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ARN AININ CYATIOAH Bit mublecaly .
Experiment 2 betevigeation Reactions enrrle § furPle-orear
D + ice-cold water Co6aL) > Pale hah green
| , ~ __+ Pare re soreer Gate. vq) duce orptalizertion
= 4mall folid_ ames
© re mn \ foryctal _ _
= weieg Hirsch Funnel @snott ‘Buchner fren
4 was CL Wemcad water) —> repeat 3x
‘
| seanctev ——
{ — som Beaker 7 —_ 2
\
& \ BAL Wp EfOt + orvetal eolid A
Rn + magnate Hier
heat C60°C) + Efott until complehe dicsslve,
Q
Raystal , Vv stratchiny op (down
a 8 Cai) inside eee Be
ice batt beat
Stiles andev eee + wah C cold tfoth 45% )
Reduced Presta.
{ Hallow evystal_dvy by enckiy air
Xoven te oye lh
. Aransher Supe a _weigted labeled, sarge bolt oe
V_metting point of trey product Citevebus value i 90 — aro)
Y¥ NRF HNMR Cin Doty) sp
V__ 1% SRecher for vanitia
2 = mang Pout eb the Product
a= Areearane of
mduct = AMARNI AHOIN GYAFIOAH BITC NiyKeAI NY
al. Kea
Baio: media =
| Prefenration af product
o_ |) CSP ge) | 4 to couched ice
Gs vavivin Gv809) + Ao mL octkec ankydide
Sperm ayer T Naolt C7 asm) SE loady » enitky nate precipitate, ove,
Flask "4 @vight yellow greed solution
o m™
= TraKe over SOaTE poviek
@ T coe rear & Cini)
+ xonctol, ¥ comtch spldowa Hack
@ we wath emalt amount Eto ie
_f transfer to a weighed labelled eampe vote.
determine tha melting goins ( #4 74°C) Hee
Rs ‘HMR Ci COG,)
IR spectra for varilin
