Professional Documents
Culture Documents
ΕΠΙΔΡΑΣΗ ΤΟΥ ΛΟΓΟΥ CN ΚΑΙ ΠΡΟΣΘΕΤΩΝ ΣΤΗΝ ΚΟΜΠΟΣΤΟΠΟΙΗΣΗ ΟΡΓΑΝΙΚΩΝ ΑΠΟΒΛΗΤΩΝ
ΕΠΙΔΡΑΣΗ ΤΟΥ ΛΟΓΟΥ CN ΚΑΙ ΠΡΟΣΘΕΤΩΝ ΣΤΗΝ ΚΟΜΠΟΣΤΟΠΟΙΗΣΗ ΟΡΓΑΝΙΚΩΝ ΑΠΟΒΛΗΤΩΝ
C/N
2010
!!!
ii
,
2010 2011.
.
,
..., . ,
.
,
.
, .
,
.
, , .
,
.
... . Tanja Kosanovic
Milickovic .
iii
iv
iii
ix
ABSTRACT
xi
1
1.1.
1.2.
1.3.
1.4.
1.4.1.
1.4.2.
1.4.3.
,
1
8
17
23
24
31
2.1.
2.2.
2.3. -
2.4.
2.4.1.
2.4.2.
2.4.3.
2.4.4.
2.4.5. / (C/N)
2.4.6.
2.5.
2.5.1.
2.5.2.
2.6.
2.7.
2.8.
3
3.1.
3.2.
3.3.
3.4.
3.4.1.
3.4.2.
3.4.3.
3.4.4.
3.4.5.
3.4.6.
3.4.7.
3.4.8.
3.4.9.
3.4.10.
3.4.11. (Teleprobes)
3.4.12.
3.4.13.
3.4.14.
3.4.15.
3.4.16.
3.5.
3.5.1.
() .
3.5.2.
3.5.3. Compost Hellas .
3.6.
32
35
35
39
42
43
44
46
47
47
49
50
50
56
59
62
63
67
67
68
69
69
70
71
71
72
72
73
73
74
74
75
75
76
76
77
77
78
78
79
81
82
3.7.
3.8.
3.8.1. Dalek
3.8.2. CompostTumbler
( )
3.8.3. Rolling or Rotating Orb Composter
( )
3.8.4. Wooden / Wire Mesh Composter
(/ )
3.8.5. Computerized Indoor Composter\
( )
3.8.6. Worm bins
85
85
85
90
96
100
101
103
4
4.1.
4.2. ,
4.3.
4.3.1.
4.3.2.
4.4.
4.4.1.
4.4.2.
4.5.
4.5.1.
4.5.2.
4.5.2.1.
4.5.2.2. /
4.5.2.3.
105
105
106
107
108
110
110
111
112
114
115
115
117
117
5
5.1.
5.2.
5.3.
5.3.1.
5.3.2.
5.3.3.
5.3.4.
5.3.5. (VSS)
5.3.6. (TOC)
5.3.7. Kjeldahl ()
5.3.8.
5.3.9.
5.3.10.
5.3.11.
5.3.12.
121
121
124
124
125
125
126
126
127
128
131
133
135
135
136
6
6.1.
6.2.
6.3.
6.3.1.
6.3.2.
6.3.3.
6.3.4.
6.3.5.
6.3.6.
6.3.7. (VSS)
6.3.8.
6.3.9. Kjeldahl
6.3.10.
6.3.11.
6.3.12.
6.4.
6.4.1.
139
140
141
141
143
145
149
152
155
157
160
164
166
169
172
175
175
vi
6.4.2.
6.4.3.
6.4.4.
6.4.5.
6.4.6.
6.4.7. (VSS)
6.4.8.
6.4.9. Kjeldahl
6.4.10.
6.4.11.
6.4.12.
7
7.1
7.2
7.2.1
7.2.2
7.2.3
7.2.4
7.3
7.3.1
7.3.2
7.3.3
7.3.4
7.4
7.4.1
7.4.2
7.4.3
7.4.4
7.5
7.5.1
7.5.2
7.5.3
7.5.4
7.6
(VSS)
7.6.1
7.6.2
7.6.3
7.6.4
7.7
7.7.1
7.7.2
7.7.3
7.7.4
7.8
Kjeldahl
7.8.1
7.8.2
7.8.3
7.8.4
7.9
7.9.1
7.9.2
7.9.3
7.9.4
7.10
7.10.1
7.10.2
7.10.3
7.10.4
7.11
7.11.1
7.11.2
7.11.3
7.11.4
177
179
182
185
188
191
194
197
199
202
204
207
207
207
209
211
213
215
215
217
219
221
223
223
225
227
229
232
232
234
236
238
240
240
242
244
246
249
249
251
253
255
257
257
259
261
263
265
265
267
269
271
273
273
275
277
279
281
281
283
285
287
vii
8
8.1
8.2
8.2.1
8.2.2
8.2.3
8.3
8.3.1
8.3.2
8.3.3
50
8.4
291
291
291
292
292
293
294
301
306
308
313
viii
,
.
,
C/N
.
.
.
,
.
,
( ).
.
, ,
. ,
.
.
.
ix
.
. ,
.
. ,
.
.
.
, .
.
ABSTRACT
The main focus of the following thesis is to study the properties of the product
derived from the composting of household waste which took place inside a
specifically designed compost reactor, as well as the results obtained from a
vast number of measurements. Four of the reactors were used in two different
batches. Measurements were taken from all four reactors. The physical and
chemical properties of the product were scrutinized during the composting
process and after its removal from the reactor. Detailed analysis has been
made on the effect of the C/N ratio and the minerals or sawdust used,
identified as major components of the process.
Environmental law for both the European Union and Greece regarding the
biodegradable organic waste is being discussed in the first chapter. A
comparison is being made for the standards set by many countries worldwide
regarding compost specifications.
The third chapter focuses on the history of the composting process and the
factors that delineate and regulate it. The chapter also focuses on the
microbiology of the process and the physical and chemical influence of
mature compost when laid on existing soil. Study is also made on the heavy
metal elements, the trace elements and the persistent organic pollutants.
Finally there is also a discussion on the benefits of composting and the means
of distribution of the mature compost.
The fourth chapter emphasizes two distinct composting procedures. The first
is the large-scale composting systems (compost factories). Each stage of the
procedure is analyzed and examples of factories practicing this procedure in
Greece are provided. The second one is the small-scale composting systems
(small compost reactors for household use). Different types of compost
reactors are being presented along with specific models drawn from the
market.
xi
In the fifth chapter, all of the methods of analysis used in the lab are cited and
thoroughly explained. The function of the instruments used for the different
types of analysis is explained along with the mathematical equations that yield
the resulting data.
The data which is derived from the methods, described in chapter five, is used
in the sixth and seventh chapters. In the sixth chapter, a comparison of data
based on the C/N ratio in the four reactors of the first and second batch is
provided in table and chart form. In the seventh chapter tables and charts are
presented that compare, based on the mineral or sawdust content, data from
the same reactor through both batches of compost.
In the final chapter of the thesis an evaluation of the compost product takes
place, along with a presentation of major factors that play an important role for
determining the maturity of the final product.
xii
1
1.1
.
,
.
1974.
1975
. 1981
(,
)
(1 1987)
. 4
,
. 1991
:
.
.
.
.
.
.
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PCBs.
5 "
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1992-2000
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2010.
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400
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300
250
200
150
100
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2004
2006
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1.2
2001/688/ 3
2006
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() . 1980/2000,
,
, 2001/688/
. :
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,
( 1.1),
.
1.1
( )
300
100
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1
100
1
100
2
1,5
10
200
(*)
.
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2.
( 2 mm) ,
0,5 %,
.
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20 % ( N
80 %).
4.
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20 % (
).
.
5.
:
:
Helminth Ova:
E. Coli: <
6. /
2
. [1]
1999/31/ 26 1999
,
,
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1.
2.
3. .
.
2010
25%
1995. 2013
50%. 2020
35%. [2]
96/61/ (IPPC) 24
1996
.
, ,
,
10
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:
1. ,
.
2. .
3. ,
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11
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.
4. .
5. .
6. .
7.
.
8. (
, 1996) [3]
() .2092/91
() .2092/91
( 1.2).[4]
1.2 (mg/kg)
0.7
70
70
25
45
0.4
200
12
75/442/,
. 1977
1991 ( 91/156/)
1989,
, .
:
1. .
2. ,
,
94/3/
.
3.
.
4.
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6.
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13
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9 14 (
, 1975).[5]
2006/12/
5 2006
1. :
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, :
i.
ii.
,
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,
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i.
,
ii.
2. 98/34/EK
, 22
1998,
,
14
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.
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B)
.
4.
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.[6]
15
2008/98/
19 2008
2008/98/EK 2006/12/ (
(75/439/, 91/689/)
- 2010.
, , ,
,
.
:
1. .
2. .
3. .
4. .
,
(IPPC
Directive).
,
.
(70%
2020),
(50% 2020)
, , 2015.
,
16
( , 2008).[7]
1.3
.
1. 50910/2727/2003 ( 1909 B)
.
.
113944/97
: 69728/824/96,
14312/1302/00.
29407/3508/2002.
2. 114218/97 ( 1016/):
.
3. 80568/91 ( 641/): ,
.
4. 49541/1424/86 ( 444/):
, 75/442/
15 1975.
1.3.1
50910/2727/2003
.
.
i.
: 91/156/
ii.
: , ,
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.
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17
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).
().
.
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18
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114218/1016/97
.
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: 91/156/.
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.
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(, , ,
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).
.
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).
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19
()
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(,
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, ...).
.
.
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, ( 1.3 1.4).
20
1.3
IV
pH
6-8
1.4
20 (kg//).
1.3.3
80568/4225/91 ,
.
80568/4225/91
86/278/C, .
:
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21
80568/4225/91, ,
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:
i.
( 3 ).
ii.
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iii.
(
).
, ,
,
1.5-1.7. [8], [9],
[10]
1.5
22
()
(VI)
1.7
1.4
.
.
, ,
/
.
23
1.4.1
,
.
:
1.8
Number of Classes
Description of Classes
Class A+ (top quality, limit values taken
from Council Regulation (EEC) No.2092/91
on organic farming)
Austria
Three
One (Ministry of
Belgium
Agriculture)
Flanders
Three (VLACO,
voluntary)
separated biowaste)
Humotex (compost from aerobically
composted digestion residuals)
Green waste (compost from sourceseparated garden waste).
Source separated biowaste and green waste.
Brussels
One
Denmark
One
24
Finland
One
Product standard.
France
One (N FU 44 051)
Two (Compost Urbain)
standards
for
physical
Germany
Two
Greece
One
green
soil
improver
Italy
from
vegetable
mixed
waste),
soil
and
composted
improver
improver
Luxembourg
Two
Netherlands
Two
Portugal
Spain
Sweden
(no law)
One in Spain
Two in Catalunya
One
Product standard.
One
Product standard.
UK
Composting
Association
Four different products defined through the
Australia
Four classes
composted
product
and
25
pasteurised
product,
each
of
which
One
Product standard.
The AAFC recognises only one class of
compost, reflective of product safety criteria.
It is based on the limits of CCMEs Category
Canada
Ministers of the
B)
elements
are
achievable
using
source-
established
for
its
use
are
26
to
obtain
good
compost.
Bureau de normalisation
A, B)
and
foreign
matter
content
are
the
Trace
element
content
is
the
One
,
, ,
,
.
, ,
(Potential toxic elements, PTEs) ( 1.9-1.10).
(Organic Pollutants, OPs) (PCBs,
PAHs, NPE, phthalates ..)
( 1.10). [11]
27
1.9 (mg/kg
) [10]
Country
Regulation
Class A+
Austria
Class A
Class B
Belgium
Royal Decree,
07.01.1998
Statutory Order
Nr.49
Denmark
Compost after
01.06.2000
Decisions of the
Finland
Ministry of
Agriculture and
Forestry (46/94)
France
NF COMPOST
URBAN
RAL
Germany
Class I
Class II
Greece
Licensing of
treatment plants
as agreed with
EPA
Ireland
Class I
Class II
Technical
Italy
regulation, DCI
27/07/84
(MSWC)
28
Draft Decree on
the use of
st
MBTC 1
quality (land
reclamation)
Law on
fertilizers (L
748/84; and
03/84)
BWC/GC/SSC
Lux
Licensing for
plants
BOOM compost
Holland
BOOM very
clean compost
Degree on
Portugal
sludge (limit
value utilized
also for MSW)
B.O.E.nm.
131.2 June
1998
Spanish draft on
composting
Class AA
(Stabilised
Spain
Biowaste) Class
A
Catalonia draft
on composting
Class A
(Stabilised
Biowaste) Class
B
Sweden
Guideline
values of QAS
29
Verordnung
ber
umweltgefhrde
Swi/land
nde Stoffe
Nr.814.013, 9
Juni 1986,
rev.28.12.01
UKROFS
fertil.org.farming
UK
Composted
Household
waste
Soilimprovers
and growing
media
EU ECO
Label
EC Reg.
2092/91
Canada
EPA
USA
CFR40/503
Sludge Rule
New
Zealand
Australia
* BNQ
**
30
1.10 (PTEs)
Limit values for Compost from source separation (BWC & GC)
min
max
limit values for MSW and MBT Composts
min
max
(*)
1.4.2
.
. ,
.
:
1.
( )
2.
3.
.
,
,
1.11
31
.
1.11 [10]
PCB
Austria
Denmark
Luxembourg
Mixed MSW
Biowaste
compost only
compost
matured compost
PCCD/F
Dioxins
PAH
AOX
Hydrocarbons
LAS
NPE
DEHP
1
hydrocarbons;
NPE:
1.4.3
, [10]
32
1.12 [10]
60
55
14
60
55
14
60 (in-vessel
65 (not in-vessel)
55
55
55-77,
60 (
3 in-vessel
(CCME)
55
15 for windrow
3 for aerated static pile
55
5 in vessel
15 for windrow
55
55 C 3
55
55 windrow composting
14 (5)
65 windrow composting
60 in-vessel composting
1 (2 )
33
34
2.1.
(composting)
(, , ).
,
.
.
.
.
,
. [14]
2.2.
Mayas, ,
, .
.
50
/ .
.
humus.
. humus
.
35
. ,
. . , ,
.
(Windrow)
.
.
1843. George Bommer
().
Bommer Method of Making Manure,
,
, .
1888 Bulletin N 61,
.
. XI. Compost-Formulas,
Analyses and Value.
1925,
Sir Albert Howard. Sir Albert Howard
. Indore
Process .
.
Bangalore Process
36
.
.
1922
. Baccari,
.
1932
N.V. Vuilafvoer Moatschapij (VAM).
Van Maanen
Indore.
VAM
.
1933 ,
DANO. DANO ,
.
DANO .
,
30m 4,5m.
150 /
. DANO .
. DANO
3,5 50 ()
1200
.
.
1970 2.1 .
37
2.1 1970
Bangalore
(Indore)
Caspari
, .
DANO
.
Earp Thomas
Fairfield Hardy
, ,
.
,
Metro Waste
1960
Gottas Goulke Composting.
. Florida
Tennessee.
,
.
1975
.
1976 Rutgers University New Jersey
Rutgers
Strategy
Rutgers
Methods.
.
65 oC,
38
. 1521 .
.
120 .
,
.
.
,
.
.
()
,
,
. [16]
2.3.
39
I.
.
II.
, ,
.
.
III.
,
.
.
.
IV.
.
(, )
.
(
, ).
2.1 pH
40
, . ,
,
.
.
.
, .
2.2
.
41
2.2 [19]
2.4.
,
(compost).
:
1.
2.
3.
4.
5.
6.
42
2.3
2.4.1
.
(.. , )
(.. , ).
.
.
3 1
.
.
.
, ( ),
.
43
. ,
.
.
.
.
.
.
,
,
.
2.4.2
:
.
.
.
,
.
44
. ,
.
.
,
,
.
.
( ), ()
, (.. ,
)
.
. ,
.
.
,
. ,
,
45
(.. ). ,
.
.
- .
. ,
( ), ,
,
( 2-3 ).
2.4.3
,
.
.
.
Thermus.
,
.
46
.
,
,
.
2.4.4
.
.
,
, .
2.4.5
1/3
47
. , ( )
(..
).
10)
(
, pH ).
,
( 35), (
),
25. ,
.
.
2.2 -
48
2.3
C/N
(, )
(, ) 8
4
()
-
()
2.4.6
, ,
. pH 5,5 -
8,5. pH,
.
,
,
, .
49
2.5.
.
.
,
.
:
1. (pen systems).
2.
(Reactor
or
enclosed
systems
or
container
2.5.1
I.
,
, .
.
, .
,
.
II.
, .
50
.
, .
,
.
:
.
.
.
.
.
- 5 ,
,
.
30 .
, 65C
10 .
51
.
: (straddle
turners) (Side-cutting windrow turners).
(straddle turners)
. ,
.
.
.
, .
III.
,
.
.
. Rudgers
Beltsville. O
, ,
. 2.1 2.2.
50
[17].
52
,
.
.
:
.
53
. .
.
PVC
. O
.
O
.
: ()
() .
.
54
.
.
15%.
.
.
.
,
. [17]
.
(..
)
.
.
..
.
.
55
2.5.2
,
, ,
,
,
.
(, ).
.
.
,
.
. ,
.
,
.
. ,
.
56
2.6 [17]
, . ,
,
.
,
, .. bulldozer
. ,
.
,
<5,
.
.
.
,
,
, .
.
57
.
2.7.
2.7 : ()
, () () [17]
2.8 [17]
58
2.6.
.
20%-30%
.
,
( )
. ,
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,
, ,
.
:
.
,
.
,
.
, .
.
.
...
59
,
.
.
,
,
.
.
, . ,
,
.
,
,
.
,
.
,
.[21]
,
60
(, , , , ).
.
.
.
:
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.
, .
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.
,
.
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:
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,
61
.
.[22]
2.7.
:
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)
,
.
, .
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..)
(
)
62
.
.
[24]
2.8.
,
.
,
.
,
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), , ,
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,
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.
.
:
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63
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, 4-10 2-4
.
, 2-6 , 2-4
.
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.
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.
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64
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.
,
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,
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. [25]
65
66
3
3.1
.
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.
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.
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.
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67
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.
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68
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,
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.
69
3.2
3.4.2
,
.
.
.
3.3
70
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(
).
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3.4.4
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71
3.4.5
, .
.
3.6
3.4.6
.
.
3.7
72
3.4.7
.
.
, .
3.4.8
3.9
73
3.4.9
.
.
.
.
3.10
3.4.10
.
.
.
3.11
74
3.4.11
(Teleprobes)
. .
.
3.12
3.4.12
3.13
.
, ,
. ,
24
.
75
3.13
3.4.13
.
.
3.14
3.4.14
, .
.
76
3.15
3.4.15
3.16
3.4.16
.
. ,
.
77
3.17
3.5
.
1996
900 . . , , ,
,
.
,
Compost Hellas A..
3.5.1.
() .
, 300tn/d 130tn/d /.
. 350tn/d
compost, 360tn/d RDF, 30tn/d , 5tn/d .
78
3.5.2.
3.18
.
:
,
40
.
,
.
.
.
.
79
. :
,
.
6 3
3.
, .
compost
.
compost ( , , ,
),
.
compost
flip- flop 10mm.
( ) ,
, compost.
compost , (
).
compost,
.
80
compost
.
,
.
,
compost,
.
4 ,
.
15% compost ,
.
, 4
, .
.
3.5.3.
Compost Hellas ..
1999.
.
POSIDONIA CMPOST HELLAS
, ,
. .
:
81
3.1 POSIDONIA
(+ CLASS COMPOST)
.
3.2
POSIDONIA
3.6
,
,
.
(
) 20-35 /
. ,
10-15 /
82
100 120 /
.
,
.
.
,
,
35-60 / 20.000 ,
.
150 / .
:
600 / (
20.000 /) 180 / ( 120.000
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120 / (
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,
:
: 150 300 /
25 40 /.
83
: 250 /
50 70/
,
(, , ...). gate fee
( )
.
84
3.7
,
, ,
.
,
.
.
.
,
.
3.8
, .
1. Dalek Composter
2. Compost Tumbler
3. Rolling or Rotating Orb
4. Wooden/Wire Mesh Composter
5. Computerized Indoor Composter
6. Worm Bin Composter
3.8.1
Dalek
Dalek ( 3.19).
,
. ,
.
85
3.19 Dalek
.
.
.
.
,
.
3.20 Horto
3.21
Horto
86
3.2 Horto.
400
.
Horto
HDPE.
6 10
.
Horto.
, . ,
,
.
3.3 Horto
11
400
10 kg
() HDPE
87
3.1
88
,
,
890
55
()
89
3.8.2
CompostTumbler
( )
Mantis ( 3.5)
,
.
3.23 Mantis
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,
.
.
.
.
. ,
, ,
.
,
. ,
,
90
, .
, ,
.
.
.
3.5 Mantis
900
65
91
,
3.6 (Acrobat Compost Tumbler).
.
,
. ,
( ).
,
,
.
. ,
,
280 .
.
,
.
.
92
290
11
()
93
3.25
( 3.7)
.
.
.
,
, .
,
, .
,
,
.
,
.
.
.
.
94
.
3.7
180
12
95
3.8.3
Rolling
or
3.26
,
,
.
,
. ,
.
,
.
.
,
.
96
.
3.8
490
10
()
97
3.9.
3.27 EcoTumbler
3.28
EcoTumbler.
5 ,
.
To
. ,
( 3.10)
4-6 .
,
.
.
,
.
,
.
270 81 .
,
,
.
98
EcoTumbler.
3.9 EcoTumbler
4-6
270
9,5
()
99
3.8.4
( 3.11) .
.
.
.
3.29
,
.
. ( 3.3 3.4)
,
( ),
( 3.4).
. , ,
.
3.3
3.4
100
3.8.5
,
.
,
.
3.5
NatureMill.
101
,
,
, ,
.
,
.
NatureMill.
3.10 NatureMill
55
8
()
102
3.8.6
Worm bins
3.6
,
.
,
. ,
,
. ,
.
,
. ,
103
.
, .
,
. ,
(pH, )
. ,
.
.
.
104
4
4.1
,
,
.
,
,
,
.
, , , ,
, , , .
,
.[23]
4.2
()
.
,
.
..
.
,
. MDF, ..
.
105
4.1
4.3
1756,
Cronstedt,
.
: , , ,
, , .
,
,
, , ,
( ) . ,
,
.
4.2
106
4.3.1
, :
, .
.
- -
.
.
.
, ,
.
,
.
,
-, .
o .
.
.
(, ,
, ), .. v
ov .
.
.[24]
107
4.3.2
.
1890 Pirson,
,
.
:
.
Si Al,
.
. [24]
4.1
108
:
.
.
.
,
.
.
.
,
.
,
.
. , ,
,
,
. [25]
109
4.4
To Vermiculair
Webb
.
:
.
.
.
.
, , .
.
.
4.4.1
4,98 .
,
.
Si4+ Al3+.
110
.
.
4.2
4.3
4.4.2
. Pb,
Zn, Cd.
111
.
, , .
(cracking) ,
. [26]
,
pH
.
4.5
,
.
,
,
.
, .
,
().
.
,
112
.
.
:
4.1
.
.
.
.
. 2003
2004 ,
( )
, (
113
( ,
, .
4.4
4.5.1
.
:
.
,
. ,
.
,
.
114
,
,
. .
.
.
4.5.2
.
: ,
,
.
:
4.5.2.1
,
(, ),
(, , ),
().
,
. ,
,
, , ,
. ,
115
.
, ,
. ,
, ,
( , ...). ,
(
) ,
.
.
()
, , ,
.
.
"Portland",
.
, ,
,
.
,
, .
.
116
4.5.2.2
.
:
, . ,
(
100% ).
.
pH ,
. ,
(container growing).
, ,
. ""
.
, ,
.
4.5.2.3
.
:
-
,
, , .
117
.
, , , , ,
.
: ..
(
(
, ).
,
,
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. S&
,
" " .
HF
F .
, ,
118
.
-
( ).
, ,
, , , , ...
,
. ,
.
.
,
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,
...
,
.
119
120
5
5.1
.
,
..., ,
.
5.2
4.1
( 4.1)
60 .
1.
2.
3.
4.
4.2
121
5 ( 4.2):
1) .
2) .
3) (2 ).
4) .
4 , 2
2
.
,
. ,
.
75
(, ,
)
.
.
.
:
122
,
, , ,
, , , ..
,
( )
,
, .
:
, ,
(,
..)
( , , ..)
( , , ..)
( , ..)
( ..)
( ..)
(1-2 cm).
,
.
123
5.3
(VSS)
(TOC)
Kheldahl (TKN)
A
(K, Na, Ca, Mg)
3 60
.
5.3.1
,
.
4.1
124
5.3.2
.
105C 12h.
105C.
(%)
.
:
(g).
: (g).
:
105C (g).
4.2 ( )
5.3.3
4.3
125
5.3.4
(VSS)
105
1
550
20 .
550 .
:
:
:
:
550C
4.4 ( )
126
5.3.6
(TOC)
100
grinder
.
(Solid Sample Module SSM 5000A)
900C.
TOCV CSH.
. %
:
:
:
:
:
:
.
.
4.5
4.6
TOCVCSH
4.8
127
5.3.7
Kjeldahl ()
).
,
,
, .
).
KJELDATHERM Gerhardt .
4.9
4.10 KJELDATHERM
, ,
. ,
, .
, ,
Vapodest 30s Gerhardt.
128
250
. 3-5
.
, magenta .
.
4.12 4.13
129
,
.
Kjeldahl
:
:
:
. [27], [28]
130
5.3.8
Kjeldahl ()
,
, Kjeldahl
,
Devarda. Devarda
:
, (
),
Devarda. Devarda, ,
KJELDATHERM.
, ,
. ,
, .
, ,
Vapodest 30s.
250
50
.
131
3-5
.
, magenta
. .
,
.
:
:
.
132
:
5.3.9
:
2-4
2 .
. .
.
133
, ,
Vapodest 30s.
250
. ,
2-4
.
, magenta .
.
:
:
:
134
5.3.10
5.3.11
( 105C 12h) compost Digesdahl
Digestion
compost
,
.
.
. .
. ,
135
:
, .
cooling pad.
ml
.
(Varian).
5.15 (Varian)
5.3.12
:
.
.
(Whatman #1).
.
( ).
.
136
:
compost .
Whatman
.
.
extract .
.
.
(..)
:
:
: [ / ]
: [ / ] * 100
:
[30], [31], [32]
137
138
6
6.1
.
.
4 .
, .
-
.
.
, (
4 ).
:
1.
2.
3.
4.
5.
6.
7. (VSS)
8.
9. Kjeldahl
10.
11.
12.
139
6.2
.
.
(, , ),
( ) ()
.
2 4
.
.
,
, ,
. 6.1
,
, , %
, % , %
Kjeldahl
, .
6.1
TKN
140
6.3
29/12/2009
18/01/2010. .
6.3.1
6.2
. .
C/N
30.
:
(, ,
)
( )
()
.
.
,
141
6.2
142
6.3.2
.
. .
.
.
6.3
1
2
3
5
6
7
8
9
11
15
18
21
,
(.. ), ,
.
6.4 6.1
143
6.4 %
1
% 4
100
90
80
%
70
60
73,21
67,99
56,31
50
59,32
40
30
20
10
0
6.1 % 4
144
6.3.3
, , ,
. ,
3 . .
, ,
.
.
.
. , , ,
.
.
,
.[33]
145
6.5
6.2
.
146
4
70
60
(0C)
50
40
30
(T>50 0C) - (4
)
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.2 4
147
6.2 .
3 7
.
.
,
3 7 .
.
,
3 8 .
. ,
.
3 7 .
.
6.2
.
, -
148
6.3.4
, ,
.
, ,
.
. ,
.
6.6 (%)
6.3
149
% 4
100
90
80
70
60
50
40
30
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.3 % 4
150
, 6.3,
,
.
,
.
.
, .
.
.
151
6.3.5
.
.
[35], [38].
pH
.
6.7 pH
6.4 pH
.
152
pH 4
10
9
8
pH
6
5
4
3
2
1
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.4 pH 4
153
9
21
9
21
, 5
,
.
21 .
9
21
6.4
. (
)
pH
154
6.3.6
,
.
.
, ,
. ,
,
.
6.8
155
4
6
(mS/cm)
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.5 4
156
6.5
.
.
, ,
, 21 ,
J.C.
Hargreaves, M.S. Adl, P.R. Warman.[36]
6.5
.
(
6.3.7
).
(VSS)
.
.
.
157
.
6.9 %
6.6 %
.
158
% (VSS) 4
100
90
80
70
% VSS
60
50
40
30
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.6 4
159
3 10 ,
( ),
.
,
.
,
.
.
.
6.3.8
.
.
160
6.10
6.7
.
161
% (Corg) 4
60
50
% Corg
40
30
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.7 %
162
,
21
.
. 21
21 .
21 .
,
21
.
o
.
.
.
,
.
. ,
163
.
.
Kjeldahl
6.3.9
, ,
.
.
6.11 %
6.8 %
Kjeldahl
164
% Kjeldahl (TKN) 4
3,0
2,5
% TKN
2,0
1,5
1,0
0,5
0,0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.8 % kjeldahl 4
165
.
21
.
21
21 .
21
.
6.3.10
.
,
.
.
. [36], [37].
35
,
.
166
. [38]
, .
30.
.
6.12
6.9
167
C/N 4
40
35
C/N
30
25
20
15
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
6.9 C/N 4
168
21 . 3
5 .
. ,
.[35], [38]
6.3.11
,
(
.
.
169
6.13
.
6.13
170
mg/kg (NO3-N) 4
2000,0
1800,0
1600,0
mg/kg NO3-N
1400,0
1200,0
1000,0
800,0
600,0
400,0
200,0
0,0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.10
171
.
,
. , ,
.
6.3.12
.
.
.
,
.
.
6.14
.
6.14
172
mg/kg (N4-N) 4
4000
3500
mg/kg N4-N
3000
2500
2000
1500
1000
500
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.11
173
. , ,
,
.
. ,
,
.
.
174
6.4
13/04/2010
03/05/2010.
.
6.4.1
6.15
. .
40.
:
(, ,
)
( )
()
.
.
,
.
.
.
175
6.15
176
6.4.2
,
,
.
.
.
.
.
.
. ,
.
6.16
,
(.. ), ,
.
6.17 6.12
177
6.17 %
1
% 4
100
90
80
70
75,79
72,45
60
62,86
57,36
50
40
30
20
10
0
6.12 % 4
178
6.4.3
.
6.18
6.13
.
179
4
70
60
(0C)
50
40
30
(T>50 0C) - (5 )
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.13 4
180
6.13 .
5
10 .
.
,
3 8.
. ,
.
,
3 7.
. ,
.
3 7 .
.
6.13
.
, -
181
6.4.4
.
6.19 (%)
6.14 %
.
182
% 4
100
90
80
70
60
50
40
30
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.14 % 4
183
.
,
.
.
.
.
.
184
6.4.5
pH
.
6.20
6.15
185
pH 4
10
9
8
7
pH
6
5
4
3
2
1
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.15
186
8.
7
21
4 .
7
21
, 4
8
21 .
7
21
6.15
,
.
( )
pH
.
187
.
6.4.6
.
6.21
188
4
6
(mS/cm)
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.16 4
189
6.16
.
.
, ,
, 21 ,
J.C.
Hargreaves, M.S. Adl, P.R. Warman.[36]
6.16
.
190
6.4.7
.
6.22 %
6.17 %
.
191
% (VSS) 4
100
90
80
70
% VSS
60
50
40
30
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.17 4
192
4 11
,
( ) ,
,
.
,
.
,
.
. ,
.
.
193
6.4.8
6.23
6.18
194
% (Corg) 4
60
50
% Corg
40
30
20
10
0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.18 %
195
,
21
.
. 21
21 .
20
.
,
21
.
o
.
.
.
,
.
. ,
196
.
.
6.4.9
Kjeldahl
.
6.24 %
6.19 %
Kjeldahl .
197
% Kjeldahl (TKN) 4
3,0
2,5
% TKN
2,0
1,5
1,0
0,5
0,0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.19 % kjeldahl 4
198
21
21
21
21 .
.
6.4.10
.
6.25
6.20
.
199
C/N 4
40
35
30
C/N
25
20
15
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
6.20 C/N 4
200
21 . 7
5 (
).
. ,
, ,
.[35], [38]
201
6.4.11
6.26
.
6.26
202
mg/kg (NO3-N) 4
1400,0
1200,0
mg/kg NO3-N
1000,0
800,0
600,0
400,0
200,0
0,0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.21
203
.
,
. , ,
,
.
6.4.12
6.14
.
6.27
204
mg/kg (N4-N) 4
2500,0
mg/kg N4-N
2000,0
1500,0
1000,0
500,0
0,0
0
10
11
12
13
14
15
16
17
18
19
20
21
22
()
6.22
205
. , ,
,
.
. ,
,
.
.
206
7
7.1
,
.
7.2
( )
.
7.2.1
.
7.1
207
70
60
(0C)
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.1
208
7.1 .
.
.
,
.
7.2.2
.
7.2
209
70
60
(0C)
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.2 .
210
7.2 .
.
.
.
.
,
.
7.2.3
.
7.3
211
70
60
(0C)
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.3 .
212
,
,
.
7.2.4
.
7.4
213
70
60
(0C)
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.4 .
214
7.4 .
.
.
, .
7.3
%
( )
.
7.3.1
%
.
7.5 (%)
215
%
100
90
80
70
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.5
216
7.5
,
.
.
,
.
.
7.3.2
%
.
7.6 (%)
217
%
100
90
80
70
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.6
218
7.6
.
.
7.3.3
.
7.7 (%)
219
%
100
90
80
70
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.7
220
7.7
7.3.4
%
.
7.8 (%)
221
%
100
90
80
70
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.8
222
,
7.8, . ,
, 21
.
, ,
.
. ,
.
7.4
( )
.
7.4.1
7.9
223
pH
10
9
8
7
pH
6
5
4
3
2
1
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.9
224
7.9
.
.
,
.
.
7.4.2
.
7.10
225
pH
9
8
7
6
pH
5
4
3
2
1
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.10
226
7.10
. ,
, .
.
.
7.4.3
.
7.11
227
pH
10
9
8
7
pH
6
5
4
3
2
1
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.11
228
7.11
. ,
.
. pH
.
7.4.4
.
7.12
229
pH
10
9
8
7
pH
6
5
4
3
2
1
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.12
230
7.12
,
,
.
pH
.
, .
.
, ,
,
.
.
231
7.5
(
) .
7.5.1
.
7.13
232
(mS/cm)
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.13
233
7.13 ,
,
.
7.5.2
.
7.14
234
(mS/cm)
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.14
235
7.14 .
,
,
.
7.5.3
.
7.14
236
(mS/cm)
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.14
237
.
.
7.14.
7.5.4
.
7.14
238
(mS/cm)
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.14
239
.
.
.
3:1:1, ,
.
7.6
(VSS)
%
(
) .
7.6.1
%
.
7.15 % (VSS)
240
% (VSS)
100
90
80
70
% VSS
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.15 % (VSS)
241
7.15
.
7,46% .
,
.
,
.
7.6.2
.
7.16 % (VSS)
242
% (VSS)
100
90
80
70
% VSS
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.16 % (VSS)
243
7.16
. 7
.
.
.
7.6.3
%
.
7.17 % (VSS)
244
% (VSS)
100
90
80
70
% VSS
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.17 % (VSS)
245
7.17
. 7
.
.
.
7.6.4
.
7.18 % (VSS)
246
% (VSS)
100
90
80
70
% VSS
60
50
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.18 % (VSS)
247
7.18
.
.
.
.
,
.
248
7.7
%
( ) .
7.7.1
%
.
7.19 %
249
% (Corg)
60
50
% Corg
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.19 %
250
7.19
.
.
.
.
.
.
7.7.2
%
.
7.20 %
251
% (Corg)
60
50
% Corg
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.20 %
252
7.20 ,
7 , .
.
.
7.7.3
%
.
7.21 %
253
% (Corg)
60
50
% Corg
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.21 %
254
7.21 ,
7 , .
. 7
.
.
7.7.4
%
.
7.22 %
255
% (Corg)
60
50
% Corg
40
30
20
10
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.22 %
256
7.22 ,
7 , .
7.8
Kjeldahl
%
Kjeldahl
( ) .
7.8.1
%
Kjeldahl
.
7.23 % Kjeldahl
257
% Kjeldahl (TKN)
2,5
2,0
% TKN
1,5
1,0
0,5
0,0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.23 % Kjeldahl
258
7.23
.
30,
40. , ,
,
, ,
,
,
. ,
,
.
7.8.2
%
Kjeldahl
.
7.24 % Kjeldahl
259
% Kjeldahl (TKN)
3,0
2,5
% TKN
2,0
1,5
1,0
0,5
0,0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.24 % Kjeldahl
260
7.24
.
30,
40. , ,
.
.
.
.
7.8.3
%
Kjeldahl
.
7.25 % Kjeldahl
261
% Kjeldahl (TKN)
3,0
2,5
% TKN
2,0
1,5
1,0
0,5
0,0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.25 % Kjeldahl
262
7.25
.
30,
40.
,
.
,
.
.
7.8.4
%
Kjeldahl
.
7.26 % Kjeldahl
263
% Kjeldahl (TKN)
3,0
2,5
% TKN
2,0
1,5
1,0
0,5
0,0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.26 % Kjeldahl
264
7.25
.
.
.
30, 40.
,
.
.
7.9
( )
.
7.9.1
.
7.27
265
C/N
40
35
C/N
30
25
20
15
10
5
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.27
266
7.27
30 .
40
.
,
.
, ,
20.
7.9.2
.
7.28
267
C/N
40
35
C/N
30
25
20
15
10
5
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.28
268
7.28
. ,
,
.
10.
.
7.9.3
.
7.29
269
C/N
40
35
C/N
30
25
20
15
10
5
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.29
270
7.28
. ,
, .
10.
.
7.9.4
.
7.30
271
C/N
40
35
C/N
30
25
20
15
10
5
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.30
272
7.28
. ,
,
.
.
7.10
( ) .
7.10.1
.
7.31
273
NO3-N
2000
1800
1600
NO3-N (mg/kg)
1400
1200
1000
800
600
400
200
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.31
274
7.31
.
.
.
, ,
, .
,
.
7.10.2
.
7.32
275
NO3-N
600
500
NO3-N (mg/kg)
400
300
200
100
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.32
276
7.32
. , ,
.
,
.
7.10.3
.
7.33
277
NO3-N
600
NO3-N (mg/kg)
500
400
300
200
100
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.33
278
7.33
. , ,
.
,
, ,
.
7.10.4
.
7.34
279
NO3-N
800
700
NO3-N (mg/kg)
600
500
400
300
200
100
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.34
280
7.34
.
,
.
,
.
7.11
( ) .
7.11.1
.
7.35
281
NH4-N
4000
3500
NH4-N (mg/kg)
3000
2500
2000
1500
1000
500
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.35
282
7.35
. , ,
,
.
.
.
7.11.2
.
7.36
283
NH4-N
600
500
NH4-N (mg/kg)
400
300
200
100
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.36
284
7.36 .
,
.
.
,
.
,
.
7.11.3
.
7.37
285
NH4-N
700
600
NH4-N (mg/kg)
500
400
300
200
100
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.37
286
, ,
( 7.37).
.
.
.
7.11.4
.
7.38
287
NH4-N
900
800
700
NH4-N (mg/kg)
600
500
400
300
200
100
0
1
10
11
12
13
14
15
16
17
18
19
20
21
()
1
7.38
288
7.38
.
.
,
.
. , ,
,
,
.
289
290
8
8.1
,
,
8.2
.
,
.
8.2.1
,
.
, ,
,
.
.
291
, ,
.
.
.
8.2.2
,
,
, ,
.
,
, ,
,
.
.
.
8.2.3
, ,
, ,
.
,
.
,
, ,
292
. ,
, ,
,
8.3
(
, ..), ,
, ,
, ..,
.
, ( 50 )
, ,
, .
.
25. ,
10 20.
.
.
,
293
,
,
.
.
.
60 , 7,8 8,5.
,
.
.
8.3.1
().
,
,
.
, .
).
.
294
. , ,
.
8.1
.
8.1 % [38],[39],[40]
8.2
.
8.1
8. 2 %
295
% 4
4,5
4
3,5
3
2,5
2
1,5
1
0,5
0
Na
Ca
Mg
8.1 %
296
.
( )
.
.
.
.
.
(
).
.
.
8.1 8.2
, ,
.
297
8.3
.
8.1.
8. 3 %
298
% 4
4,5
4
3,5
3
2,5
2
1,5
1
0,5
0
Na
Ca
Mg
8.2 %
299
.
( )
,
.
.
.
.
..).
.
8.2 8.3
, ,
.
300
8.3.2
.
,
.
,
, .
,
.
, , .
. [41]
.
, Tinella, , Parris Island Cos,
B. Rio Grande, , , , Mini
Safaa F1, , A/ Z B.
(..) .
:
( )
( )
( )
( )
301
20 4
450
400
350
300
250
200
150
100
50
0
Tinella
Parris
T
Island Cos
. Rio
Grande
Mini
Safaa F1
25
65
100
8.3
302
50 4
450
400
350
300
250
200
150
100
50
0
Tinella
Parris
T
Island Cos
. Rio
Grande
Mini
Safaa F1
25
65
100
8.4 50
303
20 4
450
400
350
300
250
200
150
100
50
0
Tinella
Parris
T
Island Cos
. Rio
Grande
Mini
Safaa F1
25
65
100
8.5
304
50 4
450
400
350
300
250
200
150
100
50
0
Tinella
Parris
T
Island Cos
. Rio
Grande
Mini
Safaa F1
25
65
100
8.6 50
305
, 8.3 8.6,
.
.
,
,
( parris island cos, ,
) .
50 ,
,
20
.
.
,
.
, Parris
Island Cos.
,
.
.[39]
8.3.3
50
50
.
306
8.4 50
50
8.5 50
50
307
8.4
,
,
. ,
,
.
:
,
.
,
.
50
( 50% 65% ..)
.
.
,
308
.
,
.
.
.
. , ,
,
,
.
,
.
,
.
, .
),
.
.
)
309
,
.
. 50
8 18,
.
( 10),
.
100%
80%
.
.
50
1, .
,
2.
,
,
Parris Island Cos.
, , ,
, .
310
6 ,
, 1
, 2 .
20 .
18
.
,
.
.
.
. ,
.
.
311
312
[1].
2001/688/ 3
2006.
[2].
1999/31/ 26 1999.
[3].
[4].
() .2092/91.
[5].
75/442/.
[6].
2006/12/
5 2006.
[7].
2008/98/
19 2008.
[8].
., . (2001),
.
[9].
[10].
http://www.et.gr
[11].
. , . , . , . , .
, " :
",
(..) " ",
...., . :
http://epem.gr/pdfs/2002_8.pdf
[12].
.,
,
, 14-14 . 2005.
: http://library.tee.gr/digital/m2093/m2093_kartsonas.pdf
[13].
313
www.wrap.org.uk/downloads/Review_of_Compost_Standards.d5ee11d
8.pdf
[14].
, ,
, , 2006.
[15].
. , . , . , . , . , .
, . , . ,
, 2007.
[16].
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,
, .
[17].
[18].
, , , 2006.
[19].
[20].
, ..
[21].
, , 2006.
[22].
, ,
, .
[23].
,
, , EM, 2006.
[24].
. , . , . , . , . , .
, . , . ,
, 2007.
314
[25].
COMWASTE, LIFE03
ENV/GR/205,
compost
, 2006.
[26].
[27].
[28].
[29].
[30].
[31].
[32].
[33].
[34].
[35].
. .
, ,
... 1990.
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