(ethoxymethyl)-9,10-anthraquinone Shamsipur et al. [620] 308–348 12.2–35.5 1 AnTValY
1-Hydroxy-2-(methoxymethyl)-9,10-anthraquinone Shamsipur et al. [620] 308–348 12.2–35.5 1 AnTValY
1-Hydroxy-2-(n-amyloxymethyl)-9,10-anthraquinone Shamsipur et al. [620] 308–348 12.2–35.5 1 AnTValY
1-Hydroxy-2,4-dimethyl-9-anthrone Karami et al. [406] 308–348 10.1–35.5 1 AnTValY
1-Hydroxy-2-ethyl-9-anthrone Karami et al. [406] 308–348 10.1–35.5 1 AnTValY
1-Hydroxy-2-methyl-9,10-anthraquinone Shamsipur et al. [620] 308–348 12.2–35.5 1 AnTValY
1-Hydroxy-2-methyl-9-anthrone Karami et al. [406] 308–348 10.1–35.5 1 AnTValY
1-Hydroxy-3-methylthioxanthone Shamsipur et al. [619] 308–348 12.1–35.4 1 AnTValY
1-Hydroxy-9,10-anthraquinone Shamsipur et al. [620] 308–348 12.2–35.5 1 AnTValY
1-Hydroxythioxanthane Shamsipur et al. [619] 308–348 12.1–35.4 1 AnTValY
1-Methyl-2-pyrrolidinone Lee et al. [441] 318–398 4.8–24.9 28 SynVisVarPc
1-Methylnaphthalene Gutiérrez and Luks [346] 219–308 0.5–7.9 7–9 SynOthVis
1-N-Butyl-3-methylimidazolium hexafluorophosphate ([bmim][PF6]) Kamps et al. [403] 293–393 0.1–9.6 30 SynVis
Kumelan et al. [433] 293–395 0.1–9.6 29.2 SynVis
1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 283–323 0–1.3 n.a. AnGrav
14 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Blanchard et al. [133] 313–313 13.7–13.7 n.a. AnPTSemY

Blanchard et al. [133] 313–333 0–9.5 10 SynT
1-n-Butyl-3-methylimidazolium methyl sulfate Kumełan et al. [433] 293–413 0.9–9.8 29.2 SynVis
([bmim][CH3SO4])
1-n-Butyl-3-methylimidazolium nitrate [bmim][NO3] Blanchard et al. [133] 313–333 0–9.3 10 SynT
1-n-Octyl-3-methylimidazolium hexafluorophosphate Blanchard et al. [133] 313–333 0–9.2 10 SynT
[C8mim][PF6]
1-n-Octyl-3-methylimidazolium tetrafluoroborate Blanchard et al. [133] 313–333 0–9.3 10 SynT
[C8mim][BF4]
1-Octanol Feng et al. [291] 328–328 3–13.3 300 AnPTSemXY
Hwu et al. [369] 328–328 3–13.3 300 AnPTSemXY
Scheidgen and Schneider [601] 393–393 0–1000 80 AnT
1-Pentanol Laursen et al. [50] 313–343 1.9–10.3 90 AnTVcirX
Silva-Oliver and Galicia-Luna [642] 333–426 3.5–18.6 40 AnTValVisPc
1-Phenylethanol Gamse and Marr [317] 303–323 3.5–9 140 AnTVcirVal
1-Propanol Laursen and Andersen [435] 308–318 0.4–8.3 570 AnTVis
Yeo et al. [732] 298–425 6.2–16 26.71 SynVisVar
2,2,3,3,4,4-Hexafluoro-1,5-pentanediol Mesiano et al. [512] 323–323 23–35 n.a. SynVisVar
2,2,3,3-Tetrafluoro-1,4-butanediol Mesiano et al. [512] 323–323 30–35 n.a. SynVisVar
2,3-Dimethylanilin Medina and Bueno [511] 313–333 8–20 15.7 AnPTSemY
2,3-Dimethylhexane Lee et al. [448] 318–328 12–24 50 AnPTSemY
2,4-Dinitrophenol Shamsipur et al. [617] 308–348 12.4–48.6 1 AnTValY
2,5-Dinitrophenol Shamsipur et al. [617] 308–348 12.4–48.6 1 AnTValY
2,Chloroethyl sulfide Shen et al. [627] 294–377 2.3–17.6 30 SynVis
2-Butanol Chen et al. [225] 331–351 4.9–12 n.a. AnTVcirVisVar
Silva-Oliver sand Galicia-Luna [640] 335–431 8.5–14.5 40 AnTValVisPc
2-Chloroethyl methyl sulfide Garach-Domech et al. [321] 308–348 1.9–13.5 30 SynVisVar
2-Ethoxyethanol Joung et al. [394] 323–344 7.3–12.4 50 AnTVLcirValVisPc
2-Ethyl hexanoic acid Ghaziaskar et al. [329] 313–323 6.8–18 10 AnPTSemY
2-Ethyl-1-hexanol Ghaziaskar et al. [329] 313–323 6.8–18 10 AnPTSemY
2-Ethyl-hexyl-2-ethyl hexanoate Ghasziaskar and Daneshfar [327] 313–353 13–25.3 10 AnPTSemY
2-Methoxyethanol Joung et al. [394] 322–343 5.2–12.4 50 AnTVLcirValVisPc
2-Methyl-1-propanol (isobutanol) Chen et al. [225] 331–351 5–12 n.a. AnTVcirVisVar
da Silva and Barbosa [247] 288–313 1.5–8.2 23 AnTVis
2-Methyl-2-butanol Heo et al. [352] 313–353 3.6–12.9 33 SynVisVar
2-Methyl-2-propanol Heo et al. [352] 313–353 4.6–12.1 33 SynVisVar
2-Methylanthracene Yamini et al. [725] 308–348 12.2–35.5 0.5 AnTValY
2-Methylpentan-2,4-diol Petrova et al. [562] 313–333 3.2–16 4.0–14.0 SynVisVar
2-Naphthol Li et al. [459] 308–328 10–30 377 AnPTSemY
Ngo et al. [124] 313–313 8.8–18 n.a. SynNonSpec
2-Nitroanisole Medina and Bueno [509] 313–333 8–20 20 AnPTSemY
2-Octanol Gamse and Marr [317] 303–323 2.2–7.2 140 AnTVcirVal
2-Pentanol Silva-Oliver and Galicia-Luna [642] 332–431 2.1–15.7 40 AnTValVisPc
2-Phenyl-1-propanol Medina and Bueno [509] 313–333 8–20 20 AnPTSemY
2-Phenylethanol Lopes et al. [484] 313–323 8.2–24.4 35 AnTValVis
2-Propanol (isopropanol) Bamberger and Maurer [160] 293–333 1.1–8.1 38 AnPTConVis
Galicia-Luna et al. [47] 324–348 1–10.4 40 AnTCapValVis
Secuianu et al. [41] 293–323 0.6–8.6 25–60 AnTVisVar
3,3,4,4,5,5,6,6-Octafluorooctan-1,8-diol Mesiano et al. [512] 323–323 9–18 n.a. SynVisVar
3,3 ,4 ,5,7-Pentahydroxyflavone (quercetin) Matsuyama et al. [506] 308–318 10.1–25.3 210 AnPTSemY
3-Methoxybenzamide Bristow et al. [189] 343–363 9–12 n.a. AnPTSemYSpec
3-Methyl-1-butanol (isopentanol) da Silva and Barbosa [247] 288–313 1.2–8.1 23 AnTVis
Lee et al. [442] 313–313 2–8.3 n.a. AnTVLcirValPc
Lopes et al. [484] 313–323 5.2–9.4 35 AnTValVis
3-Methyl-2-butanol Lee et al. [442] 313–313 2–8.2 n.a. AnTVLcirValPc
3-Nitrotoluol Medina and Bueno [511] 313–333 8–20 15.7 AnPTSemY
4-(N,N-Diethylamino)-4 -nitroazobenzene Fasihi et al. [290] 308–348 12.2–35.5 1 AnTValY
4-(N,N-Dimethylamino)-4 -nitroazobenzene Fasihi et al. [290] 308–348 12.2–35.5 1 AnTValY
4-Methoxybenzamide Bristow et al. [189] 343–363 9–14 n.a. AnPTSemYSpec
4-Methoxyphenylacetic acid Lee and McHugh [451] 308–367 13.4–89.2 n.a. SynVisVar
4-Phenyl-toluene Leeke et al. [453] 353–383 9.4–30.7 25 SynVis
4-Vinylbenzyl acetylacetone Powell et al. [572] 273–333 10–25.6 n.a. SynVisVar
5,10,15,20- Sane et al. [31] 313–373 10.3–32.4 45 AnTVisVarVal
Tetrakis(3,5bis(trifluoromethyl)phenyl)porphyrin
5,10,15,20-Tetrakis(pentafluorophenyl)porphyrin Sato et al. [598] 313–333 10.3–25.2 40 AnTVcirSpec
5-Fluorouracil Guney and Akgerman [344] 308–328 11–21 n.a. AnPTSemY
7,8-Dihydroxyflavone Matsuyama et al. [506] 308–318 9.1–25.3 210 AnPTSemY
8-Hydroxyquinoline Shamsipur et al. [621] 308–338 10.1–35.5 1 AnTValY
9-nitroanthracene Yamini et al. [725] 308–348 12.2–35.5 0.5 AnTValY
␣-Asarone Chen et al. [228] 308–322 9–18 1500 AnPTSemY
Acenaphthene Yamini and Bahramifar [722] 308–348 12.1–35.4 1 AnTValY
Acetaminophen Bristow et al. [189] 313–353 8–25 n.a. AnPTSemYSpec
Acetic acid (ethanoic acid) Bamberger et al. [61] 313–353 1.1–11.1 38 AnPTCon
Byun et al. [195] 313–393 2.7–16.5 28 SynVisVar
Acetoacetate Powell et al. [572] 273–333 7.2–31.7 n.a. SynVisVar
Acetoacetate fluoroacrylate polymer Powell et al. [572] 293–293 9.5–11 n.a. SynVisVar
Acetone Bamberger and Maurer [160] 303–333 1.1–8.1 38 AnPTConVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 15

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Chen et al. [226] 323–336 8.9–9.9 20–50 SynVisVarPcTc

Wu et al. [709] 322–363 9.2–11 14 SynVis
Acetonitrile (ethanenitrile) Corazza et al. [236] 313–343 4.8–11.7 25 SynVisVar
␣-Cyclodextrin octadecaacetate Potluri et al. [569] 298–298 20–47 100 SynVisVar
␣-Methylstyrene Phiong and Lucien [563] 308–323 2.9–9.1 70 AnTLcirVis
Amical-48 (diiodomethyl p-tolyl sulfone) Sahle-Demessie et al. [595] 318–338 10–30 43.92 AnPTSemYVis
␣-Naphthol Abaroudi et al. [143] 308–318 10.6–16.2 n.a. AnPTSemY
Anthracene Goodarznia and Esmaeilzadeh [334] 308–308 10.2–18.1 n.a. AnPTSemY
Li et al. [459] 308–328 10–30 377 AnPTSemY
Ngo et al. [124] 313–313 7–20.8 n.a. SynNonSpec
Shinoda and Tamura [635] 323–323 10–30 2.3 AnPTSemY
Anthraquinone Mishima et al. [516] 308–333 15.2–25.3 210 AnPTSemY
␣-Pinene Chouchi et al. [232] 323–323 9.3–9.3 50 SynVis
Cruz Francisco and Sivik [239] 313–333 8–25 30 AnPTSemY
Artemisinin (artemisia annua L,) Xing et al. [720] 310–338 10–27 0.83 AnPTSemYSpec
Aspirin Huang et al. [365] 308–328 12–25 10 AnPTSemY
␣-Tetralol (1,2,3,4-tetrahydro-1-naphtol) Borg et al. [185] 303–333 12.5–25.8 1.7–12.4 SynVisVar
␣-Tocopherol Chen et al. [222] 313–333 9.8–24.1 n.a. SynOthVLcirVis
Fang et al. [289] 313–353 5.6–29.6 170 AnTVLcirBlo
Skerget et al. [644] 313–353 8.4–30.3 120 AnT
Skerget et al. [644] 303–353 1.6–11.2 120 AnT
Atropine Yamini et al. [724] 308–348 12.2–35.5 1 AnTValY
Azobenzene Maeda et al. [489] 308–318 9.1–25.3 210 AnPTSemY
Mishima et al. [516] 333–333 10.1–25.3 210 AnPTSemY
␤-Carotene Hansen et al. [348] 313–343 6.8–34.2 n.a. AnSpecY
Sovova et al. [649] 313–333 12–28 12 AnPTSemY
␤-Cyclodextrin heneiicosaacetate Potluri et al. [569] 298–298 20–47 100 SynVisVar
Benzocaine Garmroodi et al. [40] 308–348 12.2–35.5 1 AnTValY
Weinstein et al. [704] 298–318 8.4–25.1 5.5–30 SynVisVar
Benzoic acid Fukné-Kokot et al. [107] 373–395 0.1–16.6 20 SynTVis
Fukné-Kokot et al. [304] 373–393 2.3–16.6 20 SynTVis
Galia et al. [56] 318–318 9–23 85.3 AnTIns
Jin et al. [385] 328–328 8–23 377 AnPTSemY
Lee et al. [448] 318–328 12–27 50 AnPTSemY
Benzoin Cheng et al. [231] 308–328 11.1–24.4 300 AnPTSemY
Bergamot peel oil—Citrus bergamia Franceschi et al. [99] 313–343 2.2–16.4 27 SynVisVar
␤-Estradiol Guney and Akgerman [344] 308–328 10.5–22 n.a. AnPTSemY
Biphenyl Fischer et al. [297] 322–342 0.1–30 n.a. SynNon
Fukné-Kokot et al. [107] 321–342 0.1–19.8 14 SynVis
Fukné-Kokot et al. [107] 321–341 0.1–14.7 20 SynTVis
Fukné-Kokot et al. [304] 321–341 0.1–14.7 20 SynTVis
Bis(acetylacetonato)copper(II) (Cu(acac)2) Guigard et al. [90] 313–318 10–10.3 2 AnOth
Bis(thenoyltrifluoroacetonato)copper(II) (Cu(tta)2) Guigard et al. [90] 313–318 9.6–10.3 2 AnOth
Bisacodyl Asghari-Khiavi and Yamini [153] 308–348 12.2–35.5 1 AnTValY
Black currant seed oil Sovova et al. [650] 313–333 12–28 8 AnPTSemY
␤-Naphthol Abaroudi et al. [143] 308–328 9.9–15.2 n.a. AnPTSemY
Borage oil Gaspar et al. [325] 283–328 6–30 334 AnPTSemY
Bromobenzene Leeke et al. [453] 353–383 9.8–20.1 25 SynVis
Butyl 2,5-dichlorobenzoate Shen et al. [628] 293–379 6.2–28.5 30 SynVisVar
Butyl acetate Ghaziaskar and Nikravesh [328] 313–353 8–18 63 AnPTSemY
Butyl methacrylate Byun and McHugh [104] 308–383 2–16 28 SynVisVar
Butyric acid Byun et al. [195] 313–393 3–18.9 28 SynVisVar
C.I. Disperse Blue 134 Tamura and Shinoda [662] 323–383 10–25 n.a. AnPTSemY
C.I. Disperse Blue 14 Gordillo et al. [335] 313–353 10–35 25.5 AnPTSemY
C.I. Disperse Blue 3 Lee et al. [445] 323–413 10.5–32.9 n.a. AnPTSemYSpec
Lee et al. [446] 323–413 10.5–32.9 n.a. AnPTSemYSpec
C.I. Disperse Blue 354 ([2-[[4-(dihexylamino)-2- Shinoda and Tamura [635] 323–383 10–30 2.3 AnPTSemY
methylphenyl]methylene]-1,1-
dioxidobenzo[b]thien-3(2H)-
ylidene]propanedinitrile)
C.I. Disperse Blue 79 Ferri et al. [74] 353–393 18–30 32 AnPTSemY
Lee et al. [445] 323–383 9.9–30.5 n.a. AnPTSemYSpec
Lee et al. [446] 323–383 9.9–30.5 n.a. AnPTSemYSpec
Lin et al. [470] 353–393 15–30 16.6 AnPTSemY
C.I. Disperse Blue 79:1 Lin et al. [472] 353–393 15–30 16.6 AnPTSemY
C.I. Disperse modified Yellow 119 Lin et al. [472] 353–393 15–30 16.6 AnPTSemY
C.I. Disperse Orange 25 (3-[N-ethyl-4-(4- Ngo et al. [535] 313–313 9.7–18.1 n.a. SynNonSpec
nitrophenylazo)phenylamino]propionitrile)
Shinoda and Tamura [635] 323–383 10–30 2.3 AnPTSemY
C.I. Disperse Orange 3 Ferri et al. [74] 353–393 16–28 32 AnPTSemY
C.I. Disperse Red 1 Shinoda and Tamura [636] 323–383 10–30 2.3 AnPTSemY
C.I. Disperse Red 13 Shinoda and Tamura [636] 323–383 10–30 2.3 AnPTSemY
C.I. Disperse Red 153 Lin et al. [470] 353–393 15–30 16.6 AnPTSemY
C.I. Disperse Red 324 Ferri et al. [74] 353–393 18–30 32 AnPTSemY
C.I. Disperse Red 82 Lin et al. [472] 353–393 15–30 16.6 AnPTSemY
C.I. Disperse Yellow 119 Lin et al. [470] 353–393 15–30 16.6 AnPTSemY
C.I. Disperse Yellow 16 Tamura and Shinoda [662] 323–383 10–25 n.a. AnPTSemY
16 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Caffeic acid Murga et al. [528] 313–333 15–50 4.4 AnPTSemY

Caffeine Burgos-Solórzano et al. [194] 313–313 10–30 32 AnTVcirValVis
Caproic acid Byun et al. [195] 308–373 2.5–20.4 28 SynVisVar
Caprylic acid Byun et al. [195] 308–373 2.3–24 28 SynVisVar
Capsaicin Hansen et al. [348] 308–328 12.9–24.9 n.a. AnPTSemYVal
Carbamazepine Yamini et al. [724] 308–348 12.2–35.5 1 AnTValY
Carbazole Goodarznia and Esmaeilzadeh [334] 308–308 10.3–20.1 n.a. AnPTSemY
Carbobenzoxy aspartic acid Vedaraman et al. [691] 323–343 20–26 7.9 AnTValY
Carbobenzoxy proline Vedaraman et al. [691] 323–343 18–26 7.9 AnTValY
Carbobenzoxy valine Vedaraman et al. [691] 313–333 20–28 7.9 AnTValY
Carbon monoxide Ke et al. [411] 280–298 8.1–9.9 n.a. SynNonPcTc
Carvacrol Leeke et al. [452] 313–323 0.2–30.8 500 AnTVcir
Carvone (p-mentha-6,8-dien-2-one) Gamse et al. [316] 303–324 1.8–10 140 AnTVcirVis
Corazza et al. [236] 313–343 7.7–15.6 25 SynVisVar
Cerium(2,2,6,6-tetramethyl-3,5-octanedionate) Andersen et al. [42] 313–333 10.1–35 2.8 AnSpecY
chelate
Cerium(2,2,7-trimethyl-3,5-octanedionate) chelate Andersen et al. [42] 313–333 9.8–24.3 2.8 AnSpecY
Chloramphenicol Li et al. [460] 313–333 14–46.3 n.a. AnTVcir
Chlorothalonil (tetrachloroisophthalonitrile) Sahle-Demessie et al. [595] 318–338 10–30 43.9 AnPTSemYVis
Cholesterol Huang et al. [366] 313–333 10–25 20 AnPTSemY
Cholesteryl acetate Huang et al. [366] 308–328 9–24 20 AnPTSemY
Cholesteryl benzoate Huang et al. [366] 308–328 12–27 20 AnPTSemY
Cholesteryl butyrate Huang et al. [366] 308–328 10–24 20 AnPTSemY
Citral Benvenuti and Gironi [170] 315–315 4.7–10 200 AnPTSemY
Fonseca et al. [59] 323–323 8.7–9.4 3.4 AnPTCon
Codeine Yamini et al. [724] 308–348 12.2–35.5 1 AnTValY
Coenzyme Q10 (ubiquinone) Matias et al. [503] 305–323 9.2–26.2 42.5 AntCapVal
CuHAsO4 Takeshita and Sato [73] 308–308 9.8–24.5 n.a. AnPTSemY
Cumene Phiong and Lucien [563] 323–323 3–9.1 70 AnTLcirVis
Cyclobutanone Cruz Duarte et al. [238] 277–368 0.4–13.6 3.5 SynVis
Cyclohexyl acetate Lee et al. [450] 333–413 2–8 600 AnPTSemY
Cyproterone acetate Asghari-Khiavi et al. [154] 308–348 12.2–35.5 1 AnTValY
Decanal da Silva et al. [245] 288–313 1.6–8.2 23 AnTValVis
Decanoic acid Heo et al. [352] 313–353 2.2–23.7 33 SynVisVar
Scheidgen and Schneider [603] 273–393 0–100 80 AnT
Decyl 2,5-dichlorobenzoate Shen et al. [628] 293–375 6.2–39 30 SynVisVar
Diazepam Yamini et al. [724] 308–348 12.2–35.5 1 AnTValY
Dibenzo-24-crown-8 (DB24C8) Shamispur et al. [616] 308–338 12.2–44.6 1 AnTValY
Dibenzo-27-crown-9 (DB27C9) Shamispur et al. [616] 308–348 12.2–48.6 1 AnTValY
Dibenzo-30-crown-10 (DB30C10) Shamispur et al. [616] 318–348 12.2–48.6 1 AnTValY
Dibenzoylmethane Shamsipur et al. [621] 308–338 10.1–35.5 1 AnTValY
Dibutyl phthalate Cheng et al. [230] 308–328 1.4–12.5 300 AnPTSemY
Dicarbonyl(h5-cyclopentadienyl)-cobalt Casimiro et al. [203] 313–363 1.8–14.8 36 AnTValVIs
Casimiro et al. [203] 313–363 1.8–14.8 3.5 SynVisVar
Dichloromethane (HCC-30) Corazza et al. [236] 313–343 4.6–10.1 25 SynVisVar
Tsivintzelis et al. [676] 308–328 1.9–8.8 202.1 AnTVLcirValVis
Vega-Gonzalez et al. [692] 311–326 4.1–9 9 SynVisVar
Diethyl carbonate Im et al. [372] 320–340 0.7–9 320 AnTVLcirValVis
Diethyl ethylmalonate Hwu et al. [370] 308–328 1.4–8.3 300 AnPTSemY
Diethyl methylmalonate Hwu et al. [370] 308–328 1.4–8.3 300 AnPTSemY
Diethyl methylphosphonate Garach-Domech et al. [321] 308–348 1.4–13.1 30 SynVisVar
Diethyl n-butylmalonate Hwu et al. [370] 308–328 1.4–8.3 300 AnPTSemY
Diethyl oxalate Cheng et al. [230] 308–328 1.4–10.1 300 AnPTSemY
Diethyl phthalate Cheng et al. [68] 308–328 1.5–12.5 300 AnPTSemXY
Diethyl succinate Feng et al. [291] 308–328 1.4–10.1 300 AnPTSemXY
Diethylene glycol (DEG) Jou et al. [388] 298–398 0–21.1 n.a. AnTVcir
Diethylene glycol butyl ether Lin et al. [471] 333–413 2–20 600 AnPTSemY
Diethylene glycol dibutyl ether Lin et al. [471] 333–413 1–17.5 600 AnPTSemY
Diethylene glycol diethyl ether Lin et al. [471] 333–413 2–16 600 AnPTSemY
Diethylene glycol hexyl ether Lin et al. [471] 333–413 1–20 600 AnPTSemY
Difluoromethane (HFC-32) Di Nicola et al. [263] 287–294 1.3–3.5 254.8 SynT
Diefenbacher and Türk [101] 304–351 5.7–7.4 1406 SynVisPcTc
Diefenbacher and Türk [268] 280–318 1.6–7.5 1406 SynVisPcTc
Rivollet et al. [587] 283–343 1.1–7.4 n.a. AnTValVis
Dimethyl 2H-1-benzopyran-2,3-dicarboxylate Bahramifar et al. [39] 308–348 12.2–35.5 0.5 AnTValY
Dimethyl Bahramifar et al. [39] 308–348 12.2–35.5 0.5 AnTValY
6-bromo-2H-1-benzopyran-2,3-dicarboxylate
Dimethyl carbonate Camy et al. [202] 322–373 1.3–12.7 14.35 SynVis
Im et al. [372] 310–340 0.8–9.9 320 AnTVLcirValVis
Dimethyl ether Laursen et al. [38] 298–320 0.6–7.3 570 AnTValVis
Dimethyl sulfoxide Vega-Gonzalez et al. [692] 309–328 4–12.5 9 SynVisVar
Dimethyl-3Hnaphtho[2,1-b]pyran-2,3-dicarboxylate Bahramifar et al. [39] 308–348 12.2–35.5 0.5 AnTValY
Dimethylsulfoxide Rajasingam et al. [581] 298–318 1–9 70 AnTLcirVis
Dimethylterephthalate Fischer et al. [297] 375–413 0.1–30 n.a. SynNon
Fischer et al. [297] 418–438 0.2–29.1 n.a. SynVis
Diphenylcarbonate Margon et al. [498] 343–453 1–13 3.5 SynVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 17

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

di-tert-Butyl-3H-naphtho[2,1-b]pyran-2,3- Bahramifar et al. [39] 308–348 12.2–35.5 0.5 AnTValY

dicarboxylate
Divinyl adipate Mesiano et al. [512] 323–323 10–35 n.a. SynVisVar
d-Lactone Xu et al. [721] 313–343 9.8–26.7 26 SynVis
Docosahexaenoic acid ethylester Jaubert et al. [382] 303–353 4.7–24.2 12.4 SynVis
Dodecanoic acid Scheidgen and Schneider [603] 273–393 0–100 80 AnT
Double Tail Fluoroalkyl Powell and Beckman [571] 295–295 6.5–15.1 n.a. SynVisVar
␦-Tocopherol Pereira et al. [561] 306–333 9–26.4 30 AnTVcirValVis
␧-Caprolactone Xu et al. [721] 313–363 8.3–27.2 26 SynVis
Echium oil Gaspar et al. [325] 283–328 6–30 334 AnPTSemY
Eflucimibe Sauceau et al. [600] 308–318 9.8–30.1 n.a. AnPTSemY
Eicosapentaenoic acid ethylester Jaubert et al. [382] 303–353 6–23.3 12.4 SynVis
Erythromycin Burgos-Solórzano et al. [194] 313–333 10–30 32 AnTVcirValVis
Ethane Horstmann et al. [356] 291–305 4.9–6.8 10 SynVisPcTc
Horstmann et al. [358] 298–300 5.1–6.8 10 SynVisTc
Ethanol Bae et al. [158] 314–314 5.5–7.9 25 SynVisVar
Chen et al. [223] 323–323 5–8.2 100 AnTVcirVis
Elbaccouch and Elliot [279] 323–333 0.7–9.4 40 AnTVLcirVal
Galicia-Luna et al. [47] 312–373 0.4–14.3 40 AnTCapValVis
Joung et al. [394] 313–344 5.4–11.9 50 AnTVLcirValVisPc
Stuart et al. [654] 313–313 4.8–7.5 28 SynVisVar
Tsivintzelis et al. [676] 313–328 1.6–9.4 202.1 AnTVLcirValVis
Vega-Gonzalez et al. [692] 314–324 7–8.2 9 SynVisVar
Yeo et al. [732] 298–413 6.1–15.1 26.71 SynVisVar
Ethoxynonafluorobutane Kho et al. [413] 298–298 0.8–6.4 130 AnTVisVar
Ethyl acetate da Silva et al. [244] 295–313 1.9–8.5 23 AnTVis
Tian et al. [670] 333–393 3.9–11.9 100 AnTCapVisVar
Ethyl acrylate Byun [197] 313–393 1.7–10.7 28 SynVisVar
Ethyl benzoate Feng et al. [291] 308–328 1.3–12.2 300 AnPTSemXY
Ethyl butyrate Ismadji and Bhatia [375] 308–333 8.5–19.5 8 AnTBlo
Ethyl caprate Hwu et al. [369] 308–328 1.7–9.2 300 AnPTSemXY
Ethyl caproate Hwu et al. [369] 308–328 1.7–9.2 300 AnPTSemXY
Ethyl caprylate Hwu et al. [369] 308–328 1.7–9.2 300 AnPTSemXY
Ethyl isovalerate Ismadji and Bhatia [375] 308–333 8.5–19.5 8 AnTBlo
Ethyl laurate Cheng et al. [230] 308–328 1.4–10.1 300 AnPTSemY
Ethyl methacrylate Byun and McHugh [104] 313–373 1–14 28 SynVisVar
Ethyl phenyl sulfide Shen et al. [627] 295–375 1.3–23.8 30 SynVis
Ethyl propanoate Tian et al. [670] 313–373 2.9–10.9 100 AnTCapVisVar
Ethyl proprionate Ismadji and Bhatia [375] 308–333 8.5–19.5 8 AnTBlo
Ethylene glycol Lopes et al. [483] 313–313 20–20 35 AnT
Ethyl-o-vanillin Fukné-Kokot et al. [107] 314–338 0.1–29.5 14 SynVis
Fukné-Kokot et al. [107] 314–338 0.1–19.8 20 SynTVis
Fukné-Kokot et al. [304] 314–338 0.1–19.8 20 SynTVis
Eucalyptus leaf oil (E, Dives) Cruz Francisco and Sivik [239] 313–333 8–25 30 AnPTSemY
Eucalyptus leaf oil (E, Polybractea) Cruz Francisco and Sivik [239] 313–333 8–25 30 AnPTSemY
Eucalyptus leaf oil (E, Radiata) Cruz Francisco and Sivik [239] 313–333 8–25 30 AnPTSemY
Eugenol Cheng et al. [68] 308–328 1.4–12.5 300 AnPTSemXY
Ferulic acid Murga et al. [528] 313–333 10–50 4.4 AnPTSemY
Sovova [651] 301–333 12–28 n.a. AnPTSemY
Florfenicol Li et al. [460] 313–333 11.7–49 n.a. AnTVcir
Fluoranthene Yamini and Bahramifar [722] 308–348 12.1–35.4 1 AnTValY
Fluorinated telechelic disulfates Shi et al. [629] 297–297 15–47 100 SynVisVar
Flurbiprofen Duarte et al. [275] 303–323 8.9–24.5 30 AnTCapValVis
Formic acid Byun et al. [195] 313–393 3.3–26.4 28 SynVisVar
Functionalized siloxane copolymer: butyl methyl Kilic et al. [418] 295–295 19–23 n.a. SynVisVar
ketone
Functionalized siloxane copolymer: methylbutyrate Kilic et al. [418] 295–295 13–22 n.a. SynVisVar
Functionalized siloxane copolymer: propy ltrimethyl Kilic et al. [418] 295–295 9–13 n.a. SynVisVar
carbon
Functionalized siloxane copolymer: propyl acetate Kilic et al. [418] 295–295 12–36 n.a. SynVisVar
Functionalized siloxane copolymer: propyl ethyl ether Kilic et al. [418] 295–295 6–44 n.a. SynVisVar
Functionalized siloxane copolymer: propyl methyl Kilic et al. [418] 295–295 11–23 n.a. SynVisVar
carbonate
Functionalized siloxane copolymer: propyl trimethyl Kilic et al. [418] 295–295 5–17 n.a. SynVisVar
silane
␥-Butyrolactone Xu et al. [721] 313–363 8.5–25.2 26 SynVis
␥-Caprolactone Xu et al. [721] 323–363 10.2–19.2 26 SynVis
␥-Cyclodextrin tetracosaacetate Potluri et al. [569] 298–298 20–47 100 SynVisVar
␥-Decalactone Xu et al. [721] 323–363 10.2–21.9 26 SynVis
Grafted poly(oxyethylene)siloxane Fink and Beckman [295] 295–338 34–42 n.a. SynVisVar
Grape seed oil Sovova et al. [650] 313–313 15–29 8 AnPTSemY
Heptadecafluorodecyl acrylate Bae et al. [157] 323–353 2.3–13.8 25 SynVisVar
Heptadecafluorodecyl methacrylate Bae et al. [157] 323–353 0.8–14 25 SynVisVar
Hexabromcyclododecane Gamse and Marr [315] 298–373 20–50 50 AnT
Hexanoic acid Ghaziaskar and Nikravesh [328] 313–353 7.5–14 63 AnPTSemY
Hexyl acetate Lee et al. [450] 333–413 1–6 600 AnPTSemY
18 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Hexyl acrylate Byun et al. [201] 313–393 2.5–14.6 28 SynVisVar

Hexyl methacrylate Byun et al. [201] 313–393 3.5–17.2 28 SynVisVar
High MW poly(2,6-dimethyl-1,4-phenylene ether) Sato et al. [599] 373–473 1.9–20.2 n.a. AnGrav
(PPO)(H)
Hydrogen Bezanehtak et al. [173] 278–290 4.8–19.2 60 AnTLcirVal
Ke et al. [411] 296–303 9.1–13.8 n.a. SynNonPcTc
Hydroquinone (1,4-dihydroxybenzene) García-González et al. [323] 333–363 10–35 50 AnTVcirVal
Deiters [259] 0 Comments
Imipramine hcl Jara-Morante et al. [378] 313–323 30–50 n.a. AnPTSemY
Iron tris(pentane-2,4-dionate) Roggeman et al. [589] 313–333 9–27.5 50 AnTVal
Iron(2,2,6,6-tetramethyl-3,5-octanedionate) chelate Andersen et al. [42] 313–333 9.4–30.6 2.8 AnSpecY
Iron(2,2,7-trimethyl-3,5-octanedionate) chelate Andersen et al. [42] 313–333 9–17.7 2.8 AnSpecY
Iron(2,4-pentanedionate) chelate Andersen et al. [42] 313–333 9.8–35.3 2.8 AnSpecY
Isoamyl acetate da Silva et al. [244] 295–313 1.7–8.1 23 AnTVis
Feng et al. [291] 308–328 1–9 300 AnPTSemXY
Isobutyraldehyde Ke et al. [411] 311–330 8–9.7 n.a. SynNonPcTc
Ketoprofen Stassi et al. [652] 313–328 9–25 125 AnPTSemY
Weinstein et al. [704] 313–313 9–25 5.5–30 SynVisVar
Komplex Double Tail Fluoroalkyl: AuCl4- Powell and Beckman [571] 295–295 6.5–18.2 n.a. SynVisVar
Komplex Double Tail Fluoroalkyl: PtCl6- Powell and Beckman [571] 295–295 6–15.6 n.a. SynVisVar
Komplex Single Tail Fluoroalkyl: PtCl6- Powell and Beckman [571] 295–295 8.3–16.2 n.a. SynVisVar
Krytox 157 FSL Casimiro et al. [204] 313–343 2–17 35 AnTValVis
Lemon oil de la Fuente and Bottini [255] 303–313 0.9–8.7 40–80 SynVisVar
Lemon peel oil—Citrus latifolia Franceschi et al. [99] 313–343 1.7–19 27 SynVisVar
Lidocaine Weinstein et al. [704] 298–318 7–25.2 5.5–30 SynVisVar
Limonene Benvenuti and Gironi [170] 315–315 3.1–8.5 200 AnPTSemY
Berna et al. [171] 318–318 6.9–10.5 n.a AnPTSemY
Corazza et al. [236] 313–323 7.9–8.1 25 SynVisVar
Cruz Francisco and Sivik [239] 313–333 8–25 30 AnPTSemY
Fonseca et al. [59] 323–323 8.7–9.5 3.4 AnPTCon
Gamse et al. [316] 303–324 3.1–8.4 140 AnTVcirVis
Leeke et al. [452] 318–323 0.3–9.6 500 AnTVcir
Linalool Berna et al. [171] 318–328 7.1–11.1 n.a. AnPTSemY
Fonseca et al. [59] 323–323 8.7–10.3 3.4 AnPTCon
Raeissi and Peters [575] 283–371 1.4–14.7 3.5 SynVis
Linoleic acid Chen et al. [222] 313–333 5.4–24.1 n.a. SynOthVLcirVis
Low MW poly(2,6-dimethyl-1,4-phenylene ether) Sato et al. [599] 373–473 2–19.9 n.a. AnGrav
(PPO)(L)
Ls-54 surfactant Liu et al. [475] 308–318 13.6–22.8 40 SynVis
Lubricating oil PAG-1 Tsuji et al. [677] 344–344 4.1–20.1 500 AnTVLcirBloVis
Tsuji et al. [677] 344–345 2.1–5.4 52.5 SynOthVisVar
Lunaria oil Gaspar et al. [325] 283–328 6–30 334 AnPTSemY
Mandelic acid Cheng et al. [231] 308–328 10.1–23 300 AnPTSemY
Medroxyprogesterone Asghari-Khiavi et al. [154] 308–348 12.2–35.5 1 AnTValY
Methane Webster and Kidney [703] 230–270 0.8–8.4 n.a. AnTVcir
Methanol Bezanehtak et al. [173] 278–308 1.5–7.4 60 AnTLcirVal
Elbaccouch and Elliot [279] 313–313 1.1–7.5 40 AnTVLcirVal
Joung et al. [394] 313–342 6–12.4 50 AnTVLcirValVisPc
Laursen et al. [38] 298–313 1.2–6.3 570 AnTValVis
Liu et al. [473] 304–512 7.4–16.3 18 SynVis
Yeo et al. [732] 298–423 5.8–16.4 26.7 SynVisVar
Methimazole Asghari-Khiavi and Yamini [153] 308–348 12.2–35.5 1 AnTValY
Yamini et al. [726] 308–348 12.2–35.5 1 AnTValY
Methoxynonafluorobutane Kho et al. [413] 298–308 1.3–7.1 130 AnTVisVar
Methyl acrylate Byun [197] 318–398 1.9–11.4 28 SynVisVar
Methyl gallate Murga et al. [527] 313–333 10–50 4.4 AnPTSemY
Methyl oleate Fang et al. [289] 313–353 5.1–22.3 170 AnTVLcirBlo
Methylcyclohexane Nasrifar et al. [533] 263–353 0.4–11.3 3.5 SynVisPcTc
Methylparaben Asghari-Khiavi and Yamini [153] 308–348 12.2–35.5 1 AnTValY
Methylsaliylate Cheng et al. [68] 308–328 1.5–13.2 300 AnPTSemXY
Metronidazole benzoate Garmroodi et al. [40] 308–348 12.2–35.5 1 AnTValY
m-Nitrophenol Shamsipur et al. [617] 308–348 12.4–48.6 1 AnTValY
Mobil EAL Arctic 22 oil Skripov et al. [645] 825–825 1.8–1.8 n.a. SynNonPcTc
Monochlorobenzene Wu et al. [709] 326–377 11.6–19.4 14 SynVis
N,N-Dibutylformamide Byun et al. [199] 318–398 2.4–22.6 28 SynVisVarPc
N,N-Diethylacetamide Byun and Jeon [196] 313–373 1.5–17.9 n.a. SynVisVarPc
N,N-Diethylformamide Byun et al. [199] 318–398 2.9–20.7 28 SynVisVarPc
N,N-Dimethylacetamide Byun and Jeon [196] 313–373 1.8–17.1 n.a. SynVisVarPc
N,N-Dimethylformamide Byun et al. [199] 318–398 3.8–20.6 28 SynVisVarPc
Duran-Valencia et al. [36] 293–338 0.4–11.5 50 AnTVal
Naphthalene Abbott et al. [94] 318–318 9–20 25 AnOth
Diefenbacher and Türk [267] 308–308 8.8–20.8 600 AnT
Diefenbacher and Türk [267] 332–334 10.6–26.3 1310 SynVis
Fukné-Kokot et al. [107] 333–353 0.1–20 14 SynVis
Fukné-Kokot et al. [107] 332–353 0.1–20 20 SynTVis
García-González et al. [322] 308–308 13.8–20.4 50 AnTVcirVal
Goodarznia and Esmaeilzadeh [334] 308–308 9.8–20 n.a. AnPTSemY
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 19

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Lee et al. [447] 328–328 12.5–25.3 50 AnPTSemY

Pauchon et al. [75] 308–308 7.1–32.1 12 AnPTSemYVal
Ren et al. [584] 328–328 7–16.2 0.8 AnPTSemY
Sauceau et al. [71] 308–318 8–29.9 5 AnPTSemY
Sherman et al. [55] 308–308 13.1–13.1 47 AnTIns
Stassi et al. [652] 308–308 9.7–25.2 125 AnPTSemY
Takeshita and Sato [73] 308–308 9.8–24.5 n.a. AnPTSemY
Wagner et al. [37] 308–328 8–30.1 10 AnTVcirVal
Wang et al. [699] 308–308 8.5–25.2 88 AnPTSemY
Naproxen Garmroodi et al. [40] 308–348 12.2–35.5 1 AnTValY
Jara-Morante et al. [378] 323–323 16–19.3 n.a. AnPTSemY
n-Butanal da Silva and Barbosa [243] 303–303 2.9–5.2 23 AnTValVis
da Silva and Barbosa [246] 303–303 2.9–5.2 23 AnTValVis
Zhang et al. [734] Comments
N-Butylpyridinium tetrafluoroborate [N-bupy][BF4] Blanchard et al. [133] 313–333 0–9.5 10 SynT
n-Butyraldehyde Ke et al. [411] 313–337 8.2–10.3 n.a. SynNonPcTc
n-Decane Eustaquio-Rincón and Trejo [286] 308–308 8.9–12.7 n.a. AnPTSemY
Shaver et al. [625] 344–344 0.8–12.7 n.a. AnTVcirVal
Tsuji et al. [677] 344–344 3.6–11.5 500 AnTVLcirBloVis
Tsuji et al. [677] 344–345 2.5–10.9 52.5 SynOthVisVar
n-Dodecane Gardeler et al. [324] 318–318 0.9–8.9 n.a. AnTVal
Nieuwoudt and du Rand [536] 313–343 7.9–14.3 132 SynVisVar
n-Eicosane Nieuwoudt du Rand [536] 315–348 7.7–30.3 132 SynVisVar
n-Heptacosane Furuya and Teja [314] 313–313 10–52.3 31.6 SynVisVar
n-Heptane Fenghour et al. [292] 301–362 3.4–4.3 207 SynNon
n-Hexacosane Furuya and Teja [314] 313–313 13.8–41.3 31.6 SynVisVar
n-Hexadecane Eustaquio-Rincón and Trejo [286] 308–308 8.3–12.4 n.a. AnPTSemY
Nieuwoudt du Rand [536] 313–323 8.5–16.8 132 SynVisVar
Rose et al. [591] 305–311 7.6–17.2 n.a. AnPTSemY
Scheidgen and Schneider [601] 393–393 0–1000 80 AnT
Skripov et al. [645] 720–720 4.8–4.8 n.a. SynNonPcTc
n-Hexane Liu et al. [473] 304–507 3–11.7 18 SynVis
n-Hexatriacontane Nieuwoudt du Rand [536] 344–366 20.1–297.5 n.a. SynVisVar
Nimodipine Medina and Bueno [510] 313–333 10–25 15 AnPTSemY
Nitrous oxide Horstmann et al. [357] 304–309 7.2–7.3 10 SynVisTc
N-Methyl-2-pyrrolidone Rajasingam et al. [581] 298–318 0.9–8.4 70 AnTLcirVis
N-Methyldiethanolamine (MDEA) Kamps et al. [400] 313–353 0.1–7.5 30 SynVis
Kamps et al. [401] 313–313 0.8–4.8 30 SynVis
n-Nonacosane Furuya and Teja [314] 313–313 12.4–17.8 31.6 SynVisVar
n-Nonadecane Elbaccouch et al. [282] 313–313 0.2–8.6 9.5 SynTVis
n-Octadecane Eustaquio-Rincón and Trejo [286] 310–353 10–20 n.a. AnPTSemY
n-Octaosane Nieuwoudt du Rand [536] 338–366 14–28.9 n.a. SynVisVar
N-Octyl-2-pyrrolidone Fischer et al. [296] 303–323 0.1–1.3 n.a. SynT
Nonanoic acid Scheidgen and Schneider [603] 273–393 0–100 80 AnT
n-Pentacosane Furuya and Teja [314] 313–313 15.2–36 31.6 SynVisVar
n-Pentane Chen et al. [226] 312–326 7.7–8.5 20–50 SynVisVarPcTc
n-Tetracosane Furuya and Teja [314] 310–310 12.9–45.9 31.6 SynVisVar
Nieuwoudt du Rand [536] 329–357 16.6–30.1 n.a. SynVisVar
n-Tetradecane Scheidgen and Schneider [601] 393–393 0–1000 80 AnT
n-Vinyl-2-pyrrolidone Bae et al. [158] 324–355 2–18.1 25 SynVisVar
octanoic acid Heo et al. [352] 313–353 5.8–20.5 33 SynVisVar
Octyl 2,5-dichlorobenzoate Shen et al. [628] 295–374 6.2–36.7 30 SynVisVar
o-Hydroxybenzoic acid Bristow et al. [189] 308–328 8–16.5 n.a. AnPTSemYSpec
Bristow et al. [189] 318–318 11.2–20.2 n.a AnTVcirVal
Galia et al. [56] 318–327 10.2–22 85.3 AnTIns
Oligo(oxyethylene)siloxane Fink and Beckman [295] 295–338 26–37 n.a. SynVisVar
Orange peel oil Stuart et al. [654] 308–343 7.3–13.5 28 SynVisVar
Palmitic acid Gordillo [336] 308–328 10–35 25.5 AnPTSemY
Iwai et al. [376] 313–313 15–15 26.5 AnTVcirSpec
p-Coumaric acid Murga et al. [527] 313–323 8.5–25 4.4 AnPTSemY
Murga et al. [528] 313–333 8.5–50 4.4 AnPTSemY
p-Dimethylaminoazobenzene Maeda et al. [489] 308–318 9.1–25.3 210 AnPTSemY
Mishima et al. [516] 333–333 10.1–25.3 210 AnPTSemY
Pentachlorophenol Curren and Burk [241] 293–332 9.7–24.6 105 AnTVal
Pentadecafluorodecyl 2,5-dichlorobenzoate Shen et al. [628] 294–366 5.9–20.3 30 SynVisVar
Pentadecanolactone Mishima et al. [515] 308–318 9.1–25.3 210 AnPTSemY
Pentafluorobutyl 2,5-dichlorobenzoate Shen et al. [628] 294–367 5.6–18.7 30 SynVisVar
Pentafluoropropyl 2,5-dichlorobenzoate Shen et al. [628] 295–367 5.9–19.7 30 SynVisVar
Perfluorohexane (PFC-72) Kho et al. [413] 298–298 1.5–6.3 130 AnTVisVar
Phenanthene Lee et al. [448] 318–328 12–27 50 AnPTSemY
Phenanthrene Goodarznia and Esmaeilzadeh [334] 308–308 10.1–18.1 n.a. AnPTSemY
Guney and Akgerman [344] 318–318 13.1–26.5 n.a. AnPTSemY
Sane et al. [31] 308–328 12–28 45 AnTVisVarVal
Sherman et al. [55] 318–318 16.5–16.5 47 AnTIns
Phenazopyridine Yamini et al. [726] 308–348 12.2–35.5 1 AnTValY
Phenol García-González et al. [322] 333–363 10–35 50 AnTVcirVal
20 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Margon et al. [498] 343–453 1–13 3.5 SynVis

Phenyl acetate Lee et al. [450] 333–413 2–9 600 AnPTSemY
p-Hydroxyazobenzene Maeda et al. [489] 308–318 9.1–25.3 210 AnPTSemY
Mishima et al. [516] 333–333 10.1–25.3 210 AnPTSemY
Picric acid Shamsipur et al. [617] 308–348 12.4–48.6 1 AnTValY
p-Nitrophenol Shamsipur et al. [617] 308–348 12.4–48.6 1 AnTValY
Poly(␣-olefin) Hauk and Weidner [350] 278–373 0.1–15 1000 AnT
Poly(␤-hydroxybutyrate) Khosravi-Darani et al. [414] 308–348 12.2–35.5 1 AnTValY
Poly(butylene succcinate-co-adipate) Sato et al. [43] 323–453 1–20.1 n.a. AnGrav
Poly(butylene succinate) Sato et al. [43] 323–453 1–20.1 n.a. AnGrav
Poly(di-1H,1H,2H,2H-perfluoroalkyl diitaconate) Li et al. [456] 294–424 8.1–40.2 30 SynVisVar
Poly(di-1H,1H,2H,2H-perfluoroalkyl monoitaconate) Li et al. [456] 293–402 14.2–53.9 30 SynVisVar
Poly(␧-caprolactone) Cotugno et al. [85] 343–358 0.2–6 n.a. AnGrav
Poly(ethyl vinyl ether) 1500 Drohmann and Beckman [272] 295–295 28–35 n.a. SynVis
Poly(ethylene glycol) 1500 Wiesmet et al. [33] 338–373 4.1–27.4 1000 AnTCap
Poly(ethylene glycol) 200 Lopes et al. [483] 313–313 20–20 35 AnT
Poly(ethylene glycol) 400 Lopes et al. [483] 313–313 20–20 35 AnT
Poly(ethylene glycol) 4000 Wiesmet et al. [33] 328–373 0.5–28 1000 AnTCap
Poly(ethylene glycol) 600 Lopes et al. [483] 313–313 20–20 35 AnT
Poly(ethylene glycol) 8000 Wiesmet et al. [33] 353–353 4–25.6 1000 AnTCap
Poly(ethylene glycol) dimethyl ether 500 Drohmann and Beckman [272] 295–295 10–11 n.a. SynVis
Poly(ethylene glycol) diol 200 Drohmann and Beckman [272] 295–295 13–24 n.a. SynVis
Poly(ethylene glycol) diol 300 Drohmann and Beckman [272] 295–295 15–25 n.a. SynVis
Poly(ethylene glycol) diol 400 Drohmann and Beckman [272] 295–295 18–31 n.a. SynVis
Poly(ethylene glycol) diol 600 Drohmann and Beckman [272] 295–295 20–32 n.a. SynVis
Poly(ethylene glycol) monomethylether 1000 Drohmann and Beckman [272] 295–295 15–23 n.a. SynVis
Poly(ethylene glycol) monomethylether 350 Drohmann and Beckman [272] 295–295 9–12 n.a. SynVis
Poly(ethylene glycol) monomethylether 550 Drohmann and Beckman [272] 295–295 13–26 n.a. SynVis
Poly(ethylene glycol) monomethylether 750 Drohmann and Beckman [272] 295–295 23–40 n.a. SynVis
Poly(ethylene glycol-block-propylene glycol) Drohmann and Beckman [272] 295–295 44–46 n.a. SynVis
EO6-PO21-EO6
Poly(ethylene glycol-block-propylene glycol) Drohmann and Beckman [272] 295–295 14–18 n.a. SynVis
EO-PO16-EO
Poly(ethylene glycol-block-propylene glycol) Drohmann and Beckman [272] 295–295 24–30 n.a. SynVis
PO15-EO10-PO15
Poly(ethylene glycol-block-propylene glycol) Drohmann and Beckman [272] 295–295 35–41 n.a. SynVis
PO9-EO23-PO9
Poly(ethylene) (LDPE) Davis et al. [252] 423–423 0.6–6.5 72 SynT
Fukné-Kokot et al. [107] 358–385 0.1–30.1 14 SynVis
Poly(methyl methacrylate) Shieh and Liu [630] 305–305 2–34 10 AnT
Poly(methyl methacrylate) (PMMA) Boudouris et al. [44] 308–308 0.1–5.2 n.a. AnOth
Poly(propylene glycol) diol 1000 Drohmann and Beckman [272] 295–295 14–21 n.a. SynVis
Poly(propylene glycol) diol 2000 Drohmann and Beckman [272] 295–295 18–25 n.a. SynVis
Poly(propylene glycol) diol 425 Drohmann and Beckman [272] 295–295 7–11 n.a. SynVis
Poly(propylene glycol) diol 725 Drohmann and Beckman [272] 295–295 8–14 n.a. SynVis
Poly(propylene glycol) monobutoxy 1200 Drohmann and Beckman [272] 295–295 10–18 n.a. SynVis
Poly(propylene glycol) monobutylether 1000 Drohmann and Beckman [272] 298–343 11–31 n.a. SynVis
Poly(propylene glycol) monomethylether 1000 Drohmann and Beckman [272] 295–295 11–19 n.a. SynVis
Poly(propylene glycol) monomethylether 1200 Drohmann and Beckman [272] 295–295 16–26 n.a. SynVis
Poly(propylene) Palamara et al. [84] 323–323 0.5–1.3 n.a. AnGrav
Poly(vinyl chloride) Muth et al. [530] 313–343 5–40 30 SynT
Poly(vinylacetate) Palamara et al. [84] 313–313 3.3–6.3 n.a. AnGrav
Sato et al. [88] 313–373 0.2–17.4 n.a. AnGrav
Polyalkylene glycol Hauk and Weidner [350] 278–373 0.1–15 1000 AnT
Polycarbonate Tang et al. [664] 313–333 20–40 10 SynT
Polydimethylsiloxane 100cst Alessi et al. [67] 313–333 10–19 n.a. AnPTSemY
Polydimethylsiloxane 20cst Alessi et al. [67] 313–333 10–19 n.a. AnPTSemY
Polydisperse fluorinated polyester (Mw = 1800) Mesiano et al. [512] 323–323 18–25 n.a. SynVisVar
Polyfluoroacrylate (poly(heptadecafluorodecyl Shi et al. [629] 297–297 8–10 100 SynVisVar
acrylate))
Polyolester Hauk and Weidner [350] 278–373 0.1–15 1000 AnT
Polystyrene Boudouris et al. [44] 308–318 0.1–5.8 n.a. AnOth
Nikitin et al. [57] 311–311 9–9 n.a. AnTMla
Nikitin et al. [58] 311–311 9–9 n.a. AnTMla
Sato et al. [88] 373–473 2.1–20.1 n.a. AnGrav
Shieh and Liu [630] 305–305 2–34 10 AnT
p-Quinone (1,4-benzoquinone) García-González et al. [323] 333–363 10–35 50 AnTVcirVal
Deiters [259] Comments
Procaine Weinstein et al. [704] 298–318 6.9–25.2 5.5–30 SynVisVar
Propane May et al. [117] 310–310 2.7–2.8 185 SynNonVcirVar
Smejkal et al. [646] 295–354 6.2–8.4 35 SynVisPcTc
Webster and Kidney [703] 230–270 0–3.1 n.a. AnTVcir
Propene Ke et al. [411] 305–343 6–7.1 n.a. SynVisVarPcTc
Propranolol Yamini et al. [726] 308–348 12.2–35.5 1 AnTValY
Propyl 2,5-dichlorobenzoate Shen et al. [628] 294–373 6.2–26.7 30 SynVisVar
Propyl 4-hydroxybenzoate Cheng et al. [231] 308–328 9.4–22 300 AnPTSemY
Propyl acrylate Byun [198] 313–393 3.5–16 n.a. SynVisVar
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 21

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Propyl methacrylate Byun [198] 313–393 1.6–16.5 n.a. SynVisVar

Propylene carbonate Williams et al. [707] 298–333 4.1–11 725 AnT
Protocatechualdehyde Murga et al. [527] 313–333 10–50 4.4 AnPTSemY
Protocatechuic acid Murga et al. [527] 313–333 10–50 4.4 AnPTSemY
P-tolylboronic acid Leeke et al. [453] 353–383 9.5–31.7 25 SynVis
Pyrocatechol García-González et al. [322] 333–363 10–35 50 AnTVcirVal
Quinizarin Ferri et al. [74] 353–393 16–30 32 AnPTSemY
Racemic (S)- and (R)-Boc-piperazine Uchida et al. [679] 308–328 10.2–20.4 240 AnPTSemY
Salicylic acid Abbott et al. [94] 318–318 9.8–19.5 25 AnOth
Stassi et al. [652] 313–328 9.6–25 125 AnPTSemY
Seawater Holder et al. [355] 275–277 15–27 40 SynVisVar
Single Tail Fluoroalkyl Powell and Beckman [571] 295–295 5.5–10.1 n.a. SynVisVar
Sodium 2-methyl-2-sulfosuccinate-semi- Fink and Beckman [295] 295–338 24–27 n.a. SynVisVar
[poly(dimethylsiloxane)ester]
Sodium 2-sulfosuccinate-semi- Fink and Beckman [295] 295–338 24–27 n.a. SynVisVar
[poly(dimethylsiloxane)ester]
Sodium Fink and Beckman [295] 295–338 26–28 n.a. SynVisVar
bis[poly(dimethylsiloxane)ester]2-sulfosuccinate
Soysolv Elbaccouch et al. [282] 298–343 0.1–9 9.5 SynTVis
Styrene Akgün et al. [149] 333–348 6–13 115 AnTBlo
Sulfathiazole Kordikowski et al. [66] 298–353 10–35 10 AnPTSemYSpec
Sulfur hexafluoride SF6 Horstmann et al. [358] 299–309 4.5–6.6 10 SynVisTc
Syringic acid Murga et al. [529] 313–333 10–50 4.4 AnPTSemY
TCMTB (2-(thiocyanomethylthio) benzothiazole) Sahle-Demessie et al. [595] 323–338 10–30 43.9 AnPTSemYVis
Tebuconazole (R-[2-(4-chlorophenyl)ethyl]-R-(1,1- Sahle-Demessie et al. [595] 323–338 10–30 43.9 AnPTSemYVis
dimethylethyl)-1H-1,2,4-triazole-1-ethanol)
Terbium(2,2,6,6-tetramethyl-3,5-octanedionate) Andersen et al. [42] 313–333 12.4–35.2 2.8 AnSpecY
chelate
Terbium(2,2,7-trimethyl-3,5-octanedionate) chelate Andersen et al. [42] 313–333 12.4–31.8 2.8 AnSpecY
tert-Butanol Chen et al. [225] 331–351 5–12 n.a. AnTVcirVisVar
Tetrabrombisphenyl-A Gamse and Marr [315] 298–373 20–50 50 AnT
Tetradecanoic acid Scheidgen and Schneider [603] 273–393 0–100 80 AnT
Tetraethylene glycol n-laurel ether (C12E4) Liu et al. [474] 313–323 10.2–19.6 40 SynVis
Tetrahydrofuran Im et al. [371] 311–331 0.8–8.1 320 AnTVLcirValVis
Tetrahydropyran Nasrifar et al. [533] 263–353 0.4–11.1 3.5 SynVisPcTc
Thiamphenicol Li et al. [460] 313–333 18.5–47.4 n.a. AnTVcir
Thioxanthone Shamsipur et al. [619] 308–348 12.1–35.4 1 AnTValY
Titanocene dichloride Wang et al. [699] 337–337 17.9–30 88 AnPTSemY
Toluene Cheng et al. [230] 311–311 1.4–7.3 300 AnPTSemY
Lee et al. [449] 352–352 0.1–3 n.a. AnT
Wu et al. [709] 323–386 11.1–15.5 14 SynVis
Zhang et al. [735] 304–335 7.4–10.5 20–50 SynVisVarTc
Tributyrin Florusse et al. [301] 278–368 1.9–14.3 3.5 SynVisVar
Tricaproin Florusse et al. [301] 278–368 1.8–14.3 3.5 SynVisVar
Tricaprylin Florusse et al. [301] 278–368 1.3–14.5 3.5 SynVisVar
Trichloromethane (HCC-20) Scurto et al. [606] 303–333 1–9.8 n.a. AnTVisVar
Scurto et al. [606] 303–333 1–9.8 5.4 SynVisPc
Tridecafluorooctyl 2,5-dichlorobenzoate Shen et al. [628] 295–375 5.8–20.1 30 SynVisVar
Triethylamine Ribeiro and Aguiar-Ricardo [586] 307–336 7.6–10.3 5 SynNonPcTc
Trifluoromethane (HFC-23) Di Nicola et al. [142] 252–285 1.5–3.8 251 SynOth
Triiodomethane Fernandez et al. [294] 272–373 0.6–30 n.a. AnSpecY
Trioctylamin Powell and Beckman [571] 295–295 5.6–8.6 n.a. SynVisVar
Triolein Chen et al. [222] 313–333 10.1–24.2 n.a. SynOthVLcirVis
Tripalmitin Rovetto et al. [592] 351–450 3.6–11.2 3.5 SynVis
Triphenylene Yamini and Bahramifar [722] 308–348 12.1–35.4 1 AnTValY
Triphenylmethane Pauchon et al. [75] 308–328 6.5–28.3 12 AnPTSemYVal
Triphenylphosphine Wagner et al. [37] 300–330 7.3–30.4 10 AnTVcirVal
Triple tail Fluoroalkyl Powell and Beckman [571] 295–295 7–14.6 n.a. SynVisVar
tris(2-Perfluorobutyl ethyl)tin fluoride Shi et al. [629] 297–297 14.5–17.5 100 SynVisVar
tris(Pentafluorophenyl)phosphine Wagner et al. [37] 300–320 6.9–12 10 AnTVcirVal
tris(p-Fluorophenyl)phosphine) Wagner et al. [37] 300–320 7–18.9 10 AnTVcirVal
Troeger’s base Ren et al. [584] 308–328 8–19 0.8 AnPTSemY
Undec-10-en-1-ol Petrova et al. [562] 313–333 1.6–13.5 4.0–14.0 SynVisVar
Undecan-2-ol Petrova et al. [562] 313–333 1.3–13.1 4.0–14.0 SynVisVar
Undecan-6-ol Petrova et al. [562] 313–333 2.4–11.6 4.0–14.0 SynVisVar
Undecanoic acid Scheidgen and Schneider [603] 273–393 0–100 80 AnT
Undecanolide Mishima et al. [515] 308–318 9.1–25.3 210 AnPTSemY
Uracil Burgos-Solórzano et al. [194] 313–333 10–29.9 32 AnTVcirValVis
Uranyl-thenoyltrifluoroaceton-tributhyl phosphate Wai and Waller [696] 313–313 10–32 3.5 or 15 AnTVal
(UO2(TTA)2 * TBP)
Uranyl-thenoyltrifluoroaceton-tributylphosphine Wai and Waller [696] 313–313 10–32 3.5 or 15 AnTVal
oxide (UO2(TTA)2 * TBPO)
Uranyl-thenoyltrifluoroaceton-triethyl phosphate Wai and Waller [696] 313–313 10–32 3.5 or 15 AnTVal
(UO2(TTA)2 * TEP)
Uranyl-thenoyltrifluoroaceton-trioctylphosphine Wai and Waller [696] 313–313 10–32 3.5 or 15 AnTVal
oxide (UO2(TTA)2 * TOPO)
22 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 4 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Uranyl-thenoyltrifluoroaceton-water (UO2(TTA) * Wai and Waller [696] 313–313 10–32 3.5 or 15 AnTVal
2H2O)
Valeric acid Byun et al. [195] 313–393 2.5–20.7 28 SynVisVar
Vanillic acid Murga et al. [529] 313–333 8.5–50 4.4 AnPTSemY
Stassi et al. [652] 313–328 8.6–25 125 AnPTSemY
Vanillin Fukné-Kokot et al. [107] 343–353 0.1–19.7 14 SynVis
Fukné-Kokot et al. [107] 343–353 0.1–17.4 20 SynTVis
Fukné-Kokot et al. [304] 343–353 0.1–17.4 20 SynTVis
Vinyl acetate Byun and Shin [200] 313–393 2.4–12.6 28 SynVisVarPc
Vinyl acrylate Byun and Shin [200] 318–398 4.6–13.8 28 SynVisVarPc
Vitamin D2 Knez and Skerget [425] 303–353 7.9–30.2 120 AnT
Knez and Skerget [425] 336–382 0.2–27.2 14 SynVis
Vitamin D3 Knez and Skerget [425] 313–353 9.7–29.8 120 AnT
Knez and Skerget [425] 411–352 0.3–30.1 14 SynVis
Vitamin K3 Knez and Skerget [425] 313–353 8.1–30.7 120 AnT
Knez and Skerget [425] 347–379 0.2–31.7 14 SynVis
Water Addicks et al. [147] 293–293 1–2.5 450 AnTVarVis
Anderson [151] 274–288 0–2.1 1119 SynT
Bamberger et al. [61] 323–351 4–14.1 38 AnPTCon
Chapoy et al. [217] 274–351 0.1–9.3 n.a. SynNonVar
Jarne et al. [381] 251–288 0.1–4.1 n.a. AnPTSemY
Jarne et al. [381] 251–288 0.1–4.1 n.a. SynVis
Kiepe et al. [134] 313–393 0–9.2 n.a. SynT
Li et al. [461] 332–332 3.3–19.8 500 AnTVar
Mooijer-van den Heuvel et al. [521] 276–286 1.8–7.3 n.a. SynVis
Servio and Englezos [614] 273–283 2–6 n.a. AnTVis
Valtz et al. [688] 278–318 0.4–7.9 28 AnTValVis
Yang et al. [729] 277–280 4.9–14.2 n.a. AnTVcirVisVar
Zatsepina and Buffett [126] 271–281 2.8–3 n.a. SynNon
Weyburn formation brine Li et al. [461] 332–332 1.7–20.8 500 AnTVar
Xenon Ribeiro et al. [585] 282–299 5.9–7.2 5 SynNonPcTc
XMPA refrigeration oil Skripov et al. [645] 890–890 7–7 n.a. SynNonPcTc
Zopiclone Medina and Bueno [510] 313–333 10–25 15 AnPTSemY

Table 5
Binary systems: water + X.

1,8-Cineol (1,8-epoxy-p-menthane or eucalyptol) Miller and Hawthorne [513] 298–473 6.4–6.8 10.4 AnPTSemY
1-Octanol Brown et al. [190] 354–542 6.8–6.8 20 SynVisVar
2,2,4-Trimethylpentane Miller and Hawthorne [514] 298–473 6.5–6.5 10.4 AnPTSemY
2-Methylpropane (isobutane) Tian et al. [669] 625–695 25.7–306 60.1 SynVis
Acetophenone Brown et al. [190] 339–502 6.8–6.8 20 SynVisVar
Air Mohammadi et al. [91] 274–283 17–45.1 150 SynNon
Ammonia Munakata et al. [526] 310–400 0.5–4.5 n.a. SynNonVar
Anisole Brown et al. [190] 344–551 6.8–8.1 20 SynVisVar
Benzene Jou and Mather [392] 279–453 0–2 n.a. AnTLcirVis
Marche et al. [497] 343–424 1.7–1.7 530 AnT
Mathis et al. [502] 298–473 5–5 10 AnT
Miller and Hawthorne [514] 298–473 0.1–40 10.4 AnPTSemY
Black oil A—Westport Technology Center Ivanic et al. [128] 287–293 6.6–16.8 300 SynNon
Black oil B—Westport Technology Center Ivanic et al. [128] 279–284 3–7.8 300 SynNon
Black oil C—Westport Technology Center Ivanic et al. [128] 282–286 4.6–16.3 300 SynNon
Carbon dioxide Addicks et al. [147] 293–293 1–2.5 450 AnTVarVis
Anderson [151] 274–288 0–2.1 1119 SynT
Bamberger et al. [61] 323–351 4–14.1 38 AnPTCon
Chapoy et al. [217] 274–351 0.1–9.3 n.a. SynNonVar
Jarne et al. [381] 251–288 0.1–4.1 n.a. AnPTSemY
Jarne et al. [381] 251–288 0.1–4.1 n.a. SynVis
Kiepe et al. [134] 313–393 0–9.2 n.a. SynT
Li et al. [461] 332–332 3.3–19.8 500 AnTVar
Mooijer-van den Heuvel et al. [521] 276–286 1.8–7.3 n.a. SynVis
Servio and Englezos [614] 273–283 2–6 n.a. AnTVis
Valtz et al. [688] 278–318 0.4–7.9 28 AnTValVis
Yang et al. [729] 277–280 4.9–14.2 n.a. AnTVcirVisVar
Zatsepina and Buffett [126] 271–281 2.8–3 n.a. SynNon
Carvone (p-mentha-6,8-dien-2-one) Miller and Hawthorne [513] 298–473 6.1–6.5 10.4 AnPTSemY
Cesium chloride Matsuo et al. [504] 273–313 0.1–400 n.a. AnTVar
Copoly(PNIPAAM/VS) Azevedo et al. [156] 310–319 0.1–40 n.a. SynVis
Cyclohexane Marche et al. [497] 343–424 1.7–1.7 530 AnT
Deuterium oxide Bazaev et al. [165] 517–680 3.5–37.4 n.a. SynOthPcTc
d-Limonene ((R)-p-mentha-1,8,diene) Miller and Hawthorne [513] 298–473 6.9–7.2 10.4 AnPTSemY
Ethane Chapoy et al. [215] 278–303 0.3–4.6 34 AnTVal
Kim et al. [422] 277–298 1.4–20.1 n.a. SynVisVar
Mohammadi et al. [518] 274–343 0.3–4.9 34 AnTValVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 23

Table 5 (Continued )

Mohammadi et al. [519] 282–293 0.5–2.9 34 AnTValVis

Morita et al. [523] 298–323 89–479 0.2 SynVisSpec
Song et al. [647] 201–281 3.4–3.4 n.a. AnPTSemY
Wang et al. [700] 283–303 0.5–4 600 AnTVal
Ethyl acetate Hu et al. [364] 523–647 3.9–22.1 18 SynVis
Ethylbenzene Haruki et al. [349] 553–583 10.4–26.4 31 AnPTConVis
Mathis et al. [502] 298–473 5–5 10 AnT
Eugenol (4-allyl-2-methoxyphenol) Miller and Hawthorne [513] 298–473 6.4–6.9 10.4 AnPTSemY
Glycine Matsuo et al. [505] 298–298 0.1–400 n.a. AnTVar
Hydrogen Morris et al. [93] 460–583 4.2–15.5 n.a. AnOth
l-Alanine Matsuo et al. [505] 298–298 0.1–400 n.a. AnTVar
l-Isoleucine Matsuo et al. [505] 298–298 0.1–400 n.a. AnTVar
Lithium sulfate Abdulagatov and Azizov [146] 423–573 0.4–8.5 95.5 SynT
l-Leucine Matsuo et al. [505] 298–298 0.1–400 n.a. AnTVar
l-Valine Matsuo et al. [505] 298–298 0.1–400 n.a. AnTVar
Methane Addicks et al. [147] 298–298 7.3–17.8 450 AnTVarVis
Chapoy et al. [214] 283–318 0.9–34.6 34 AnTVal
Chapoy et al. [214] 283–293 10–35 34 AnTVal
Chapoy et al. [218] 275–313 0.9–17.9 34 AnTVal
Chapoy et al. [220] 283–318 0.9–34.6 34 AnTVal
Chapoy et al. [220] 283–293 10–35 34 AnTVal
Huo et al. [367] 275–275 30–30 1 AnTSpec
Kharrat and Dalmazzone [412] 281–284 5.7–7.7 n.a. SynNon
Kiepe et al. [415] 313–373 0–9.2 n.a. SynT
Kim et al. [422] 276–298 2.3–16.6 n.a. SynVisVar
Link et al. [102] 278–293 8.6–9.6 40 SynVis
Mohammadi et al. [519] 282–313 2–0.5 34 AnTValVis
Mohammadi et al. [91] 278–278 4.7–4.7 150 SynNon
Ohmura et al. [547] 273–281 2.6–5.7 201 SynNon
Servio and Englezos [615] 274–284 3.5–6.5 n.a. AnTVis
Song et al. [647] 196–270 3.4–6.9 n.a. AnPTSemY
Wang et al. [700] 283–303 2–40 540 AnTVLcirVar
Yang et al. [730] 298–298 2.3–12.6 n.a. AnTVcirVisVar
Yang et al. [730] 273–286 3.6–19.3 n.a. AnTVcirVisVar
Methanol Bazaev et al. [166] 373–673 0–90.9 n.a. SynOthPcTc
Yokoyama and Uematsu [733] 320–420 0–1.3 16–24 SynNonVar
m-Xylene Mathis et al. [502] 298–473 5–5 10 AnT
Miller and Hawthorne [514] 298–473 6–6 10.4 AnPTSemY
Na2 SO4 Hodes et al. [354] 342–362 25–25 n.a. SynVisCon
Natural near critical reservoir fluid (C1–C20+) Ostergaard et al. [551] 277–288 1–13.9 540 SynVis
n-Butane Tian et al. [669] 622–695 23.2–306 60.1 SynVis
n-Decane Haruki et al. [63] 573–593 12.1–30.3 31 AnPTConVis
Shimoyama et al. [634] 573–593 15–20 31 AnPTConVis
Nerol (cis-3,7-dimethyl-2,6-octadien-1-ol) Miller and Hawthorne [513] 298–473 6.8–7 10.4 AnPTSemY
n-Heptyltetraoxyethylene (C7E4) Rudolph et al. [594] 315–331 3.5–98.9 n.a. SynVis
n-Hexane Abdulagatov et al. [145] 643–651 8–35 n.a. SynOthPcTc
Kamilov et al. [399] 395–494 0.6–5.2 n.a. SynNon
n-Hexyltetraoxyethylene (C6E4) Rudolph et al. [594] 339–352 3.7–99.3 n.a. SynVis
Nitrogen Chapoy et al. [216] 274–363 0.9–7.1 28 AnTValVis
Mohammadi et al. [91] 274–283 19–45.3 150 SynNon
n-Octane Miller and Hawthorne [514] 298–473 6.5–6.5 10.4 AnPTSemY
n-Pentane Jou and Mather [48] 273–453 0–3.6 n.a. AnTVcir
Oxygen Mohammadi et al. [91] 273–284 13.5–43.7 150 SynNon
Tan et al. [69] 300–300 1–10 500 AnPTSemX
p-Cymene Miller and Hawthorne [514] 298–473 6–6 10.4 AnPTSemY
poly(ethylene) 68 000 Fang et al. [98] 298–943 110–2600 0.00005 SynVisSpec
Poly(N-isopropylacrylamide) (PNIPAAM) Azevedo et al. [156] 305–321 0.1–40 n.a. SynVis
Potassium sulfate Hodes et al. [354] 373–382 25–25 n.a. SynVisCon
Propane Chapoy et al. [219] 277–368 0.3–3.9 28 AnTValVis
Makogon [495] 278–278 0.5–35 160–210 SynVisVar
Mooijer-van et al. [522] 276–278 0.3–9.8 n.a. SynVis
Song et al. [647] 211–276 0.8–1.1 n.a. AnPTSemY
p-Xylene Haruki et al. [349] 553–583 10.2–26.5 31 AnPTConVis
Jou and Mather [392] 288–448 0–1.1 n.a. AnTLcirVis
Silicone dioxide Sue et al. [30] 573–673 34.5–39.9 17.4 AnTBlo
Sodium sulfate Valyashko et al. [122] 590–647 0–0 101 SynNon
Synthethic natural gas Jarne et al. [380] 244–288 0.1–4.1 n.a. SynVis
Synthetic Green Canyon gas Ivanic et al. [128] 288–296 4–14 300 SynNon
Synthetic natural gas Avila et al. [155] 224–270 0.2–7.3 n.a. AnPTCon
Avila et al. [155] 224–270 0.2–7.3 n.a. SynVis
Tetrafluoromethane (CFC-14) Sugahara et al. [655] 276–317 7.4–317 0.2 SynVisSpec
Toluene Brown et al. [190] 340–524 6.8–6.8 20 SynVisVar
Haruki et al. [349] 573–583 10.5–15.3 31 AnPTConVis
Haruki et al. [63] 553–573 15.1–30.5 31 AnPTConVis
Jou and Mather [392] 273–458 0–1.7 n.a. AnTLcirVis
Kiselev et al. [424] 623–673 11.4–39.1 n.a. SynOthPcTc
Miller and Hawthorne [514] 298–473 5–5 10.4 AnPTSemY
Rabezkii et al. [574] 630–641 19.4–28.8 n.a. SynOthPcTc
Xenon Ohgaki et al. [545] 283–320 0.9–69 n.a. SynVis
24 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 6
Binary systems: ammonia + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Potassium iodide Brandt et al. [187] 134–668 1.9–76.2 n.a. SynVisVarPcTc

Sodium bromide Brandt et al. [187] 404–408 11–11.9 n.a. SynVisVarPcTc
Sodium iodide Brandt et al. [187] 406–408 11.5–11.8 n.a. SynVisVarPcTc
Sodium thiocyanate Brandt et al. [187] 409–409 11.9–12 n.a. SynVisVarPcTc
Water Munakata et al. [526] 310–400 0.5–4.5 n.a. SynNonVar

Table 7
Binary systems: hydrogen sulfide + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Benzene Fischer et al. [296] 304–323 0.1–1.2 n.a. SynT

Carbonyl sulfide Guilbot et al. [343] 232–293 0.1–1.7 30 SynVis
Guilbot et al. [343] 366–378 6.3–8.9 10 SynVisConPcTc
Diethylene glycol (DEG) Jou et al. [388] 298–398 0–7.4 n.a. AnTVcir
N-Methyldiethanolamine (MDEA) Kamps et al. [400] 313–353 0.1–2.7 30 SynVis
N-Octyl-2-pyrrolidone Fischer et al. [296] 306–323 0.1–1.1 n.a. SynT

Table 8
Binary systems: hydrogen + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Butanol d’Angelo and Francesconi [242] 295–524 3.9–8.8 1128 SynT

1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 298–298 0–1.3 n.a. AnGrav
1-Propanol d’Angelo and Francesconi [242] 299–513 3.6–10.1 1128 SynT
␣-Methylbenzyl alcohol Giles and Wilson [330] 323–423 3.4–10.3 2000 AnT
␣-Methylstyrene Phiong and Lucien [54] 308–323 3–13 60 AnTLcirX
Carbon dioxide Bezanehtak et al. [173] 278–290 4.8–19.2 60 AnTLcirVal
Ke et al. [411] 296–303 9.1–13.8 n.a. SynNonPcTc
Cumene Phiong and Lucien [54] 323–323 1–11.7 60 AnTLcirX
Cyclohexane Ronze et al. [590] 304–373 0.1–4.6 300 AnTVal
Ethanol d’Angelo and Francesconi [242] 299–476 3.7–9 1128 SynT
Gasoil Ronze et al. [590] 298–645 0.2–5.6 300 AnTVal
Methanol Bezanehtak et al. [173] 278–308 2–11 60 AnTLcirVal
d’Angelo and Francesconi [242] 314–476 4.4–10.9 1128 SynT
Methyl palmitate Rovetto et al. [593] 361–450 3.5–14.2 3.5 SynVisVar
n-Decane Florusse et al. [300] 283–450 1.2–14.2 n.a. SynVis
n-Hexadecane Florusse et al. [300] 298–448 1.1–15.1 n.a. SynVis
n-Hexane Gao et al. [318] 504–505 3–3.1 50 SynVisVarPcTc
Gao et al. [319] 344–410 1.2–6.2 25 SynT
n-Octacosane Florusse et al. [300] 342–447 1.4–14 n.a. SynVis
Water Morris et al. [93] 460–583 4.2–15.5 n.a. AnOth

Table 9
Binary systems: nitrogen + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 298–298 0–1.3 n.a. AnGrav
2-Methyltetrahydrofuran Fischer and Wilken [129] 311–311 0–9 n.a. SynT
␣-Pinene Laursen et al. [50] 298–318 3.1–14.5 90 AnTVcirX
Dimethyl ether Laursen et al. [38] 298–318 0.6–10.3 570 AnTValVis
Teodorescu Rasmussen [666] 278–318 0.4–8.4 700 AnTVal
Dimethylether Wallbruch et al. [697] 160–276 20.4–200 n.a. SynVisVar
Ethane Raabe et al. [53] 209–270 1.1–9 n.a. AnTLcirBlo
Raabe and Köhler [573] 114–138 0.7–3.2 n.a. AnTLcirBlo
Ethanol Fischer and Wilken [129] 298–398 0–9.2 n.a. SynT
Methanol Laursen and Andersen [434] 298–318 0.6–3 570 AnTValVis
1-Propanol Fischer and Wilken [129] 298–398 0–9.9 n.a. SynT
Oleic acid Laursen et al. [50] 298–318 3.2–14.6 90 AnTVcirX
Poly(ethylene glycol) 1500 Wiesmet et al. [33] 323–373 4.9–19.2 1000 AnTCap
Poly(ethylene glycol) 4000 Wiesmet et al. [33] 338–373 6.2–20 1000 AnTCap
Poly(ethylene glycol) 8000 Wiesmet et al. [33] 353–393 5.8–17.8 1000 AnTCap
Poly(ethylene) (LDPE) Davis et al. [252] 423–423 0.6–6.5 72 SynT
Polyvinylidene fluoride Grolier et al. [341] 411–436 0.1–190 36.3 SynNon
Vitamin K3 Knez and Skerget [425] 377–383 0.6–27.6 14 SynVis
Water Chapoy et al. [216] 274–363 0.9–7.1 28 AnTValVis
Mohammadi et al. [91] 274–283 19–45.3 150 SynNon
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 25

Table 10
Binary systems: oxygen + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 298–298 0–1.3 n.a. AnGrav
Acetonitrile (ethanenitrile) Horstmann et al. [362] 305–353 0–2.6 n.a. SynT
Dibutyl ether Fischer and Wilken [129] 298–298 0–2.1 n.a. SynT
Methanol Fischer and Wilken [129] 298–348 0–9.1 n.a. SynT
n-Octane Fischer and Wilken [129] 298–348 0–8.9 n.a. SynT
1-Propanol Fischer and Wilken [129] 298–348 0–9.2 n.a. SynT
Toluene Fischer and Wilken [129] 298–348 0–9 n.a. SynT
Water Mohammadi et al. [91] 273–284 13.5–43.7 150 SynNon
Tan et al. [69] 300–300 1–10 500 AnPTSemX

Table 11
Binary systems: carbon monoxide + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 298–298 0–1.3 n.a. AnGrav
Carbon dioxide Ke et al. [411] 280–298 8.1–9.9 n.a. SynNonPcTc
Cyclohexane Gao et al. [319] 344–410 1.5–5.1 25 SynT
Dichloromethane (HCC-30) Jónasson et al. [386] 303–363 0.4–7 700 AnTVal
n-Hexane Gao et al. [318] 501–505 3–3.3 50 SynVisVarPcTc

Table 12
Binary systems: nitrous oxide + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Biphenyl Fischer et al. [297] 388–413 0.1–13.2 n.a. SynNon

Fischer et al. [297] 352–352 0–13.6 n.a. SynVis
C.I. Disperse modified Yellow 119 Lin et al. [472] 353–393 15–30 16.6 AnPTSemY
C.I. Disperse Red 60 Tuma et al. [678] 310–310 7–130 n.a. SynVisSpec
Dimethylterephthalate Fischer et al. [297] 314–342 0.1–7.5 n.a. SynNon
Fischer et al. [297] 419–419 0–14.3 n.a. SynVis
Fluoromethane (HFC-41) Di Nicola et al. [266] 283–345 0.1–4.9 105 SynOth

Table 13
Binary systems: methane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 298–298 0–1.3 n.a. AnGrav
2-Ethyl-hexyl-C8C10 Bureau et al. [193] 363–423 30–60 n.a. AnTVar
2-Ethyl-hexyl-oleate Bureau et al. [193] 363–423 35–70 n.a. AnTVar
Bureau et al. [193] 363–423 70–100 220 AnTVisVar
Acenaphthene Tobaly et al. [672] 398–453 4.6–144.1 2.4–9.3 AnSpecVar
Carbon dioxide Webster and Kidney [703] 230–270 0.8–8.4 n.a. AnTVcir
cis-Decahydronaphthaline (decalin) Tohidi et al. [674] 323–423 34.6–66.1 1 SynVis
Decalin Tobaly et al. [672] 294–423 0.1–76.7 2.4–9.3 AnSpecVar
Ethane Raabe et al. [53] 239–270 1.5–6.6 n.a. AnTLcirBlo
Ethanol Ukai et al. [681] 280–280 1.5–5.6 134 SynOthX
Isobutyl-C12C14 Bureau et al. [193] 363–423 30–60 n.a. AnTVar
Methanol Ukai et al. [681] 280–280 2.1–6 134 SynOthX
Xia et al. [719] 298–298 5.4–12 200–360 AnTLcirVar
n-Butane Dandekar and Stenby [250] 311–344 11.5–12.6 80 SynVisVar
n-Hexane Cebola et al. [206] 348–383 2.3–19.6 n.a. AnTVLcirPc
Chylinski et al. [51] 348–348 2.2–11.6 650 AnTVLcirValVis
Uribe-Vargas and Trejo [682] 338–338 0.3–10.3 n.a. AnTVal
Xia et al. [719] 310–310 2.1–6 200–360 AnTLcirVar
Propane May et al. [507] 290–293 5.3–8.6 n.a. SynNonVcirVar
Webster and Kidney [703] 230–270 0–9.2 n.a. AnTVcir
Tetracosane Randzio et al. [125] 317–322 30–103.8 n.a. SynNon
Triacontane Machado and de Loos [488] 337–472 1.6–193.1 n.a. SynVisPcTc
Water Addicks et al. [147] 298–298 7.3–17.8 450 AnTVarVis
Chapoy et al. [214] 283–318 0.9–34.6 34 AnTVal
Chapoy et al. [214] 283–293 10–35 34 AnTVal
26 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 13 (Continued )

X Reference T (K) P (MPa) V (cm3 ) Method

Chapoy et al. [218] 275–313 0.9–17.9 34 AnTVal

Chapoy et al. [220] 283–318 0.9–34.6 34 AnTVal
Chapoy et al. [220] 283–293 10–35 34 AnTVal
Huo et al. [367] 275–275 30–30 1 AnTSpec
Kharrat and Dalmazzone [412] 281–284 5.7–7.7 n.a. SynNon
Kiepe et al. [415] 313–373 0–9.2 n.a. SynT
Kim et al. [422] 276–298 2.3–16.6 n.a. SynVisVar
Link et al. [102] 278–293 8.6–9.6 40 SynVis
Mohammadi et al. [519] 282–313 2–0.5 34 AnTValVis
Mohammadi et al. [91] 278–278 4.7–4.7 150 SynNon
Ohmura et al. [547] 273–281 2.6–5.7 201 SynNon
Servio and Englezos [615] 274–284 3.5–6.5 n.a. AnTVis
Song et al. [647] 196–270 3.4–6.9 n.a. AnPTSemY
Wang et al. [700] 283–303 2–40 540 AnTVLcirVar
Yang et al. [730] 298–298 2.3–12.6 n.a. AnTVcirVisVar
Yang et al. [730] 273–286 3.6–19.3 n.a. AnTVcirVisVar

Table 14
Binary systems: ethane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Butanol Kodama et al. [428] 313–313 2.3–5.4 320 AnTVLcirVal

1-Decanol Gardeler et al. [324] 448–448 0.5–14.3 n.a. AnTVal
1-Methylnaphthalene Shaver et al. [626] 344–344 0.1–14.2 n.a. AnTVcirVal
1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 283–283 0–1.3 n.a. AnGrav
1-Propanol Kodama et al. [426] 314–314 1.6–5.5 320 AnTVLcirVal
2-Propanol (isopropanol) Kodama et al. [427] 308–313 2.1–5.3 320 AnTVLcirVal
Acetone Mu et al. [524] 309–309 4.8–4.9 20–50 SynVisVarTc
Adamantane Poot and de Loos [568] 293–505 0.3–192.1 n.a. SynVisPcTc
Carbon dioxide Horstmann et al. [356] 291–305 4.9–6.8 10 SynVisPcTc
Horstmann et al. [358] 298–300 5.1–6.8 10 SynVisTc
Eicosane Gregorowicz [340] 310–370 3.4–12.4 43 AnPTSemY
Ethanol Mu et al. [524] 309–309 5–5.1 20–50 SynVisVarTc
Hydrogen chloride Florusse and Peters [299] 278–324 2.7–8.2 3.5 SynVis
Lemon oil de la Fuente and Bottini [255] 298–308 0.4–4.9 40–80 SynVisVar
Limonene Raeissi and Peters [576] 283–357 3.1–6.1 n.a. SynVisPcTc
Raeissi and Peters [579] 273–372 0.5–10.5 3.5 SynVis
Linalool Raeissi et al. [577] 278–368 2.6–11.4 3.5 SynVis
Raeissi and Peters [578] 280–350 3–6 3.5 SynVis
Methane Raabe et al. [53] 239–270 1.5–6.6 n.a. AnTLcirBlo
N.N-Dimethylformamide Duran-Valencia et al. [277] 264–313 0.5–18.2 n.a. AnTVal
n-Butane Horstmann et al. [357] 305–424 3.7–5.8 10 SynVisTc
n-Decane Gardeler et al. [324] 410–444 0.7–11.4 n.a. AnTVal
Singh et al. [643] 309–324 5.3–6.5 55 SynVisPcTc
N-Formyl morpholine Jou et al. [391] 298–403 0–20.3 n.a. AnTVcir
Jou et al. [391] 298–403 0–20.3 n.a. AnTVcir
n-Heptane Singh et al. [643] 310–325 5.2–6.4 55 SynVisPcTc
n-Hexadecane du Rand and Nieuwoudt [273] 312–352 4.9–10.5 132 SynVis
n-Hexane Singh et al. [643] 308–324 5.1–6 55 SynVisPcTc
Nitrogen Raabe et al. [53] 209–270 1.1–9 n.a. AnTLcirBlo
Raabe and Köhler [573] 114–138 0.7–3.2 n.a. AnTLcirBlo
Nitrous oxide Horstmann et al. [357] 299–309 4.8–7.2 10 SynVisTc
n-Nonane Singh et al. [643] 312–327 5.4–6.5 55 SynVisPcTc
n-Octacosane du Rand and Nieuwoudt [273] 337–352 4.9–10.5 132 SynVis
n-Octane Singh et al. [643] 308–326 5.1–6.4 55 SynVisPcTc
n-Pentane Mu et al. [525] 309–309 3.1–5 73 SynNonPcTc
Singh et al. [643] 306–324 4.9–5.8 55 SynVisPcTc
n-Tetracosane du Rand and Nieuwoudt [273] 332–352 9.3–14.4 132 SynVis
Orange peel oil de Sousa et al. [256] 282–363 1–7.3 3.5 SynVis
de Sousa et al. [256] 282–363 1.3–9.9 3.5 SynVis
Raeissi and Peters [580] 284–363 3.1–7.3 3.5 SynVis
Poly(propylene glycol) Martin et al. [500] 295–373 6–30 50 SynVisVar
Propane Horstmann et al. [357] 305–369 4.2–5 10 SynVisTc
Squalane Nanu et al. [532] 248–472 0.3–16.2 n.a. SynVis
Sulfur hexafluoride SF6 Horstmann et al. [358] 300–312 3.9–4.6 10 SynVisTc
Tetracosane Gregorowicz [339] 310–350 5.4–12.2 43 AnPTSemY
Water Chapoy et al. [215] 278–303 0.3–4.6 34 AnTVal
Kim et al. [422] 277–298 1.4–20.1 n.a. SynVisVar
Mohammadi et al. [518] 274–343 0.3–4.9 34 AnTValVis
Mohammadi et al. [519] 282–293 0.5–2.9 34 AnTValVis
Morita et al. [523] 298–323 89–479 0.2 SynVisSpec
Song et al. [647] 201–281 3.4–3.4 n.a. AnPTSemY
Wang et al. [700] 283–303 0.5–4 600 AnTVal
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 27

Table 15
Binary systems: propane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,2-Pentafluoroethane (HFC-125) Bobbo et al. [184] 258–303 0.2–1.8 n.a. AnTVcirVis

Kim et al. [420] 253–323 0.2–2.8 150 AnTVcirVis
Lim et al. [468] 268–313 0.4–2.2 85 AnTVLcirVis
Park and Jung [558] 273–313 0.4–2 128 AnTVcir
Takagi et al. [118] 243–333 0.2–3.8 n.a. SynNon
1,1,1,2,3,3,3-Heptafluoropropane (HFC-227ea) Bobbo et al. [182] 278–308 0.2–1.2 50 AnTVcirVis
Valtz et al. [685] 293–353 0.4–3.3 n.a. AnTValVis
1,1,1,2,3,3-Hexafluoropropane (HFC-236ea) Bobbo et al. [179] 283–313 0.1–1.3 50 AnTVcirVis
1,1,1,3,3,3-Hexafluoropropane (HFC-236fa) Bobbo et al. [180] 283–323 0.1–1.7 50 AnTVcirVis
1,2,3,4-Tetrahydronaphthalene Marteau et al. [499] 394–419 2.9–7 2.4–9.3 AnSpecVar
1-Decanol Gardeler et al. [324] 408–448 0.3–6.2 n.a. AnTVal
1-Methylnaphthalene Marteau et al. [499] 394–444 0.7–7.3 2.4–9.3 AnSpecVar
2-Methylpropane (isobutane) Lim et al. [467] 273–303 0.1–1 85 AnTVLcirVis
Adamantane Poot and de Loos [568] 301–503 0.3–10 n.a. SynVisPcTc
␣-Tocopherol Skerget et al. [644] 303–353 9.6–31.1 120 AnT
Carbon dioxide May et al. [117] 310–310 2.7–2.8 185 SynNonVcirVar
Smejkal et al. [646] 295–354 6.2–8.4 35 SynVisPcTc
Webster and Kidney [703] 230–270 0–3.1 n.a. AnTVcir
Cyclobutanone Cruz Duarte et al. [238] 277–368 0.4–3.8 3.5 SynVis
Decahydronaphthalene (decalin) Tobaly et al. [673] 392–439 1.7–7.7 2.4–9.3 AnSpecVisVar
Difluoromethane (HFC-32) Bobbo et al. [183] 248–294 0.2–1.9 n.a. AnTVcirVis
Coquelet et al. [26] 278–343 0.5–5.4 n.a. AnTValVis
Coquelet et al. [26] 342–344 5.2–5.5 n.a. AnTValVisVar
Kim et al. [421] 253–323 0.2–3.6 150 AnTVcirVis
Lee et al. [440] 268–318 0.4–3.2 85 AnTVLcirVis
Dimethyl ether Giles and Wilson [330] 273–323 0.2–1.7 300 SynT
Horstmann et al. [360] 313–313 0.9–1.3 n.a. AnTValVis
Horstmann et al. [360] 298–313 0.5–1.3 n.a. SynT
Dotriacontane Schwarz and Nieuwoudt [605] 378–408 4.6–9.3 40 SynVisVar
Ethane Horstmann et al. [357] 305–369 4.2–5 10 SynVisTc
Ethanol Joung et al. [396] 313–349 0.3–2.8 50 AnTVLcirValVis
Hexacontane Schwarz and Nieuwoudt [604] 378–408 8.2–14.2 40 SynVisVar
Hexatetracontane Schwarz and Nieuwoudt [604] 378–408 6.2–11.6 40 SynVisVar
Hexatriacontane Schwarz and Nieuwoudt [604] 378–408 4.3–9.9 40 SynVisVar
Methane May et al. [507] 290–293 5.3–8.6 n.a. SynNonVcirVar
Webster and Kidney [703] 230–270 0–9.2 n.a. AnTVcir
Methanol Joung et al. [396] 313–343 0.2–2.5 50 AnTVLcirValVis
Methyl palmitate Rovetto et al. [593] 312–450 1.2–9.7 3.5 SynVisVar
Naphthalene Tobaly et al. [673] 373–443 0.6–8.7 2.4–9.3 AnSpecVisVar
n-Dodecane Gardeler et al. [324] 419–457 0.4–7.6 n.a. AnTVal
Nitrous oxide Horstmann et al. [357] 309–369 4.2–7.2 10 SynVisTc
Octatriacontane Schwarz and Nieuwoudt [604] 378–408 4.6–10 40 SynVisVar
Poly (4-methyl styrene) Tan et al. [663] 303–453 36.3–132.9 10 SynVisVarPc
Poly(ethylene glycol) 1500 Wiesmet et al. [33] 323–393 0.1–18 1000 AnTCap
Poly(ethylene glycol) 200 Wiesmet et al. [33] 303–393 0.8–24.6 1000 AnTCap
Poly(ethylene glycol) 4000 Wiesmet et al. [33] 333–393 0.9–25 1000 AnTCap
Poly(ethylene glycol) 8000 Wiesmet et al. [33] 353–393 1.1–25 1000 AnTCap
Poly(ethylene-co-hexene-1) Chan et al. [211] 453–453 44.6–44.8 10 SynVisVarPc
Poly(ethylene-co-octene-1) Chan et al. [212] 302–453 18–140 10 SynVisVar
Poly(propylene) Oliveira et al. [549] 368–403 19–26.3 28 SynVisVar
Polystyrene Tan et al. [663] 303–453 35.7–154.6 10 SynVisVarPc
Squalane Nanu et al. [532] 263–473 0.1–11.9 n.a. SynVis
Sulfur hexafluoride SF6 Horstmann et al. [358] 318–369 3.7–4.2 10 SynVisTc
tert-Butyl mercaptan Giles and Wilson [330] 283–333 0–2.1 300 SynT
Tetracontane Chan et al. [213] 300–433 4.3–120.8 10 SynVisVar
Łuszczyk and Radosz [485] 312–435 2–118.9 10 SynVisVar
Schwarz and Nieuwoudt [604] 378–408 5.1–11 40 SynVisVar
Tetrapentacontane Schwarz and Nieuwoudt [604] 378–408 7.4–13.6 40 SynVisVar
Tetratetracontane Schwarz and Nieuwoudt [604] 378–408 5.2–11.4 40 SynVisVar
Titanocene dichloride Wang et al. [699] 383–408 10–35.2 88 AnPTSemY
Vitamin D2 Knez and Skerget [425] 303–353 0.4–10.9 120 AnT
Knez and Skerget [425] 323–378 0.8–26.5 14 SynVis
Vitamin D3 Knez and Skerget [425] 303–353 0.9–14.4 120 AnT
Knez and Skerget [425] 308–318 0.5–0.8 14 SynVis
Vitamin K3 Knez and Skerget [425] 313–353 1.1–10.6 120 AnT
Knez and Skerget [425] 367–375 0.7–26.5 14 SynVis
Water Chapoy et al. [219] 277–368 0.3–3.9 28 AnTValVis
Makogon [495] 278–278 0.5–35 160–210 SynVisVar
Mooijer-van et al. [522] 276–278 0.3–9.8 n.a. SynVis
Song et al. [647] 211–276 0.8–1.1 n.a. AnPTSemY
28 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 16
Binary systems: n-butane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1-Difluoroethane (HFC-152a) Shimawaki and Fujii [632] 283–313 0.1–2.4 163 AnTVLcirValVis
Adamantane Poot et al. [565] 285–493 0.2–5.7 n.a. SynVisVar
Diamantane Poot et al. [565] 343–523 0.8–6.9 n.a. SynVisVar
Ethane Horstmann et al. [357] 305–424 3.7–5.8 10 SynVisTc
Ethyl mercaptan Giles and Wilson [330] 323–373 0.1–1.5 300 SynT
Methane Dandekar and Stenby [250] 311–344 11.5–12.6 80 SynVisVar
Poly(propylene) Oliveira et al. [549] 358–423 1.2–11.4 28 SynVisVar
Poly(propylene) (metallocene) Ndiaye et al. [534] 358–423 1.7–11 27 SynVisVar
Poly(propylene) (Ziegler Natta) Ndiaye et al. [534] 358–423 1.7–11 27 SynVisVar
Water Tian et al. [669] 622–695 23.2–306 60.13 SynVis

Table 17
Binary systems: n-hexane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Propanol Oh et al. [543] 483–513 2–43.4 100 AnTVLcirValVisPc

2-Propanol (isopropanol) Seo et al. [611] 483–503 2.1–4.5 100 AnTVLcirVisPc
Carbon dioxide Liu et al. [473] 304–507 3–11.7 18 SynVis
Carbon monoxide Gao et al. [318] 501–505 3–3.3 50 SynVisVarPcTc
Ethane Singh et al. [643] 308–324 5.1–6 55 SynVisPcTc
Ethanol Seo et al. [609] 473–503 18.1–55.6 100 AnTVLcirVis
FCC-DO (PAHs mixture) Kim et al. [420] 493–553 1.1–4.3 100 AnPTConVis
Hexatriacontane Joyce et al. [397] 521–621 0.7–6.4 12 AnPTConVis
Hydrogen Gao et al. [318] 504–505 3–3.1 50 SynVisVarPcTc
Gao et al. [319] 344–410 1.2–6.2 25 SynT
Methane Cebola et al. [206] 348–383 2.3–19.6 n.a. AnTVLcirPc
Chylinski et al. [51] 348–348 2.2–11.6 650 AnTVLcirValVis
Uribe-Vargas and Trejo [682] 338–338 0.3–10.3 n.a. AnTVal
Xia et al. [719] 310–310 2.1–6 200–360 AnTLcirVar
Methanol Liu et al. [473] 480–512 3–8.1 18 SynVis
n-Hexadecane Belonenko et al. [169] 298–298 31–148 0.8 SynNonVar
Nitrobenzene Drozd-Rzoska et al. [114] 285–297 0–112 n.a. SynNon
Poly(ethylene) (LDPE) Chen et al. [229] 393–473 0.6–7.2 6–20 SynVisVar
Poly(ethylene) 108k Chen et al. [229] 373–473 0.4–8.2 6–20 SynVisVar
Poly(ethylene) 15k Chen et al. [229] 373–473 0.4–4.7 6–20 SynVisVar
Tetracosane Joyce et al. [397] 473–622 0.6–5.1 12 AnPTConVis
Water Abdulagatov et al. [145] 643–651 8–35 n.a. SynOthPcTc
Kamilov et al. [399] 395–494 0.6–5.2 n.a. SynNon

Table 18
Binary systems: ethene + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Decanol Gardeler et al. [324] 308–318 1–12.4 n.a. AnTVal

1-n-Butyl-3-methylimidazolium hexafluorophosphate [bmim][PF6] Anthony et al. [83] 298–323 0–1.3 n.a. AnGrav
1-Propanol Kodama et al. [116] 283–283 2.2–5.4 320 AnTVLcirValVis
Kodama et al. [116] 283–283 5.1–5.7 78–134 SynNonVLcirVisVar
Benzene Liu et al. [478] 282–563 5–11.5 n.a. SynVisPcTc
Eicosane Gregorowicz [340] 287–348 4.6–15.8 43 AnPTSemY
Impact poly(propylene) copolymer (ICP–PP) Sato et al. [78] 323–363 0.3–3 90 SynT
N,N-Dimethylformamide Duran-Valencia et al. [277] 293–323 0.7–18.7 n.a. AnTVal
Poly(ethylene) Moore and Wanke [86] 301–361 0.1–3.5 n.a. AnGrav
Poly(ethylene) (LDPE) Davis et al. [252] 423–423 0.6–6.5 72 SynT
Poly(ethylene) (LLDPE) Trumpi et al. [675] 395–440 139.8–172.5 n.a. SynVis
Poly(ethylene-co-octene-1) Chan et al. [210] 385–453 18–166.8 10 SynVisVar
Poly(ethylene-co-propylene) de Vries et al. [257] 312–342 141.3–218.1 n.a. SynVis
Tetracosane Gregorowicz [339] 330–350 4.9–14 43 AnPTSemY
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 29

Table 19
Binary systems: propene + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2-Tetrafluoroethane (HFC-134a) Ho et al. [353] 273–313 0.2–1.9 85 AnTVLcirVis

2,2,4,6,6-Pentamethylheptane Dariva et al. [251] 299–328 0.1–0.5 23 SynT
Acetophenone Horstmann et al. [361] 323–323 0–2 n.a. SynT
Benzene Guo et al. [345] 453–543 1.5–6 500 AnTCap
Wang et al. [698] 364–562 4.6–6.7 18 SynVisPcTc
Carbon dioxide Ke et al. [411] 305–343 6–7.1 n.a. SynVisVarPcTc
Cumene Wang et al. [698] 562–631 3.3–4.8 18 SynVisPcTc
Dichloromethane (HCC-30) Jónasson et al. [386] 303–363 0.2–2 700 AnTVal
Dimethyl ether Horstmann et al. [360] 313–313 0.8–1.6 n.a. AnTValVis
Horstmann et al. [360] 313–313 0.8–1.6 n.a. SynT
Impact poly(propylene) copolymer (ICP–PP) Sato et al. [78] 323–363 0.2–3 90 SynT
Poly(propylene) Oliveira et al. [549] 368–388 22–26.7 28 SynVisVar
Sato et al. [78] 323–363 0.2–3.6 90 SynT
Toluene Dariva et al. [251] 299–328 0.1–0.5 23 SynT

Table 20
Binary systems: 1-butene + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Dichloromethane (HCC-30) Jónasson et al. [386] 303–363 0.1–1.1 700 AnTVal

Poly(ethylene) Moore and Wanke [86] 301–361 0.1–1.2 n.a. AnGrav
Poly(propylene) Oliveira et al. [549] 358–423 1.4–13.3 28 SynVisVar
Poly(propylene) (metallocene) Ndiaye et al. [534] 348–422 1.7–13.5 27 SynVisVar
Poly(propylene) (Ziegler Natta) Ndiaye et al. [534] 348–422 1.7–13.5 27 SynVisVar

Table 21
Binary systems: methanol + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Carbon dioxide Bezanehtak et al. [173] 278–308 1.5–7.4 60 AnTLcirVal

Elbaccouch and Elliot [279] 313–313 1.1–7.5 40 AnTVLcirVal
Joung et al. [394] 313–342 6–12.4 50 AnTVLcirValVisPc
Laursen et al. [38] 298–313 1.2–6.3 570 AnTValVis
Liu et al. [473] 304–512 7.4–16.3 18 SynVis
Yeo et al. [732] 298–423 5.8–16.4 26.7 SynVisVar
Dimethyl ether Teodorescu Rasmussen [666] 353–353 0.1–2.2 700 AnTVal
Hydrogen Bezanehtak et al. [173] 278–308 2–11 60 AnTLcirVal
d’Angelo [242] 314–476 4.4–10.9 1128 SynT
Methane Ukai et al. [681] 280–280 2.1–6 134 SynOthX
Xia et al. [719] 298–298 5.4–12 200–360 AnTLcirVar
n-Hexane Liu et al. [473] 480–512 3–8.1 18 SynVis
Nitrogen Laursen and Andersen [434] 298–318 0.6–3 570 AnTValVis
Oxygen Fischer and Wilken [129] 298–348 0–9.1 n.a. SynT
Propane Joung et al. [396] 313–343 0.2–2.5 50 AnTVLcirValVis
Water Bazaev et al. [166] 373–673 0–90.9 n.a. SynOthPcTc
Yokoyama and Uematsu [733] 320–420 0–1.3 16–24 SynNonVar

Table 22
Binary systems: ethanol + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Butyl-3-methylimidazoium hexyfluorophosphate [bmim][PF6] Najdanovic-Visak et al. [103] 284–325 0.1–40.1 1 SynVisVar

Acetic acid (ethanoic acid) Hu et al. [364] 516–590 5.7–7.5 18 SynVis
Carbon dioxide Bae et al. [158] 314–314 5.5–7.9 25 SynVisVar
Chen et al. [223] 323–323 5–8.2 100 AnTVcirVis
Elbaccouch and Elliot [279] 323–333 0.7–9.4 40 AnTVLcirVal
Galicia-Luna et al. [47] 312–373 0.4–14.3 40 AnTCapValVis
Joung et al. [394] 313–344 5.4–11.9 50 AnTVLcirValVisPc
Stuart et al. [654] 313–313 4.8–7.5 28 SynVisVar
Tsivintzelis et al. [676] 313–328 1.6–9.4 202.1 AnTVLcirValVis
Vega-Gonzalez et al. [692] 314–324 7–8.2 9 SynVisVar
Yeo et al. [732] 298–413 6.1–15.1 26.71 SynVisVar
Chlorodifluoromethane (HCFC-22) Elbaccouch and Elliot [279] 343–382 0.5–4.8 40 AnTVLcirVal
Cyclohexanone oxime Dahlhoff et al. [248] 300–463 0–2.2 70 SynT
Dimethyl ether Elbaccouch et al. [280] 332–373 0.1–3.1 40 AnTVLcirVal
Ethane Mu et al. [524] 309–309 5–5.1 20–50 SynVisVarTc
Ethyl acetate Hu et al. [364] 515–523 3.9–6.2 18 SynVis
Hydrogen d’Angelo and Francesconi [242] 299–476 3.7–9 1128 SynT
Methane Ukai et al. [681] 280–280 1.5–5.6 134 SynOthX
n-Heptane Seo et al. [610] 483–523 1.1–5.6 100 AnTVLcirVis
n-Hexane Seo et al. [609] 473–503 18.1–55.6 100 AnTVLcirVis
Nitrogen Fischer and Wilken [129] 298–398 0–9.2 n.a. SynT
n-Pentane Seo et al. [608] 422–500 0.9–5.7 100 AnTVLcirVisPcTc
Propane Joung et al. [396] 313–349 0.3–2.8 50 AnTVLcirValVis
30 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 23
Binary systems: dimethyl ether + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,2-Pentafluoroethane (HFC-125) Bobbo et al. [184] 258–303 0.1–1.5 n.a. AnTVcirVis

1,1,1,2,3,3-Hexafluoropropane (HFC-236ea) Bobbo et al. [179] 283–313 0.1–0.8 50 AnTVcirVis
1,1,1,3,3,3-Hexafluoropropane (HFC-236fa) Bobbo et al. [179] 283–283 0.1–0.3 50 AnTVcirVis
2-Methylpropane (isobutane) Bobbo et al. [176] 280–320 0.2–1 50 AnTVcirVis
2-Propanol (isopropanol) Elbaccouch and Elliot [281] 323–373 0.1–1.5 40 AnTVLcirVal
Argon Wallbruch et al. [697] 157–267 23.5–202 n.a. SynVisVar
Carbon dioxide Laursen et al. [38] 298–320 0.6–7.3 570 AnTValVis
Ethanol Elbaccouch et al. [280] 332–373 0.1–3.1 40 AnTVLcirVal
Ethyl cellulose Li and McHugh [458] 314–432 1–20 28 SynVisVar
Krypton Wallbruch et al. [697] 130–149 20.6–138 n.a. SynVisVar
Methanol Teodorescu Rasmussen [666] 353–353 0.1–2.2 700 AnTVal
Nitrogen Laursen et al. [38] 298–318 0.6–10.3 570 AnTValVis
Teodorescu Rasmussen [666] 278–318 0.4–8.4 700 AnTVal
Nitrogen Wallbruch et al. [697] 160–276 20.4–200 n.a. SynVisVar
n-Propyl acetate Daiguji and Hihara [249] 253–443 0.1–3.9 156 SynT
Poly(d,l-lactide) Kuk et al. [431] 327–375 1.6–13.8 31 SynVisVar
Poly(d,l-lactide-co-glycolide) Kuk et al. [431] 303–373 8.5–61.3 31 SynVisVar
Propane Giles and Wilson [330] 273–323 0.2–1.7 300 SynT
Horstmann et al. [360] 313–313 0.9–1.3 n.a. AnTValVis
Horstmann et al. [360] 298–313 0.5–1.3 n.a. SynT
Propene Horstmann et al. [360] 313–313 0.8–1.6 n.a. AnTValVis
Horstmann et al. [360] 313–313 0.8–1.6 n.a. SynT
Tripalmitin Florusse et al. [298] 288–450 0.9–10 3.5 SynVis
Vitamin D2 Knez and Skerget [425] 378–380 0.3–0.6 14 SynVis
Vitamin D3 Knez and Skerget [425] 289–289 0.3–0.3 14 SynVis
Vitamin K3 Knez and Skerget [425] 341–366 0.8–1.6 14 SynVis
Xenon Wallbruch et al. [697] 130–206 19.2–167 n.a. SynVisVar

Table 24
Binary systems: chlorodifluoromethane (HCFC-22) + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Ethanol Elbaccouch and Elliot [279] 343–382 0.5–4.8 40 AnTVLcirVal

Ethyl cellulose Li and McHugh [458] 305–403 2–26 28 SynVisVar
Poly(d,l-lactide) Kuk et al. [432] 338–383 3–15.6 31 SynVisVar
Lee et al. [443] 346–392 4.2–15.7 31 SynVisVar
Poly(d,l-lactide-co-glycolide) Lee et al. [443] 313–383 3.4–31.4 31 SynVisVar
Poly(dimethylsiloxane) (PDMS) Pfohl et al. [132] 298–343 0–0.2 345 SynTVis
Poly(l-lactide) Lee et al. [443] 334–393 3.2–20.2 31 SynVisVar
Poly(methyl methacrylate) (PMMA) Boudouris et al. [44] 308–348 0.1–2 n.a. AnOth
Polystyrene Boudouris et al. [44] 308–358 0.1–3.9 n.a. AnOth

Table 25
Binary systems: trifluoromethane (HFC-23) + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,2-Pentafluoroethane (HFC-125) Lim et al. [463] 283–293 0.9–4.1 85 AnTVLcirVis

1,1,1,2,3,3,3-Heptafluoropropane (HFC-227ea) Lim et al. [464] 283–293 0.2–4.2 85 AnTVLcirValVis
1,1,1,2-Tetrafluoroethane (HFC-134a) Lim et al. [464] 283–293 0.4–4.2 85 AnTVLcirValVis
1,1,1-Trifluoroethane (HFC-143a) Lim et al. [465] 283–293 0.8–4.2 85 AnTVLcirValVis
1,1-Difluoroethane (HFC-152a) Lim et al. [465] 283–293 0.3–4.2 85 AnTVLcirValVis
1-Ethyl-3-methylimidazolium hexafluorophosphate Shariati and Peters [622] 308–367 1.6–51.6 3.5 SynVisVar
Carbon dioxide Di Nicola et al. [142] 252–285 1.5–3.8 251 SynOth
Difluoromethane (HFC-32) Lim et al. [463] 283–293 1.1–4.1 85 AnTVLcirVis
Naphthalene Diefenbacher and Türk [267] 345–346 9.2–20.6 1310 SynVis
Poly(d,l-lactide) Kuk et al. [432] 303–373 49–84.7 31 SynVisVar
Sulphur hexafluoride Diefenbacher and Türk [268] 265–295 1.6–4.3 1406 AnTVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 31

Table 26
Binary systems: difluoromethane (HFC-32) + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,2-Pentafluoroethane (HFC-125) Horstmann et al. [359] 308–308 1.7–2.1 n.a. SynT

Jung et al. [398] 268–308 0.5–2.1 128 AnTVcir
Kato et al. [407] 318–349 2.3–5.5 n.a. AnTVisPcTc
Kato et al. [408] 318–349 2.3–5.5 n.a. AnTVisPcTc
Weber [702] 294–333 1.4–3.9 550 AnTVLcir
1,1,1,2,3,3,3-Heptafluoropropane (HFC-227ea) Koo et al. [429] 298–312 0.4–2.4 320 AnTVLcirValVis
Park et al. [555] 283–303 0.2–1.9 85 AnTVLcirVis
1,1,1,2,3,3-Hexafluoropropane (HFC-236ea) Bobbo et al. [177] 288–318 0.1–2.7 50 AnTVcirVis
Deiters [258] Comments
Di Nicola et al. [261] 254–364 0.1–1.9 254.8 SynT
1,1,1,2-Tetrafluoroethane (HFC-134a) Lim et al. [462] 303–323 0.7–3.1 85 AnTVLcirValVis
1,1,1-Trifluoroethane (HFC-143a) Kim and Park [419] 263–313 0.4–2.4 128 AnTVcirVis
Anthracene Abbott et al. [94] 363–363 7.9–22 25 AnOth
␤-Carotene Hansen et al. [348] 313–343 5.8–26.2 n.a. AnSpecY
Capsaicin Hansen et al. [348] 328–358 5.5–14.8 n.a. AnPTSemYVal
Carbon dioxide Di Nicola et al. [263] 287–294 1.3–3.5 254.8 SynT
Diefenbacher and Türk [101] 304–351 5.7–7.4 1406 SynVisPcTc
Diefenbacher and Türk [268] 280–318 1.6–7.5 1406 SynVisPcTc
Rivollet et al. [587] 283–343 1.1–7.4 n.a. AnTValVis
Ethyl cellulose Li and McHugh [458] 392–450 75–115 28 SynVisVar
m-Hydroxybenzoic acid Abbott et al. [94] 363–363 8.9–25.2 25 AnOth
o-Chlorobenzoic acid Abbott et al. [94] 363–363 10–24.8 25 AnOth
p-Aminobenzoic acid Abbott et al. [94] 363–363 6.9–22 25 AnOth
p-Aminophenol Abbott et al. [94] 363–363 8.9–18.8 25 AnOth
p-Chlorobenzoic acid Abbott et al. [94] 363–363 13.5–22.1 25 AnOth
p-Chlorophenol Abbott et al. [94] 363–363 12.2–25.8 25 AnOth
Pentaerythritol tetra-2-ethylbutanoate Wahlström and Vamling [695] 323–363 0.1–1.7 n.a. AnT
Pentaerythritol tetra-2-ethylhexanoate Wahlström and Vamling [695] 303–363 0.1–1.7 n.a. AnT
Pentaerythritol tetranonanoate Wahlström and Vamling [695] 303–363 0.2–1.9 n.a. AnT
Perfluoropolyether lubricant oil Fomblin YLOX100 Tesser et al. [668] 238–323 0.1–3.1 n.a. SynOthVis
Perfluoropolyether lubricant oil Fluorolink D10H Tesser et al. [668] 239–277 0.1–0.1 n.a. SynOthVis
p-Hydroxybenzoic acid Abbott et al. [94] 363–363 8.9–24 25 AnOth
Poly(d,l-lactide) Kuk et al. [432] 305–375 33–55.5 31 SynVisVar
Propane Bobbo et al. [183] 248–294 0.2–1.9 n.a. AnTVcirVis
Coquelet et al. [26] 278–343 0.5–5.4 n.a. AnTValVis
Coquelet et al. [26] 342–344 5.2–5.5 n.a. AnTValVisVar
Kim et al. [421] 253–323 0.2–3.6 150 AnTVcirVis
Lee et al. [440] 268–318 0.4–3.2 85 AnTVLcirVis
p-Toluic acid Abbott et al. [94] 363–363 9–18 25 AnOth
Salicylic acid Abbott et al. [94] 363–363 14–24.1 25 AnOth
Sulphur dioxide Valtz et al. [35] 288–403 0.4–7.3 n.a. AnTCapValVis
Sulphur hexafluoride Diefenbacher and Türk [268] 265–310 1.2–3.9 1406 AnTVis
Trifluoromethane (HFC-23) Lim et al. [463] 283–293 1.1–4.1 85 AnTVLcirVis

Table 27
Binary systems: 1,1,1,2,2-pentafluoroethane (HFC-125) + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,3,3-Hexafluoropropane (HFC-236ea) Bobbo et al. [177] 288–318 0.1–2.2 50 AnTVcirVis

Deiters [258] Comments
Di Nicola et al. [261] 254–364 0.1–1.9 254.8 SynT
1,1,1,3,3,3-Hexafluoropropane (HFC-236fa) Di Nicola et al. [262] 253–372 0.1–2.3 254.8 SynT
1,1-difluoroethane (HFC-152a) Lim et al. [463] 293–293 0.5–1.2 85 AnTVLcirVis
2-Methylpropane (isobutane) Lee et al. [439] 293–313 0.3–2 80 AnTVLcirVal
Carbon dioxide Di Nicola et al. [263] 284–304 1.6–3.3 254.8 SynT
Difluoromethane (HFC-32) Horstmann et al. [359] 308–308 1.7–2.1 n.a. SynT
Jung et al. [398] 268–308 0.5–2.1 128 AnTVcir
Kato et al. [407] 318–349 2.3–5.5 n.a. AnTVisPcTc
Kato et al. [408] 318–349 2.3–5.5 n.a. AnTVisPcTc
Weber [702] 294–333 1.4–3.9 550 AnTVLcir
Dimethyl ether Bobbo et al. [184] 258–303 0.1–1.5 n.a. AnTVcirVis
Pentaerythritol tetra-2-ethylbutanoate Wahlström and Vamling [695] 323–36 0.1–1.7 n.a. AnT
Pentaerythritol tetra-2-ethylhexanoate Wahlström and Vamling [695] 303–363 0.1–1.8 n.a. AnT
Pentaerythritol tetranonanoate Wahlström and Vamling [695] 302–363 0–2.1 n.a. AnT
Pentafluoromethoxyethane Otake et al. [554] 339–406 2.8–3.7 16 SynVisVarPcTc
Perfluoropolyether lubricant oil fomblin ylox100 Tesser et al. [668] 273–313 0.1–1.8 n.a. SynOthVis
Propane Bobbo et al. [184] 258–303 0.2–1.8 n.a. AnTVcirVis
Kim et al. [420] 253–323 0.2–2.8 150 AnTVcirVis
Lim et al. [468] 268–313 0.4–2.2 85 AnTVLcirVis
Park and Jung [558] 273–313 0.4–2 128 AnTVcir
Takagi et al. [118] 243–333 0.2–3.8 n.a. SynNon
Trifluoromethane (HFC-23) Lim et al. [463] 283–293 0.9–4.1 85 AnTVLcirVis
Trifluoromethoxymethane Uchida et al. [680] 339–377 3.6–3.7 16 SynVisVarPcTc
Trifluoromethyl methyl ether (HFC-143m) Widiatmo et al. [706] 279–349 0.4–2.5 n.a. SynVisVar
32 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 28
Binary systems: 1,1,1,2-tetrafluoroethane (HFC-134a) + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,3,3,3-Heptafluoropropane (HFC-227ea) Koo et al. [429] 298–312 0.4–0.9 320 AnTVLcirValVis

Park et al. [555] 303–323 0.5–1.3 85 AnTVLcirVis
1,1,1,3,3,3-Hexafluoropropane (HFC-236fa) Di Nicola et al. [262] 253–372 0.1–2.3 254.8 SynT
1,1,1,3,3-Pentafluoropropane (HFC-245fa) Bobbo et al. [181] 293–313 0.1–1 50 AnTVcir
1,1,1-Trifluoroethane (HFC-143a) Kim et al. [49] 263–313 0.2–1.8 128 AnTVcirBloVis
Lim et al. [466] 273–313 0.2–1.8 85 AnTVLcirVis
1,1-Difluoroethane (HFC-152a) Shimawaki et al. [631] 263–293 0.2–1.3 163 AnTVLcirValVis
1-Chloro-2,2,2-trifluoroethane (HCFC-133a) He et al. [351] 300–357 0.2–2.6 25 SynVis
␤-Carotene Hansen et al. [348] 313–343 6.4–34.3 n.a. AnSpecY
Capsaicin Hansen et al. [348] 308–328 10.3–18.8 n.a. AnPTSemYVal
Carbon dioxide Duran-Valencia et al. [276] 252–292 0.1–2 50 AnTVal
Silva-Oliver et al. [641] 329–354 1.9–7.3 40 AnTValVis
Difluoromethane (HFC-32) Lim et al. [462] 303–323 0.7–3.1 85 AnTVLcirValVis
Heptylbenzene Poot and de Loos [566] 258–414 0.1–12.1 n.a. SynVis
Oleic acid Catchpole and Proells [205] 303–363 4–20 n.a. AnPTCon
Pentaerythritol tetra-2-ethylbutanoate Wahlström and Vamling [695] 323–363 0.1–1 n.a. AnT
Pentaerythritol tetra-2-ethylhexanoate Wahlström and Vamling [695] 303–363 0–1 n.a. AnT
Pentaerythritol tetranonanoate Wahlström and Vamling [695] 302–363 0.1–1.2 n.a. AnT
Pentafluoromethoxyethane Otake et al. [554] 374–406 2.8–4 16 SynVisVarPcTc
Perfluoropolyether lubricant oil Fomblin YLOX100 Tesser et al. [668] 239–323 0.1–1.2 n.a. SynOthVis
Perfluoropolyether lubricant oil Fluorolink D10H Tesser et al. [668] 239–248 0.1–0.1 n.a. SynOthVis
Phenyloctane Poot and de Loos [567] 259–398 0.1–12.4 n.a. SynVisPcTc
Poly(d,l-lactide) Kuk et al. [432] 302–373 21.7–40.1 31 SynVisVar
Polyalkylene glycol Park et al. [559] 253–333 0–1.6 72 SynVis
Propene Ho et al. [353] 273–313 0.2–1.9 85 AnTVLcirVis
Squalene Catchpole and Proells [205] 303–353 6–6 n.a. AnPTCon
Triethylene glycol dimethyl ether Coronas et al. [237] 283–353 0–2.2 149 SynT
Trifluoromethane (HFC-23) Lim et al. [464] 283–293 0.4–4.2 85 AnTVLcirValVis
Trifluoromethoxymethane Uchida et al. [680] 374–377 3.6–4 16 SynVisVarPcTc
Trifluoromethyl methyl ether (HFC-143m) Widiatmo et al. [706] 279–349 0.3–2.3 n.a. SynVisVar

Table 29
Binary systems: 1,1,1-trifluoroethane (HFC-143a) + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2-Tetrafluoroethane (HFC-134a) Lim et al. [466] 273–313 0.2–1.8 85 AnTVLcirVis

Kim et al. [49] 263–313 0.2–1.8 128 AnTVcirBloVis
1,1,1,3,3,3-Hexafluoropropane (HFC-236fa) Bobbo et al. [178] 283–313 0.1–1.8 50 AnTVcirVis
1,1-Difluoroethane (HFC-152a) Lim et al. [466] 273–313 0.2–1.8 85 AnTVLcirVis
2-Methylpropane (isobutane) Lim et al. [462] 323–333 0.6–2.8 85 AnTVLcirValVis
␤-Carotene Hansen et al. [348] 313–343 6.1–33.2 n.a. AnSpecY
Difluoromethane (HFC-32) Kim and Park [419] 263–313 0.4–2.4 128 AnTVcirVis
Pentaerythritol tetra-2-ethylbutanoate Wahlström and Vamling [695] 323–363 0.1–1.9 n.a. AnT
Pentaerythritol tetra-2-ethylhexanoate Wahlström and Vamling [695] 303–363 0.1–1.8 n.a. AnT
Pentaerythritol tetranonanoate Wahlström and Vamling [695] 303–363 0.1–1.9 n.a. AnT
Perfluoropolyether lubricant oil Fomblin YLOX100 Tesser et al. [668] 237–323 0.1–2.2 n.a. SynOthVis
Perfluoropolyether lubricant oil Fluorolink D10H Tesser et al. [668] 239–239 0.1–0.1 n.a. SynOthVis
Trifluoromethane (HFC-23) Lim et al. [465] 283–293 0.8–4.2 85 AnTVLcirValVis

Table 30
Binary systems: 1,1-difluoroethane (HFC-152a) + X.

X References. T (K) P (MPa) V (cm3 ) Method

1,1,1,2,2-Pentafluoroethane (HFC-125) Lim et al. [463] 293–293 0.5–1.2 85 AnTVLcirVis

1,1,1,2,3,3,3-Heptafluoropropane (HFC-227ea) Park et al. [555] 283–303 0.2–0.6 85 AnTVLcirVis
1,1,1,2-Tetrafluoroethane (HFC-134a) Shimawaki et al. [631] 263–293 0.2–1.3 163 AnTVLcirValVis
1,1,1-Trifluoroethane (HFC-143a) Lim and McHugh et al. [466] 273–313 0.2–1.8 85 AnTVLcirVis
Ethyl cellulose Li and McHugh [458] 392–450 55–78 28 SynVisVar
n-Butane Shimawaki and Fujii [632] 283–313 0.1–2.4 163 AnTVLcirValVis
Pentaerythritol tetranonanoate Wahlström and Vamling [695] 303–363 0.1–1 n.a. AnT
Poly(methyl methacrylate) (PMMA) Boudouris et al. [44] 308–348 0.1–1.7 n.a. AnOth
Polystyrene Boudouris et al. [44] 308–348 0.1–1.7 n.a. AnOth
Trifluoromethane (HFC-23) Lim et al. [465] 283–293 0.3–4.2 85 AnTVLcirValVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 33

Table 31
Binary systems: X + Y.

X Y Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2,3,3,3-Heptafluoropropane 2-Methylpropane (isobutane) Lee et al. [439] 303–323 0.4–1 80 AnTVLcirVal

(HFC-227ea)
Pentafluoromethoxyethane Otake et al. [554] 375–406 2.8–2.9 16 SynVisVarPcTc
1,1,1,2,3,3-Hexafluoropropane Pentafluoromethoxyethane Otake et al. [554] 406–412 2.8–3.4 16 SynVisVarPcTc
(HFC-236ea)
1-Chloro-1,1-difluoroethane Ethyl cellulose Li and McHugh [458] 340–430 20–82 28 SynVisVar
1-Hexene Poly(ethylene) Moore and Wanke [86] 301–361 0.1–0.2 n.a. AnGrav
2-Methyl-1-propanol (isobutanol) 1-Butyl-3-methylimidazoium Najdanovic-Visak et al. [103] 284–303 0.1–4.4 1 SynVisVar
bis(trifluoromethylsulfonyl)amide
[bmim][NTf2]
2-Methylpropane (isobutane) 1,1,1,3,3-Pentafluoropropane Bobbo et al. [181] 293–313 0.1–0.6 50 AnTVcir
(HFC-245fa)
Acetonitrile (ethanenitrile) Uusi-Kyyny and Liukkonen [683] 358–358 0.1–1.4 66 AnTLcirVal
Diamantane van Miltenburg et al. [690] 328–503 0.7–7.8 n.a. SynVis
2-Methylpropene Acetonitrile (ethanenitrile) Uusi-Kyyny and Liukkonen [683] 358–358 0.1–1.3 66 AnTLcirVal
Acetone Titanyl phthalocyanine Sue et al. [30] 508–553 4.7–26.1 17.4 AnTBlo
Argon 1-n-Butyl-3-methylimidazolium Anthony et al. [83] 298–298 0–1.3 n.a. AnGrav
hexafluorophosphate [bmim][PF6]
Vitamin K3 Knez and Skerget [425] 375–378 0.7–19.8 14 SynVis
Benzene Cumene Wang et al. [698] 364–631 3.3–8 18 SynVisPcTc
Ethylbenzene Al-Ghamdi and Kabadi [150] 453–553 0.3–4.2 590 AnPTCon
Chlorotrifluoromethane (CFC-13) 1-Amino-4-hydroxy-2-phenoxy- Tuma et al. [678] 310–310 7–130 n.a. SynVisSpec
9,10-anthraquinone (C, I, Disperse
Red 60)
Cyclohexane Eicosane Domanska and Morawski [269] 313–363 16.2–523.1 n.a. SynNonVar
n-Hexadecane Domanska and Morawski [269] 293–353 9.2–678.2 n.a. SynNonVar
n-Octadecane Domanska and Morawski [269] 303–353 11.2–455.1 n.a. SynNonVar
n-Tridecane Domanska and Morawski [269] 293–353 23.3–932.7 n.a. SynNonVar
Deuterium Deuterium oxide Morris et al. [93] 446–583 10.3–10.3 n.a. AnOth
Ethylbenzene Quinoline Zhao and Kabadi [743] 498–653 0.1–3.4 590 AnPTCon
Helium Biphenyl Fischer et al. [297] 342–352 0–30 n.a. SynNon
Dimethylterephthalate Fischer et al. [297] 413–425 0–39.9 n.a. SynNon
Methyl 1,1-dimethylethyl ether n-Eicosane Domanska and Morawski [115] 313–353 12.2–980 n.a. SynNonVar
n-Octacosane Domanska and Morawski [115] 313–353 50.1–1090 n.a. SynNonVar
n-Decane Polystyrene Imre et al. [373] 284–288 0.1–100 n.a. SynVis
n-Dodecane 1-Octanol Yang et al. [728] 263–293 20.1–174.7 n.a. SynVis
Polystyrene Imre et al. [373] 293–300 0.1–100 n.a. SynVis
n-Heptane 2-Propanol (isopropanol) Oh et al. [544] 483–523 1.1–4.7 100 AnTVLcirVis
n-Hexadecane 1-Octanol Yang et al. et al. [100] 275–332 5.3–230.9 n.a. SynVis
n-Hexane 1-Propanol Oh et al. [543] 483–513 2–43.4 100 AnTVLcirValVisPc
n-Octane 1-Octanol Yang et al. [728] 262–292 47.1–201 n.a. SynVis
Polystyrene Imre et al. [373] 275–279 0.1–100 n.a. SynVis
n-Pentane Poly(dimethylsiloxane) (PDMS) Pfohl et al. [132] 308–423 0–1.5 345 SynTVis
n-Tetradecane 1-Octanol Yang et al. [100] 263–313 16.1–178.5 n.a. SynVis
Polystyrene Imre et al. [373] 302–306 0.1–100 n.a. SynVis
n-Tridecane n-Alkane mixture Daridon et al. [106] 301–321 0.1–99.3 0.03 SynVis
n-Tetradecane Daridon et al. [106] 270–290 0.1–99.8 0.03 SynVis
Perdeuterated nitroethane Polystyrene perdeuterated 90 000 de Sousa and Rebelo [109] 308–312 0.2–6.3 1 SynVis
Polystyrene perprotonated 90 000 de Sousa and Rebelo [109] 336–341 0.3–4.9 1 SynVis
Perprotonated nitroethane Polystyrene perdeuterated 90 000 de Sousa and Rebelo [109] 286–288 0.2–5.2 1 SynVis
Polystyrene perprotonated 13 000 de Sousa and Rebelo [109] 265–345 0.1–6.5 1 SynVis
Polystyrene perprotonated 130 000 de Sousa and Rebelo [109] 318–323 0.1–6.1 1 SynVis
Polystyrene perprotonated 26 600 de Sousa and Rebelo [109] 268–270 0.3–5.3 1 SynVis
Polystyrene perprotonated 30 000 de Sousa and Rebelo [109] 289–298 0–5.6 1 SynVis
Polystyrene perprotonated 90 000 de Sousa and Rebelo [109] 309–317 0.1–5.3 1 SynVis
Poly(dimethylsiloxane) Poly(hexylmethylsiloxane) Imre et al. [374] 320–379 0.1–120 n.a. SynVis
Propylene oxide 2-Methylpentane Horstmann et al. [359] 323–323 0–0.1 n.a. SynT
Sulfur dioxide 1,1,1,2,3,3,3-Heptafluoropropane Valtz et al. [689] 288–403 0.2–5.5 n.a. AnTValVis
(HFC-227ea)
Sulfur hexafluoride 1-Amino-4-hydroxy-2-phenoxy- Tuma et al. [678] 310–310 7–130 n.a. SynVisSpec
9,10-anthraquinone (C,I, Disperse
Red 60)
Tetralin quinoline Mahmood et al. [62] 598–643 0.5–1.5 590 AnPTCon
Trifluoroacetic acid Hydrogen chloride Giles and Wilson [330] 258–278 0–2.9 300 SynT
Trifluoromethane (HFC-23) 2-Methylpropane (isobutane) Lim et al. [462] 283–293 0.2–4.2 85 AnTVLcirValVis
Trifluoromethoxymethane 1,1,1,2,3,3,3-Heptafluoropropane Uchida et al. [680] 375–377 2.9–3.6 16 SynVisVarPcTc
(HFC-227ea)
1,1,1,2,3,3-Hexafluoropropane Uchida et al. [680] 377–412 3.4–3.6 16 SynVisVarPcTc
(HFC-236ea)
Vinylidene fluoride Polyvinylidene fluoride Grolier et al. [341] 408–445 0.1–190 36.3 SynNon
34 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 32
Ternary systems: carbon dioxide + water + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,4-Dioxane Lazzaroni et al. [436] 313–313 2.8–5.7 n.a. SynVisVar

1-Butanol Chen et al. [224] 333–353 6–8 100 AnTVcirVis
1-Butyl-3-methylimidazolium tetrafluoroborate Zhang et al. [742] 278–297 3.5–16 50 AnTBloVis
2,3,4,5-Tetrachlorophenol Curren and Burk [241] 314–314 10–27 105 AnTVal
2,4-Dichlorophenoxyacetic acid Curren and Burk [241] 313–313 10–27 105 AnTVal
2-Amino-2-ethyl-1,3-propanediol Park et al. [557] 313–333 0–2.8 450 AnTVal
2-Amino-2-hydroxymethyl-1,3-Propanediol Park et al. [556] 313–333 0–1.8 450 AnTVal
2-Methoxyacetophenone Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
3-Buten-2-one Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
3-Methoxyacetophenone Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
3-Methyl-1-butanol (isopentanol) Lee et al. [442] 313–313 2–8.3 n.a. AnTVLcirVal
3-Methyl-2-butanol Lee et al. [442] 313–313 2–8.2 n.a. AnTVLcirVal
Acetic acid (ethanoic acid) Bamberger et al. [161] 313–353 6–15 38 AnPTCon
Acetonitrile (ethanenitrile) Lazzaroni et al. [436] 313–313 1.9–5.2 n.a. SynVisVar
Acetophenone Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Acetylacetone Gervais et al. [326] 323–323 27–27 280 AnTVal
Ammonium acetate Xia et al. [712] 313–433 0.1–9.6 30 SynVis
Xia et al. [716] 313–433 0.1–9.6 30 SynVis
Benzaldehyde Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Benzene Brandt et al. [186] 303–605 1.9–304 40 SynVisVar
Bis(2,2,3,3,4,4,5,5-octafluoro-1-pentyl)-2-sulfosuccinate Dong et al. [111] 288–329 6–36 54 SynVis
Bromobenzene Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Chlorobenzene Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Cobalt(II) diacetylacetonate Gervais et al. [326] 323–323 27–27 280 AnTVal
Cobalt(II) dihexafluoroacetylacetonate Gervais et al. [326] 323–323 27–27 280 AnTVal
Cobalt(III) diethyldithiocarbamate Gervais et al. [326] 323–323 27–27 280 AnTVal
Cobalt(III) fluorodiethyldithiocarbamate Gervais et al. [326] 323–323 27–27 280 AnTVal
Copper(II) sulfate Clarke et al. [233] 273–286 0.7–4.3 n.a. SynVisVar
Cyclobutanone Mooijer-van den Heuvel et al. [521] 279–315 0.3–11.9 n.a. SynVis
Cyclohexane Mooijer-van den Heuvel et al. [521] 274–288 0.9–10.4 n.a. SynVis
Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Cyclohexene Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Cyclopentene Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Diethanolamine (DEA) Sidi-Boumedine et al. [637] 298–348 0–4.6 n.a. SynT
Dimethyl ether Laursen et al. [38] 298–318 0.5–6.1 570 AnTValVis
Ethanol Budich and Brunner [192] 333–333 10–10 800 AnTBlo
Chen et al. [223] 323–323 9–9 100 AnTVcirVis
Ethyl acetate Hu et al. [364] 304–546 7.1–14.9 18 SynVis
Ethylbenzoate Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Ethylene glycol Majumdar et al. [493] 264–276 1.2–3.1 n.a. SynVisVar
Fluorobenzene Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Hexafluoroacetylacetone Gervais et al. [326] 323–323 27–27 280 AnTVal
Magnesium sulfate (1:1) Clarke et al. [233] 275–280 1.8–3.8 n.a. SynVisVar
Methane Seo et al. [612] 273–285 1.5–6.7 50 AnTValVis
Methanol Jarne et al. [381] 246–289 0.1–4.3 n.a. AnPTSemY
Jarne et al. [381] 246–289 0.1–4.3 n.a. SynVis
Levitin et al. [454] 342–343 11.9–20 5–20 SynVisVar
Levitin et al. [455] 342–343 11.9–20 5–20 SynVisVar
Xia et al. [718] 313–395 0–9.7 30 SynVis
Methylbenzoate Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Methylcyclohexane Mooijer-van den Heuvel et al. [521] 277–280 1.8–11.3 n.a. SynVis
Monoethanolamine (MEA) Park et al. [557] 313–313 0–2.1 450 AnTVal
n-Hexane Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Nitrogen Kang et al. [404] 272–284 1.3–32.3 70 AnTValVis
N-methyldiethanolamine (MDEA) Addicks et al. [147] 313–313 1.1–4 450 AnTVarVis
Sidi-Boumedine et al. [637] 313–313 0.5–4.3 n.a. AnTVal
Sidi-Boumedine et al. [637] 298–348 0–4.5 n.a. SynT
Sidi-Boumedine et al. [637] 313–313 0–1.7 n.a. SynT
Palmitic acid Iwai et al. [376] 313–313 15–15 26.5 AnTVcirSpec
Pentachlorophenol Curren and Burk [241] 292–332 10.7–28 105 AnTVal
Piperazine Kamps et al. [402] 313–393 0–9.5 30 SynVis
Potassium chloride Kiepe et al. [134] 313–353 0–10.5 n.a. SynT
Potassium nitrate Clarke et al. [233] 275–278 1.8–3.5 n.a. SynVisVar
Kiepe et al. [416] 313–373 0–10.2 n.a. SynT
Propylbenzoate Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Sodium acetate Xia et al. [712] 313–433 0–9.7 30 SynVis
Xia et al. [716] 313–433 0–9.7 30 SynVis
Sodium chloride Bando et al. [162] 303–333 10–20 414 AnT
Kiepe et al. [134] 313–353 0–10.1 n.a. SynT
Sodium hydroxide Ziegler et al. [745] 295–295 8.1–48.5 28 AnSpec
Sodium nitrate Kiepe et al. [416] 313–373 0–10.6 n.a. SynT
Tetrahydrofuran Lazzaroni et al. [436] 298–333 0.9–5.2 n.a. SynVisVar
Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Tetrahydropyran Mooijer-van den Heuvel et al. [521] 280–291 0.4–4.2 n.a. SynVis
Toluene Timko et al. [671] 300–300 8–8 50 AnTVLcirValVis
Triisopropanolamine Chauhan et al. [221] 313–333 0–2.8 450 AnTVal
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 35

Table 33
Ternary systems: carbon dioxide + methanol + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,4-Naphthoquinone Ngo et al. [124] 313–313 8.9–12.2 n.a. SynNonSpec

1-Butyl-3-methylimidazolium hexafluorophosphate ([bmim][PF6]) Wu et al. [711] 313–313 15–15 55 AnPTSemYVis
1-Methylnaphthalene Gutiérrez and Luks [140] 288–313 4.7–8.3 7–9 SynOthVis
2-Methyl-2-butanol Lee et al. [442] 313–313 2–8.1 n.a. AnTVLcirVal
2-Naphthol Ngo et al. [124] 313–313 8.5–12.4 n.a. SynNonSpec
Carbon monoxide Zang et al. [737] 294–327 8.1–13 20–50 SynVisVar
Cholesterol Huang et al. [366] 318–328 10–24 20 AnPTSemY
Cholesteryl benzoate Huang et al. [366] 318–328 13–27 20 AnPTSemY
Dimethyl ether Teodorescu Rasmussen [666] 313–333 0.1–6.4 700 AnTVal
Ethyl cellulose Li and McHugh [458] 305–403 13–75 28 SynVisVar
Hydrogen Bezanehtak et al. [174] 278–298 2–20 60 AnTVLcirValVis
m-Hydoxybenzoic acid Bristow et al. [189] 318–318 8.5–20 n.a. AnPTSemYSpec
n-Hexane Liu et al. [473] 304–500 3.7–12.3 18 SynVis
n-Tetradecane Foreman and Luks [302] 293–313 5.5–8.5 7–9 SynVis
Sulfathiazole Kordikowski et al. [66] 298–353 10–20 10 AnPTSemYSpec
TCMTB (2-(thiocyanomethylthio) benzothiazole) Sahle-Demessie et al. [595] 323–338 10–30 43.92 AnPTSemYVis
Tebuconazole (R-[2-(4-chlorophenyl)ethyl]-R-(1,1-dimethylethyl)- Sahle-Demessie et al. [595] 323–338 10–30 43.92 AnPTSemYVis
1H-1,2,4-triazole-1-ethanol)
Water Jarne et al. [381] 246–289 0.1–4.3 n.a. AnPTSemY
Jarne et al. [381] 246–289 0.1–4.3 n.a. SynVis
Levitin et al. [454] 342–343 11.9–20 5–20 SynVisVar
Levitin et al. [455] 342–343 11.9–20 5–20 SynVisVar
Xia et al. [718] 313–395 0–9.7 30 SynVis

Table 34
Ternary systems: carbon dioxide + ethanol + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Butyl-3-methylimidazolium tetrafluoroborate ([bmim][BF4]) Wu et al. [711] 313–313 15–15 55 AnPTSemYVis

2-Naphthol Li et al. [459] 308–328 10–30 377 AnPTSemY
Acetaminophen Bristow et al. [189] 313–353 8–25 n.a. AnPTSemYSpec
Bristow et al. [189] 313–353 10.5–24.6 n.a. AnTVcirVal
Wubbolts et al. [95] 295–317 7–15 30 SynVisVar
Acetic acid (ethanoic acid) Hu et al. [364] 304–547 7.4–17.3 18 SynVis
Anthracene Li et al. [459] 308–328 10–30 377 AnPTSemY
␣-Tetralol (1,2,3,4-tetrahydro-1-naphtol) Borg et al. [185] 303–333 9.4–21.6 1.7–12.4 SynVisVar
␤-Carotene Sovova et al. [649] 313–333 15–28 12 AnPTSemY
Benzoic acid Jin et al. [385] 308–328 8–23 377 AnPTSemY
Catechin Berna et al. [65] 313–313 8–13 10 AnPTSemY
Coenzyme Q10 (ubiquinone) Matias et al. [503] 313–313 15–15 42.5 AntCapVal
Dimethyl ether Laursen and Andersen [435] 298–318 0.4–3.8 570 AnTVis
Eflucimibe Sauceau et al. [600] 308–318 9.8–30.3 n.a. AnPTSemY
Epicatechin Chafer et al. [208] 313–313 8–12 10 AnPTSemY
Ethyl cellulose Li and McHugh [457] 319–413 20–82 28 SynVisVar
Ferulic acid Sovova [651] 313–333 12–28 n.a. AnPTSemY
Flurbiprofen Duarte et al. [275] 313–313 18–18 30 AnTCapValVis
Griseofulvin De Gioannis et al. [254] 312–326 10–10 n.a. SynVisVar
o-aminobenzoic acid Liu et al. [480] 308–318 1.4–4.1 200 AnTVcirVis
Orange peel oil Drescher et al. [271] 333–333 5–10 3000 AnTCap
p-aminobenzoic acid Liu et al. [480] 308–318 1.9–6.5 200 AnTVcirVis
Polystyrene Tassaing et al. [665] 398–423 15–30 n.a. AnTVcirSpec
Quercetin Chafer et al. [209] 313–313 8–12 10 AnPTSemY
Resveratrol Berna et al. [172] 313–313 8–14 10 AnPTSemY
Water Budich and Brunner [192] 333–333 10–10 800 AnTBlo
Chen et al. [223] 323–323 9–9 100 AnTVcirVis

Table 35
Ternary systems: carbon dioxide + ethyl acetate + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Behenic acid Liu et al. [481] 318–318 2.7–8 200 AnTVcirVis

Benzoic acid Jin et al. [385] 308–328 8–23 377 AnPTSemY
o-Hydroxybenzoic acid Liu et al. [479] 308–318 2–8.5 200 AnTVcirBlo
p-Hydroxybenzoic acid Liu et al. [479] 308–318 2–8.5 200 AnTVcirBlo
Stearic acid Liu et al. [481] 308–318 2.8–7.8 200 AnTVcirVis
Tetradecanoic acid Liu et al. [481] 308–318 3.1–8.2 200 AnTVcirVis
Water Hu et al. [364] 304–546 7.1–14.9 18 SynVis
36 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 36
Ternary systems: carbon dioxide + dimethyl ether + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Propanol Laursen and Andersen [435] 298–318 0.4–3.5 570 AnTVis

Ethanol Laursen and Andersen [435] 298–318 0.4–3.8 570 AnTVis
Methanol Teodorescu Rasmussen [666] 313–333 0.1–6.4 700 AnTVal
Poly(d,l-lactide) Kuk et al. [431] 303–373 2.4–72.4 31 SynVisVar
Poly(l-lactide) 110 000 Lim et al. [469] 331–412 3.1–22.8 n.a. SynVisVar
Poly(l-lactide) 230 000 Lim et al. [469] 332–411 6.3–24.9 n.a. SynVisVar
Poly(l-lactide) 80 000 Lim et al. [469] 333–410 3.6–22.6 n.a. SynVisVar
Water Laursen et al. [38] 298–318 0.5–6.1 570 AnTValVis

Table 37
Ternary systems: carbon dioxide + acetone + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1-Methylnaphthalene Gutiérrez and Luks [347] 288–315 4.7–8.5 7–9 SynOthVis

2-(Thiocyanomethylthio) benzothiazole (TCMTB) Hassan et al. [141] 298–308 4–5.2 40 SynOthVis
2-Naphthol Li et al. [459] 308–328 10–30 377 AnPTSemY
Anthracene Li et al. [459] 308–328 10–30 377 AnPTSemY
Aspirin Huang et al. [365] 318–328 10–20 10 AnPTSemY
Cholesterol Huang et al. [366] 318–328 10–24 20 AnPTSemY
Liu et al. [482] 308–318 0.1–7.3 n.a. AnTVcirBlo
Cholesteryl benzoate Huang et al. [366] 318–328 13–27 20 AnPTSemY
Griseofulvin De Gioannis et al. [254] 312–326 6–10 n.a. SynVisVar
Limonene Corazza et al. [235] 313–343 5.3–10.5 25 SynVisVar
n-Pentane Chen et al. [227] 311–334 7.8–9.4 20–50 SynVisVarPcTc
n-Tetradecane Foreman and Luks [303] 294–313 5.5–8.5 7–9 SynVis
TCMTB (2-(thiocyanomethylthio) benzothiazole) Sahle-Demessie et al. [595] 323–338 10–30 43.9 AnPTSemYVis
Tebuconazole (R-[2-(4-chlorophenyl)ethyl]-R-(1,1-dimethylethyl)- Sahle-Demessie et al. [595] 323–338 10–30 43.9 AnPTSemYVis
1H-1,2,4-triazole-1-ethanol)

Table 38
Ternary systems: carbon dioxide + limonene + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,8-Cineole Cruz Francisco and Sivik [239] 313–333 8–25 30 AnPTSemY

Acetone Corazza et al. [235] 313–343 5.3–10.5 25 SynVisVar
Acetonitrile (ethanenitrile) Corazza et al. [235] 313–343 5.6–10.4 25 SynVisVar
Black currant seed oil Sovova et al. [72] 313–313 8–12 8 AnPTSemY
Carvone (p-mentha-6,8-dien-2-one) Corazza et al. [235] 313–343 7.9–12.4 25 SynVisVar
Citral Benvenuti and Gironi [170] 315–315 8.4–8.4 200 AnPTSemY
Fonseca et al. [59] 323–323 9.5–10.3 3.4 AnPTCon
Dichloromethane (HCC-30) Corazza et al. [235] 313–343 6.2–12.3 25 SynVisVar
Linalool Cháfer et al. [207] 318–328 7–11 10 AnPTSemY
Fonseca et al. [59] 323–323 8.7–9.4 3.4 AnPTCon
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 37

Table 39
Ternary systems: carbon dioxide + X + Y.

X Y Reference T (K) P (MPa) V (cm3 ) Method

1,1,1,2-Tetrafluoroethane (HFC-134a) Salicylic acid Abbott et al. [144] 323–343 12.1–29 n.a. AnOth
1,8-Cineole ␣-Pinene Cruz Francisco and Sivik 313–333 8–25 30 AnPTSemY
[239]
1-Butyl-3-methylimidazolium Acetonitrile (ethanenitrile) Wu et al. [711] 313–313 15–15 55 AnPTSemYVis
hexafluorophosphate ([bmim][PF6])
1-Decanol n-Tetradecane Scheidgen and Schneider 393–393 0–1000 80 AnT
[601]
Scheidgen and Schneider 280–316 5–61 80 AnT
[602]
1-Heptanol n-Pentadecane Scheidgen and Schneider 393–393 0–1000 80 AnT
[601]
Scheidgen and Schneider 281–384 5–95 80 AnT
[602]
1-Hexanol 1-Heptanol Scheidgen and Schneider 393–393 0–1000 80 AnT
[601]
n-Pentadecane Scheidgen and Schneider 272–297 5–90 80 AnT
[602]
n-Tetradecane Scheidgen and Schneider 393–393 0–1000 80 AnT
[601]
1-Hexene Carbon monoxide Ke et al. [410] 308–316 8–10.2 4 SynNonPcTc
1-n-Hexene Hydrogen Ke et al. [410] 312–320 8.8–10.9 4 SynNonPcTc
1-Octanol n-Hexadecane Scheidgen and Schneider 393–393 0–1000 80 AnT
[601]
1-Propanol Salicylic acid Shariati and Peters [105] 273–367 1–13.9 3.5 SynVisVar
2-Ethyl-1-hexanol 2-Ethyl hexanoic acid Ghaziaskar et al. [329] 313–343 13.8–13.8 10 AnPTSemY
2-Naphthol Cyclohexane Li et al. [459] 308–328 10–30 377 AnPTSemY
3,3,4,4,5,5,6,6-Octafluorooctan-1,8-diol Divinyl adipate Mesiano et al. [512] 323–323 9–15 n.a. SynVisVar
9-Nitroanthracene 2-Methylanthracene Yamini et al. [725] 308–348 12.2–35.5 0.5 AnTValY
␣-Linolenic acid Poly(ethylene glycol) Funazukuri et al. [308] 308–343 8.5–30.1 3.3 AnPTChro
Anthracene Cyclohexane Li et al. [459] 308–328 10–30 377 AnPTSemY
␣-Pinene Pinane Chouchi et al. [232] 323–323 9.3–9.3 50 SynVis
Arachidonic acid Poly(ethylene glycol) Funazukuri et al. [307] 308–343 9.5–30.2 3.3 AnPTChro
␣-Tocopherol Poly(ethylene glycol) Funazukuri et al. [77] 313–323 12.1–22 3.3 AnPTChro
Funazukuri et al. [306] 308–333 8.5–30.3 3.3 AnPTChro
␤-Carotene Grape seed oil Sovova et al. [649] 313–333 19–28.3 12 AnPTSemY
Poly(ethylene glycol) Funazukuri et al. [77] 313–323 12.1–23 3.3 AnPTChro
Funazukuri et al. [306] 308–333 9.1–30.2 3.3 AnPTChro
Funazukuri et al. [309] 313–313 16.1–16.1 3.2 AnPTChro
Butyl methacrylate Poly(butylmethacrylate) Byun and McHugh [104] 298–503 6–210 28 SynVisVar
C,I, Disperse Blue 134 C.I. Disperse Yellow 16 Tamura and Shinoda [662] 323–383 10–25 n.a. AnPTSemY
C,I, Disperse Orange 25 Poly(methyl methacrylate) Ngo et al. [535] 313–313 8.8–9.5 n.a. SynNonSpec
Carbon monoxide Hydrogen Ke et al. [411] 281–302 8.3–13.7 n.a. SynNonPcTc
Chlorodifluoromethane (HCFC-22) Poly(l-lactide) Lee et al. [444] 302–393 3.6–71.4 31 SynVisVar
Poly(l-lactide) 100 000 Lee et al. [438] 303–373 3.6–68.5 31 SynVisVar
Poly(l-lactide) 2000 Lee et al. [438] 302–372 3.6–71.4 31 SynVisVar
Poly(l-lactide) 50 000 Lee et al. [438] 303–373 4–64 31 SynVisVar
Clove oil Cellulosic structure Rodrigues et al. [588] 283–308 6.6–10 500 AnPTSemY
Coenzyme Q10 (ubiquinone) Poly(ethylene glycol) Funazukuri et al. [305] 308–328 8.5–30.1 3.3 AnPTChro
Cyclohexane Polybutadiene Joung et al. [395] 353–473 0.5–21.5 33 SynVisVar
Decanoic acid 1-Dodecanol Scheidgen and Schneider 273–393 0–100 80 AnT
[603]
n-Tetradecane Scheidgen and Schneider 273–393 0–100 80 AnT
[603]
Dichloromethane (HCC-30) Poly(l-lactide) Lee ad Kuk [437] 304–375 4.8–84.7 31 SynVisVar
Diethyl ether Cholesterol Wubbolts et al. [95] 292–314 7–10 30 SynVisVar
Dimethylsulfoxide Eflucimibe Sauceau et al. [600] 308–318 12.2–29.1 n.a. AnPTSemY
Diolein Poly(ethylene glycol) Funazukuri et al. [310] 313–313 10–25 3.2 AnPTChro
Docoahexaenoic acid Poly(ethylene glycol) Funazukuri et al. [308] 308–343 9.2–30.1 3.3 AnPTChro
Eicosapentaenoic acid Poly(ethylene glycol) Funazukuri et al. [308] 308–343 8.6–30.1 3.3 AnPTChro
Ethene Poly(ethylene-co-1-hexene) Dörr et al. [270] 393–493 118.6–168.3 14.5–19.0 SynVisVar
copolymer
Poly(ethylene-co-propylene) de Vries et al. [257] 312–342 171.8–213.2 n.a. SynVis
Poly(ethylene-co-vinyl Kinzl et al. [423] 393–493 108.3–130.3 14.5–19.0 SynVisVar
acetate) copolymer
Ethyl methacrylate Poly(ethylmethacrylate) Byun and McHugh [104] 298–488 25–100 28 SynVisVar
Eucalyptus oil Cellulosic structure Rodrigues et al. [588] 283–288 6.6–7.8 500 AnPTSemY
Ginger oil Cellulosic structure Rodrigues et al. [588] 293–313 15–30 500 AnPTSemY
Hexyl acrylate Poly(hexyl acrylate) Byun et al. [201] 303–435 6.7–255.3 28 SynVisVar
Hexyl methacrylate Poly(hexyl methacrylate) Byun et al. [201] 313–472 6.7–220.8 29 SynVisVar
Hydrogen Methylcyclohexane Zhang et al. [736] 304–326 7.3–14 20–50 SynVisVarPc
Toluene Zhang et al. [735] 307–313 8.3–11.3 20–50 SynVisVarTc
Hydroquinone (1,4-dihydroxybenzene) p-Quinone Deiters [259] Comments
(1.4-benzoquinone)
García-González et al. [323] 333–363 10–35 50 AnTVcirVal
38 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 39 (Continued )

X Y Reference T (K) P (MPa) V (cm3 ) Method

Ligand bis-(2,4,4-trimethyl ion Ag(I) in solid matrix Pourmortazavi [570] 308–328 10–30 1 AnPTSemY
pentyl)-dithiophosphinic acid (cyanex
301)
Ion Au(III) in solid matrix Pourmortazavi [570] 308–328 10–30 1 AnPTSemY
Ion Bi(III) in solid matrix Pourmortazavi [570] 308–328 10–30 1 AnPTSemY
Ion In(III) in solid matrix Pourmortazavi [570] 308–328 10–30 1 AnPTSemY
Ion Mn(II) in solid matrix Pourmortazavi [570] 308–328 10–30 1 AnPTSemY
Ion Pd(II) in solid matrix Pourmortazavi [570] 308–328 10–30 1 AnPTSemY
Linoleic acid Poly(ethylene glycol) Funazukuri et al. [307] 308–343 8.5–30.3 3.3 AnPTChro
Low MW poly(2,6-dimethyl-1,4-phenylene Polystyrene Sato et al. [599] 373–473 2.1–20.1 n.a. AnGrav
ether) (PPO)(L)
Ls-54 surfactant 1-Pentanol Liu et al. [475] 308–308 14.8–16.1 40 SynVis
1-Propanol Liu et al. [475] 308–308 14.3–15.7 40 SynVis
Benzyl alcohol Liu et al. [475] 308–308 21.8–21.8 40 SynVis
n-Heptanol Liu et al. [475] 308–323 15.5–22.1 40 SynVis
Medroxyprogesterone Cyproterone acetate Asghari-Khiavi et al. [154] 308–348 12.2–35.5 1 AnTValY
Methane Propane Webster and Kidney [703] 230–270 0.8–8 n.a. AnTVcir
Microalga Haematococcus pluvialis Astaxantine Valderrama et al. [684] 333–333 30–30 450 AnPTSemY
Microalga Spirulina maxima Phycocyanine Valderrama et al. [684] 333–333 30–30 450 AnPTSemY
Monoolein Poly(ethylene glycol) Funazukuri et al. [310] 313–313 10–25 3.2 AnPTChro
n-Heptane Poly(ethylene) Joung et al. [395] 383–503 0.6–33.5 33 SynVisVar
Polyisobutylene Joung et al. [395] 323–493 0.4–23.7 33 SynVisVar
Nitrogen Oleic acid Laursen et al. [50] 298–318 2.5–14.6 90 AnTVcirX
N-methyldiethanolamine (MDEA) Sodium sulfate Kamps et al. [401] 313–413 3.8–4.5 30 SynVis
Sulfuric acid Kamps et al. [401] 313–413 7.8–10.6 30 SynVis
n-Vinyl-2-pyrrolidone Poly(vinyl pyrrolidone) Bae et al. [158] 321–458 18.4–212 25 SynVisVar
Oleic acid Poly(ethylene glycol) Funazukuri et al. [310] 313–313 9.4–30.1 3.2 AnPTChro
Oleic acid ethyl ester Poly(ethylene glycol) Funazukuri et al. [310] 313–313 8.6–11 3.2 AnPTChro
Oleic acid methyl ester Poly(ethylene glycol) Funazukuri et al. [310] 313–313 8–11 3.2 AnPTChro
Phenol Poly(ethylene glycol) Funazukuri et al. [77] 308–328 8.7–30.2 3.3 AnPTChro
Funazukuri et al. [309] 313–313 17.8–17.8 3.2 AnPTChro
Poly(ethylene oxide) Poly(methyl methacrylate) Shieh et al. [82] 305–305 35–35 10 AnSpec
Poly(l-lactide) 110 000 1,1-Difluoroethane Lim et al. [469] 352–415 54.3–61.3 n.a. SynVisVar
(HFC-152a)
Chlorodifluoromethane Lim et al. [469] 333–410 3.7–26.1 n.a. SynVisVar
(HCFC-22)
Difluoromethane (HFC-32) Lim et al. [469] 342–416 77.3–93.6 n.a. SynVisVar
Trifluoromethane (HFC-23) Lim et al. [469] 333–414 94.1–115.1 n.a. SynVisVar
Poly(l-lactide) 2000 Chlorodifluoromethane Lim et al. [469] 314–395 3.6–44.1 n.a. SynVisVar
(HCFC-22)
Poly(l-lactide) 230 000 1,1-Difluoroethane Lim et al. [469] 354–414 56.8–64.2 n.a. SynVisVar
(HFC-152a)
Chlorodifluoromethane Lim et al. [469] 332–409 3.6–26.1 n.a. SynVisVar
(HCFC-22)
Difluoromethane (HFC-32) Lim et al. [469] 334–413 81.4–111.3 n.a. SynVisVar
Trifluoromethane (HFC-23) Lim et al. [469] 333–413 96.1–116 n.a. SynVisVar
Poly(l-lactide) 80 000 1,1-Difluoroethane Lim et al. [469] 354–413 53.2–59.5 n.a. SynVisVar
(HFC-152a)
Chlorodifluoromethane Lim et al. [469] 334–408 3.6–25.2 n.a. SynVisVar
(HCFC-22)
Difluoromethane (HFC-32) Lim et al. [469] 344–412 77–91.6 n.a. SynVisVar
Trifluoromethane (HFC-23) Lim et al. [469] 333–415 93.1–112.1 n.a. SynVisVar
Polychlorinated biphenyl St. Lawrence River sediments Zhou et al. [744] 313–333 6.5–27 50 AnTVcirVal
Propane Tripalmitin Rovetto et al. [592] 317–451 1.4–14.5 3.5 SynVis
Propene Carbon monoxide Ke et al. [410] 299–303 7.5–7.9 4 SynNonPcTc
Hydrogen Ke et al. [410] 305–305 8.3–9 4 SynNonPcTc
Squalene Methyl oleate Ruivo et al. [60] 313–343 11–21 n.a. AnPTCon
Sulfur hexafluoride SF6 Ethane Horstmann et al. [358] 292–304 4.4–6.2 10 SynVisTc
Tetraethylene glycol n-laurel ether (C12E4) n-Pentane Liu et al. [474] 313–323 8.8–19.6 40 SynVis
Tetrahydrofuran Polysulfone Zhang and Kiran [740] 296–426 13.8–54.9 24.8 SynVisVar
Zhang and Kiran [741] 296–426 13.8–54.9 24.8 SynVisVar
Toluene Polybutadiene Joung et al. [395] 323–473 1.9–23.7 33 SynVisVar
Trichloromethane (HCC-20) Iron Roggeman et al. [589] 333–333 13.7–27.5 50 AnTVal
tris(pentane-2.4-dionate)
Trifluoromethane (HFC-23) Naphthalene Diefenbacher and Türk 335–338 7.8–29.6 1310 SynVis
[267]
Triolein Poly(ethylene glycol) Funazukuri et al. [310] 313–313 9.1–14 3.2 AnPTChro
Undecanoic acid n-Hexadecane Scheidgen and Schneider 273–393 0–100 80 AnT
[603]
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 39

Table 40
Ternary systems: water + methane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,3-Dioxolane De Deugd et al. [253] 282–299 2–14 n.a. SynVis

1,4-Dioxane Seo et al. [613] 280–292 1.7–8.9 50 SynVis
2,2-Dimethylpentane Ostergaard et al. [550] 274–285 2.6–9.8 540 SynVis
2-Methylbutane (isopentane) Ostergaard et al. [550] 277–287 3.7–12 540 SynVis
2-Methylcyclohexanone Ohmura et al. [547] 273–280 1.4–3.2 201 SynNon
3,3-Dimethyl-2-Butanol (pinacolyl alcohol) Ohmura et al. [546] 273–280 1.5–3.4 200 SynNon
3,3-Dimethyl-2-butanone (pinacolone) Ohmura et al. [546] 273–280 1.1–2.8 200 SynNon
3-Methyl-1-butanol (isopentanol) Ohmura et al. [548] 273–281 2.2–6.1 200.0 SynNon
3-Methylcyclohexanone Ohmura et al. [547] 273–279 1.6–3.4 201 SynNon
4-Methylcyclohexanone Ohmura et al. [547] 237–280 1.5–3.3 201 SynNon
Acetone Seo et al. [613] 279–288 1.9–7.6 50 SynVis
Calcium chloride Kharrat and Dalmazzone [412] 260–284 4.9–10.3 n.a. SynNon
Carbon dioxide Seo et al. [612] 273–285 1.5–6.7 50 AnTValVis
Cis-1,4-dimethylcyclohexane Nakamura et al. [531] 274–287 1.6–9.1 150 SynVis
Cyclobutanone Mooijer-van et al. [520] 293–301 3.8–12.7 n.a. SynVis
Cyclohexane Sun et al. [659] 273–291 0.6–9.4 n.a. SynVisVar
Cyclooctane Makino et al. [494] 274–288 1.6–9.3 150 SynVis
Cyclopentane Sun et al. [659] 282–301 0.1–7.3 n.a. SynVisVar
Ethane Wang et al. [700] 275–283 1–4 540 AnTVLcirVar
Zhang et al. [738] 274–274 2.5–4 60 AnTVarVis
Ethene Ma et al. [486] 273–287 0.6–6 60 SynVis
Sugahara et al. [656] 284–293 1.9–19 100 AnTVis
Sugahara et al. [656] 293–293 8.5–20.8 0.1 SynVisSpec
Ethylene glycol Mahmoodaghdam and Bishnoi [492] 267–277 2–4.4 n.a. SynVisVar
Wang et al. [700] 283–303 5–40 540 AnTVLcirVar
Helium Maekawa [490] 273–284 3.4–10.2 500 SynVis
Hydrogen Zhang et al. [739] 274–278 3.7–6.6 60 SynVisVar
Lithium bromide Kiepe et al. [415] 313–313 0–8.7 n.a. SynT
Kiepe et al. [417] 313–313 0–8.7 n.a. SynT
Lithium cloride Kiepe et al. [415] 313–353 0–9.4 n.a. SynT
Methanol Wang et al. [700] 283–303 5–40 540 AnTVLcirVar
Methylcyclohexane Mooijer-van et al. [520] 279–288 2.6–9.1 n.a. SynVis
Ohmura et al. [547] 275–281 1.5–3.3 201 SynNon
Sun et al. [660] 273–290 1.3–11.9 n.a. SynVisVar
Methylcyclopentane Makino et al. [494] 274–287 1.7–9.3 150 SynVis
Neohexane Ohmura et al. [546] 274–280 1.3–2.7 200 SynNon
n-Heptane Bruinsma et al. [191] 263–323 6.9–6.9 40–280 AnTVcirValVar
Potassium bromide Kiepe et al. [415] 313–353 0–8.4 n.a. SynT
Potassium chloride Kiepe et al. [415] 313–373 0–9.7 n.a. SynT
Propene Ma et al. [486] 273–283 0.5–6.5 60 SynVis
Propylene oxide Seo et al. [613] 283–294 1.9–8.7 50 SynVis
Sodium chloride Jager and Sloan [110] 270–303 6.6–72.2 1 SynVisSpec
Kharrat and Dalmazzone [412] 269–278 4.2–8.6 n.a. SynNon
Sodium dodecyl sulfate Link et al. [102] 276–293 3.9–9.6 40 SynVis
Tetrafluoromethane (CFC-14) Mooijer-van et al. [520] 273–290 3.4–12.9 n.a. SynVis
Tetrahydrofuran De Deugd et al. [253] 289–306 2–14 n.a. SynVis
Tetrahydrofuran (THF) Seo et al. [613] 292–302 2–8.9 50 SynVis
Tetrahydropyran De Deugd et al. [253] 288–302 2–14 n.a. SynVis
Mooijer-van et al. [520] 293–303 3.4–13.5 n.a. SynVis
Trifluoromethane (HFC-23) Mooijer-van et al. [520] 282–297 0.9–12.9 n.a. SynVis

Table 41
Ternary systems: water + ethane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Diethylene glycol (DEG) Mahmoodaghdam and Bishnoi [492] 274–282 0.6–2.2 n.a. SynVisVar
Ethylene glycol Majumdar et al. [493] 271–282 0.5–2.6 n.a. SynVisVar
Wang et al. [700] 283–303 0.5–4 600 AnTVal
Helium Maekawa [490] 273–287 0.7–4 500 SynVis
Methane Wang et al. [700] 275–283 1–4 540 AnTVLcirVar
Zhang et al. [738] 274–274 2.5–4 60 AnTVarVis
Methanol Wang et al. [700] 283–303 0.5–4 600 AnTVal
Propane Ballard et al. [159] 276–279 0.5–2 3 SynVis
Ballard et al. [159] 277–282 0.5–2.5 n.a. SynVis
40 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 42
Ternary systems: water + propane + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Cyclobutanone Mooijer-van et al. [522] 276–277 0.2–12.8 n.a. SynVis

Cyclohexane Mooijer-van et al. [522] 274–276 0.1–9.9 n.a. SynVis
Diethanolamine (DEA) Jou et al. [390] 313–348 1.7–3.4 250 AnTVcirVal
Diglycolamine® (DGA) Jou et al. [390] 313–348 1.7–3.4 250 AnTVcirVal
Di-isopropanolamine Jou et al. [390] 313–348 1.7–5.5 250 AnTVcirVal
Ethane Ballard et al. [159] 276–279 0.5–2 3 SynVis
Ballard et al. [159] 277–282 0.5–2.5 n.a. SynVis
Hydrogen Zhang et al. [739] 274–278 0.8–4 60 SynVisVar
Methylcyclohexane Mooijer-van et al. [522] 274–277 0.1–7.8 n.a. SynVis
Monoethanolamine (MEA) Jou et al. [390] 313–313 1.7–1.7 250 AnTVcirVal
N-methyldiethanolamine (MDEA) Jou et al. [390] 313–348 1.7–3.4 250 AnTVcirVal
Tetrahydropyran Mooijer-van et al. [522] 274–276 0.1–4.8 n.a. SynVis

Table 43
Ternary systems: water + nitrogen + X.

X Reference T (K) P (MPa) V (cm3 ) Method

1,4-Dioxane Seo et al. [613] 275–283 3.7–11.8 50 SynVis

2,2-Dimethylpentane Ostergaard et al. [550] 275–280 15–26.4 540 SynVis
2-Methylbutane (isopentane) Ostergaard et al. [550] 276–282 14.9–30.2 540 SynVis
Acetone Seo et al. [613] 274–280 4.4–11.3 50 SynVis
Carbon dioxide Kang et al. [404] 272–284 1.3–32.3 70 AnTValVis
Dimethyl ether Laursen et al. [38] 298–318 0.5–9.9 570 AnTValVis
Propylene oxide Seo et al. [613] 279–285 4–11.7 50 SynVis
Tetrahydrofuran (THF) Seo et al. [613] 287–293 4.3–10.8 50 SynVis

Table 44
Ternary systems: water + hydrogen sulfide + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Ammonium acetate Xia et al. [715] 313–393 0.1–8.8 30 SynVis

Ammonium chloride Xia et al. [714] 313–393 0.1–9.6 30 SynVis
Ammonium nitrate Xia et al. [713] 313–393 0.1–8.3 30 SynVis
Ammonium sulfate Xia et al. [714] 313–393 0.1–9.5 30 SynVis
Diethanolamine (DEA) Sidi-Boumedine et al. [638] 313–373 0–1.3 n.a. SynT
Ethylene glycol Majumdar et al. [493] 272–295 0.2–1.5 n.a. SynVisVar
N-methyldiethanolamine (MDEA) Sidi-Boumedine et al. [638] 313–373 0–1 n.a. SynT
Piperazine Xia et al. [717] 313–393 0.1–8.7 30 SynVis
Sodium acetate Xia et al. [715] 313–393 0.1–9.7 30 SynVis
Sodium chloride Xia et al. [714] 313–393 0.1–9.7 30 SynVis
Sodium hydroxide Xia et al. [713] 313–393 0–9.3 30 SynVis
Sodium nitrate Xia et al. [713] 313–393 0.1–9.3 30 SynVis
Sodium sulfate Xia et al. [714] 313–393 0.1–9.7 30 SynVis

Table 45
Ternary systems: water + X + Y.

X Y Reference T (K) P (MPa) V (cm3 ) Method

Ammonia Potassium hydroxide Brass et al. [188] 303–318 0.1–1.1 n.a. AnTLcirVis
Sodium hydroxide Brass et al. [188] 303–318 0.1–1.3 n.a. AnTLcirVis
Chlorodifluoromethane Ethanol Elbaccouch and Elliot [279] 351–371 0.6–3.7 40 AnTVLcirVal
(HCFC-22)
Dimethyl ether 2-Propanol (isopropanol) Elbaccouch and Elliot [281] 323–373 0.1–2.4 40 AnTVLcirVal
Ethanol Elbaccouch et al. [280] 333–373 0.2–2.5 40 AnTVLcirVal
Ethanethiol Tetraethylene glycol Jou et al. [389] 298–403 0–1 n.a. AnTVcir
Ethene 1-Propanol Freitag et al. [52] 287–352 3.5–21.6 30 AnTVLcirVisVal
2-Propanol (isopropanol) Freitag et al. [52] 288–353 6.1–17.9 30 AnTVLcirVisVal
Methanol Natural near critical reservoir fluid (C1-C20+) Ostergaard et al. [551] 276–283 5.3–24.2 540 SynVis
n-Decane 2-Butanol Shimoyama et al. [634] 573–573 20–20 31 AnPTConVis
2-Propanol (isopropanol) Shimoyama et al. [634] 573–593 15–20 31 AnPTConVis
n-Hexane 2-Propanol (isopropanol) Shimoyama et al. [634] 573–573 20–20 31 AnPTConVis
n-Hexadecane Shimoyama et al. [633] 573–573 20–20 31 AnPTConVis
Oxygen Sodium carbonate Tan et al. [69] 300–300 0.7–10 500 AnPTSemX
Propene Diethanolamine (dea) Jou and Mather [393] 313–373 1.7–20.6 250 AnTVcirVar
Di-isopropanolamine Jou and Mather [393] 313–333 1.7–2.7 250 AnTVcirVar
Monoethanolamine (mea) Jou and Mather [393] 280–373 0.1–5.5 250 AnTVcirVar
N-methyldiethanolamine (MDEA) Jou and Mather [393] 313–333 1.7–2.7 250 AnTVcirVar
Synthethic natural gas Methanol Jarne et al. [380] 247–288 0.1–2 n.a. SynVis
Toluene Ethylbenzene Shimoyama et al. [633] 553–553 20–20 31 AnPTConVis
n-Decane Shimoyama et al. [633] 553–573 20–20 31 AnPTConVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 41

Table 46
Ternary systems: methane + X + Y.

X Y Reference T (K) P (MPa) V (cm3 ) Method

Ethane n-Butane Blanco et al. [175] 253–273 1.2–9.2 n.a. SynVisCon

Ethene Poly(ethylene-co-1-hexene) copolymer Dörr et al. [270] 393–493 118.6–202 14.5–19.0 SynVisVar
Poly(ethylene-co-vinyl acetate) copolymer Kinzl et al. [423] 393–493 108.3–173.8 14.5–19.0 SynVisVar
n-Butane n-Decane Dandekar and Stenby [250] 311–364 16.9–19 80 SynVisVar
n-Heptane Cyclohexane Xia et al. [719] 303–303 2.6–12 200–360 AnTLcirVar
ethanol Xia et al. [719] 291–303 2.6–12 200–360 AnTLcirVar
n-Hexane n-Tetradecane Chylinski et al. [51] 383–383 6.5–12 650 AnTVLcirValVis
Tetracosane Triacontane Machado and de Loos [487] 320–473 65.4–193.1 n.a. SynVisPcTc

Table 47
Ternary systems: ethene + X + Y.

X Y Reference T (K) P (MPa) V (cm3 ) Method

1-Hexene Poly(ethylene-co-1-hexene) copolymer Dörr et al. [270] 393–493 25.6–156 14.5–19.0 SynVisVar
2,6-Di-tertbutyl-4-methylphenol Ethylene–butyl acrylate copolymers Becker et al. [167] 354–530 95.3–114.4 n.a. SynVisVar
Ethylene–ethyl acrylate copolymers Becker et al. [167] 353–533 98.2–163.1 n.a. SynVisVar
Ethylene–methyl acrylate copolymers Becker et al. [167] 373–493 124.4–211.5 n.a. SynVisVar
Ethylene–methyl methacrylate copolymers Becker et al. [167] 353–528 103.9–185.5 n.a. SynVisVar
Ethylene–propyl acrylate copolymers Becker et al. [167] 353–532 97.8–152.7 n.a. SynVisVar
Ethylene-butyl methacrylate copolymers Becker et al. [167] 353–533 81.3–138 n.a. SynVisVar
Poly(ethyl acrylate) Becker et al. [167] 354–533 101–161.3 n.a. SynVisVar
Poly(ethylene) (ldpe) Becker et al. [167] 403–521 120.4–163.7 n.a. SynVisVar
Poly(propyl acrylate) Becker et al. [167] 352–531 87.4–109.3 n.a. SynVisVar
Benzene Ethylbenzene Liu et al. [477] 282–572 5–11.9 n.a. SynVisPcTc
Ethane Poly(ethylene-co-1-hexene) copolymer Dörr et al. [270] 393–493 112–156 14.5–19.0 SynVisVar
Poly(ethylene-co-vinyl acetate) copolymer Kinzl et al. [423] 393–493 107.5–126 14.5–19.0 SynVisVar
Helium Poly(ethylene-co-1-hexene) copolymer Dörr et al. [270] 393–493 118.6–214.6 14.5–19.0 SynVisVar
Poly(ethylene-co-vinyl acetate) copolymer Kinzl et al. [423] 393–493 108.3–209.4 14.5–19.0 SynVisVar
n-Butane Poly(ethylene-co-1-hexene) copolymer Dörr et al. [270] 393–493 101–156 14.5–19.0 SynVisVar
Poly(ethylene-co-vinyl acetate) copolymer Kinzl et al. [423] 393–493 94.3–125.9 14.5–19.0 SynVisVar
n-Hexane Impact poly(propylene) copolymer (icp–pp) Sato et al. [78] 323–363 0.6–2.4 n.a. AnPTChro
Poly(ethylene) (ldpe) Chen et al. [229] 393–473 0.6–15.7 6–20 SynVisVar
Poly(ethylene) 108k Chen et al. [229] 373–473 0.4–17 6–20 SynVisVar
Poly(ethylene) 15k Chen et al. [229] 373–473 0.4–20.9 6–20 SynVisVar
Propane Poly(ethylene-co-1-hexene) copolymer Dörr et al. [270] 393–493 106.6–156 14.5–19.0 SynVisVar
Poly(ethylene-co-vinyl acetate) copolymer Kinzl et al. [423] 393–493 98–125.9 14.5–19.0 SynVisVar

Table 48
Ternary systems: X + Y + Z.

X Y Z Reference T (K) P (MPa) V (cm3 ) Method

1-Butene Toluene Poly(propylene) Oliveira et al. [549] 352–423 1.1–12.7 28 SynVisVar

Benzene Propene Cumene Wang et al. [698] 364–596 4.6–7 18 SynVisPcTc
Cyclohexane Polystyrene Polystyrene ter Horst et al. 496–516 2.4–16 3.5 SynVis
[667]
Difluoromethane Propane 1,1,1,2,3,3,3-Heptafluoropropane Coquelet et al. 269–329 0.4–2.2 n.a. SynVisVar
(HFC-32) (HFC-227ea) [234]
Dimethyl ether N,N-dimethyl formamide Polysulfone Li and McHugh 294–452 35–210 28 SynVisVar
[457]
Tetrahydrofuran Polysulfone Li and McHugh 293–450 35–210 28 SynVisVar
[457]
Ethane Carbon tetrachloride Poly(propylene glycol) Martin et al. [500] 295–373 4.5–21.5 50 SynVisVar
Cyclohexane Polystyrene ter Horst et al. 388–513 3.4–14.4 3.5 SynVis
[667]
Propane Trans-␤-carotene Nobre et al. [542] 313–348 5.1–30.1 32 AnPTSemY
Trichloromethane (HCC-20) Poly(propylene glycol) Martin et al. [500] 295–373 6–30 50 SynVisVar
Hydrogen Carbon monoxide n-Hexane Gao et al. [318] 505–506 3–3 50 SynVisVarPcTc
n-Hexadecane Anthracene Minicucci et al. n.a.–650 n.a.–14 n.a. SynNon
[113]
Propane Methyl palmitate Rovetto et al. [593] 361–450 5.3–11.6 3.5 SynVisVar
Hydrogen sulfide N-methyldiethanolamine Sodium sulfate Anoufrikov et al. 313–393 0–3.8 30 SynVis
(MDEA) [152]
N-methyldiethanolamine Sulfuric acid Anoufrikov et al. 313–393 0–3.6 30 SynVis
(MDEA) [152]
n-Butane n-Heptane n-Hexadecane Fenghour et al. 404–447 0.5–0.7 207 SynNon
[292]
Toluene Poly(propylene) Oliveira et al. [549] 358–423 1–10.8 28 SynVisVar
n-Hexane Impact poly(propylene) Ethene Sato et al. [78] 323–363 0.6–2.4 n.a. AnPTChro
copolymer (ICP–PP)
Impact poly(propylene) Propene Sato et al. [78] 323–363 1.2–2.4 n.a. AnPTChro
copolymer (ICP–PP)
Poly(ethylene) 15k Poly(ethylene) 108k Chen et al. [229] 443–473 2.1–7.6 6–20 SynVisVar
42 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 48 (Continued )

X Y Z Reference T (K) P (MPa) V (cm3 ) Method

Nitrogen Cyclohexane Polystyrene ter Horst et al. 437–513 7.5–16 3.5 SynVis
[667]
Dimethyl ether Methanol Teodorescu 288–313 0.1–9.2 700 AnTVal
Rasmussen [666]
n-Hexane n-Decane Uribe-Vargas and 258–298 1.4–20.1 n.a. AnTVal
Trejo [682]
n-Tridecane n-Tetradecane n-Pentadecane Daridon et al. [106] 273–293 0.1–100 0.03 SynVis
Propane cyclohexane Polystyrene ter Horst et al. 438–513 2.5–12.4 3.5 SynVis
[667]
Propene 2,6-Di-tertbutyl-4- Poly(methyl acrylate) Becker et al. [167] 473–531 139.9–275 n.a. SynVisVar
methylphenol
2,6-Di-tertbutyl-4- Poly(methyl methacrylate) Becker et al. [167] 427–532 107.8–270 n.a. SynVisVar
methylphenol
Vinyl acetate Ethene Poly(ethylene-co-vinyl acetate) Kinzl et al. [423] 393–493 4.8–125.9 14.5–19.0 SynVisVar
copolymer

Table 49
Multicomponent systems: carbon dioxide + water + X (+Y + . . .).

X (+Y + . . .) Reference T (K) P (MPa) V (cm3 ) Method

1,8-Cineole + lecithin Cruz Francisco et al. [80] 308–353 15–15 n.a. AnSpecVis
1,8-Cineole + monoolein Cruz Francisco et al. [240] 308–353 15–15 n.a. AnSpecVis
1-Octene + tetrahydrofuran Lazzaroni et al. [436] 298–298 0.2–25.6 350 AnTValVis
1-Pentanol + fluorosurfactant F-53B Gao et al. [320] 290–334 7.5–13.5 n.a. SynVisVar
1-Propanol + adenine Adrian et al. [148] 313–333 7.1–16.1 30 AnTVcirLcir
1-Propanol + anthranilate Adrian et al. [148] 313–333 7.1–16.1 30 AnTVcirLcir
1-Propanol + caffeine Adrian et al. [148] 313–333 7.1–16.1 30 AnTVcirLcir
1-Propanol + fluorosurfactant F-53B Gao et al. [320] 308–334 12–14.5 n.a. SynVisVar
1-Propanol + l-phenylalanine Adrian et al. [148] 313–333 7.1–16.1 30 AnTVcirLcir
1-Propanol + salicyclic alcohol Adrian et al. [148] 313–333 7–16.1 30 AnTVcirLcir
1-Propanol + vanillin Adrian et al. [148] 313–333 7.1–16.1 30 AnTVcirLcir
Acetic acid (ethanoic acid) + sodium acetate Sieder and Maurer [639] 313–353 6–16.1 38 AnPTCon
Acetic acid (ethanoic acid) + sodium chloride Sieder and Maurer [639] 313–353 6.1–16.3 38 AnPTCon
Diethanolamine (DEA) + N-methyldiethanolamine (MDEA) Sidi-Boumedine et al. [637] 298–348 0–4.5 n.a. SynT
Ethanol + capsaicin Duarte et al. [34] 313–323 12–14 36 AnTCapVal
Ethanol + dimethyl ether Laursen and Andersen [435] 298–318 0.5–4.2 570 AnTVis
Ethanol + fluorosurfactant F-53B Gao et al. [320] 308–334 8–24.5 n.a. SynVisVar
Ethylene glycol + sodium cloride Majumdar et al. [493] 264–272 1.3–3.1 n.a. SynVisVar
Fluorosurfactant F-53B + butanol Gao et al. [320] 308–334 12–14.5 n.a. SynVisVar
Fluorosurfactant F-53B + heptanol Gao et al. [320] 308–334 12–14.5 n.a. SynVisVar
Fluorosurfactant F-53B + hexanol Gao et al. [320] 308–334 8.5–15.5 n.a. SynVisVar
Fluorosurfactant F-53B + octyl alcohol Gao et al. [320] 308–334 15–17 n.a. SynVisVar
Methane + hydrogen sulfide Sun et al. [658] 274–299 0.5–8.6 60 SynVisVar
Methane + methanol Jarne et al. [379] 241–288 0.1–5.9 n.a. SynVis
Methane + N-methyldiethanolamine (MDEA) Addicks et al. [147] 313–353 10–20 450 AnTVarVis
Methanol + dimethyl ether Laursen et al. [38] 298–318 0.4–5.5 570 AnTValVis
Methanol + tetramethylammonium bicarbonate Levitin et al. [454] 298–343 1.5–27.1 5–20 SynVisVar
Methanol + tetramethylammonium bicarbonate Levitin et al. [455] 298–343 1.5–27.1 5–20 SynVisVar
Nitric acid + tri-n-butyl phosphate Enokida et al. [285] 313–333 7–16.5 n.a. SynVis
Nitrogen + tetrahydrofuran Kang et al. [404] 274–295 0.2–12.9 70 AnTValVis
N-methyldiethanolamine (MDEA) + diethanolamine (DEA) Rebolledo-Libreros and Trejo [582] 313–393 0–1.9 320 AnTVcir
Phenol + potassium chloride Wagner et al. [694] 313–313 22–22 200 AnTVLcirVis
Phenol + sodium bromide Wagner et al. [694] 313–313 22–22 200 AnTVLcirVis
Phenol + sodium chloride Wagner et al. [694] 313–313 8–30 200 AnTVLcirVis
Phenol + tetramethylammonium bromide Wagner et al. [694] 313–313 8–30 200 AnTVLcirVis
Piperazine + N-methyldiethanolamine (MDEA) Kamps et al. [402] 353–353 0.1–6.4 30 SynVis
2,2,3,3,4,4,5,5-Octafluoro-1-pentanol + sodium Liu et al. [476] 311–311 34.5–34.5 2.2 AnSpec
bis(2-ethylhexyl)sulfosuccinate + dimidium bromice
2,2,3,3,4,4,5,5-Octafluoro-1-pentanol + sodium Liu et al. [476] 311–311 34.5–34.5 2.2 AnSpec
bis(2-ethylhexyl)sulfosuccinate + methyl orange
2,2,3,3,4,4,5,5-Octafluoro-1-pentanol + sodium Liu et al. [476] 311–311 34.5–34.5 2.2 AnSpec
bis(2-ethylhexyl)sulfosuccinate + thymol blue
Ethanol + didecyldimethylammonium chloride + soysolv Elbaccouch et al. [282] 298–333 0.2–8.7 9.5 SynTVis
Methane + diethanolamine (DEA) + ethanethiol Jou and Mather [387] 313–343 6.8–6.8 n.a. AnTVcir
Methane + diethanolamine (DEA) + methanethiol Jou and Mather [387] 313–343 6.8–6.8 n.a. AnTVcir
Methane + toluene + N-methyldiethanolamine (MDEA) Valtz et al. [686] 333–333 0.5–0.5 n.a. AnTValVis
Nitrogen + dimethyl ether + methanol Laursen et al. [38] 298–318 0.4–9.9 570 AnTValVis
N-methyldiethanolamine (MDEA) + diethanolamine Rebolledo-Libreros and Trejo [582] 313–393 0–1.9 320 AnTVcir
(DEA) + 2-amino-2-methyl-1-propanol
Methane + diethanolamine (DEA) + hydrogen Jou and Mather [387] 313–343 6.8–6.8 n.a. AnTVcir
sulfide + ethanethiol
Methane + diethanolamine (DEA) + hydrogen Jou and Mather [387] 313–343 6.8–6.8 n.a. AnTVcir
sulfide + methanethiol
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 43

Table 50
Multicomponent systems: carbon dioxide + X + Y (+ . . .).

X (+ Y + . . .) Reference T (K) P (MPa) V (cm3 ) Method

1,8-Cineole + limonene + ␣-pinene Cruz Francisco 313–333 8–25 30 AnPTSemY

and Sivik [239]
2-Ethyl-1-hexanol + 2-ethyl hexanoic acid + 2-ethyl-hexyl-2-ethyl hexanoate Ghasziaskar 313–353 9.4–25.3 10 AnPTSemY
and Daneshfar
[327]
1-Butyl-3-methylimidazolium hexafluorophosphate ([bmim][PF6]) + acetone + n-hexane Wu et al. [711] 313–313 15–15 55 AnPTSemYVis
Oleic acid + ␣-pinene + abietic acid Laursen et al. 298–318 2.1–14.4 90 AnTVcirX
[50]
Ethanol + astaxantine + microalga Haematococcus pluvialis Valderrama et 333–333 30–30 450 AnPTSemY
al. [684]
1-n-Hexene + carbon monoxide + hydrogen Ke et al. [410] 305–315 8.3–12 4 SynNonPcTc
Propene + carbon monoxide + hydrogen Ke et al. [410] 295–304 7.9–10.8 4 SynNonPcTc
1-Butyl-3-methylimidazolium hexafluorophosphate ([bmim][PF6]) + ethanol + acetone Wu et al. [711] 313–313 15–15 55 AnPTSemYVis
1-Butyl-3-methylimidazolium hexafluorophosphate ([bmim][PF6]) + ethanol + n-hexane Wu et al. [711] 313–313 15–15 55 AnPTSemYVis
Ethanol + ethyl acetate + benzoic acid Jin et al. [385] 308–328 8–23 377 AnPTSemY
Acenaphthene + fluoranthene + triphenylene Yamini and 308–338 12.1–35.4 1 AnTValY
Bahramifar
[723]
Methane + hydrogen sulfide + sulfur Sun and Chen 303–363 20–45 300 AnTVar
[657]
Propane + nitrogen + oxygen Smejkal et al. 327–369 4.2–6.3 35 SynVisPcTc
[646]
Anthracene + phenanthrene + carbazole Goodarznia 308–308 11.1–20.1 n.a. AnPTSemY
and
Esmaeilzadeh
[334]
Ethanol + phycocyanine + microalga Spirulina maxima Valderrama et 333–333 30–30 450 AnPTSemY
al. [684]
Methanol + polychlorinated biphenyl + St. Lawrence River sediments Zhou et al. 313–333 6.5–27 50 AnTVcirVal
[744]
Nitrogen + oleic acid + ␣-pinene + abietic acid Laursen et al. 298–318 2.5–14.5 90 AnTVcirX
[50]
Eugenol + ␤-caryophyllene + eugenol acetate + ␣-humulene Souza et al. 303–328 5.8–16.7 25 SynVisVar
[648]
Carbon monoxide + hydrogen + 1-hexene + heptanal Jiang et al. 303–348 6.5–18.2 25–50 SynVisVar
[384]
Trans-2-hexen-1-ol + diisopropyl-l-tartrate + n-decane + tert-butylhydroperoxide Stradi et al. 313–323 2.8–6.2 100 AnTCap
[653]
Propane + nitrogen + oxygen + acetic acid (ethanoic acid) + acrylic acid Smejkal et al. 294–300 8.7–9.4 35 SynVisPcTc
[646]
Propene + carbon monoxide + hydrogen + n-butyraldehyde + isobutyraldehyde Ke et al. [411] 297–338 8.1–11.8 n.a. SynNonPcTc
Propane + nitrogen + oxygen + acetic acid (ethanoic acid) + methanol Smejkal et al. 301–306 7–7.8 35 SynVisPcTc
[646]
Trans-2-hexen-1-ol + diisopropyl-l-tartrate + n-decane + tert-butylhydroperoxide + tert- Stradi et al. 313–323 3.4–7.4 100 AnTCap
butanol + titanium(IV) [653]
isopropoxide + (2R,3R)-(+)-3-propyloxiranemethanol

Table 51
Multicomponent systems: methane + X + Y (+. . .).

X (+Y + . . .) Reference T (K) P (MPa) V (cm3 ) Method

Diglycolamine (DGA) + ethylbenzene + water Valtz et al. [686] 298–393 0.5–5 n.a. AnTValVis
Ethane + water + ethylene glycol Wang et al. [700] 275–283 0.5–40 540 AnTVLcirVar
Ethane + water + methanol Wang et al. [700] 275–283 1.3–40 540 AnTVLcirVar
Ethane + water + n-butane Blanco et al. [175] 250–288 0.4–9.9 n.a. SynVisCon
Chapoy et al. [218] 278–313 0.9–14.4 34 AnTVal
Ethane + water + tetrahydrofuran Zhang et al. [738] 274–284 2–3 60 AnTVarVis
Ethylene glycol + water + sodium chloride Eichholz et al. [278] 262–281 2.1–9.5 64–74 SynVisVar
n-Butane + n-heptane + n-hexadecane Fenghour et al. [293] 340–372 4.8–3.6 207 SynNon
n-Hexane + n-decane + n-tetradecane Chylinski et al. [51] 296–296 5.8–5.8 650 AnTVLcirValVis
Nitrogen + water + 2,2-dimethylpentane Ostergaard et al. [550] 276–286 6.2–22.6 540 SynVis
Nitrogen + water + 2-methylbutane (isopentane) Ostergaard et al. [550] 276–284 5.1–15.4 540 SynVis
Water + benzene + diglycolamine (DGA) Valtz et al. [686] 298–393 0.5–5 n.a. AnTValVis
Water + ethane + propane Ostergaard et al. [552] 276–290 1.4–7.9 540 SynVis
Water + hydrogen + propane Zhang et al. [739] 274–280 0.6–4.9 60 SynVisVar
Water + methanethiol + diethanolamine (DEA) Jou and Mather [387] 313–343 6.8–6.8 n.a. AnTVcir
Water + methanol + sodium chloride Jager et al. [377] 249–281 2–16 n.a. SynVis
Jager et al. [377] 260–292 7.4–73.2 1 SynVisSpec
Water + sodium chloride + magnesium chloride Link et al. [102] 269–293 7.9–9.6 40 SynVis
Water + toluene + diglycolamine (DGA) Valtz et al. [686] 298–393 0.5–5 n.a. AnTValVis
Water + toluene + N-methyldiethanolamine (MDEA) Valtz et al. [686] 298–393 0.4–8.1 n.a. AnTValVis
n-Pentane + 2-methylbutane Jensen et al. [383] 277–410 11.7–40 150 SynVisVar
(isopentane) + n-hexane + naphthalene
n-Pentane + 2-methylbutane Jensen et al. [383] 279–413 9.8–39.5 150 SynVisVar
(isopentane) + n-hexane + n-tetracosane
44 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 51 (Continued )

X (+Y + . . .) Reference T (K) P (MPa) V (cm3 ) Method

Propane + n-pentane + n-decane + n- Gozalpour et al. [32] 303–353 19.4–30.4 9000 AnTValVisVar
hexadecane Gozalpour et al. [337] 278–383 10.4–41.4 9000 SynVisVar
Gozalpour et al. [338] 278–383 10.4–41.4 9000 SynVisVar
Water + ethane + cyclohexane + propane Sun et al. [659] 273–289 0.6–6.2 n.a. SynVisVar
Water + ethane + propane + 2-methylbutane Ostergaard et al. [552] 275–282 2–5.1 540 SynVis
(isopentane)
Water + ethane + propane + methylcyclohexane Sun et al. [660] 273–288 0.9–6.1 n.a. SynVisVar
Ostergaard et al. [552] 280–288 2.6–8.1 540 SynVis
Water + ethane + propane + methylcyclopentane Ostergaard et al. [552] 278–288 2–7.7 540 SynVis
Water + ethylene glycol + potassium chloride + sodium Masoudi et al. [501] 259–283 3.9–46.6 n.a. SynNon
chloride
Water + hydrogen + ethane + propane Zhang et al. [739] 274–279 1.1–7 60 SynVisVar
Water + methanethiol + diethanolamine Jou and Mather [387] 313–343 6.8–6.8 n.a. AnTVcir
(DEA) + hydrogen sulfide
n-Pentane + 2-methylbutane (isopentane) + n- Jensen et al. [383] 278–419 8.9–40 150 SynVisVar
hexane + n-tetracosane + naphthalene
Water + benzene + N-methyldiethanolamine Valtz et al. [686] 333–333 0.5–0.5 n.a. AnTValVis
(MDEA) + ethylbenzene + toluene
Water + ethane + propane + n-pentane + n-decane Ostergaard et al. [552] 279–286 1.2–3.8 540 SynVis
Ethane + propane + 2-methylpropane Dandekar and Stenby [250] 298–298 7.4–7.4 80 SynVisVar
(isobutane) + n-butane + 2-methylbutane
(isopentane) + n-pentane
Water + ethane + propane + n-pentane + n-decane + 2,2- Ostergaard et al. [552] 278–286 0.9–3.4 540 SynVis
dimethylpropane
(neopentane)
Water + ethane + propane + n-pentane + n- Ostergaard et al. [552] 276–284 0.8–3.1 540 SynVis
decane + cyclohexane
Water + ethane + propane + n-pentane + n- Ostergaard et al. [552] 278–287 0.2–4.2 540 SynVis
decane + cyclopentane
Water + ethane + propane + n-pentane + n- Ostergaard et al. [552] 278–288 0.4–2.6 540 SynVis
decane + cyclopentane + 2,2-dimethylpropane
(neopentane)

Table 52
Multicomponent systems: X + Y (+ . . .).

X (+Y + . . .) Reference T (K) P (MPa) V (cm3 ) Method

Benzene + water + deuterium oxide + deuterium protium oxide Furutaka and Ikawa [312] 473–648 10–35 n.a. AnSpecVis
Ethene + n-hexane + poly(ethylene) 15k + poly(ethylene) 108k Chen et al. [229] 443–473 2.8–14.8 6–20 SynVisVar
Ethene + toluene + norbornene + cyclic olefin copolymer Lee et al. [449] 323–423 0.5–2.5 n.a. AnT
Ethylbenzene + water + deuterium oxide + deuterium protium Furutaka and Ikawa [313] 473–623 10–35 n.a. AnSpecVis
oxide
Hydrogen + carbon monoxide + methanol + n-hexane Gao et al. [318] 504–506 3–3.3 50 SynVisVarPcTc
Hydrogen sulfide + N-methyldiethanolamine Rebolledo-Libreros and Trejo [583] 313–393 0–1 320 AnTVcir
(MDEA) + diethanolamine (DEA) + water
Hydrogen sulfide + N-methyldiethanolamine Sidi-Boumedine et al. [638] 313–373 0–1.1 n.a. SynT
(MDEA) + water + diethanolamine (DEA)
Hydrogen sulfide + water + ethylene glycol + sodium cloride Majumdar et al. [493] 273–289 0.2–1.4 n.a. SynVisVar
Hydrogen Xia et al. [717] 353–353 0.1–6.2 30 SynVis
sulfide + water + piperazine + N-methyldiethanolamine
(MDEA)
Nitrogen + dimethyl ether + water + methanol Laursen et al. [38] 298–318 0.4–10.2 570 AnTValVis
Nitrogen + ethanol + water + dimethyl ether Laursen and Andersen [435] 298–318 0.4–10.2 570 AnTVis
Nitrogen + ethene + 1-hexene + poly(ethylene-co-1-hexene) Dörr et al. [270] 393–493 12.7–206.5 14.5–19.0 SynVisVar
copolymer
Nitrogen + oleic acid + ␣-pinene + abietic acid Laursen et al. [50] 298–318 3.7–14.7 90 AnTVcirX
Nitrogen + vinyl acetate + ethene + poly(ethylene-co-vinyl Kinzl et al. [423] 393–493 26.7–193 14.5–19.0 SynVisVar
acetate) copolymer
n-Tridecane + n-tetradecane + n-pentadecane + n-hexadecane Daridon et al. [106] 277–296 0.1–100.3 0.03 SynVis
Hydrogen sulfide + N-methyldiethanolamine Rebolledo-Libreros and Trejo [583] 313–393 0–1 320 AnTVcir
(MDEA) + diethanolamine
(DEA) + 2-amino-2-methyl-1-propanol + water
n-Tridecane + n-tetradecane + n-pentadecane + n- Daridon et al. [106] 279–298 0.1–100.3 0.03 SynVis
hexadecane + n-heptadecane
Toluene + water + deuterium oxide + deuterium protium Furutaka and Ikawa [313] 473–623 10–35 n.a. AnSpecVis
oxide +
n-Tridecane + n-tetradecane + n-pentadecane + n- Daridon et al. [106] 283–302 0.1–100 0.03 SynVis
hexadecane + n-heptadecane + n-octadecane
n-Tridecane + n-tetradecane + n-pentadecane + n- Daridon et al. [106] 286–305 0.1–98 0.03 SynVis
hexadecane + n-heptadecane + n-octadecane + n-nonadecane
n-Tridecane + n-tetradecane + n-pentadecane + n- Daridon et al. [106] 289–309 0.1–100 0.03 SynVis
hexadecane + n-heptadecane + n-octadecane + n-
nonadecane + n-eicosane
n-Tridecane + n-tetradecane + n-pentadecane + n- Daridon et al. [106] 295–315 0.1–100 0.03 SynVis
hexadecane + n-heptadecane + n-octadecane + n-
nonadecane + n-eicosane + n-heneicosane + n-docosane
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 45

Table 53
Complex systems: X + Y (+ . . .).

X Y Z Reference T (K) P (MPa) V (cm3 ) Method

Gas condensate reservoirs Elsharkawy [284] 278–444 10.8–81.6 n.a. SynVis

Paraffinic system (n-c6 to n-c36) Pauly et al. [45] 256–290 0.1–50 n.a. AnTVar
Synthetic legendre gas condensate May et al. [508] 300–310 6.2–9.5 40 SynNonVcirVar
Synthetic reservoir fluid #1 Yan et al. [727] 312–404 6.5–58.1 n.a. SynVis
Synthetic reservoir fluid #2 Yan et al. [727] 312–425 6.1–51 n.a. SynVis
Synthetic reservoir fluid #3 Yan et al. [727] 303–421 5.9–49.5 n.a. SynVisPcTc
Synthetic reservoir fluid #4 Yan et al. [727] 303–421 6–48.4 n.a. SynVisPcTc
Synthetic reservoir fluid #5 Yan et al. [727] 303–422 5.9–46.4 n.a. SynVisPcTc
Reservoir fluid (North Sea) Water Pedersen et al. [560] 308–473 70–100 120 AnTVar
Synthethic natural gas Water Ostergaard et al. [552] 276–290 1.2–7.6 540 SynVis
Natural Gas—Alinta Gas Ltd., Perth, Para-toluene sulfonic acid Water Gnanendran and Amin [333] 285–293 1.4–8 700 SynNonVisVar
Australia
Synthethic natural gas Water Cyclohexane Ostergaard et al. [552] 277–292 1.1–9.6 540 SynVis
Cyclopentane Ostergaard et al. [552] 283–288 1.2–3.1 540 SynVis
Methylcyclopentane Ostergaard et al. [552] 278–289 1.7–7 540 SynVis

Table 54
Binary systems with hydrates: water + X.

X Reference T (K) P (MPa) V (cm3 ) Method

Air Mohammadi et al. [91] 274–283 17–45.1 150 SynNon

Black oil A—Westport Technology Center Ivanic et al. [128] 287–293 6.6–16.8 300 SynNon
Black oil B—Westport Technology Center Ivanic et al. [128] 279–284 3–7.8 300 SynNon
Black oil C—Westport Technology Center Ivanic et al. [128] 282–286 4.6–16.3 300 SynNon
Carbon dioxide Mooijer-van den Heuvel et al. [521] 276–286 1.8–7.3 n.a. SynVis
Servio and Englezos [614] 273–283 2–6 n.a. AnTVis
Yang et al. [729] 277–280 4.9–14.2 n.a. AnTVcirVisVar
Zatsepina and Buffett [126] 271–281 2.8–3 n.a. SynNon
Ethane Kim et al. [422] 277–298 1.4–20.1 n.a. SynVisVar
Morita et al. [523] 298–323 89–479 0.2 SynVisSpec
Song et al. [647] 201–281 3.4–3.4 n.a. AnPTSemY
Methane Chapoy et al. [214] 283–293 10–35 34 AnTVal
Chapoy et al. [220] 283–293 10–35 34 AnTVal
Huo et al. [367] 275–275 30–30 1 AnTSpec
Kharrat and Dalmazzone [412] 281–284 5.7–7.7 n.a. SynNon
Kim et al. [422] 276–298 2.3–16.6 n.a. SynVisVar
Link et al. [102] 278–293 8.6–9.6 40 SynVis
Mohammadi et al. [91] 278–278 4.7–4.7 150 SynNon
Ohmura et al. [547] 273–281 2.6–5.7 201 SynNon
Servio and Englezos [615] 274–284 3.5–6.5 n.a. AnTVis
Song et al. [647] 196–270 3.4–6.9 n.a. AnPTSemY
Yang et al. [730] 273–286 3.6–19.3 n.a. AnTVcirVisVar
Natural near critical reservoir fluid (C1−C20+) Ostergaard et al. [551] 277–288 1–13.9 540 SynVis
Nitrogen Mohammadi et al. [91] 274–283 19–45.3 150 SynNon
Oxygen Mohammadi et al. [91] 273–284 13.5–43.7 150 SynNon
Propane Makogon [495] 278–278 0.5–35 160–210 SynVisVar
Mooijer-van et al. [522] 276–278 0.3–9.8 n.a. SynVis
Song et al. [647] 211–276 0.8–1.1 n.a. AnPTSemY
Synthetic Green Canyon gas Ivanic et al. [128] 288–296 4–14 300 SynNon
Tetrafluoromethane (CFC-14) Sugahara et al. [655] 276–317 7.4–317 0.2 SynVisSpec
Xenon Ohgaki et al. [545] 283–320 0.9–69 n.a. SynVis
46 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54

Table 55
Ternary systems with hydrates: water + X + Y.

X Y Reference T (K) P (MPa) V (cm3 ) Method

Carbon Copper(II) sulfate Clarke et al. [233] 273–286 0.7–4.3 n.a. SynVisVar
dioxide Cyclobutanone Mooijer-van den Heuvel et al. [521] 279–315 0.3–11.9 n.a. SynVis
Cyclohexane Mooijer-van den Heuvel et al. [521] 274–288 0.9–10.4 n.a. SynVis
Ethylene glycol Majumdar et al. [493] 264–276 1.2–3.1 n.a. SynVisVar
Magnesium sulfate (1:1) Clarke et al. [233] 275–280 1.8–3.8 n.a. SynVisVar
Methane Seo et al. [612] 273–285 1.5–6.7 50 AnTValVis
Methylcyclohexane Mooijer-van den Heuvel et al. [521] 277–280 1.8–11.3 n.a. SynVis
Nitrogen Kang et al. [404] 272–284 1.3–32.3 70 AnTValVis
Potassium nitrate Clarke et al. [233] 275–278 1.8–3.5 n.a. SynVisVar
Tetrahydropyran Mooijer-van den Heuvel et al. [521] 280–291 0.4–4.2 n.a. SynVis
Ethane Diethylene glycol (DEG) Mahmoodaghdam and Bishnoi [492] 274–282 0.6–2.2 n.a. SynVisVar
Ethylene glycol Majumdar et al. [493] 271–282 0.5–2.6 n.a. SynVisVar
Helium Maekawa [490] 273–287 0.7–4 500 SynVis
Propane Ballard et al. [159] 276–279 0.5–2 3 SynVis
Ballard et al. [159] 277–282 0.5–2.5 n.a. SynVis
Hydrogen Propane Zhang et al. [739] 274–278 0.8–4 60 SynVisVar
Hydrogen sulfide Ethylene glycol Majumdar et al. [493] 272–295 0.2–1.5 n.a. SynVisVar
Methane 1,3-Dioxolane De Deugd et al. [253] 282–299 2–14 n.a. SynVis
1,4-Dioxane Seo et al. [613] 280–292 1.7–8.9 50 SynVis
2,2-Dimethylpentane Ostergaard et al. [550] 274–285 2.6–9.8 540 SynVis
2-Methylbutane (isopentane) Ostergaard et al. [550] 277–287 3.7–12 540 SynVis
2-Methylcyclohexanone Ohmura et al. [547] 273–280 1.4–3.2 201 SynNon
3,3-Dimethyl-2-butanol (pinacolyl alcohol) Ohmura et al. [546] 273–280 1.5–3.4 200 SynNon
3,3-Dimethyl-2-butanone (pinacolone) Ohmura et al. [546] 273–280 1.1–2.8 200 SynNon
3-Methyl-1-butanol (isopentanol) Ohmura et al. [548] 273–281 2.2–6.1 200 SynNon
3-Methylcyclohexanone Ohmura et al. [547] 273–279 1.6–3.4 201 SynNon
4-Methylcyclohexanone Ohmura et al. [547] 237–280 1.5–3.3 201 SynNon
Acetone Seo et al. [613] 279–288 1.9–7.6 50 SynVis
Calcium chloride Kharrat and Dalmazzone [412] 260–284 4.9–10.3 n.a. SynNon
cis-1,4-Dimethylcyclohexane Nakamura et al. [531] 274–287 1.6–9.1 150 SynVis
Cyclobutanone Mooijer-van et al. [520] 293–301 3.8–12.7 n.a. SynVis
Cyclohexane Sun et al. [659] 273–291 0.6–9.4 n.a. SynVisVar
Cyclooctane Makino et al. [494] 274–288 1.6–9.3 150 SynVis
Cyclopentane Sun et al. [659] 282–301 0.1–7.3 n.a. SynVisVar
Ethane Zhang et al. [738] 274–274 2.5–4 60 AnTVarVis
Ethene Ma et al. [486] 273–287 0.6–6 60 SynVis
Sugahara et al. [656] 284–293 1.9–19 100 AnTVis
Sugahara et al. [656] 293–293 8.5–20.8 0.1 SynVisSpec
Ethylene glycol Mahmoodaghdam and Bishnoi [492] 267–277 2–4.4 n.a. SynVisVar
Helium Maekawa [490] 273–284 3.4–10.2 500 SynVis
Hydrogen Zhang et al. [739] 274–278 3.7–6.6 60 SynVisVar
Methylcyclohexane Mooijer-van et al. [520] 279–288 2.6–9.1 n.a. SynVis
Ohmura et al. [547] 275–281 1.5–3.3 201 SynNon
Sun et al. [660] 273–290 1.3–11.9 n.a. SynVisVar
Methylcyclopentane Makino et al. [494] 274–287 1.7–9.3 150 SynVis
Neohexane Ohmura et al. [546] 274–280 1.3–2.7 200 SynNon
Propene Ma et al. [486] 273–283 0.5–6.5 60 SynVis
Propylene oxide Seo et al. [613] 283–294 1.9–8.7 50 SynVis
Sodium chloride Jager and Sloan [110] 270–303 6.6–72.2 1 SynVisSpec
Kharrat and Dalmazzone [412] 269–278 4.2–8.6 n.a. SynNon
Sodium dodecyl sulfate Link et al. [102] 276–293 3.9–9.6 40 SynVis
Tetrafluoromethane (CFC-14) Mooijer-van et al. [520] 273–290 3.4–12.9 n.a. SynVis
Tetrahydrofuran De Deugd et al. [253] 289–306 2–14 n.a. SynVis
Tetrahydrofuran (THF) Seo et al. [613] 292–302 2–8.9 50 SynVis
Tetrahydropyran De Deugd et al. [253] 288–302 2–14 n.a. SynVis
Mooijer-van et al. [520] 293–303 3.4–13.5 n.a. SynVis
Trifluoromethane (HFC-23) Mooijer-van et al. [520] 282–297 0.9–12.9 n.a. SynVis
Methanol Natural near critical reservoir fluid (C1−C20+) Ostergaard et al. [551] 276–283 5.3–24.2 540 SynVis
Nitrogen 1,4-Dioxane Seo et al. [613] 275–283 3.7–11.8 50 SynVis
2,2-Dimethylpentane Ostergaard et al. [550] 275–280 15–26.4 540 SynVis
2-Methylbutane (isopentane) Ostergaard et al. [550] 276–282 14.9–30.2 540 SynVis
Acetone Seo et al. [613] 274–280 4.4–11.3 50 SynVis
Propylene oxide Seo et al. [613] 279–285 4–11.7 50 SynVis
Tetrahydrofuran (THF) Seo et al. [613] 287–293 4.3–10.8 50 SynVis
Propane Cyclobutanone Mooijer-van et al. [522] 276–277 0.2–12.8 n.a. SynVis
Cyclohexane Mooijer-van et al. [522] 274–276 0.1–9.9 n.a. SynVis
Methylcyclohexane Mooijer-van et al. [522] 274–277 0.1–7.8 n.a. SynVis
Tetrahydropyran Mooijer-van et al. [522] 274–276 0.1–4.8 n.a. SynVis
 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54 47

Table 56
Multicomponent and complex systems with hydrates: water + X + Y (+. . .).

X (+Y + . . .) Reference T (K) P (MPa) V (cm3 ) Method

Carbon dioxide + ethylene glycol + sodium cloride Majumdar et al. [493] 264–272 1.3–3.1 n.a. SynVisVar
Carbon dioxide + methane + hydrogen sulfide Sun et al. [658] 274–299 0.5–8.6 60 SynVisVar
Carbon dioxide + nitrogen + tetrahydrofuran Kang et al. [404] 274–295 0.2–12.9 70 AnTValVis
Hydrogen + methane + propane Zhang et al. [739] 274–280 0.6–4.9 60 SynVisVar
Hydrogen sulfide + ethylene glycol + sodium cloride Majumdar et al. [493] 273–289 0.2–1.4 n.a. SynVisVar
Methane + ethane + propane Ostergaard et al. [552] 276–290 1.4–7.9 540 SynVis
Methane + ethane + tetrahydrofuran Zhang et al. [738] 274–284 2–3 60 AnTVarVis
Methane + ethylene glycol + sodium chloride Eichholz et al. [278] 262–281 2.1–9.5 64–74 SynVisVar
Methane + magnesium chloride + sodium chloride Link et al. [102] 269–293 7.9–9.6 40 SynVis
Methane + methanol + sodium chloride Jager et al. [377] 249–281 2–16 n.a. SynVis
Jager et al. [377] 260–292 7.4–73.2 1 SynVisSpec
Methane + nitrogen + 2,2-dimethylpentane Ostergaard et al. [550] 276–286 6.2–22.6 540 SynVis
Methane + nitrogen + 2-methylbutane (isopentane) Ostergaard et al. [550] 276–284 5.1–15.4 540 SynVis
Hydrogen + methane + ethane + propane Zhang et al. [739] 274–279 1.1–7 60 SynVisVar
Methane + ethane + cyclohexane + propane Sun et al. [659] 273–289 0.6–6.2 n.a. SynVisVar
Methane + ethane + propane + methylcyclohexane Ostergaard et al. [552] 280–288 2.6–8.1 540 SynVis
Methane + ethane + propane + methylcyclopentane Ostergaard et al. [552] 278–288 2–7.7 540 SynVis
Methane + ethane + propane + 2-methylbutane (isopentane) Ostergaard et al. [552] 275–282 2–5.1 540 SynVis
Methane + ethane + propane + methylcyclohexane Sun et al. [660] 273–288 0.9–6.1 n.a. SynVisVar
Methane + ethylene glycol + potassium chloride + sodium chloride Masoudi et al. [501] 259–283 3.9–46.6 n.a. SynNon
Methane + ethane + propane + n-pentane + n-decane Ostergaard et al. [552] 279–286 1.2–3.8 540 SynVis
Methane + ethane + propane + n-pentane + n-decane + cyclohexane Ostergaard et al. [552] 276–284 0.8–3.1 540 SynVis
Methane + ethane + propane + n-pentane + n-decane + cyclopentane Ostergaard et al. [552] 278–287 0.2–4.2 540 SynVis
Methane + ethane + propane + n-pentane + n-decane + 2,2- Ostergaard et al. [552] 278–286 0.9–3.4 540 SynVis
dimethylpropane
(neopentane)
Methane + ethane + propane + n-pentane + n- Ostergaard et al. [552] 278–288 0.4–2.6 540 SynVis
decane + cyclopentane + 2,2-dimethylpropane
(neopentane)
Synthethic natural gas Ostergaard et al. [552] 276–290 1.2–7.6 540 SynVis
Natural gas—Alinta Gas Ltd., Perth, Australia + para-toluene sulfonic Gnanendran and Amin [333] 285–293 1.4–8 700 SynNonVisVar
acid
Synthethic natural gas + cyclohexane Ostergaard et al. [552] 277–292 1.1–9.6 540 SynVis
Synthethic natural gas + cyclopentane Ostergaard et al. [552] 283–288 1.2–3.1 540 SynVis
Synthethic natural gas + methylcyclopentane Ostergaard et al. [552] 278–289 1.7–7 540 SynVis

Table 57
Articles containing corrigenda, comments or rebuttals to comments.

Original article Year Components Article with corrigendum, comment, or rebuttal

Nikitin et al. [537] 1998 1-Alkanols (C13–C22) Nikitin et al. [538] 2000 Corrigendum
Xia et al. [712] 1999 CO2 , water, sodium acetate, Xia et al. [713] 2000 Corrigendum
ammonium acetate
Bobbo et al. [177] 2000 HFC-125, HFC-236ea, HFC-32 Deiters [258] 2001 Comments
da Silva and Barbosa [243] 2000 CO2 , n-butanal Coquelet et al. [234] 2002 Comments
da Silva and Barbosa [246] 2002 Rebuttal to Comments
Lee et al. [445] 2000 CO2 , C.I. Disperse Blue 3, C.I. Lee et al. [446] 2001 Corrigendum
Disperse Blue 79
Sako et al. [596] 2001 5 fluorinated ethers and 2 Sako et al. [597] 2002 Corrigendum
fluorinated ketones
García-González et al. [323] 2002 CO2 , hydroquinone, p-quinone Deiters [259] 2003 Comments
Kato et al. [407] 2002 HFC-32, HFC-125 Kato et al. [408] 2004 Corrigendum
Zhang and Kiran [740] 2003 CO2 , tetrahydrofuran, polysulfone Zhang and Kiran [741] 2006 Corrigendum
Gozalpour et al. [337] 2003 Methane, propane, n-pentane, Gozalpour et al. [338] 2003 Corrigendum
n-decane, n-hexadecane
Chapoy et al. [214] 2003 Methane, water, methane hydrate Chapoy et al. [220] 2005 Corrigendum
Kamps et al. [403] 2003 CO2 , [bmim][PF6] Kumelan et al. [433] 2006 Corrigendum
Kiepe et al. [415] 2003 Methane, water, lithium bromide Kiepe et al. [417] 2004 Corrigendum
Nikitin et al. [57] 2003 CO2 , polystyrene Nikitin et al. [58] 2003 Corrigendum
Glos et al. [331] 2004 Propane, 2-methylpopane, Glos et al. [332] 2006 Corrigendum
n-butane, propylene
Levitin et al. [454] 2004 CO2 , methanol, water, Levitin et al. [455] 2005 Corrigendum
tetramethylammonium
bicarbonate
48 R. Dohrn et al. / Fluid Phase Equilibria 288 (2010) 1–54
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