Successful applications of cryogenic treatment of metals go back decades.

Numerous articles have been published touting tool life improvements of 5 times or more compared with untreated cutters. However, widespread acceptance of this process has been relatively slow in part because deep freezing tools for longer life seems unbelievable, and there is a perceived lack of scientific data to conclusively document what s actually happening. However, there are theories that explain what happens in ferrous materials and carbide when cryogenically treated, but they fall down when trying to explain why the process works for nonferrous materials. This article concentrates on cutting tools for metalworking, not golf balls, nylon stockings, plastics and other materials that use cryogenics to enhance their performance characteristics. Giving it the Treatment The cryogenic treatment process is relatively simple albeit time consuming. A typical treatment cycle takes around 48 hours to complete. However, time is the key to a proper cryogenic treatment. Each step is timed usually based on the weight of the parts being treated. The cool-down phase, going from ambient to minus 300-310°F (the temperature of liquid nitrogen) usually runs in a 4- to 6-hour range (1 to 2 degrees per minute). This is followed by a soak lasting around 24 hours. Once the parts have soaked, warm up to room temperature is another 4 to 6 hours. Most cryogenic chambers are equipped with a small heater that raises the temperature to almost 300°F for the final couple of hours to ensure there are no cold spots in the material and to provide tempering. Because nitrogen in its gaseous form is used as the cooling agent, parts and tools to be cooled remain dry. During the cool-down phase any oxygen in the chamber is purged by the nitrogen, so no rust can form. Only arrangement of the parts is needed, no fixtures or racks are required. The flow rate for the nitrogen and the various timed steps are controlled by a computer and use data collected from experience. Once the time temperature information is programmed, the process is automatic. The cryogenic unit looks not unlike a chest freezer or refrigerator. The tools or other parts come out of the cryogenic unit with no discernible changes in color or cosmetic appearance. No dimensional changes will appear either, with the exception of items that were improperly heat treated prior to the cryogenic treatment, leaving internal stress that may be released during cooling. According to Bill Groschen, president of Diversified Cryogenics, This lack of cosmetic change can be a detriment. For many of my customers, the fact that there is no physical change makes some of them doubt the efficacy of the process. However, those doubts disappear when they see the increase in tool life from cryogenic treatment.

Here. In addition to longer time in the cut. Make it Part of the Process Taking advantage of cryogenics can result in significant cost savings from increased tool life. Randall Barron from Louisiana State University.to five-fold improvement over the normal life of these tools. so . thereby resulting in an overall improvement in wear resistance. there are two primary mechanisms at work in the cryogenic treatment process. which is very hard and brittle. Barron writes. the martensite is tempered to provide better toughness properties as the metal returns to room temperature. Those principles involve the well-known heat and quench cycle employed for centuries to control the performance characteristics of ferrous materials. reamers and other cutting tools have been the subject of most of the research of the cryogenic treatment effect. mostly because it is based on the known principles of metallurgy. The slow warming to room temperature from the cryogenic temperatures of minus 320°F tempers the martensite so that it is better able to resist impact than untempered martensite. the belief is that the carbide inserts shrink slightly during the cool-down phase of the treatment. he writes. creating some plastic flow within the micro-voids in between the carbide and the binder. However. results in the formation of very small carbide particles dispersed within the martensite structure between the larger carbide particles present in the steel. it is treated for life. Dr. such as tool steels. Second. it leaves compressive stresses on the surface of the voids. Cryogenics simply takes the quench to new lows minus 300°F. these tools wear less. When the carbide returns to ambient temperature. tend to counteract localized weakening caused by the voids. According to cryogenic treatment research done by Dr. Once a cutter is treated. The way these smaller particles act to strengthen the steel is analogous to concrete made from large aggregate versus concrete made from very small aggregate (course sand). The theory that accounts for these results in cutting tools is widely accepted. These compressive stresses. The smaller aggregate makes a much stronger concrete mix than one using the larger rocks. twist drills. in turn. hard carbide particles within the martensite matrix help support the matrix and resist penetration by foreign particles in abrasive wear. The research has demonstrated that using deep cryogenic treatment results typically in a two.More Than Just a Leap of Faith Alloy tool steels such as those used to make end mills. Carbide inserts and form tools also show an increase in wear resistance from cryogenic treatment. First. Super cold treatment seems to convert retained austenite structures in the metal into martensite. The cryogenic treatment of high alloy steels. The small. The martensite structure resists plastic deformation much better than an austenite structure because the small atoms in the martensite lattice lock together the iron atoms more effectively than in the more open-centered cubic austenite lattice.

predictable tool life can make the transition to unmanned operation less stressful.resharpening requires less material to be removed. to take full advantage of cryogenic treatment. It s really no different than sending parts out for plating or coating. For lights-out operation or lightly tended machining. so the time needed to send cutters to be treated needs to be calculated into the production schedule. the cryogenic treatment process itself takes 2 days. The turn around time must be calculated into the delivery schedule. Of course. like many machine shops. longer. so more regrinds can be done. However. . a shop must include it in the planning process. Likewise. Diversified Cryogenics included. one can bring the process in-house.