Name: Loo Fu Hong

Class : 6R1O Hong

Experiment 5
Topic
: Volumetric – stochiometry
Purpose
: to determine the exact concentration of monobasic acid, HX
Question : you are provided with a monobasic acid, HX, with a concentration in the range of 0.5 mol dm-3
to 1.0 mol dm-3. You are required to plan and carry out an experiment to determine the
exact concentration of the HX solution provided.
Materials
KA 1 is a solution containing an unknown acid, HX with a concentration varying
from
0.5 mol dm-3 to 1.0 mol dm-3
KA2 is a solution containing sodium hydroxide, NAOH with a concentration of 1.0
mol
dm-3
Phenolphthalein as indicator
Apparatus
Weighing bottle, volumetric flask 500 ml or 500 cm3, electric balance, filter funnel, wash
bottles, droppers, beaker, retort stand, burette, pipette, sucker, conical flasks, white tiles,
distilled water and a spatula.
Precaution
1. Sodium in metal form is highly reactive. Wearing protective gears and precautionary steps
are taken to minimize accidents during the process of cutting Sodium (natrium , Na) solids.
2.Handle sodium metal with gloves. Sodium is reactive when come in contact
with
water.
Introduction
Preparation of a standard solution of sodium hydroxide, NaOH is done by dissolving pure
sodium metals in water, H2O. In the process, small sparks are seen as the reaction takes
place. The Na+ ions react with OH- ions to form sodium hydroxide solution which used in
second part of the experiment. Sodium hydroxide solution can be prepared by dissolving
sodium hydroxide pellets with certain amount of water to get suitable molarity.
Procedure:
Part 1: preparing a standard solution of 1.0 mol dm-3 sodium hydroxide,
NaOH.
1. A electronic balance and weighing bottle are used to weigh 10 g of sodium
hydroxide powder using a spatula.
2. The solid are carefully tipped into a beaker containing distilled water.
3. Any solids remaining in the weighing bottle is washed into the beaker into the
beaker with a wash bottle.
4.After dissolving the solid, the final solution is carefully transferred into the
volumetric flask using a glass rod and a filter funnel.
5. About reaching the volume needed, stop at 1 or 2 cm from the line. By using
a
dropper or a wash bottle, carefully filling it until the mark.
6. The flask is then shaken to mix the solution thoroughly.
7.The solution prepared is a standard solution of 1.0 mol dm-3 or 1.0M.
Part 2: Titration of 1.0 mol dm-3 sodium hydroxide, NaOH, with an unknown
acid, HX with a concentration between 0.5 mol dm-3 to 1.0 mol dm-3
Pipette 25cm3 of KA1 into the titration flask. Titre the solution with KA2.
Repeat titration as many times as you think it is necessarily to achieve accurate
results.
Results:
Part1 : calculation
Molar mass of NaOH = 23+16+1 =40g

massmolar mass×1volume=molarity@number of moles of solutevolume of solution

number of moles=MV1000

mass ofsolute=number of moles of solution ×molecular mass of the solution

Use: MV1000×molecular mass of NaOH

1mol dm-3 1000×500×40g

=20g of NaOH powder required to prepare 500cm 3 1.0 mol dm-3sodium hydroxide solution

,NaOH solution
Part 2
Titration
Rough
Accurate
First
Second
Third
Final reading
/ cm3
Intitial

reading/ cm3
Volume of
KA2/ cm3
i)
25cm3 of KA 1 required__________cm3 of KA 2 for a complete reaction.
Calculation:

Experiment 5 Chemistry
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monoabasic acid
exact concentation
chemistry experiments
stoichiometry
stpm practical
acid hx
(more tags)
monoabasic acid
exact concentation
chemistry experiments
stoichiometry
stpm practical
acid hx
form
exact concentration
hydroxide
determine
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hong
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Mah Chunkit left a comment

whr the calculations of part 2?
08 / 13 / 2010

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