WY Expeniment No-1: Detonminadion of PER, Cu! and ty’lin dhe supphiod rriktinna . meelesledions 2 Deloowinaion of PE Wt. of bhonk. anneible = IRI 4 WH. of crucible usith Psp, = BH 208 4 . leigh of Ply = [24-2998 68.4245) = D452 9 Sobag PlSDy Contoins = 2072 PLP “1g Pes» = eg re eyes D'4525 4 Peso) = pe O-BRe g PBT DSnl soluben enntoms 0-S088 j PLT Ds 20¢Q at Ea » Cos i Pb 0-40 88 X 100 ot = tpomk » ees Sue = 12050 4 petADetenminodlion af Cr” attordanizedion os Nay3,0n, rq shandond D-1 N” KoCny 0}: % Preponadion of ghardore @-LN Kats by 201” Moleaulan use toh} of Ko CnOz > 9944. Equi walerr} aati of K,Cn,07 = a4 > 42 g 5 1000 mL AN KCno7 194 KC, b7 co dmk TNT KytnDe ~ o » ‘Boom DLN Kitagde = OREO J Ky Gngb7- = [12269 J Qe ~ 199599. height token = 12260 3: : Strength od Kathy bg = og Ee olg® ele 227 9, TopRS X01 =D0-10N% Stondonizadson of NowSs0e by stordond 0. DAN Kany D7: [No of - Volume. Panels naa ing (m1), | Moon bs ton| KyCny Oz (mt) —— a 0! vomvodion Cry DF | ) The. The. [De Benne (¢ 0) To |» | oo | os | os jo. ; 4° | 25 1% | BY “* On» | to | 1% 28.4 | 5 ~ t : Vesenady XS ta - Shenath ot NOS0>,Siag.0, = nee 10 XO-1 O65 - = 0-105 Nr ® Expenim to dota -bon determination of Ayer: No. o} obson! Volume. of Pouncte reading (md), Mean ¢ : Or . vokion ds Oe ; Tip. roe. D: Honanea| fr). DL 50 DD 48 4g oo 50 We O65 ap | RAF On, 50 Oe Blt 2) WF*Tidnodion value ton (50m) Awl AN Na S05 = D-D6%5y a Cit Hm 0-105 Ne Noy, = 206954 X47 D105 4 = 0-0514 J C2. 5D mi soludion contains, - o-0aN4 9 yet * Lmk " ” = DDI 4 Ott = 25pm» n, DDBIYXEED a, 24 5 a DIST | Oy? 25 ml soluction- D eortoany ~ pists Get. os sil ” ” = a q Ox IBIX S00 mo hoe eng ut = D608 O y+ot , x Detenrinak Kon ot 2 Fe standond EDTA sobuko or. (c 0-01 MD, 3 Peeponation of standond Moleenlon wsoight of EOIN 142-049 Jboom 1m EDTA nequinas O24 9 BF2:24 Tmt am» . ie 072-24 YOrp yp.p} 250ml dorm » ave2t x2 = 02406 g- kt of EDTA talon = D:20I6 4. ie of EDTA to bo Ae = D- 20064 stnanerh Weight foleon ee h of EDTA = Nephi to be Tolen® 0-2 0.9916 D.Smp6 7 XO-01 = 0-D1D AEM,® Experimental Doska bon deranminelion (Ge an): TNo.of Molume of | Pounetle ne di (rd. Meon dbsonvotion soludion-1s — - =a ith (ind), (oh) Tp. Poe | Di ot 5 | po | &6 a6 | a os 86 | red ab | 6 2 | 259 oF | _|___ ~. Ttnodtion value e [e-o-4F)m = B.oml. Novo, ooorl 1M EDTA 65-8 4 Dye 65:28 X0-0, i - tml 01 M EDTA = a 0 Bet é ; ~ SE BIDDIKS® 5 aft BOmk 0-DIM FDTD) = a 4 = Op2BE OG met5Bmi ro Lukion. D> Lortoms D.00 8550 q En? Meena: D aoa q nt = asp mi POpeeE REO Bo - DuD764 at 25m soludon-p domtodns ome apr Sm ” ee , J a 7.100 mh ” ” D:1D75 X10. 2+ oS = 0-51 q Dy Result! OArourt of Pe : Sronsng pet CO Drrouest ob Cut: 06289 Cu* Gi) Amount of 2Pt: 0-510 d BP® Experiwnerd No-2.: tolemtodion’ @ Prepanestion of tho. somplex [ilens|4 Weight ot NiUy:6Ho0, hh = eq Weiaht at blonk. ansible = Oi 1569 4: Weight of enueible usd Ni2t complex = MP 8626 (] i height of N12 comple, tary = (0% 86% - ay -1569)9 DURA Molecule veg of NiMy- Hoo. My = 287-FG Molecular poate of [Ni lene] Uy Mp_= 302-699 . | of of geld > iM, X 400 hip, - 22 , 2tF Bae *— 2 %100 = 104-11 >Theoni tial takeutodton of Ni2 ww complex: Height taken bon the enbiradion of Ni* comple = 0: +751 q oer Ni - comple avytotins 5269 q Niet ol . . ~ DBOD yt d * 109-6 JJ N DFS 9 ” ; Sees) N = D146 4 Ny 2r ® Poapanokion of 0-01 M shandand EDT soludgon: Hert, Mpleanlan uscight of EDTA = 92.049 . “Weight ty be token tl = am _ Binoy 25 x01 IDob = D-O06 a ’ Weight taken = 9.94 0-914, J:: tne : ht taken S gt of Epra - te an The yooim . “Ben OM IL OP vpn 0-B%06 = 0.0D10M. mona dota, Ebon sp bucion-D Na. oF | [Volume ol - tanstlo neodting (rh, _ | meer obsons so Hey [a The. | T ERE Di oe + (ml), | of 5 D0 ou 24 DD, 5 | Ou 1GD. Qu1 Oo. 5 % IRD. O+4 OD el & Amount of Nit in solution L: 1000 4m EDTA = 68.69 q Nit Yok gm = E69 g yee » ooo “O1tpl ODLM n= PROT qin= 000584 J Nowo, Bint toluton-D anelains ~ D-0D5%4 q Nye ink B » _ 00584 qa = 3 \ “0D or -. BOnt " rine Ooms x50 1 eo 0:0554 d Niet Fon. colucion¢, 1D mb soilittions cere = D654 4 Not +, 25 wh ” 7 — DDESHXOS roe to 0 7 Buena Niet .Pgcin. nom Aibnoclion, 4 . Stoogh By ED) s = 0.01 SyVi = Sy Vo 001M Ni Vo Lume of Eh . OD XO1 = Sy XE ~ o1mib So°9 “S, = = Vp=Nolume of sal = DD1g2 M -D= Smt. 5 himos dilide Sp < (0-0182x6) =0):091 M. ss ae _toleuledd value 5, re | , = 01595 D.1449 X10 = WHR a of onnon Troon’ tual value calonladed aloe : loo 0146 294090® Exlimation af Ni-eontort by speednosporie methed Fon stondand solution Dbsonphion, As = D-4yoy previ of Ni ‘0 the kenoumn sobition, ty = 58a 4l~ r Length of the ell, b= 1am. 7 lenovo, A, - cal Ae é v7 2 D-4Oy Seqaxr — ~ 8 lxio® gen Fon Bala -“4, Hone, D=-etd Dibsengetion “bon Hho. solhtim a at -2 90 =D.46% meen ation of Ni% in em 62 Lids 8414 XID XL dohnieer tet) = 55 1Y qe: fon nner ee oreo liar in mrodye a oe R62 = 0.09497 wattWe. lanow, tmoll Ni2t contain ~ 58 699 2.00945 moll? Nit | (59-69 x0-02497)F = 55TH 4 S000 mk Ni aortain 5.574 dq: pel nw Sg 2 OBmL NA nL STA a © 0190854 - % of gid - Spat ni _ a xi00 = O4.86 a ab alt ee ne (100 - 94-22) = By Tnlanmodacte vanictlion of -h of gield berhus +o method = (94-%6- 29.372) = 0.08 _ ni Rossakt: @ Paspanachion of the om lax [Nilene Jy MWNegh} of the complax a 2.1104 4 @ yf. of qield = y0y.a1 . ® Estimation of Ni-¢onton! 4 Aedes mot ate. method: a) Dour} of Nieleel = DABS g (i) 4 of fel = B.VPQ (in) ‘} o} onron = 9.409. © Esdimodion os Ny carton npootnosenpie method : © Amount o} Nicol = 0:199454 . Gi) tf. of gel! = BY.2g If o} enon = 514 Trtonmectiats voniohion (1 of ie = [24%6-90.878) ~ = .2%9 ,