Professional Documents
Culture Documents
Introduction
Fatigue is the progressive and localized structural damage
that occurs when a material is subjected to cyclic loading.
If the local stresses are high enough, this will lead to
the initiation of a crack, the growth of the crack and
finally fracture. Many dramatic and severe accidents are
caused by fatigue and it is essential that the structural
engineer includes fatigue into design considerations.
This issue of Acom focuses first on one very specific
application where the combined effect of fatigue and
corrosion is present. This is an application where the
fatigue data generated is crucial for the design.
The second paper is on the fatigue of lap joins.
These joints are very common in many applications,
such as in the automotive industry. Extensive testing
has shown that different joining methods gives similar
fatigue strength. Further on, the fatigue strength of spot
welded joints is independent of the strength of the
base material.
www.outokumpu.com
|
acom 3 - 2010 2
Summary of corrosion
fatigue test data
for duplex suction roll
shell material
Hans Groth, Asko Kähönen, Claes Tigerstrand, Sophia Ekman,
Marcus Andersson and Daniel Eyzop, Outokumpu Stainless AB, Sweden
Abstract
Corrosion fatigue is a process in which a metal fractures prematurely under conditions
of simultaneous corrosion and repeated cyclic loading. This process takes place at lower
stress levels and/or fewer cycles than would be required in the absence of the corrosive
environment. Corrosion fatigue is an especially important area for products like suction
rolls in paper machinery. High corrosion fatigue strength is crucial for the long life and
reliable performance of a suction roll. The combination of a complicated component and
a corrosive environment put high requirements on the material. Since extensive machining
and gun-drilling is carried out, the machinability of the material must be satisfactory; up
to 1 million holes need to be drilled in the largest suction rolls.
The present paper summarize results from corrosion fatigue testing from 1987 to 2009
of duplex stainless steels for suction rolls in paper machines. Testing of materials for suction
rolls actually started in 1973–74, but the production route for the material has changed
since then and only material relevant to the production route of today is included in this
summary. The presented test data includes 3RE60 SRG (Suction Roll Grade), 2304 SRG,
2205 SRG and LDX 2101®.
Keywords: corrosion fatigue, suction roll, duplex stainless steels, paper machine,
improved machinability, fatigue testing, testing frequency.
Background
Outokumpu Prefab AB
Outokumpu Prefab AB, henceforth called simply “Prefab”, is a fully owned subsidiary of
Outokumpu Stainless, located in Avesta, Sweden. Prefab processes stainless steel plates
into value added products and has over 80 years experience in fabrication of stainless steel
products. Prefab is one of the world’s leading producers of stainless steel Suction Roll
Shells (SRS:s) for the paper machine industry and the only global producer fabricating
these shells from thick plates, see Figure 1.
Fig. 3 D
imension range of suction In 1973 the first SRS was produced by Prefab made of the stainless steel grade 3RE60.
roll shells. The customer was the Swedish Paper machine company KMW, now Metso Paper
Karlstad AB. Prefab has since then produced over 2500 stainless SRS:s with very
few failures despite the use of shells in very demanding applications.
12 m
30–105
mm Manufacturing of suction roll shells
500–2000
mm Fabrication of a SRS from heavy plates at Prefab includes hot roll-bending of plates to
round segments, see Figure 2, longitudinally joining using the electro-slag (ES) welding
process and circumferential joining by narrow gap submerged arc welding (SAW). All welds
are ultrasonically tested by automatic equipment. Finally, the SRS is heat treated vertically
for stress-relieving. The manufacturing process is described in more detail below. Figure 3
shows the typical dimension range of a SRS.
Fig. 4 A
nnealing of a large suction
The manufacturing process begins with an ultrasonic test of the plate. Thereafter, the
roll shell. plate is heated up and the edges are pre-bent to produce the correct curvature in the edge
zone of the plate and then roll-bent into a cylindrical segment – also at high temperature.
Before welding a SRS segment, the segment undergoes further ultrasonic inspection and
the machined joint surface is checked using dye penetrant. ES-welding is then used to
produce the longitudinal weld, using a filler metal specially produced for this purpose.
ES welding is one of the best controlled welding processes and the resultant weld metal
is of the highest quality. Somewhere between two and seven of these roll-bent segments
are welded together to form one SRS. The circumferential welds are produced using a
machined double-J groove configuration. The inside of the shell is welded and then
back gouged from the outside. The weld is then filled from the outside using a specially
developed narrow gap SAW, again using a filler metal designed to match the properties
of the plate in the final annealed condition. For the ultrasonic testing of the ES weld, six
probes with different angles are used and for the narrow gap weld, seven probes are used
to ensure the reliability of the method applied for thick plates.
The most critical step in the manufacture of a shell is the annealing. The shells are
annealed in a vertical position, see Figure 4. The roll is monitored by pairs of thermocouples
located at matching positions both inside and outside the roll and at various positions
along the length. The thermocouples make it possible to confirm the uniformity of the
shell temperature during the period that the shell remains at the annealing temperature.
Even more important is to control the air cooling to ensure that the entire roll cools
uniformly. At no time should the difference in temperature exceed 150°C between any
two of the thermocouples on the roll. In practice, this temperature difference is typically
around 100°C in the beginning of the cooling process and then falls below 50°C. This
Fig. 5 A suction roll shell ready uniformity assures low residual stress in the SRS:s. Finally, Figure 5 shows a suction roll
for delivery. shell ready for delivery.
Typical chemical properties of materials tested. All values given in weight percent. SRG = Suction Roll Grade. Table 1
Grade C Si Mn P S Cr Ni Mo N Cu
3RE60 SRG 0.02 1.50 1.50 0.02 0.02 18.50 4.90 2.80 0.08 0.2
LDX 2101 ®
0.03 0.70 5.00 – – 21.50 1.50 0.30 0.22 0.2
2304 SRG 0.02 0.80 1.45 0.02 0.02 22.70 4.65 0.30 0.09 0.2
2205 SRG 0.02 0.63 1.35 0.02 0.02 22.00 5.70 2.92 0.13 0.12
|
acom 3 - 2010 4
welded together from hot rolled duplex stainless steel plates with filler having chemical
and mechanical properties optimized for suction roll applications.
Due to very similar microstructure and mechanical properties of weld and base material
the inherent fatigue strength of the weld material is on the same level as the base material.
The microstructure of the weld is in many ways similar to that of a casting, the alternative
manufacturing approach. However, the weld is subjected to much greater control, will
have a much finer structure, will solidify with few, if any, casting defects (and these will
be removed when detected by testing) and with less segregation of the major alloying
elements during solidification.
Enhanced machinability
The suction roll grades, also called SRG:s, have undergone a special treatment to enhance
the machinability, called PRODEC® treatment. This is a special metallurgical treatment in the
melting shop that controls the amount, size, shape and distribution of non-metallic inclusions
within the steel, primarily oxides and sulphides. The PRODEC® treatment vastly improves the
machinability of the steel. Turning and drilling can be performed much faster and tools last
longer. The machinability of LDX 2101® is very good in itself so no “SRG” version is needed.
Corrosion
Corrosion fatigue can be initiated by pitting corrosion. This may occur on martensitic
stainless steels in paper machines, but has not been reported for duplex stainless steels.
This is probably due to their higher pitting resistance by virtue of the increased amount of
chromium, nitrogen and molybdenum. The PRE-value (Pitting Resistance Equivalent)
is calculated according to equation (1) and provides a rough estimation of the pitting
corrosion resistance; a higher PRE-value indicates a higher corrosion resistance.
Table 3 shows PRE-values and measured critical pitting temperatures (CPT) determined
according to a modified version of ASTM G150, in a synthetic white water solution
(400 ppm Cl- + 250 ppm SO42-) with samples wet surface ground to 320 mesh. The CPT
values are given as the range (min-max) seen in four measurements (except for 2205 SRG
which is for two measurements).
The PRE- and CPT-values in Table 3 give similar ranking of the corrosion resistance of
the grades and reflect the differences in alloy composition.
Resistance to chloride induced pitting corrosion becomes more important when the
chloride content of white waters increases as a consequence of closed paper mill process
systems. In such circumstances, the high pitting resistance of 2205 SRG could be favourable
and also contribute to the resistance to corrosion fatigue.
Corrosion fatigue
Fatigue strength is sensitive to the service environment. Corrosion fatigue is the result
of the combined action of fluctuating stress and a corrosive environment. The fatigue
process is thought to cause rupture of the protective passive film, so corrosion is accelerated.
The introduction of a corrosive environment often eliminates the normal “fatigue limit”
of a ferrous alloy, thereby creating a finite life regardless of stress level. More aggressive
corrosive conditions and lower loading frequencies will reduce the fatigue life. During
very high frequency loading there is less time for the corrosion process to act. At lower
frequencies, the corrosion process is more pronounced and can cause local attack that acts
as a stress concentration site and thus contributes to a shorter life.
Experimental technique
Tests were all conducted by Outokumpu Stainless AB at Avesta Research Centre (ARC),
in three rotating bending fatigue machines, type Schenk seen in Figure 6, with specimen
design according to Figure 7.
Fig. 6 Corrosion fatigue testing machine Fig. 7 Corrosion fatigue test specimen geometry. Final polishing in the
at Avesta Research Centre. longitudinal direction.
226 ±1
1,5 x 45° 96 ±2 65
0,4
ø 7,52 h6
R 25
Tests were carried out with smooth polished specimens tested in a four point rotating
bending machine where R = s min/s max = -1. To attain the closest resemblance to the
actual loading environment in a paper machine a test frequency of about 5 Hz should be
used. Due to the fact that the testing is very time-consuming, a frequency of 25 Hz was
used for all tests conducted before 1987. The test data presented here is based on either
5 or 25 Hz. One typical series consists of 30 test specimens. The test results have been
evaluated before year 2000 by the staircase method and later by use of the Probit method.
During testing, the specimens have been flushed with synthetic white water at room
temperature (pH = 3.5, Cl- = 400 ppm, SO42- = 250 ppm). Other fluids have also been
used historically, but the synthetic white water is by far the most common.
An example of fatigue test data, both for base material and welds, is presented in
Figure 8. The results for the welded joints are included for comparison.
acom 3 - 2010 | 6
Fig. 8 Some selected test results from test specimens including welds.
All tests at 5 Hz.
400
350
250
200
150
100
50
0
105 106 107
Number of cycles to failure
Fig. 9 Fatigue strength at 50% failure probability at 107 cycles for suction roll materials at 5 and 25 Hz. The tests are sorted by
grade and testing frequency. The following notation is used: /SAW/ or /ES/ refers to submerged arc welding and
electroslag welding respectively, /5/ or /25/ refers to the testing frequency, and /Giga/ refers to testing at 108 cycles.
5 Hz measurement 25 Hz measurement
300
250
Stress amplitude (MPa)
200
150
100
50
0
3RE60 SRG/5
3RE60 SRG/5
3RE60 SRG/5
3RE60 SRG/5
3RE60 SRG/5
LDX 2101® /5
2304 SRG/5
2304 SRG/5
2205 SRG/5
2205 SRG/5
2205 SRG/5
2205 SRG/5
2205 SRG/5
2205 SRG/5
2304 SRG/ES/5
3RE60 SRG/25
2205 SRG/25
2205 SRG/25
2205 SRG/25
2205 SRG/25
2205 SRG/ES/25
2205 SRG/ES/25
2205 SRG/SAW/25
2205 SRG/SAW/25
3RE60 SRG/Giga/25
2205 SRG/ES/5
Welded Welded
|
acom 3 - 2010 7
For 2205 SRG this effect is around 50 MPa if the frequency is decreased from 25 to
5 Hz. Many tests have been made on both levels. The drop is in the same range for
3RE60 SRG, but there has only been one test made at 25 Hz for this grade.
The fatigue strength of the base material at 5 Hz is lowest for 3RE60 SRG, slightly
below 200 MPa, for 2205 SRG slightly over 200 MPa, a little higher for 2304 SRG at
about 220 MPa and the highest value for LDX 2101®. For LDX 2101®, that is a
relatively new grade, only one test series have been performed.
Figure 9 shows a ranking of the different grades, based on the PRE, CPT, Rp0.2 and
the actual fatigue test data. The fatigue ranking from testing does not seem to be related
to the typical proof strength values, Table 2, or to the PRE/CPT in Table 3. In normal
cases without a corrosive environment, the proof strength of a material gives an indication
of the fatigue strength level. Here this correlation is not at all clear. The difference in
proof strength is relatively small, which would suggest that the fatigue strength should
be on the same level for all grades.
The corrosion parameters, PRE and CPT, have an almost reversed correlation to the
corrosion fatigue result, suggesting that the environment is so mild that the corrosiveness
has little influence.
The conclusion that can be drawn from Figure 10 is that it is not possible to rank
materials, simply by comparing PRE, CPT and proof strength. Instead, real testing
has to be carried out.
Fig. 10 Relative ranking of properties for suction roll materials in terms of PRE,
CPT, Rp0.2 and 50% fracture probability at 107 cycles at 5Hz. A value of
1.0 corresponds to the mean value of the parameter.
1.60
1.20
1.00
0.80
0.60
0.40
0.20
0
PRE CPT Rp0.2 Testing at 5 Hz
Influence of welding
Quite extensive testing of welds has been made for 2205 SRG at 25 Hz. With one exception,
the welds for this material have about the same fatigue strength as the base material.
For 2304 SRG the only tested weld is on the same level as the base material.
Based on the relative large number of tests for 2205 SRG welds it can be concluded
that the fatigue strength of the weld is at a similar level to the base material. The data
available for 2304 SRG and 3RE60 SRG are very limited and no clear conclusion can
be made. More testing is advisable for 2304 SRG and 3RE60 SRG in different welded
conditions.
|
acom 3 - 2010 8
Fig. 11 3RE60 SRG test data at 108 cycles. RO stands for Run Outs, not failed
at 108 cycles.
200
180
4 xRO
160
5 xRO
140
Stress amplitude (MPa)
2 xRO
120
100
80
60
40
20
0
107 Number of cycles 108
Fig. 12 Fatigue strength for grade 3RE60 SRG, with a comparison between data
at 107 and 108 cycles.
300
250
Stress amplitude (MPa)
200
150
100
50
0
3RE60 SRG/Giga/25
3RE60 SRG/5
3RE60 SRG/5
3RE60 SRG/5
3RE60 SRG/5
3RE60 SRG/5
3RE60 SRG/25
|
acom 3 - 2010 9
Conclusions
– When the testing frequency is reduced from 25 to 5 Hz the fatigue strength will be
significantly reduced, probably due to longer exposure times in the corrosive solution.
– A conclusion that can be made is that it is not possible to rank materials simply by
comparing PRE, CPT (in the actual testing solution) or proof strength. Instead, real
testing has to be performed.
– More testing is advisable for 2304 SRG and 3RE60 SRG in different welded
conditions and for LDX 2101® for both base material and welds.
– LDX 2101® and 2304 SRG seem to have a somewhat higher fatigue life than
2205 SRG and 3RE60 SRG in the particular testing environment used. However,
the 2205 SRG grade offers a larger safety margin in more corrosive environments.
– The 107 cycles fatigue life was decided as an appropriate level for the fatigue
strength analysis in the past. Longer lives have seldom been tested because it is
so time-consuming. This is especially true for low testing frequencies of 5 Hz.
The tendency today, however, is to consider longer lifetimes.
– Testing at 108 cycles compared to 107 cycles reduces the fatigue strength for
3RE60 SRG from roughly 250 MPa down to 150 MPa.
References
[1] Outokumpu Corrosion Handbook, Tenth Edition, 2009.
|
acom 3 - 2010 10
Fatigue properties
of thin sheet stainless
steel lap joints
Hans Nordberg, Formerly head of Outokumpu
Stainless Research Foundation, Sweden
Hans Groth, Outokumpu Stainless AB, Sweden
Abstract
A review of a number of studies performed within the Outokumpu Stainless Research
Foundation covering properties of stainless steel overlap joints is presented. The type of
joints covered are:
i) spot welded stainless to stainless and stainless to galvanised carbon steel,
ii) adhesive bonded stainless to stainless,
iii) weld bonded stainless to stainless,
iv) laser welded stainless to stainless and stainless to galvanised carbon steel,
v) clinched stainless to stainless steel.
The materials studied are 4301(304) and 4310 (301) stainless steels and high strength
duplex stainless steels. The thickness range is 0.7 – 4.0 mm. Fatigue properties in terms
of Wöhler curves are compared between the different joining methods using the concept
of load transfer capacity per unit length of the joints.
Fatigue strength is shown to be independent of material strength for spot welded joints.
Spot welded, laser welded and clinched joints show similar fatigue properties for 1 mm
sheet. Adhesive bonded joints are stronger than spot-weld bonded joints.
Keywords: fatigue lap joints, stainless steel, spot-welding, laser welding, adhesive bonding
clinching.
Introduction
Structural applications represent one of the fastest growing segments for stainless steel. In
the US market, 20 percent of all stainless steel is estimated to be used in this market sector.
A good example of a growing sub-segment is in transportation, e.g. in buses and trains.
It is not only the corrosion resistance of stainless steels which is of interest. To further
increase the penetration of this market it is important to develop understanding of the
mechanical properties of stainless steel and stainless steel structural elements. This implies,
among other things, a need to develop joining techniques suitable for these applications,
to establish the behaviour of structural elements under static and dynamic loads and to
develop design guidelines.
In the basic mill-annealed condition stainless steel grades are available with typical yield
strengths ranging from 260 to 620 MPa. In the temper rolled (cold rolled) condition, grades
are available with yield strengths of from 350 to over 2000 MPa. The high strengths
available will lead to lighter, more slender structures based on thin sheet panels, shells
and other components. Design aspects are important if the high strength can be utilized
or not.
The thin sections will call for new and innovative techniques for fabrication and joining.
Traditional butt welding techniques will still be used, but the thin section will make it
feasible to join with other methods using overlap type of joints.
In present paper, a number of overlap joining methods are considered with special
focus on the fatigue properties of such joints. Most of the results presented are results
|
acom 3 - 2010 11
Single-overlap joint
The basic types of overlap joints are shown schematically in Figure 1. The joining
technique is illustrated as adhesive bonding but could equally well be spot welding, laser
welding, clinching, riveting or a combination of these. The single lap joint with some
modification is, for obvious reason, the most widely used.
For a spot welded joint the line load is thus calculated as load per nugget divided by
the pitch calculated by Eq. (1), where t1 and t2 are the thickness of the joined sheets.
|
acom 3 - 2010 12
Materials
The nominal chemical compositions of the materials in this paper are given in Table 1.
Material C Cr Ni Mo Mn Other
4301 (304) 0.02 18 9
4310 (301) 0.10 17 7
4401 (316) 0.02 18 12 2.5
LDX 2101®1 0.02 21 1.5 5 N
2304 0.02 23 4 N
2205 0.02 22 5 3 N
1
LDX 2101® is an Outokumpu registered trade mark
Fig. 2 Stress intensity ranges versus number of cycles to failure for all specimen
types, sheet thickness and steel grades. 95% confidence limits are shown.
100
Stress intensity range ∆Keff [MPa . m1/2]
10
1
10 000 100 000 1 000 000 10 000 000
Fig. 3 S-N curve for 4 mm flanged specimen and 1.5 mm specimen overlap
joint in grade 4301.
1000
100
10
1 000 10 000 100 000 1 000 000 10 000 000
Number of cycles to failure
For the 4 mm thick material using the stiff “Box” specimen the fatigue strength at 2 . 106
cycles is estimated to be 500 N.mm-1 compared with 80 N.mm-1 for the thinner material
in the overlap joint configuration. For longer lives the increased bond-line thickness does
not affect the strength.
Although results from dry air testing [8 –10] indicate a dramatic increase in fatigue
strength going from spot welding to adhesive bonding, a number of questions about
adhesive bonding have to be resolved. The long-term behaviour and the effect of different
environments on bonded joints needs special attention.
1000
10
1 000 10 000 100 000 1 000 000 10 000 000
Number of cycles to failure
1.2 mm V1437 (top) 1 mm 304 lap weld 1 mm 304 (top) 1.2 mm V1437 lap weld
1.2 mm V1437 (top) 0.78 mm 2205 lap weld 0.78 mm 2205 (top) 1.2 mm V1437 lap weld
1 mm LDX 2101® lap weld 1.2 mm V1437 (top) 1 mm LDX 2101®
1.2 mm V1437 (top) 1 mm 2205 1 mm LDX 2101® 1.2 mm V1437 butt weld
Fig. 5 S-N curves for 1 mm clinched lap shear joints, grade 4301
with two different Ni-levels.
10
Round clinch
CrNi18 12
CrNi18 10
Load range (kN)
2.2 kN
1.6 kN
1
100 000 1 000 000 10 000 000
Number of cycles to failure
Sjöström [15] tested three grades with different austenite stability; 4301, 4310 and 4401,
all annealed. As opposed to [14] for round clinch the fatigue properties increases rapidly
with increasing degree of microstructural stability and decreasing strength for the rectangular
clinch. The fact that rectangular clinches contains macrocracks (clinch size) normal
to the loading direction could explain the different response to the strength in the
deformed (clinched) area. Round clinched joints have about twice the fatigue strength
of the rectangular clinched joints.
|
acom 3 - 2010 15
Summary
– Fatigue strength is shown to be independent of material strength for spot welded
joints.
– Spot welded, laser welded and clinched joints show similar fatigue properties
for 0.8 – 1.5 mm sheet thickness of about 70 N.mm-1.
– Adhesive bonded joints are five times stronger in fatigue loading compared to spot
welded joints.
– Weld-bonded joints show a fatigue strength between spot welded and adhesive
bonded joints.
References
[1] Nordberg H., Fatigue Properties of Stainless Steel Lap Joints, SAE paper
2005-01-1324.
[2] Final Technical Report, Light & Safe-Weight Reduction for Safer, Affordable
Passenger Cars by using extra Formable High Strength Austenitic Steel, European
Community under the ‘Competitive and Sustainable Growth’ Programme, 2005.
[3] Goland M. and Reissner E. J., Appl. Mech., 1944, Vol. 2, p. A-17.
[4] Linder, J. et al. Swedish Institute for Metals Research, Report IM-3475, 1997.
[5] Linder, J. et al. Fatigue Data and Design Methods for Spot Welded Austenitic
and Duplex Stainless Sheet Steels. In Stainless Steels in Transport Industry.
Espoo, Finland, 1998.
[6] Wray T., Resistance Spot Welding Of Duplex Stainless Steel, PhD Thesis,
Sheffield Hallam University, 2004.
[7] Marples M., PhD programme, Sheffield Hallam University, 2002.
[8] Boyes R., Adhesive Bonding of Stainless Steel; Strength and durability.
PhD Thesis, Sheffield Hallam University, 1998.
[9] S.McCann S., PhD programme, Sheffield Hallam University, 2003.
[10] Ring-Groth M., Adhesive Bonding and Weldbonding of Stainless Steel,
Lic. thesis, Luleå University of Technology, Luleå, 1998.
[11] Kaitanov A., Static and Fatigue Strengths of Laser Welded Over-Lap Joints
with Controlled Penetration. Progress Rep., State Univ. of Marine Tech.,
St.Petersburg, 2002.
[12] Dinsley C., Laser Welding of Austenitic and Duplex Stainless Steel to
Zinc-Coated Mild Steel. PhD thesis. Sheffield Hallam University, 2004.
[13] Linder J., et al., Fatigue Strength of Laserwelded Stainless Steel Sheets,
Swedish Institute for Metals Research Report IM-2000-529.
[14] Jacobsen J., Beitrag zum umformtechnischen Fügen von Stahlblechteilen
mit vorwiegend Austenitischem Gefüge, Tech. Univ. Hamburg-Harburg,
Dr.-Ing Dissertation, 1997.
[15] Sjöström P., Mechanical Properties of stainless steel clinched joint, Linköping
studies in science and technology, thesis no 1247, Linköping University, 2006.
This document is for information only and seeks to provide professionals with the best possible
information to enable them to make appropriate choices. Although every effort has been made to ensure
the accuracy of the information provided in this document, Outokumpu can not accept any responsibility
for any loss, damage or other consequence resulting from the use of this publication.
The information provided herein may be subject to alterations without notice.
www.outokumpu.com