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NERACA PANAS SEKITAR VAPORIZER

Nama alat :

OX tank

Kode alat :

T-01

P operasi :

760

T operasi :

303.15

T reff :

298.15

a. Menghitung panas masuk vaporizer
T reff (K) :

298.15

T out (K) :

303.15

Komponen

BM

O-xylene

106.167

M-xylene

106.167

TOTAL

F1 (kg/jam)
3547.76

ni (kmol/jam)

Xi

A

B

C

D

E

33.42

0.9800

8.1200E-01

5.1344E-01

-2.0212E-04

-2.1615E-08

2.3212E-11

72.40

0.68

0.0200

-1.6725E+01

5.6424E-01

-2.6465E-04

1.3381E-08

1.5869E-11

3620.16

34.10

1.0000

b. Menentukan panas keluar vaporizer
Nama alat :

Vaporizer

Kode alat :

V-01

P operasi :

1026

A. Menentukan T bubble
T bubble (K)
Komponen

:

429.28 k
BM

F1 (kg/jam)

ni (kmol/jam)

1.5613E+02 C
Xi

A

B

C

D

E

O-xylene

106.167

3547.76

33.4168

0.9800

3.7241E+01

-3.4573E+03

-1.0126E+01

9.0676E-11

2.6123E-06

M-xylene

106.167

72.40

0.6820

0.0200

3.4680E+01

-3.2981E+03

-9.2570E+00

-4.3563E-10

2.4103E-06

3620.16

34.0988

1.0000

TOTAL

B. Menentukan T dew
T dew (K)

:

Komponen

1.5615E+02

429.30 K
BM

F1 (kg/jam)

ni (kmol/jam)

Yi

A

C
B

C

D

E

O-xylene

106.167

3547.76

33.4168

0.9800

3.7241E+01

-3.4573E+03

-1.0126E+01

9.0676E-11

2.6123E-06

M-xylene

106.167

72.40

0.6820

0.0200

3.4680E+01

-3.2981E+03

-9.2570E+00

-4.3563E-10

2.4103E-06

3620.16

34.0988

1.0000

TOTAL

Jadi OX keluar vaporizer pada 429,3 K dan 1026 mmHg
T input :

303.15

T output :

429.30

Menghitung panas penguapan
T dew (K) :

Komponen

429.30

BM

F1 (kg/jam)

ni (kmol/jam)

A

Tc (K)

n

Hv (kJ/jam)

O-xylene

106.167

3547.76

33.42

5.5606E+01

6.3037E+02

3.7500E-01

36.23

M-xylene

106.167

72.40

0.68

6.0216E+01

6.1705E+02

4.5800E-01

34.92

3620.16

34.10

TOTAL

71.14

Menghitung panas sensibel
T reff (K) :

298.15

T out (K) :

429.30

Komponen

BM

O-xylene

106.167

M-xylene

106.167

TOTAL

F1 (kg/jam)
3547.76

ni (kmol/jam)

Xi

A

B

C

D

E

33.42

0.9800

8.1200E-01

5.1344E-01

-2.0212E-04

-2.1615E-08

2.3212E-11

72.40

0.68

0.0200

-1.6725E+01

5.6424E-01

-2.6465E-04

1.3381E-08

1.5869E-11

3620.16

34.10

1.0000

NERACA PANAS
Cp mean medium pemanas (kJ/kg K) :

4.39

Kebutuhan medium pemanas (kJ/jam)

:

Kebutuhan medium pemanas (kg/jam)

:

691320.85
5520.64

Panas yang dilepas pemanas (kJ/jam) :

2369296.94

H input (kJ/jam) :

23250.13

T in med (K) =

473.15

H output (kJ/jam) :

714570.98

T out med (K) =

375.37

1677976.09

A
NERACA PANAS SEKITAR HE-01
Nama alat :

9.2053E+01
Air Blower

Kode alat :

B-01

T in (K) :

303.15

P in

(mmHg) :

760.00

T trial (K) :

303.18

P out (mmHg) :

1064.00

Komponen

BM

F2 (kg/jam)

ni (kmol/jam)

Yi

A

B

C

D

E

Oxygen

32.000

17558.50

548.70

0.1888

2.9526E+01

-8.8889E-03

3.8083E-05

-3.2629E-08

8.8607E-12

Nitrogen

28.014

66053.50

2357.87

0.8112

2.9342E+01

-3.5395E-03

1.0076E-05

-4.3116E-09

2.5935E-13

83612.00

2906.58

1.0000

TOTAL
a. Menentukan panas masuk HE-01
T reff (K) :

298.15

T in (K) :

303.18

Komponen

BM

F2 (kg/jam)

ni (kmol/jam)

Yi

A

B

C

D

E

9342E+01 -3.0000 TOTAL b.50 2357.5395E-03 1.55 473.014 66053.0076E-05 -4.15 T out (K) : 429. Menentukan panas keluar HE-01 T reff (K) : 298.3116E-09 2.64 T in med (K) = T out med (K) = 541.70 0.30 K Komponen BM F2 (kg/jam) 1.87 0.0076E-05 -4.014 66053.50 548.58 1.5395E-03 1.5935E-13 83612.9342E+01 -3.15 A 9.88 Kebutuhan medium pemanas (kJ/jam) : 10754663.2053E+01 NERACA PANAS SEKITAR GAS MIXER .1888 2.74 Kebutuhan medium pemanas (kg/jam) : 5520.1888 2.3116E-09 2.Oxygen 32. Menentukan kebutuhan pamanas Cp mean medium pemanas (kJ/kg K) : 4.000 17558.00 2906.5935E-13 83612.64 Panas laten (kJ/jam) : 1614.50 548.08 TOTAL (kJ/jam) : H input (kJ/jam) : H output (kJ/jam) : 1948.5615E+02 ni (kmol/jam) Yi A B C D E Oxygen 32.08 426184.2629E-08 8.0000 TOTAL c.8112 2.8112 2.8083E-05 -3.2629E-08 8.8607E-12 Nitrogen 28.70 0.87 0.9526E+01 -8.9526E+01 -8.8607E-12 Nitrogen 28.8889E-03 3.8889E-03 3.50 2357.90 11180848.8083E-05 -3.58 1.00 Panas sensibel (kJ/jam) : 334.00 2906.000 17558.

30 (K) : 2.0114 3.000 17558.87 0. Menentukan panas masuk HE-02 T reff (K) : 298.4139E-11 87232.0114 3.Menentukan T bubble T bubble (K) : Komponen 81.7241E+01 -3.4103E-06 Oxygen 32.68 1.36 BM F3 (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.6689E+00 2.16 2940.8832E-13 Nitrogen 28.167 72.8018 2.014 66053.3857E+01 -4.76 33.3563E-10 2.7668E+02 -8.014 66053.68 0.76 33.2570E+00 -4.7062E+00 1.4573E+03 -1.96 BM F3 (kg/jam) ni (kmol/jam) Yi A B C D E O-xylene 106.2697E+02 -6.4680E+01 -3.7241E+01 -3.0002 3.1866 2.68 0.7062E+00 1.0128E-02 -2.0128E-02 -2.42 0.6123E-06 B.0000 TOTAL 2. Menentukan T dew T dew (K) Komponen : 307.7668E+02 -8.167 3547.0670E+01 -5.50 2357.87 0.0126E+01 9.6123E-06 .2981E+03 -9.0126E+01 9.70 0.40 0.8832E-13 Nitrogen 28.3563E-10 2.0676E-11 M-xylene 106.70 0.50 548.0002 3.8018 2.0676E-11 M-xylene 106.0000 TOTAL NERACA PANAS SEKITAR HE-02 a.1866 2.2926E-02 -9.16 2940.000 17558.4103E-06 Oxygen 32.2926E-02 -9.40 0.2570E+00 -4.4680E+01 -3.50 548.4139E-11 87232.15 T in 429.50 2357.2697E+02 -6.167 72.167 3547.6689E+00 2.68 1.3857E+01 -4.0670E+01 -5.42 0.4573E+03 -1.2981E+03 -9.

87 0.52 T in med (K) = 633.167 3547.3212E-11 M-xylene 106.42 0.87 0.3381E-08 1.3116E-09 2.42 0.9342E+01 -3.014 66053.15 (K) : Komponen BM F3 (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.0114 1.8889E-03 3.0000 TOTAL b.5395E-03 1.8200E-01 5.15 H output (kJ/jam) : 29225216.1866 2.000 17558.34 Kebutuhan medium pemanas (kJ/jam) : 17332629.0114 1.167 72.0000 TOTAL c.000 17558.8607E-12 Nitrogen 28.15 NERACA PANAS SEKITAR REAKTOR a.13 H input (kJ/jam) : 11892587.70 0.68 1.3116E-09 2.014 66053.8083E-05 -3.Komponen BM F3 (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.3212E-11 M-xylene 106.2629E-08 8. Menentukan kebutuhan pamanas Cp mean oiltherm (kJ/kg K) : 2.5935E-13 87232.5395E-03 1.0076E-05 -4.5869E-11 Oxygen 32.6424E-01 -2.8607E-12 Nitrogen 28.50 2357.9526E+01 -8.40 0. Mencari harga panas pembentukan standar T (K) : 623.0002 -1.50 2357.16 2940.40 0.8889E-03 3.0002 -1.6725E+01 5.8200E-01 5.8018 2.6424E-01 -2.38 Kebutuhan medium pemanas (kg/jam) : 148142. Menentukan panas keluar HE-02 T reff (K) : 298.6465E-04 1.70 0.68 1.0212E-04 -2.6725E+01 5.8018 2.16 2940.50 548.5935E-13 87232.9526E+01 -8.1344E-01 -2.167 72.50 548.15 .167 3547.0212E-04 -2.5869E-11 Oxygen 32.68 0.68 0.76 33.90 T out med (K) = 583.1615E-08 2.3381E-08 1.9342E+01 -3.6465E-04 1.2629E-08 8.1344E-01 -2.76 33.8083E-05 -3.1866 2.15 T out 613.0076E-05 -4.1615E-08 2.

00 7.0000E+00 0.8644E-04 199.0000E+00 0.014 66053.167 72.7437E+01 4.97 TOTAL 87232.14 268.3933E+01 -8.058 Ortho tolualdehide Phthalide F4 (kg/jam) ni (kmol/jam) Xi A B C 0.71 Carbon dioxide 44.8716E-03 1.16 Ortho tolualdehide 136.6405E-03 2.00 Water 18.2015E+01 136.016 TOTAL c.0212E-04 0.6767E-11 1.00 0.5869E-11 9.00 4839.0000 134.00 0.9906E-05 -1.01 Carbon monoxide 28.6084E-02 137.0000E+00 0.50 2357.06 0.1480E-01 5.70 13170.1344E-01 -2.0000 -1.50 2357.00 8.50 Water 18.00 137.0083E+01 3.31 89966.19 Phthalic anhydride 148.5807E-03 2.8607E-12 2357.9556E+01 -6.40 40.50 Oxygen 32.07 46.00 0.5935E-13 1909.00 1800.00 0.7486E-08 5.2227E-08 2.011 1800.98 23.54 105.6465E-04 1.0824E-01 -1.3161E-01 -3.6823E-11 0.41 -1.2315E-02 -1.00 0.79 0.7825E-08 3.00 Nitrogen 28.87 66053.3381E-08 1.00 0.0824E-01 4.6934E-12 87037.50 Nitrogen 28.78 0.0824E-01 -42052.8201E+01 1.79 0.016 0.118 Maleic anhydride 98.7656E-06 -244.0000E+00 -393.00 0.06 -4.000 13170. Menentukan kebutuhan pendingin 70.03 1.62 -1.50 Carbon dioxide 44.76 -1.058 0.58 0 0.0283E-05 -393.1353E+00 -2.40 0.0138 2.58 1.90 12.3 6.136 8.9980E-04 1.150 0.6424E-01 3521.76 -1.150 7.5395E-03 1.14 Phthalide 134.8083E-05 -3.7979 2.00 3521.Komponen BM Reaktan F3 (kg/jam) ni (kmol/jam) Produk F4 (kg/jam) ni (kmol/jam) A B C H standar (kJ/mol) O-xylene 106.50 411.9555E-05 3.0000E+00 0.00 0.87 0.50 548.91 0 0.0423E+00 -1.2341E-06 4.0043 2.3212E-11 -2.9526E+01 -8.5447E-05 -409.2256E-02 2.2629E-08 8.68 0.0000 .167 Phthalic anhydride 148.90 12.31 -8.0000E+00 -110.136 0.96 D E -2.0000 Carbon monoxide 28.60 -238.8146E-03 2.011 355.011 0.6527E-06 -5.58 1.1393 2.0130E-05 -1.91 0.15 Komponen BM O-xylene 106.8889E-03 3.167 M-xylene 106.01 2955.96 0.0002 1.16 -1.67 0.2617E-12 40.40 Oxygen 32.6725E+01 5.014 66053.9872E-13 411.76 33.5647E-10 5.00 46.87 0.6610E-03 1.9342E+01 -3.00 0.93 Maleic anhydride 98.000 17558.98 23.00 0.8200E-01 5.9968E-09 -2.61 b.67 46.167 3547.4063E-02 3.5956E-04 -1.07 0.3116E-09 2.42 70.40 -401.0076E-05 -4.011 0.3371E-05 -4.0005 -7.6597E-10 1.9928E-05 M-xylene 106.0000E+00 0.0080 4.0359 3.9986E+01 7.40 0.118 0.87 0 0.15 T out (K) : 623.00 355.87 0.44E+01 6.1615E-08 2. Mencari panas keluar reaktor T reff (K) : 298.99 0.0000E+00 0.78 -371.71 0 0.58 0.4764E-06 -1.7860E-01 2.

55 1614.34 Panas laten : 60395497.90 T in med (K) = 598.41 NERACA PANAS SEKITAR SG-01 Panas yang dibawa molten salt Massa BFW keluar dari HE-04 : 37419.15 H output (kJ/jam) : -66349776.41 Kebutuhan medium pendingin (kg/jam) : 1225320.15 : 95574993.43 H input (kJ/jam) : 29225216.74 TOTAL : 69201042.52 T out med (K) = 648.56 Kebutuhan medium pendingin (kJ/jam) : 95574993.08 NERACA PANAS SEKITAR HE-03 -26373951.55 Cp mean (kJ/kg K) : Panas sensibel : 4. shg tekanan menjadi 53 atm Dari steam table diperoleh temperatur jenuh uap (K) Panas laten (kJ/kg) : : 541.Cp mean molten salt (kJ/kg K) : 1.11 T out (K) : 541.83 Asumsi : pressure drop 1 atm.96 8805544.00 T in (K) : 494.34 .

5647E-10 Ortho tolualdehide 136.79 0.15 Komponen BM F4 (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.9555E-05 3.87 0.01 2955.90 T out med (K) = 604.07 0.84 T in med (K) = 541.0005 -7.0000 5.9526E+01 -8.7056 2.0138 2. Mencari panas keluar HE-03 T reff (K) : 298.6527E-06 -5.a.3933E+01 -8.40 40.99 0.2341E-06 4.8200E-01 5.71 12.136 8.40 0.7013 TOTAL b.90 12.1615E-08 2.2227E-08 2.00 0.78 0.0130E-05 -1.8146E-03 2.8716E-03 1.6465E-04 1.5869E-11 Phthalic anhydride 148.87 0.5956E-04 -1.50 2357.7860E-01 2.014 66053.9906E-05 -1.011 355.0002 1.98 Kebutuhan medium pendingin (kJ/jam) : Kebutuhan medium pendingin (kg/jam) Panas sensibel medium pendingin (kJ) 3807476.35 Digunakan steam jenuh sebagai pendingin 168161.6084E-02 9.98 23.7979 2.2015E+01 1.0000 1.150 7.03 13. Menentukan kebutuhan pendingin Cp mean steam (kJ/kg K) : 1.75 A 3.1353E+00 -2.0359 3.6934E-12 87037.6405E-03 2.9980E-04 1.4764E-06 3.000 13170.8889E-03 3.55 H output (kJ/jam) : 26142505.8083E-05 -3.3212E-11 M-xylene 106.9872E-13 Water 18.58 1.0212E-04 -2.9556E+01 -6.9986E+01 7.19 : H input (kJ/jam) : 29949982.91 0.2315E-02 -1.3381E-08 1.167 0.7437E+01 4.5935E-13 Carbon monoxide 28.6725E+01 5.3933E+01 PROFIL SUHU F4 .011 1800.7290E-10 Phthalide 134.2617E-12 Carbon dioxide 44.8607E-12 Nitrogen 28.67 0.3116E-09 2.8201E+01 1.7486E-08 5.6823E-11 Oxygen 32.9968E-09 -2.2629E-08 8.6597E-10 Maleic anhydride 98.15 T out (K) : 583.7825E-08 3.95 : 31899.50 411.96 0.118 3521.0000 -1.54 105.0076E-05 -4.06 0.0083E+01 3.6424E-01 -2.1344E-01 -2.58 0.9342E+01 -3.1393 2.058 137.167 70.0080 4.5807E-03 2.80 3975638.5395E-03 1.016 1909.00 0.0423E+00 -1.

54 105.0000 -4.87 0.58 0.0002 3.58 1.43 BM F4 (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.8090E-06 Oxygen 32.1522E+03 -7.4384E+01 6.7241E+01 -3.0005 -4.0082 3.0670E+01 -5.72 2901.016 1909.8783E+03 -7.1760E-08 -2.000 13170.014 66053.2981E+03 -9.2697E+02 -6.6928E+03 2.0046E-07 1.2926E-02 -9.42 1.4680E+01 -3.54 105.136 8.2978E+01 -1.0633E+01 -3.0633E+01 -3.98 23.79 0.3161E-01 -3.167 0.8127 2.0670E+01 -5.1320E-06 Water 18.058 137.8671E+00 1.4573E+03 -1.79 0.0000 2.06 0.058 137.4139E-11 84880.5463E+03 -7.1707E-05 Ortho Tolualdehide 136.0126E+01 9.00 0.58 0.40 0.167 70.8974E+00 1.Menentukan T bubble T bubble (K) : Komponen 80.2570E+00 -4.2981E+03 -9.4680E+01 -3.67 0.2570E+00 -4.2978E+01 -1.8644E-04 9.5463E+03 -7.96 0.0128E-02 -2.00 0.06 0.0128E-02 -2.118 3521.4103E-06 Phthalic anhydride 148.07 0.118 3521.00 0.9657E+01 -3.0000 3.6123E-06 M-xylene 106.87 0.50 411.58 1.4247E-09 1.78 0.3563E-10 2.4247E-09 1.3030E+00 2.3563E-10 2.07 0.98 23.7241E+01 -3.7062E+00 1.5885E-06 Maleic anhydride 98.000 13170.1419 2.1146E-09 2.2697E+02 -6.016 1909.72 2901.4139E-11 84880.2430E+01 -2.9861E+01 -3.7668E+02 -8.87 0.0676E-11 2.50 2357.1760E-08 -2.2430E+01 -2.150 7.4573E+03 -1.3161E-01 -3.3030E+00 2.4103E-06 Phthalic anhydride 148.99 0.6123E-06 M-xylene 106.167 0.6689E+00 2.8783E+03 -7.8974E+00 1.50 411.0365 2.8090E-06 Oxygen 32.0000 3.0126E+01 9.9657E+01 -3.6689E+00 2.136 8.0676E-11 2.5885E-06 Maleic anhydride 98.8832E-13 Nitrogen 28.0000 -4.50 2357.78 0.42 1.167 70.0000 2.3857E+01 -4.87 0.2926E-02 -9.4384E+01 6.8671E+00 1.8644E-04 9.7668E+02 -8.1146E-09 2.7916E-02 1.9424E-12 Phthalide 134.32 BM F4 (kg/jam) ni (kmol/jam) Yi A B C D E O-xylene 106.1707E-05 Ortho Tolualdehide 136.0046E-07 1.3857E+01 -4.8832E-13 Nitrogen 28.0005 -4.0000 TOTAL Menentukan T dew T dew (K) Komponen : 407.8127 2.0082 3.67 0.9861E+01 -3.014 66053.7062E+00 1.1419 2.00 0.1522E+03 -7.9424E-12 Phthalide 134.150 7.1320E-06 Water 18.6928E+03 2.0000 TOTAL NERACA PANAS SEKITAR HE-04 .7916E-02 1.96 0.40 0.99 0.0002 3.0365 2.

07 0.2341E-06 4.3212E-11 M-xylene 106.6597E-10 Maleic anhydride 98.118 3521.8889E-03 3.8716E-03 1.4384E+01 6.78 0.5935E-13 82971.9986E+01 7.0083E+01 3.06 0.8083E-05 -3.15 T out (K) : 407.8200E-01 5.167 0.48 Kebutuhan medium pendingin (kJ/jam) : 16934710.7860E-01 2.058 137.6823E-11 Oxygen 32.1472 2.67 0.88 Kebutuhan medium pendingin (kg/jam) : 37419.000 13170.6084E-02 9.014 66053.0000 -1.8607E-12 Nitrogen 28.0005 -7.50 2357.0423E+00 -1.6424E-01 -2.58 0.136 8.5869E-11 Phthalic anhydride 148.5647E-10 Ortho Tolualdehide 136.87 0.9526E+01 -8.15 H output (kJ/jam) : 9207795.3381E-08 1.8644E-04 9.0000 -4.90 T in med (K) = 393.01 T out med (K) = 494.32 Komponen BM F4 (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.5395E-03 1.3116E-09 2.43 1.1344E-01 -2.3161E-01 -3. Menentukan kebutuhan pendingin Cp mean (kJ/kg K) : 4.40 0.Didinginkan hingga T dew arus F4 a. Mencari panas keluar HE-04 T reff (K) : 298.6527E-06 -5.11 Digunakan BFW bertekanan 54 atm (high pressure) A 9.79 0.7290E-10 Phthalide 134.0002 1.0000 TOTAL b.0085 4.7486E-08 5.9342E+01 -3.2053E+01 .50 411.0076E-05 -4.00 0.5956E-04 -1.167 70.8435 2.9980E-04 1.87 0.98 23.1760E-08 3.2629E-08 8.96 0.2015E+01 1.18 2795.1615E-08 2.0000 1.150 7.6725E+01 5.0212E-04 -2.6465E-04 1.00 0.58 1.83 H input (kJ/jam) : 26142505.

NERACA PANAS SEKITAR SWITCH CONDENSER (SC-01)
a. Tahap receiving
Terjadi proses desublimasi dan separasi antara condensable dan non-condensable gas
Menghitung panas keluar
Komponen terdesublimasi
T reff (K) :

298.15

T out (K) :

333.15

Komponen

BM

F4 (kg/jam)

ni (kmol/jam)

Xi

A

B

C

D

E

Phthalic anhydride

148.118

3521.98

23.78

0.9948

2.6320E+01

3.9060E-01

2.1260E-04

0.0000E+00

0.0000E+00

ortho tolualdehide

136.150

7.87

0.06

0.0024

-4.2265E+01

7.2871E-01

0.0000E+00

0.0000E+00

0.0000E+00

Phthalide

134.136

8.79

0.07

0.0027

3.4220E+01

6.1431E-01

0.0000E+00

0.0000E+00

0.0000E+00

3538.64

23.90

1.0000

TOTAL
Komponen non-condensable gas
T reff (K) :

298.15

T out (K) :

333.15

Komponen

BM

Carbon monoxide

28.011

Carbon dioxide

44.011

Oxygen

32.000

Nitrogen

28.014

TOTAL

F4 (kg/jam)
137.58

Xi

A

4.91

0.0017

2.9556E+01

1800.40

40.91

0.0145

13170.50

411.58

0.1462

66053.50

2357.87

0.8375

81161.98

2815.27

1.0000

Komponen yang tercairkan
T reff (K) :

ni (kmol/jam)

298.15

B

C

-6.5807E-03

2.0130E-05

2.7437E+01

4.2315E-02

2.9526E+01

-8.8889E-03

2.9342E+01

-3.5395E-03

D

E

-1.2227E-08

2.2617E-12

-1.9555E-05

3.9968E-09

-2.9872E-13

3.8083E-05

-3.2629E-08

8.8607E-12

1.0076E-05

-4.3116E-09

2.5935E-13

T out (K) :
Komponen

333.15
BM

F4 (kg/jam)

O-xylene

106.167

M-xylene
Maleic anhydride
Water

ni (kmol/jam)

Xi

A

70.96

0.67

0.0062

106.167

0.00

0.00

0.0000

98.058

137.58

1.40

0.0130

18.016

1909.54

105.99

0.9808

9.2053E+01

2118.07

108.06

1.0000

TOTAL

5.6460E+01

B

C

D

-2.4902E-03

2.6838E-06

0.0000E+00

7.0916E+01

8.0450E-01

-2.1885E-03

2.5061E-06

0.0000E+00

-1.2662E+01

1.0564E+00

-2.3244E-03

2.0518E-06

0.0000E+00

-3.9953E-02

-2.1103E-04

5.3469E-07

0.0000E+00

Menghitung panas desublimasi pada 134,2 oC
Komponen

F4 (kg/jam)

BM

ni (kmol/jam)

Xi

Hd (J/mol)

Hd (kJ/jam)

Phthalic anhydride

148.118

3521.9800

23.7782

0.9948

21437.50

509745.25

ortho tolualdehide

136.150

7.8699

0.0578

0.0024

24044.70

1389.86

Phthalide

134.136

8.7921

0.0655

0.0027

11926.00

3538.6420

23.9016

1.0000

TOTAL

781.70
511916.80

Menghitung panas pencairan pada 134,2 oC
Komponen

F4 (kg/jam)

BM

O-xylene

106.17

M-xylene

ni (kmol/jam)

A

Tc (K)

70.96

0.67

5.5606E+01

6.3037E+02

3.7500E-01

n

Hk (kJ/jam)
28033.17

106.17

0.00

0.00

6.0216E+01

6.1705E+02

4.5800E-01

0.00

Maleic anhydride

98.06

137.58

1.40

5.9574E+01

7.2100E+02

2.1600E-01

73107.19

Water

18.02

1909.54

105.99

5.2053E+01

6.4713E+02

3.2100E-01

4374147.33

2118.07

108.06

TOTAL

E

9.4926E-01

4475287.69

Menentukan kebutuhan pendingin
Cp mean oiltherm (kJ/kg K) :

2.34

Kebutuhan medium pendingin (kJ/jam)

:

10872630.16

Kebutuhan medium pendingin (kg/jam)

:

232321.16

H input (kJ/jam) :

9207795.01

T in med (K) =

328.15

H output (kJ/jam) :

-1664835.15

T out med (K) =

348.15

b. Tahap melting
Menghitung panas pelelehan pada T = 106,57 oC
Komponen

BM

379.72

F6 (kg/jam)

ni (kmol/jam)

Xi

Hm (J/mol)

Hm (kJ/jam)

Phthalic anhydride

148.118

3521.98

23.78

0.9948

3897.00

92663.78

ortho tolualdehide

136.150

7.87

0.06

0.0024

3536.00

204.39

Phthalide

134.136

8.79

0.07

0.0027

9775.00

640.71

3538.65

23.90

1.0000

TOTAL

93508.89

Menghitung panas sensibel
Fase padat
T reff (K) :

298.15

T out (K) :

379.72

Komponen

BM

F6 (kg/jam)

ni (kmol/jam)

Xi

A

B

C

D

E

Phthalic anhydride

148.118

3521.98

23.78

0.9948

2.6320E+01

3.9060E-01

2.1260E-04

0.0000E+00

0.0000E+00

ortho tolualdehide

136.150

7.87

0.06

0.0024

-4.2265E+01

7.2871E-01

0.0000E+00

0.0000E+00

0.0000E+00

Phthalide

134.136

8.79

0.07

0.0027

3.4220E+01

6.1431E-01

0.0000E+00

0.0000E+00

0.0000E+00

3538.65

23.90

1.0000

TOTAL
Fase cair
T reff (K) :

298.15

T out (K) :

379.72

Komponen

BM

F6 (kg/jam)

ni (kmol/jam)

Xi

A

B

C

D

E

O-xylene

106.167

70.96

0.67

0.0257

5.6460E+01

9.4926E-01

-2.4902E-03

2.6838E-06

0.0000E+00

Maleic anhydride

98.058

137.58

1.40

0.0540

-1.2662E+01

1.0564E+00

-2.3244E-03

2.0518E-06

0.0000E+00

Phthalic anhydride

148.118

3521.98

23.78

-1.0563E+02

1.9840E+00

-3.8847E-03

2.8513E-06

0.0000E+00

ortho tolualdehide

136.150

7.87

0.06

5.8201E+01

1.1353E+00

-2.6405E-03

2.4764E-06

0.0000E+00

Tahap cooling Pada tahap ini condenser tidak mempunyai beban.34 Kebutuhan medium pemanas (kJ/jam) : 5484061.3244E-03 2.167 70.0025 -8.4304E+00 -3.0563E+02 1.Phthalide 134.0022 5.136 TOTAL 8.53 H input (kJ/jam) : -4552894.58 1.22 Komponen BM Vo (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.0518E-06 0.0000E+00 Phthalic anhydride 148.0000E+00 Maleic anhydride 98.058 137.40 0.78 0.118 3521.0350E+00 2.79 T in med (K) = 398. Panas sensibel T reff (K) : 298.136 8.53 25.07 0.0350E+00 2.8847E-03 2.06 0.6405E-03 2.6541E-07 0.0000E+00 0.79 0.15 H output (kJ/jam) : 931166.4764E-06 0.150 7.49 T out med (K) = 368.15 T out (K) : 396.79 0.6460E+01 9.15 c.0000E+00 ortho tolualdehide 136.9155 -1.67 0.0257 5.0000E+00 Phthalide 134.96 0.98 23.0564E+00 -2.2662E+01 1.0000E+00 .4902E-03 2.14 NERACA PANAS SEKITAR PRE DISTILLATION COLUMN Panas yang dibawa oleh uap masuk kondensor (Vo) a.6838E-06 0.07 208.6541E-07 0.1353E+00 -2.0540 -1.4304E+00 -3.9847E-03 1.4926E-01 -2.9847E-03 1.97 -8.87 0. namun karena waktu operasi cooling 1/8 waktu operasi receiving maka : Kebutuhan oil pendingin = 29040.0798 Menentukan kebutuhan pemanas Cp mean oiltherm (kJ/kg K) : 2.8513E-06 0.28 Kebutuhan medium pemanas (kg/jam) : 78120.9840E+00 -3.8201E+01 1.

1344E-01 -2.118 Maleic anhydride 98.15 T out (K) : 377.76 1381173.5495E+01 7.0000 TOTAL b.6084E-02 9.40 Panas yang keluar dari kondensor a.5869E-11 Phthalic anhydride 148.6465E-04 1.0023 5.0423E+00 -1.00 23.0001 1.2100E+02 2.67 5.40 5.0083E+01 3.058 79.4926E-01 C -2.0001 4.03 0.81 0.22 BM O-xylene 106.85 0.6838E-06 E 0.0212E-04 -2.50 Komponen O-xylene BM 106.2015E+01 1.0216E+01 6.71 70357.09 0.167 M-xylene 106.0000 b.016 4613.8200E-01 5. Panas cairan destilat T reff (K) : 298.6725E+01 5.9934 3.02 0.5800E-01 0.99 256.5606E+01 6.0000E+00 .167 2.18 25.00 6.6597E-10 Maleic anhydride 98.36 ni (kmol/jam) 0.2341E-06 4.6527E-06 -5.3933E+01 -8.7825E-08 3.6460E+01 B 9.98 n Hv (kJ/jam) 25634.118 3.8146E-03 2.0032 -7.16 0.11 0.TOTAL 3747.85 70.93 137.058 TOTAL Vo (kg/jam) ni (kmol/jam) A Tc (K) 0.71 0.167 F12 (kg/jam) 0.52 25.5956E-04 -1.7500E-01 0.81 1.82 257.167 Phthalic anhydride 148.3212E-11 M-xylene 106. Panas uap T reff (K) : 298.3381E-08 1.96 3521.167 90.00 Xi A 0.9574E+01 7.15 T out (K) : 377.6424E-01 -2.9906E-05 -1.9100E+02 3.78 5. Panas laten penguapan T dew (K) : Komponen 396.1615E-08 2.8716E-03 1.5647E-10 Water 18.4902E-03 D 2.0033 -1.6934E-12 4789.87 0.97 1.1705E+02 4.46 Komponen BM F11 (kg/jam) ni (kmol/jam) Xi A B C D E O-xylene 106.58 1.3037E+02 3.1600E-01 3730.8000E-02 1285180.

118 1.2188 -1.9840E+00 -3.2053E+01 -3.0563E+02 1.50 Komponen BM Lo (kg/jam) ni (kmol/jam) Xi A O-xylene 106.02 0.0000E+00 .68 0.5495E+01 7.0564E+00 -2.0518E-06 0.50 A Tc (K) O-xylene 106.92 0.0000E+00 7.9953E-02 -2.1885E-03 2.M-xylene 106.118 48.8847E-03 2.2100E+02 2.118 48.058 2.167 0.0000E+00 365.167 0.0916E+01 8.0000 TOTAL Panas laten kondensasi refluks 5.15 T out (K) : 377.12 6.167 12.26 0.46 M-xylene 106.167 12.0000E+00 Phthalic anhydride 148.79 1.1103E-04 5.5606E+01 6.5061E-06 0.4926E-01 -2.016 200.33 5.65 Water 18.0096 Phthalic anhydride 148.01 0.00 0.42 c. Panas cairan refluks T reff (K) : 298.8513E-06 0.77 0.0260 Maleic anhydride 98.0000E+00 9.2053E+01 -3.058 102.24 Phthalic anhydride 148.8847E-03 2.12 0.57 11.2662E+01 1.44 0.50 1.6460E+01 B C D E 9.31 0.3244E-03 2.32 1.8000E-02 17795.4123 9.9840E+00 -3.30 1.67 0.8814 8.0830 Water 18.05 5.0564E+00 -2.167 BM F12 (kg/jam) 0.9574E+01 7.0000E+00 -1.32 12.0916E+01 8.1600E-01 53204.00 0.5800E-01 4750.4713E+02 3.0450E-01 -2.0563E+02 1.0216E+01 6.1705E+02 4.13 7.21 Maleic anhydride 98.0000E+00 -1.57 11.05 0.16 0.016 4.36 0.016 200.0810 7.3244E-03 2.64 TOTAL ni (kmol/jam) n Hk (kJ/jam) 513416.13 5.0000 TOTAL Panas laten kondensasi destilat T dew (K) : Komponen 377.5061E-06 0.058 102.68 0.0450E-01 -2.79 1.1103E-04 5.7500E-01 135.33 0.0000 M-xylene 106.2053E+01 6.2100E-01 437530.6838E-06 0.9100E+02 3.92 0.9953E-02 -2.00 5.6979 -1.00 0.0000E+00 Water 18.3469E-07 0.0518E-06 0.0000E+00 Maleic anhydride 98.4902E-03 2.1885E-03 2.8513E-06 0.2662E+01 1.3037E+02 3.3469E-07 0.86 365.

16 0.77 0.0216E+01 6.94 Menentukan kebutuhan pendingin Cp mean cooling water (kJ/kg K) : 4.01 5.7500E-01 0.67 9.3037E+02 3.9100E+02 3.34 8.02 5.67 0.9574E+01 7.1705E+02 4.4713E+02 3.19 T in med (K) = 303.15 T out med (K) = 323.81 Maleic anhydride 98.5495E+01 7.31 0.016 4.44 0.1600E-01 1264.15 Panas yang dibawa oleh residu T reff (K) : 298.2100E-01 10395.94 Kebutuhan medium pendingin (kg/jam) : 20302.118 1.00 0.00 5.00 6.26 5.058 2.T dew (K) : Komponen 377.2100E+02 2.167 BM Lo (kg/jam) 0.2053E+01 6.15 A T out (K) : 571.8000E-02 422.15 Menghitung muatan kondensor Qc = 1697019.2053E+01 Komponen BM F13 (kg/jam) ni (kmol/jam) Xi A B C D E .87 Phthalic anhydride 148.18 Kebutuhan medium pendingin (kJ/jam) : 1697019.5606E+01 6.167 0.5800E-01 112.13 Water 18.30 TOTAL ni (kmol/jam) n Hk (kJ/jam) 12195.00 M-xylene 106.50 A Tc (K) O-xylene 106.

00 0.2662E+01 1.5101E-06 0.15 T out med (K) = 566.0563E+02 1.00 0.8513E-06 0.0564E+00 -2.0686E+02 2.0000E+00 5203.15 T out (K) : 480.118 6655.8847E-03 2.10 0.0686E+02 2.0350E+00 2.04 0.118 5186.3244E-03 2.1576E+00 -4.1576E+00 -4.49 Menentukan kebutuhan pemanas Cp mean oiltherm (kJ/kg K) : 2.9961 -1.05 0.0518E-06 0.0027 -8.0564E+00 -2.9978 -1.0001 -1.150 0.4304E+00 -3.72 0.9840E+00 -3.0001 -1.3244E-03 2.9847E-03 1.0010 -1.8513E-06 0.0000E+00 Maleic anhydride 98.15 1.0563E+02 1.0011 -1.150 0.23 T in med (K) = 583.02 0.49 Kebutuhan medium pemanas (kg/jam) : 116566.26 Komponen Phthalic anhydride BM Vo (kg/jam) ni (kmol/jam) Xi A B C D E 148.39 0.058 3.90 T reff (K) : 298.51 0.6541E-07 0.89 NERACA PANAS SEKITAR MAIN DISTILLATION COLUMN Panas yang dibawa oleh uap masuk kondensor (Vo) a. Panas sensibel -31575.02 44.4616E-03 3.5101E-06 0.93 0.0000E+00 Phthalide 134.8847E-03 2.34 Kebutuhan medium pemanas (kJ/jam) : 4435650.9840E+00 -3.31 35.50 0.0000 TOTAL Menghitung muatan reboiler Qr = 4435650.0000E+00 .0000E+00 ortho tolualdehide 136.136 12.0000E+00 Ortho Tolualdehide 136.058 4.Phthalic anhydride 148.0000E+00 Maleic anhydride 98.4616E-03 3.2662E+01 1.45 35.75 0.0518E-06 0.

1530E+02 1.1600E-01 2155.136 4.20 0.0004 -1.6541E-07 0.2256E-03 1.1000E+02 3.82 3554.33 0.6527E-06 -5.5956E-04 -1.0423E+00 -1.5647E-10 b.79 Phthalide 134.9847E-03 1.150 0.00 9.30 343.47 .15 T out (K) : 477.5495E+01 7.31 Ortho Tolualdehide 136.0350E+00 2.1444E+01 7.23 45.118 6655.8000E-02 1365.4304E+00 -3.05 5.93 5.98 0.0000 TOTAL b.0000E+00 Phthalic acid 166.52 Maleic anhydride 98.2100E+02 2.43 6664.1640E-07 0.9943 4.2015E+01 1.0007 -8.02 0.31 0.03 4.03 0.96 0.45 Komponen BM F15 (kg/jam) ni (kmol/jam) Xi A B C D E Phthalic anhydride 148. Panas laten penguapan T dew (K) : Komponen 480.50 0.6084E-02 9.8000E-02 2406445.51 0.4157E+00 -1.26 A Tc (K) 148.0000E+00 6667.0000 -7.83 411.20 0.25 Panas yang keluar dari kondensor a.8800E-01 231.05 3266.133 2.058 4.02 44.Phthalide 134.0057 1. Panas cairan destilat T reff (K) : 298.9574E+01 7.17 4408394.99 4415627.15 T out (K) : 477.65 2.01 Phthalic anhydride BM TOTAL Vo (kg/jam) ni (kmol/jam) n Hv (kJ/jam) input 2410197.136 4.5100E+02 3.118 342.2341E-06 4.21 45.01 2.03 1. Panas uap T reff (K) : 298.5551E+01 7.6597E-10 Maleic anhydride TOTAL 98.8716E-03 1.9100E+02 3.0083E+01 3.058 1.

44 10.77 0.02 0.5100E+02 3.40 TOTAL F18 (kg/jam) ni (kmol/jam) n Hk (kJ/jam) 1037.0001 -1.8847E-03 2.01 0.00 0.12 0.118 BM 4791.0686E+02 2.0000E+00 Phthalide 134.2662E+01 1.40 1.6541E-07 0.77 c.98 Ortho Tolualdehide 136.28 1.0008 -1.47 A Tc (K) Phthalic anhydride 148.4304E+00 -3.47 .9100E+02 3.01 0.0008 -1.0563E+02 1.9984 -1.0000E+00 4797.39 0.4616E-03 3.5551E+01 7.94 32.8000E-02 1733344.9847E-03 1.2100E+02 2.3244E-03 2.8513E-06 0.058 0.0000E+00 Maleic anhydride 98.058 2.2662E+01 1.4304E+00 -3.01 0.19 0.0001 -1.1576E+00 -4.42 0.8847E-03 2.0563E+02 1.02 5.058 2.1000E+02 3.27 0.150 0.35 0.1576E+00 -4.150 0.0007 -8.47 Komponen BM Lo (kg/jam) ni (kmol/jam) Xi A B C D E Phthalic anhydride 148.0000E+00 Ortho Tolualdehide 136.0686E+02 2.9984 -1.29 Maleic anhydride 98.35 5.3244E-03 2.0518E-06 0.42 0.Komponen BM F18 (kg/jam) ni (kmol/jam) Xi A B C D E Phthalic anhydride 148.6541E-07 0.8800E-01 176.0000E+00 Maleic anhydride 98.0000E+00 Phthalide 134.0000E+00 1522.39 0.0350E+00 2.9847E-03 1.93 32.8000E-02 4797.93 32.136 1.00 0.136 3.19 0.02 0.0350E+00 2.0564E+00 -2.94 32.34 10.9574E+01 7.00 9.02 4.0000E+00 Ortho Tolualdhide 136.4616E-03 3.118 1520.118 4791.9840E+00 -3.0000 TOTAL Panas laten kondensasi refluks T dew (K) : 477.32 1735720.136 3. Panas cairan refluks T reff (K) : 298.5101E-06 0.1600E-01 1162.15 T out (K) : 477.0564E+00 -2.5101E-06 0.150 0.9840E+00 -3.0518E-06 0.19 Phthalide 134.8513E-06 0.5495E+01 7.0007 -8.0000 TOTAL Panas laten kondensasi destilat T dew (K) : Komponen 477.1444E+01 7.

01 0.13 1522.01 5.136 1.7620 -1.14 1.07 0.34 Menentukan kebutuhan pendingin Cp mean (kJ/kg K) : 4.9840E+00 -3.5100E+02 3.1530E+02 1.0000E+00 285.2100E+02 2.29 Ortho Tolualdehide 136.0000E+00 Phthalic acid 166.118 BM Lo (kg/jam) 1520.12 0.90 Phthalide 134.38 Maleic anhydride 98.27 5.8000E-02 329.35 0.0000 TOTAL .34 Kebutuhan medium pendingin (kg/jam) : 146428.Komponen A Tc (K) Phthalic anhydride 148.5551E+01 7.86 0.34 10.9574E+01 7.1000E+02 3.56 0.15 A T out med (K) = 330.1978 -1.74 T in med (K) = 323.4304E+00 -3.01 4.1640E-07 0.97 9.1600E-01 369.92 126126.8847E-03 2.35 0.77 0.9100E+02 3.17 Kebutuhan medium pendingin (kJ/jam) : 4775654.5495E+01 7.28 TOTAL ni (kmol/jam) n Hk (kJ/jam) 550728.8800E-01 55.56 1.8000E-02 549974.0403 -8.6541E-07 0.4157E+00 -1.150 0.2256E-03 1.9847E-03 1.058 0.1444E+01 7.70 Menghitung muatan kondensor Qc = 4775654.8513E-06 0.136 9.133 224.0563E+02 1.118 51.2053E+01 Panas yang dibawa oleh residu T reff (K) : 298.52 Komponen BM F20 (kg/jam) ni (kmol/jam) Xi A B C D E Phthalic anhydride 148.0000E+00 Phthalide 134.00 9.77 1.15 T out (K) : 556.0350E+00 2.44 10.

0000E+00 Maleic anhydride 98.6597E-10 Maleic anhydride 98.2662E+01 1.0563E+02 1.118 94. Panas uap keluar T reff (K) : 298.0040 -1.31 1.6084E-02 9.15 Komponen BM F17 (kg/jam) ni (kmol/jam) Xi A B C D E Phthalic anhydride 148.2015E+01 1.3244E-03 2.Menghitung muatan reboiler Qr = 2177721.15 T out (K) : 477.34 0.03 Kebutuhan medium pemanas (kg/jam) : 180981.8513E-06 0.9960 -1.0518E-06 0.46 Menghitung neraca panas sekitar kondensor (CN-03) a.9840E+00 -3.03 Menentukan kebutuhan pemanas Cp mean oiltherm (kJ/kg K) : 2.0000 TOTAL b.34 Kebutuhan medium pemanas (kJ/jam) : 2177721.0000E+00 .68 0.0103 -7. Panas destilat T reff (K) : 298.75 64415.8847E-03 2.9897 4.65 0.118 248.8716E-03 1.5956E-04 -1.058 0.64 0.01 0.2341E-06 4.6527E-06 -5.15 T out (K) : 477.64 1.99 0.89 T out med (K) = 561.01 0.65 0.5647E-10 94.15 Komponen BM F16 (kg/jam) ni (kmol/jam) Xi A B C D E Phthalic anhydride 148.058 0.0564E+00 -2.0083E+01 3.70 T in med (K) = 566.0423E+00 -1.

42 90137.8000E-02 Maleic anhydride 98.0000 Panas laten kondensasi destilat T dew (K) : Komponen 477.058 0.118 BM F17 (kg/jam) 248.97 1.68 5.97 317.5495E+01 7.9574E+01 7.97 1.47 NERACA PANAS SEKITAR MIXING VALVE T in med (K) = 330.31 1.68 TOTAL ni (kmol/jam) n Hk (kJ/jam) 89823.07 57063.2100E+02 2.15 A Tc (K) Phthalic anhydride 148.87 input 56745.01 5.85 T out med (K) = 331.19 Menghitung muatan kondensor Qc = 57944.9100E+02 3.68 1.33 .1600E-01 248.58 Kebutuhan medium pendingin (kg/jam) : 146565.65 0.TOTAL 248.17 Kebutuhan medium pendingin (kJ/jam) : 57944.77 313.58 Menentukan kebutuhan pendingin Cp mean cooling water (kJ/kg K) : 4.

76 0.04 Xi A 136.08 1.5101E-06 0.1133E+01 -3.0046E-07 1.9657E+01 -3.9984 -1.15 T out (K) : 477.0165E-02 1.7916E-02 1.136 3.2430E+01 -2.1587E-05 Phthalide 134.58 34.1707E-05 Ortho Tolualdehide 136.2662E+01 1.0000E+00 Maleic anhydride 98.2354E+03 2.118 5040.136 3.8783E+03 -7.150 0.46 T reff (K) : 298.1320E-06 5046.00 0.94 B C D E Phthalic anhydride 148.39 0.8847E-03 2.08 1.0000E+00 Ortho Tolualdehide 136.8671E+00 1.0518E-06 0.26 .22 T keluar mixing valve (trial) = 477.4616E-03 3.1576E+00 -4.6928E+03 2.9984 3.03 0.0564E+00 -2.46 Komponen BM F19 (kg/jam) ni (kmol/jam) 0.00 0.5463E+03 -7.6541E-07 0.9840E+00 -3.0350E+00 2.5885E-06 Maleic anhydride 98.058 2.0563E+02 1.058 2.0000E+00 Phthalide 134.8513E-06 0.0007 2.2978E+01 -1.0001 -3.19 0.118 5040.0000 TOTAL Menentukan T dew T dew (K) : 558.8974E+00 1.25 34.0000E+00 5046.0686E+02 2.39 0.25 34.0001 -1.76 0.03 0.0008 -4.0633E+01 -3.4304E+00 -3.02 0.03 0.1146E-09 2.5882E+01 -3.9847E-03 1.0008 -1.150 0.02 0.3244E-03 2.19 0.58 34.Panas total pencampuran = 1493229.0000 TOTAL NERACA PANAS SEKITAR FLAKER Asumsi : kebutuhan air dihitung pada saat aliran dari pure PA tank hanya menuju flaker (maksimum) PROFIL SUHU ARUS F19 PADA 1 ATM Menentukan T bubble T bubble (K) : Komponen 557.0007 -8.83 BM Phthalic anhydride F19 (kg/jam) ni (kmol/jam) Xi A B C D E 148.03 0.

5882E+01 -3.1576E+00 -4.9847E-03 1.0046E-07 1.0000 TOTAL Menghitung panas pembekuan pada T = 131 oC Komponen Phthalic anhydride Maleic anhydride BM F19 (kg/jam) ni (kmol/jam) Xi Hb (J/mol) Hb (kJ/jam) 148.6541E-07 0.39 0.0000E+00 Maleic anhydride 98.118 5040.0007 8664.2662E+01 1.5885E-06 Maleic anhydride 98.0007 -8.0008 2911.03 0.08 1.0165E-02 1.2354E+03 2.08 1.136 3.9984 3.3244E-03 2.39 0.00 94803.118 5040.58 34.58 34.0518E-06 0.00 Ortho Tolualdehide 136.0000E+00 Phthalide 134. Panas sensibel T reff (K) : 298.1146E-09 2.25 34.9657E+01 -3.02 0.8847E-03 2.Komponen BM F19 (kg/jam) ni (kmol/jam) Yi A B C D E Phthalic anhydride 148.9984 -1.00 0.19 0.15 Komponen BM F19 (kg/jam) ni (kmol/jam) Xi A B C D E Phthalic anhydride 148.15 95098.9840E+00 -3.0000E+00 Orto Tolualdehide 136.058 2.0686E+02 2.03 0.058 2.0008 -4.0633E+01 -3.76 0.25 34.28 .19 0.8974E+00 1.87 98.136 3.02 0.00 0.9984 2786.58 34.150 0.0350E+00 2.0563E+02 1.64 81.39 0.0008 -1.25 34.7916E-02 1.76 0.0007 2.1587E-05 Phthalide 134.1320E-06 5046.136 3.4304E+00 -3.91 Phthalide 134.00 0.150 0.8671E+00 1.150 0.2430E+01 -2.85 5046.03 0.1707E-05 Ortho Tolualdehide 136.118 5040.08 1.5101E-06 0.4616E-03 3.00 6.5463E+03 -7.76 0.058 2.8783E+03 -7.0001 -3.6928E+03 2.0001 -1.2978E+01 -1.0001 2425.00 205.02 0.19 0.03 0.15 T out (K) : 404.8513E-06 0.0564E+00 -2.03 0.0000E+00 5046.0000 TOTAL Menghitung panas keluar a.03 0.0000 TOTAL Didinginkan hingga 35 oC T reff (K) : 298.1133E+01 -3.

0007 3.79 T out med (K) = 317.0000E+00 0.058 2.7330E-04 0.2500E+01 0.7578 0.T out (K) : Komponen Phthalic anhydride 308.9060E-01 0.118 5040.0000E+00 7.2265E+01 0.2871E-01 0.9984 Maleic anhydride 98.08 1.1431E-01 0.0000 Menghitung kebutuhan pendingin Cp mean cooling water (kJ/kg K) : 4.58 TOTAL B 2.15 C D E 2.0000E+00 2.0001 -4.1870 5046.0000E+00 .69 H input (kJ/jam) : 1493229.15 BM Berat F19 (kg/jam) ni (kmol/jam) Xi A 148.1260E-04 0.22 T in med (K) = 303.0029 Phthalide 134.0238 0.150 0.18 Kebutuhan medium pendingin (kJ/jam) : 494187.43 Kebutuhan medium pendingin (kg/jam) : 8444.136 3.0960E-01 2.3882 0.0008 3.6320E+01 3.0000E+00 0.0000E+00 0.0000E+00 0.0000E+00 0.0000E+00 6.0000E+00 0.0286 0.4220E+01 34.2462 34.15 H output (kJ/jam) : 999041.0281 Ortho Tolualdehide 136.

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0229E+03 1026.28 1.52 1.48 429.42 H sensibel (kJ/jam) 22808.0229 23.9771 1002.1460E+00 0.28 1.53 23250.60 441.1758E+03 1026.0000 .9702E-01 0.13 T bubble (K) Pi (mmHg) P (mmHg)total Ki Yi Parsial 429.55 647.00 9.00 1.Cpl dT (J/mol) 682.

30 1.82 13779.30 1.00 9.1762E+03 1026.96 20205.87 714499.10 700719.83 .T dew (K) Pi (mmHg) P (mmHg) Ki Xi 429.9826 429.9740E-01 0.0174 1.00 1.1464E+00 0.0000 Cpg dT (J/mol) H sensibel (kJ/jam) 20969.0233E+03 1026.

Yi (J/mol K) 0.0000E+00 T input (K) : 473.36 Cpg dT (J/mol) H sensibel (kJ/jam) 29.B C -3.9953E-02 D -2.55 5.87 2056.1103E-04 T out (K) : Cpg dT (J/mol) H sensibel(Kj/jam) E 5.15 T output (K) : 375.37 Cp mean (kJ/kg K) : 4.57 0.16 0.80 23.88 485.59 2542.3469E-07 303.3890 .18 Cpg.

15 Cp mean (kJ/kg K) : 4.16 H sensibel (kJ/jam) 2153746.148.49 9027102.29 81368.1103E-04 D 5.13 426184.10 3828.0000E+00 : : 541.64 T input (K) T output (K) B -3.76 146.24 344816.9953E-02 C -2.90 Cpg dT (J/mol) 3925.55 473.8843 .3469E-07 E 0.54 11180848.

6284E-28 0.20 1.20 2.36 2.9798E-27 0.7752E+03 0.0001 1.96 8.9838 307.5901E+03 0.0000 81.36 1.0000 T dew (K) Pi (mmHg) P (mmHg) Ki Xi 307.0000 81.20 1.96 1.9496 1.T bubble (K) Pi (mmHg) P (mmHg) Ki Yi 81.0160 307.96 1.9893E-24 1003.96 1.0001 307.20 1.7809E+06 1003.20 2.0504 81.36 2.1587E+01 1003.20 1.4518E-02 0.1550E-02 0.6176E+06 1003.20 2.20 8.7082E+02 1003.6368E-25 1003.6996E-01 0.4564E+01 1003.1843E+00 0.1881E+03 1003.36 2.0000 .

52 Cpg dT (J/mol) 59676.12 58433.16 2153746.54 11892587.56 29225216.82 13779.45 21882147.90 .49 9027102.87 3925.60 H sensibel (kJ/jam) 1994200.24 9675.10 3828.98 9280.58 5309018.Cpg dT (J/mol) 20886.48 H sensibel (kJ/jam) 697959.55 39850.01 20205.

15 66016.00 11511.00 -551611.10 0.50 29949982.83 87382.00 42766.28 4114659.51 1196378.05 47053.00 0.79 -2860.69 22590068.66 0.08 11511.19 9997.84 .71 13984.75 41478.54 9586.00 122875.78 1231777.76 0.89 9580.76 0.41 -551611.00 0.72 -96299759.36 Cpg dT (J/mol) H sensibel (kJ/jam) 62062.75 60797.00 0.24 11287.60 -872.97 146259.81 2860.23 0.00 -9747333.58 0.41 0.10 -9747333.00 -65800371.08 0.00 -2756335.00 51802.82 572090.Hr (kJ/mol) Hp (kJ/mol) Hf (kJ/mol) -43639.00 0.23 -16097280.00 -1403966.36 -96346259.42 -65800371.27 -2756335.00 -16097280.00 0.71 9671.00 0.58 -1403966.42 -46500.44 5050.27 0.

1103E-04 D 5.A 9.9606 .11 T output (K) : 541.55 Cp mean (kJ/kg K) : 4.9953E-02 C -2.0000E+00 T input (K) : 494.3469E-07 E 0.2053E+01 B -3.

57 495705.86 1039865.6934E-12 T input (K) : 541.06 8449.93 107361.42 8382.54 1043435.24 19764264.94 4595.Cpg dT (J/mol) H sensibel (kJ/jam) 52677.54 0.52 79503.35 Cp mean (kJ/kg K) : 1.00 3587315.7825E-08 E 3.55 T output (K) : 604.32 7987.23 35206.57 121856.18 8716.90 B -8.9906E-05 -1.89 56770.00 26142505.8146E-03 C D 2.9845 .07 9844.00 43731.08 40462.27 12117.08 51504.65 0.

00 1.32 1.43 3.0453 1.0000 407.00 2.3740E+07 836.5003E-24 836.0000 407.00 4.0044E-33 0.32 5.43 1.6513E+02 836.00 2.0195E+01 836.8189E-24 836.2980E+03 836.0000 0.9561E-01 0.0251E-03 0.3650E+00 836.1360E-45 836.00 4.43 2.1988E-45 836.0000 80.0406 80.0000 80.0753E+03 836.0000 80.0133 407.8634E-01 0.0225E-48 0.43 3.5162E-26 836.7351E+02 836.00 1.1774E+05 0.2195E-02 0.3938E+02 836.1383E-28 0.43 9.00 1.00 2.00 4.6955 .0003 407.43 2.32 1.6436E+04 0.0000 80.9604E-27 0.00 4.2863E+00 1.2934E-36 0.43 1.00 3.0056 407.00 6.32 4.0000 80.00 1.8601E-01 0.3477E-30 836.7488E+00 0.3463E-27 0.32 2.1255E-24 836.32 6.7533E-33 836.1870E-27 0.9474E-48 0.00 7.43 4.32 1.8203E+08 836.1387E-01 0.00 6.T bubble (K) Pi (mmHg) P (mmHg) Ki Yi 80.0000 80.6720 407.0859 T dew (K) Pi (mmHg) P (mmHg) Ki Xi 407.00 5.0000 407.00 1.00 1.43 5.0042 407.32 3.0000 80.5197E+01 836.32 9.

00 13673.3469E-07 E 0.9953E-02 C -2.0000E+00 T input (K) : 393.01 B -3.15 36454.68 325135.11 Cp mean (kJ/kg K) : 4.15 T output (K) : 494.14 7507807.Cpg dT (J/mol) H sensibel (kJ/jam) 16958.26 2389.00 1340921.55 15295.08 16371.52 13772.45 9207795.05 19322.87 884.66 11334.43 3258.83 3184.1103E-04 D 5.48 .70 0.

64 .36 1035.42 Cpg dT (J/mol) H sensibel (kJ/jam) 1019.37 2401188.23 6571.59 142160.35 143063.22 426073.83 55791.44 523.37 1018.33 379.46 2888059.32 5006.Cps dT (J/mol) H sensibel (kJ/jam) 5978.84 7984.45 1363.

83 291246.76 4500.41 6497.42 0.28 .17 279198.Cpl dT (J/mol) H sensibel (kJ/jam) 6733.11 7547.00 5379.04 2634.

64 19251.04 965.67 1112.11 1296.65 H sensibel (kJ/jam) 10726.Cps dT (J/mol) 14947.53 16699.60 H sensibel (kJ/jam) 355427.55 12898.96 Cpl dT (J/mol) 16049.18 357688.29 18096.26 19775.78 448095.81 .65 18844.

96 2309.53 13005.75 23307.77 15656.99 479968.29551.73 1936.11 21965.94 1347.27 35238.95 A B C D E T Pi P .50 22901.64 Cpl dT (J/mol) H sensibel (kJ/jam) 19459.94 544567.

44 9709.51 .583196.80 9539.47 238.17 241.97 Cpl dT (J/mol) 15595.85 11442.23 Cpg dT (J/mol) H sensibel (kJ/jam) 11890.58 7924.23 2675.34 703360.53 H sensibel (kJ/jam) 53.65 685246.76 9728.

00 15055.93 18304.62 6016.94 12530.70 43.15055.09 5971.70 1831.10 Cpl dT (J/mol) H sensibel (kJ/jam) 15595.53 18304.90 66485.19 .09 12530.54 87522.96 13135.90 1579.64 2078.96 312.62 142.53 0.03 5971.

B -3.0000E+00 .1103E-04 H sensibel (kJ/jam) D 5.3469E-07 T input (K) : 303.18 E 0.9953E-02 Cpl dT (J/mol) C -2.15 T output (K) : 323.15 Cp mean (kJ/kg K) : 4.

17 7418.09 78059.11 47892.52 2001949.70016.54 2461163.99 1850.27 30513.87 .82 179.96 1399.63 2451679.11 75790.90 Cpl dT (J/mol) H sensibel (kJ/jam) 44556.16 48715.34 216.

78 -239.90 4544302.17 46236.18 23901.07 Cpg dT (J/mol) 24529.20 1850.16 4531616.64 216.60744.47 317.36 830.20 .11 3688.02 2006259.09 424.00 -359197.01 2461163.44 output -359414.32 H sensibel (kJ/jam) 56745.95 4774824.33 input output 2451679.54 8573.21 1901.05 -55.35 7418.24 512.85 57063.

84E+01 0.19E-01 6.91E-01 9.38 42.33 449735.60E-02 -2.15E-01 .62E+01 2.00E-02 2.39 740.19 1425.45E+00 1.69E-02 6.60 60018.3 Cpl dT (J/mol) H sensibel (kJ/jam) 43812.00E+00 2.99 29996.29 47087.25 60018.54 ai xf 2.15E+02 0 0.13E+02 8.07 47087.99 2083138.42 29996.33 1417422.08 0.01E-01 1.49E+01 2.00E+00 1.39 235.19 452.99E-01 -8.01 0.00E+00 7.16E+00 1.85E-01 2.38 134.29 1419723.Cpl dT (J/mol) H sensibel (kJ/jam) 43812.46 450465.53 1.03 0.88 0.01E+02 1.97E+01 1.

23 5429.9953E-02 Cpl dT (J/mol) 65634.0000E+00 T input (K) : 323.1103E-04 H sensibel (kJ/jam) 22982.1698 .46 76171.34 69490.91 93752.15 T output (K) : 330.3469E-07 E 0.52 5.72 122164.78 C D -2.B -3.97 Cp mean (kJ/kg K) : 4.

25 Cp dT (J/mol) H sensibel (kJ/jam) 43727.62 158.09 73306.97 H sensibel (kJ/jam) 15591.Cpg dT (J/mol) 24479.15 199.41 23856.06 .64 29937.63 15750.

2053E+01 57944.51 44.69 output -925.1103E-04 D 5.1684 .9953E-02 C -2.25 A 9.97 T output (K) : 331.07 Cp mean (kJ/kg K) : 4.26 -881.3469E-07 E 0.73505.58 B -3.0000E+00 T input (K) : 330.

00 1.0001 0.0050 557.9945 557.83 7.91 134.00 6.3770E+03 760.5940E+03 760.Cpl dT (J/mol) H sensibel (kJ/jam) 43810.83 1.45 843.46 29995.83 4.00 9.59 47085.83 9.2058E-01 0.97 1490825.1643E+01 760.9614E-01 0.25 60016.8118E+00 0.9998 .00 1.0002 557.5707E+02 760.26 T bubble (K) Pi (mmHg) P (mmHg) Ki Yi 557.96 1493229.0447E+00 0.85 1425.

13 37911.48 900.0057 0.26 7.0000 558.26 4.01 478.6394E+02 760.00 1.0001 558.00 1.2135E-01 0.T dew (K) Pi (mmHg) P (mmHg) Ki Xi 558.00 1.26 1.50 76.3900E+03 760.6303E+03 760.08 26702.75 847953.9992 Cpl dT (J/mol) H sensibel (kJ/jam) 24876.9932 558.22 16999.00 6.09 846498.18 .0052E+00 0.26 9.2228E+01 760.8289E+00 0.0926E+00 0.

15 T output (K) : 317.48 52.3469E-07 E 0.1103E-04 T input (K) : 303.Cps dT (J/mol) H sensibel (kJ/jam) 1642.2053E+01 B -3.33 A 9.15 Cp mean (kJ/kg K) : 4.0000E+00 .38 55990.70 55898.59 34.18 D 5.09 2204.9953E-02 C -2.43 5.79 1211.07 1786.

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1670 1.9342E+01 -3.1442E-04 M-xylene 106.9130E+00 8.0000 0.0000 0.167 0.2315E-02 -1.0000 Phthalide 134.0000E+00 -7.3244E-03 0.8146E-03 2.2708E-01 32.0000 -3.167 2.9953E-02 -2.9800 M-xylene 106.0000 0.15 T out (K) : 433.058 0.0094 1.0707E-02 44.011 0.6320E+01 3.0000 0.0000E+00 2.2662E+01 1.016 0.0000 0.1885E-03 -1.0000E+00 2.0000 0.0000 0.150 0.0000E+00 1.9060E-01 2.0000E+00 1.6405E-03 0.8201E+01 1.011 0.0000 0.6725E+01 5.0000 0.9506E-01 -7.150 0.7101E-02 6.0000E+00 9.1233 Phthalic anhydride 148.0000 0.0000E+00 -4.8716E-03 136.011 0.0000E+00 5.0000 0.0000 0.3161E-01 -3.0000 0.4926E-01 -2.0000 0.0000E-02 148.0916E+01 8.0000 0.0000 0.0000E+00 -8.70 Komponen BM Berat (kg) ni (kmol) Xi A B C O-xylene 106.014 0.1353E+00 -2.0563E+02 1.9800 4.0000 0.000 0.058 0.136 0.167 1.2053E+01 -3.0000E+00 7.6690E-03 Water 18.0083E+01 3.9556E+01 -6.0000 0.0450E-01 -2.0437 0.15 Komponen BM Berat (kg) ni (kmol) O-xylene 106.0000 0.2500E+01 2.8782E-01 -8.4304E+00 -3.4118E-05 .1431E-01 0.7330E-04 Ortho Tolualdehide 136.0000E+00 3.2015E+01 1.0200 2.8644E-04 134.118 148.000 0.011 Carbon dioxide Oxygen B C 9.0960E-01 2.0000 0.4085E-01 0.1470E-02 6.9906E-05 106.0000 0.KAPASITAS PANAS GAS T reff (K) : 298.9980E-04 Carbon monoxide 28.0000 TOTAL KAPASITAS PANAS CAIRAN T reff (K) : 298.0000 0.8200E-01 5.1260E-04 Maleic anhydride 98.0000 2.0212E-04 0.0000 4.6460E+01 KAPASITAS PANAS PADATAN T reff (K) : 298.9555E-05 Oxygen 32.0000 0.167 M-xylene Phthalic anhydride Berat (kg) ni (kmol) Xi A 104.0000 3.0000 5.1344E-01 -2.6424E-01 -2.9810E+03 5.6084E-02 9.4383E+01 6.0000 0.0423E+00 -1.9526E+01 -8.0000 3.1233 0.0000 0.3933E+01 -8.6465E-04 0.7022E+00 1.15 T out (K) : 379.0000 1.6452E+01 -3.4305E-03 Phthalic anhydride 148.0000 0.7860E-01 2.0000 TOTAL 5.0076E-05 Water 18.5807E-03 2.011 0.118 0.0437 0.5395E-03 1.7437E+01 4.118 0.0000 0.9986E+01 7.9840E+00 -3.0130E-05 Carbon dioxide 44.0000E+00 Carbon monoxide 28.4220E+01 6.0000 0.0000 0.2850 2.0000 0.0000E+00 2.2560E+02 -1.150 0.0000 2.0000E+00 2.0000E+00 -3.4357E-01 -1.0000 0.0000 0.6432E+01 3.058 Ortho Tolualdehide Phthalide Xi A B C 9.0000 Carbon monoxide 28.4073E-03 Carbon dioxide 44.1830E+01 -4.0000E+00 Phthalide 134.0000 3.0000 0.0000E-02 -1.167 104.0000 0.0000E+00 Ortho Tolualdehide 136.3836E+01 6.2511E+01 -2.1180 1.0350E+00 2.0000E+00 4.0000 0.5226E-01 -2.0000 Maleic anhydride 98.0000 1.0000 0.8000E-01 1.0000 0.011 0.1103E-04 254.0000 0.0000 0.0200E-01 7.0000 0.00 Komponen BM O-xylene 106.8083E-05 Nitrogen 28.0564E+00 -2.9000E-01 106.9847E-03 0.1195E+01 3.0000 0.0000 0.0200 1.0000 0.0522E-03 Nitrogen 28.0000E-01 Maleic anhydride 98.136 0.0000 0.5956E-04 0.4902E-03 7.014 0.8847E-03 -1.00 T out (K) : 298.0000 0.0000E+00 4.0000 0.136 0.016 0.8889E-03 3.0000 3.167 2.

0000 -1.4334E+01 2.014 0.0000 0.0094 1.0000 0.0000 9.0000 0.1577E-03 Water 18.0000 TOTAL -2.0000 0.5584E-05 1.6950E+00 7.8866E-01 1.5925E+00 Nitrogen 28.0000 0.000 0.016 0.4955E-02 -1.9859E-03 .Oxygen 32.0000 0.6683E+01 1.0000 2.0000 0.

5796E+03 0.4623E+03 0.0000E+00 0.0000E+00 0.7486E-08 5.5869E-11 2.6541E-07 0.0000E+00 0.0518E-06 0.0000E+00 0.0000E+00 Maleic anhydride 9.0000E+00 0.1578E+04 TOTAL D E Cpl dT (J/mol) H sensibel (kJ) 0.8607E-12 4.0000E+00 0.0000E+00 6.9770E+04 0.4764E-06 0.0000E+00 0.5935E-13 3.0000E+00 5.1592E+04 2.0000E+00 0.0000E+00 1.1615E-08 2.0000E+00 5.0000E+00 0.0000E+00 0.1016E+04 0.0000E+00 0.0000E+00 0.0000E+00 Nitrogen -1.9424E-12 1.2341E-06 4.0000E+00 0.7825E-08 3.0000E+00 1.2866E-04 0.0000E+00 2.0000E+00 2.0000E+00 0.0170E+04 0.6838E-06 0.1584E-06 0.0000E+00 0.0000E+00 D E Cps dT (J/mol) H sensibel (kJ) 0.0000E+00 4.0000E+00 Water 2.0000E+00 0.5647E-10 1.6527E-06 -5.0000E+00 0.3469E-07 0.2617E-12 3.0000E+00 1.4133E+04 1.0000E+00 2.0000E+00 0.2629E-08 8.0000E+00 1.0000E+00 2.0000E+00 2.7408E+04 0.3116E-09 2.9551E+03 0.0000E+00 0.1791E+02 M-xylene -1.6870E+04 0.9897E-05 0.5061E-06 0.0000E+00 Phthalide -1.0000E+00 0.1760E-08 -2.3212E-11 2.0000E+00 0.0000E+00 0.0000E+00 Oxygen -4.4953E+04 0.0000E+00 0.0000E+00 Ortho Tolualdehide 1.0896E+04 4.3312E+02 0.0000E+00 1.1160E+04 O-xylene 1.0000E+00 Phthalic anhydride 1.0789E+04 0.0000E+00 0.0000E+00 0.0426E+03 0.0000E+00 .0000E+00 0.8328E+03 0.0000E+00 0.0000E+00 0.0000E+00 1.9968E-09 -2.0000E+00 Carbon dioxide -3.8513E-06 0.6823E-11 4.7488E+04 0.2227E-08 2.8751E+04 0.3381E-08 1.0000E+00 0.4943E+04 0.9872E-13 5.0000E+00 3.9416E+03 0.0000E+00 0.0000E+00 0.0000E+00 0.0000E+00 0.0000E+00 0.0057E-05 0.0000E+00 Carbon monoxide 3.6597E-10 1.0000E+00 1.ENTHALPY PENGUAPAN T dew (K) : D E Cpg dT (J/mol) H sensibel (kJ) Komponen -2.0000E+00 3.0000E+00 0.6934E-12 4.0000E+00 4.0000E+00 0.

0000E+00 0.0000E+00 0.7156E+03 0.0000E+00 0.0000E+00 2.0860E+04 0.3312E+02 .0000E+00 0.0000E+00 1.0000E+00 2.4549E+04 0.0000E+00 1.0000E+00 0.0.

0000E+00 134.0419E+02 2.0000 5.1705E+02 4.0000 0.3300E-01 0.000 0.0000 0.5100E+02 3.0000 0.8000E-02 0.9100E+02 3.1800E-01 0.5606E+01 6.8000E-02 0.0000 8.5216E+04 106.118 0.0100E-01 0.5907E+04 .0000 0.0000 5.011 0.0000 0.3037E+02 3.1670 1.0000E+00 28.0000 0.0000E+00 98.4000E-01 0.0000 4.2100E-01 0.2053E+01 6.1600E-01 0.0000E+00 44.8800E-01 0.0000E+00 0.0000 0.150 0.167 2.7500E-01 3.0000E+00 18.0000 8.5551E+01 7.0000 0.0000 0.016 106.0437 0.0216E+01 6.0400E+00 1.4713E+02 3.5495E+01 7.0000E+00 32.136 0.0000 5.167 104.3292E+02 3.5458E+02 2.0000E+00 28.014 0.0000 9.1000E+02 3.9098E+02 148.8260E+01 3.0000 3.1233 0.0200 6.0000 1.1444E+01 7.0000E+00 136.9574E+01 7.0000 9.2100E+02 2.0030E+00 1.60 BM Berat (kg) ni (kmol) A Tc (K) n H vap (kJ) 106.5800E-01 6.4300E+00 1.2610E+02 5.9800 5.011 0.ALPY PENGUAPAN 433.058 0.

.

55 Cp mean (kJ/kg K) : 4.3469E-07 0.2053E+01 -3.9263 .0000E+00 T input (K) : 485.9953E-02 -2.15 T output (K) : 541.1103E-04 D E 5.MENGHITUNG CP MEAN COOLING WATER A B C 9.

.

COOLING WATER .