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polymers
2.2.4 The Polyaniline
2.2.4.1 Methods of Synthesis
2.2.4.2 Polymerization Mechanism
2.2.4.3 Protonic Acid Doping of Polyaniline
2.2.4.4 Properties of Polyaniline
2.3 Light Scattering Methods
1. Dynamic light scattering (DLS)
2.3.1 Dynamic Light Scattering (DLS)
2.3.2 Static Light Scattering (SLS)
transmitted laser beam
2.3.3 Advantages and Disadvantages of Light Scattering
2.4 Viscosity
2.5 Carbon Nanotubes and Conducting Polymers
2.6 Conducting Polymer and Thermoplastic Composites
2.7 Mechanical Properties of Composites
3.1 Materials
3.2 Instrumentation
3.2.1 DC-Conductivity Measurements
3.2.2 Elemental Analysis
3.2.3 Thermal Analysis
3.2.3.1 Thermogravimetric Analysis
3.2.3.2 Differential Scanning Calorimetry
3.2.4 Fourier Transform Infrared Spectroscopy
3.2.6 X-Ray Powder Diffraction Analysis
3.2.7 Light Scattering Methods
3.2.8 Intrinsic Viscosity Measurement
3.2.9 Scanning Electron Microscope
3.2.10 Tensile Strength
EXPERIMENTAL PROCEDURES
4.1 Synthesis of Polyaniline (Emeraldine Base) at 25o
yields polyaniline (emeraldine) hydrochloride
to polyaniline (emeraldine) base
4.2 Synthesis of Polyaniline (Emeraldine Base) at 0o
4.3 Synthesis of Polyaniline (Emeraldine Base) at -25o
4.4 Preparation of Leucoemeraldine Base
4.5 Sample Preparation for Light Scattering Measurements
RESULTS AND DISCUSSION
5.1 Synthesis and Characterization of Polyaniline
5.1.1 Polyaniline Synthesis
5.1.2 Characterization of Polyaniline
5.1.2.1 Conductivity Measurement Analysis
5.1.2.2 Elemental Analysis
5.1.2.3 Thermal Analysis
Figure 5.1: TGA of Emeraldine Base (EB) synthesized at different temperatures
5.1.2.5 X-Ray Analysis
C-CPMAS Chemical shifts of Emeraldine Base powder
5.1.2.7 Morphological Analysis
5.2 Solution Properties of Polyaniline
5.2.1 Static Light Scattering (SLS)
prepared at deferent temperatures
5.2.2 Intrinsic Viscosity Measurement
C using three different EB molecular weights
5.2.3 Dynamic Light Scattering (DLS)
5.3.1 Thermal Analysis
Figure 5.23: DSC melting curves of LDPE and its PANI powder composites
5.3.2 Mechanical Properties
5.3.4 Morphological Analysis
composite
6.2 Solution Properties of Polyaniline
REFERENCES
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Published by: ahmadpoly on Apr 26, 2011
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02/18/2013

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