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  • Trip To Fano

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    Rosa Velásquez
    31 views2 pages
    Calculo para digestión Kjeldahl triptofano

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    Trip to Fano

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    Calculo para digestión Kjeldahl triptofano

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    31 views2 pages

    Trip To Fano

    Uploaded by

    Rosa Velásquez
    Calculo para digestión Kjeldahl triptofano

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 2

    KjelOptimizer Report

    Options
    Analyte Nitrogen

    Unit nitrogen content %

    Distillation type Standard Kjeldahl

    Distillation instrument K-375 (stand-alone)

    Digestion instrument K-449/K-446

    Tube size 300 mL

    Digestion type Standard Kjeldahl

    Catalyst type Powder

    Sample unit g

    Boric acid concentration 4 % H₃BO₃

    Sample Information
    Sample composition Ok.

    Nitrogen 12.70 %

    Fat 0.0 %

    Water 0.0 %

    Carbohydrate 87.3 %

    Sample amount 0.2000 g Organic sample is 0.125 – 2 g.

    Titrant normality 0.250 N Ok.

    Digestion Parameters
    Amount Kjeldahl Catalyst 4.5 g Ok.

    Triptofano 1/2 20171220


    KjelOptimizer Report
    Amount Kjeldahl Catalyst 4.5 g Ok.

    Volume 98 % H₂SO₄ 9 mL Ok.

    Digestion time 120 min Standard Kjeldahl digestion using Kjeldahl Tablets

    Distillation Parameters
    Volume H₂O 35 mL General rule: For autosamplers K-371, K-376, K-377 use 2.5 mL per
    used mL H₂SO₄ (digestion). For manual distillation use 4 mL per
    used mL H₂SO₄ (digestion).
    Volume 32 % NaOH 42 mL General rule: Use 4.5 mL NaOH per used mL H₂SO₄ (digestion).

    Boric acid pH 4.65

    Boric acid volume in receiver 60 mL

    Distillation time 150 s

    Titration Parameters
    Blank titrant consumption 0.230 mL The calculated and the measured blank values do not necessarily
    match exactly.

    Sample+blank titrant 7.484 mL Ok.


    consumption Note: The calculated and the measured
    consumption value do not necessarily match exactly.
    Relative standard deviation 0.34 % Ok.

    Amount N 25.40 mgN/sample Ok.

    Triptofano 2/2 20171220

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