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Specimen
Eyepiece
Projector CRT
Cathode
Ray Tube
detector
OM TEM SEM
Glass Magnetic
coils
Under vacuum
PERBEDAAN MO DAN SEM
W or LaB6 Filament
Thermionic or Field Emission Gun
ELEKTRON YANG BERHAMBUR DAN
DITANGKAP SEM SAAT SAMPEL
DITEMBAK ELEKTRON
HAMBURAN ELEKTRON DIDETEKSI DAN
ENERGINYA DITAMPILKAN DALAM BENTUK
GAMBAR DAN GRAFIK
Tiap Jenis hamburan elektron
ditangkap detektor yang
berbeda
Tempat Sampel
TEMPAT SAMPEL DI SCANNING
ELECTRON MICROSCOPE
PENGAMATAN DENGAN SCANNING
ELECTRON MICROSCOPE
Perbesaran
OM 4x – 1000x
SEM 10x – 3000000x
Aplikasi :
•Mengamati struktur maupun
bentuk permukaan yang
berskala lebih halus
•Dilengkapi Dengan EDS
(Electron Dispersive X ray
Spectroscopy)
•Dapat mendeteksi unsur2
dalam material.
•Permukaan yang diamati
harus penghantar elektron
Keuntungan SEM terhadap OM
Perbesaran Depth of Field Resolusi
OM 4x – 1000x 15.5mm – 0.19mm ~ 0.2mm
SEM 10x – 3000000x 4mm – 0.4mm 1-10nm
A More e- beam
Detaile
d Look
Inside
Source: L. Reimer,
“Scanning Electron
Microscope”, 2nd Ed.,
Springer-Verlag, 1998, p.2
Preparasi Sampel
• Hindari semua air, larutan atau
material-material lain yang mudah
menguap dalam vakum.
• Permukaan harus rata untuk BSE dan
OIM
• Tentukan jumlah sample.
• Samples Non-logam, seperti building
materials, insulating ceramics, harus di
caoting agar konduktivitas listriknya
baik. Logam dan samples konduktivitas
dapat diletakan langsung kedalam SEM.
Image Magnification
• A tungsten filament
heated by DC to
approximately 2700K or
LaB6 rod heated to around
2000K
• A vacuum of 10-3 Pa (10-4
Pa for LaB6) is needed to
prevent oxidation of the
filament
• Electrons “boil off” from
the tip of the filament
• Electrons are accelerated
by an acceleration voltage
of 1-50kV
Field Emission Gun
• The tip of a tungsten needle is
made very sharp (radius < 0.1
mm)
• The electric field at the tip is
very strong (> 107 V/cm) due
to the sharp point effect
• Electrons are pulled out from
the tip by the strong electric
field
• Ultra-high vacuum (better than
10-6 Pa) is needed to avoid ion
bombardment to the tip from
the residual gas.
• Electron probe diameter < 1
nm is possible
Source of Electrons
Thermionic Gun E: >10MV/cm
T: ~1500oC
W
Filament
(5-50mm)
(5nm)
Objective
lens
Sample stage
Coating Techniques