RSRM (8gram)

Silica gel 60 Chloroform: Methanol: Water

(60-100mm) 70:30:4 65:35:5 60:40:5 50:50:0 100 Methanol
M1 M! M3 M4 M5 M6 M7 M8 M"
3040mg 440mg "5mg 8"mg "6mg "0mg 83mg 70mg !0mg
J (370 mg) # M3$M4$M5$ M6
Silica gel 60 (0%040 & 0%063 mm) 'th(l acetate: Methanol: Water
"8:14:7 77:13:10 70:!0:1! 10:15 100 Methanol

)1 )! )3 )4 )5
*
)
6
)7 )8
*
)"

8!mg 68 mg 57 mg 4" mg 6 mg 30 mg 4! mg 5 mg 5mg
+ (150mg) # )1$)!
Silica gel 60 Chloroform: Methanol: Water
(0%040 & 0%063 mm) 70:30:4 65:35:5 60:40:5 5:5:1 100 Methanol
+1* +! +3 +4 +5 +6
8 mg 40 mg 1! mg 7 mg !0 mg !1 mg
RSR, (10gram)
Silica gel 60 Chloroform: Methanol
(60-100mm) "":1 8":1 7":1 6":1 5":1 3":1 1":1 ":1 1:1
100 Methanol
,! ,4 ,6 ,8 ,10 ,1!
760mg 110mg 155mg 68mg !!"mg 340mg
,1 ,3 ,5 ,7 ," ,11 ,13
1710mg 3110mg "0mg 160mg 350mg 4"7mg 650mg
,- (!00 mg) # ,4$,5
Silica gel 60 n: ./ !":1 14:1 ":1 5:5 1:1
(0%040-0%063mm)
,-1 ,-! ,-3 ,-4
64mg 46mg 30mg 40mg
,-0 (110mg) # ,-1 $ ,-!
Silica gel 60 n: 1/ 1":1 ":1 5:1 1:1
(0%040-0%063mm)
,-01 ,-0! ,-03 ,-04 ,-05 ,-06
!0mg !6mg 14mg 18mg 8mg 5mg
,0C (3%80g) # ,! $ ,3
Silica gel 60 n: 'th 1":1 ":1 5:1 1:1
(0%040-0%063mm)
,0C! ,0C4 ,0C6 ,0C8 ,0C10 ,0C1! ,014 ,0C16
1"mg 16mg !8mg !7mg 30mg 310mg 446mg 700mg
,0C1 ,0C3 ,0C5 ,0C7 ,0C" ,0C11 ,0C13 ,0C15
36mg 1!mg "mg 30mg 40mg 771mg !10mg 3!0mg
,'
,' ("00mg) # ,0C1! $ ,0C13 $ ,0C14
Silica gel 60 C.: ./ 4":1 3":1 !":1 1":1 ":1 5:1 1:1
(0%040-0%063mm)
,'! ,'4 ,'6 ,'8 ,'10 ,'1!
30mg "0mg 31mg 10mg 1"mg 10mg
,'1 ,'3 ,'5 ,'7 ,'" ,'11
,'13
!0mg !70mg !0mg !8mg 8mg 10mg 5mg
,'4 ("0mg)
Silica gel 60 n: 1 ":1 ":1 1:1
(0%040-0%063mm)
,'4- ,'40 ,'4C ,'4, ,'4' ,'41 ,'42 ,'43 ,'4.
3mg 8mg 15mg 16mg "mg 6mg 7mg 1!mg 7mg