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Analytical Methods for Determination of Metals in Environmental Samples

Analytical Methods for Determination of Metals in Environmental Samples

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Published by: kenzu_mu on Apr 10, 2011
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08/19/2013

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Analytical methods for determination of metals in environmental samples
G.de Gennaro, B.E.Daresta, P. Ielpo, M. Placentino
LEnviroS, Laboratoryof EnvironmentalSustainabilityDepartmentof Chemistry-University of Bari
 
An analytical method for the determination of the heavy metals iscomposed of 3 steps:
Sampling
Pretreatmentof the sample:
it depends on analyteof interest and consists in acidification(e.g. Fe
3+
in waters), acid digestion(e.g. Zn
2+
in sediments), filtration (in order to remove coarse particlesto preserve the analytical instrumentation), preconcentration,etc
Analysis
seawatersgroundwatersrainwatersriverwaterssedimentssludges
The samplingdependson matrix 
AASICP-MSICICP-AES
particulate
XRF
 
Analytical technique choose
CostSensitivity (Limit Of DetectionPhysical state of matrixAvailability of instrumentation !!!

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