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MASS ANALYSIS

The mass of following fragments were observed after doing MALDI.

STRUCTURE

(MASS 395.45)

After first Fmoc-cleavage by usual 20% piperidine in DMF, some of Fmoc has still been left.

STRUCTURE

(MASS 492.57)

Fmoc-cleavage is ineffective even after using 2% DBU in DMF. Cleave done twice for 5 minutes.

STRUCTURE

(MASS 648.76)

This is desired peptide.