Professional Documents
Culture Documents
5 D
5 D
.
) ( )-(
- .
.
.
.
) (
. ) (
.
- .
:
154
] .[12
].[43
) (adhesive ) (cohesive ] .[5
) (ASTM C633
) ( )
( ] .[56
] .[5 , ) (
] .[6
,
] .[5
.
] .[7 ) (Knoop ].[8
.
,
) (Vickers Indentation ].[109
, ,
.
-
].[9
155
.
= )DOC (%
)(1
I HA XRD ,IHA HA XRD
. HA %100 .
.
, Uniteck 400A
.
SiC , .
, 5 .
200 m.
Marshall ] .[8
) (E :
)(2
b b
H
=
E
a a
156
b a b/a
)1/(7/11 0/45 H .
) (KC Evans
]:[7
1/ 2
P E
K C = 0.016 3 / 2
C H
)(3
P , C ) .(1
Lesage ] [9
) (KCa .
) :(1
) (d/2 )(a ) (P ) ln) P ln (d/2 )(ln P ln (a
) (PC, aC ) , , (.
) (KCa :
1/ 2
E
H
i
)(4
PC
a C3 / 2
K Ca = 0.015
(E / H )1i / 2 .
.
.
]:[10
( E / H ) 1S / 2
)(5
1 + (H S / H C )1 / 2
H ) 1C/ 2
(E /
1 + (H C / H S )1 / 2
= (E / H )1i / 2
, C i S .
110 GPa 310 kgf/mm2
].[12
157
2 .
.
.
] [13
.
.
.
.
.
3
. ) (
.
.
) ( ) ( ] [13
.
4 H/E . H/E
. H/E
.
5 .
, ,
,
.
6
.
/ .
158
, .
,6 C2 .
, .
.
7
. .
, . 8 KCa 7
5 . ,
.
.
,
. KCa
) (9
)
( . ,
. 9
.
,
.
. /
.
.
.
, .
159
.
.
[1] Mohammadi Z., Mesgar A. S.; Digest of the first Iranian seminar on plasma spray;
Jahad Daneshgahi (IUST) - Ministry of Industries, 7 July 1997.
[2] Mohammadi Z., Mesgar A. S., Ziaie-Moaied A. A.; Plasma spray and
hydroxyapatite; 9th Conference of Iranian Biomedical Engineering, IUST, 91-94,
2000.
[3] Sun L., Berndt C.C., Gross K.A. and Kucuk A.; Materials fundamental and clinical
performance of plasma-sprayed hydroxyapatite coatings; J Biomed Mater Res, 58:
570-592; 2001.
[4] Gross K. A., Walsh W., Swarts E.; Analysis of Retrieved Hydroxyapatite-Coated
Hip Prostheses; J Thermal Spray Technology; 13(2): 190-199, 2003.
[5] Tsui Y. C., Doyle C, Clyne T. W.; Plasma sprayed hydroxyapatite coatings on
titanium substrates Part1: Mechanical properties and residual stress levels;
Biomaterials, 19: 2015-2029; 1998.
[6] Yang Y. C., Chang E.; Influence of residual stress on bonding strength and fracture
of plasma-sprayed hydroxyapatite coatings on Ti-6Al-4V substrate; Biomaterials,
22: 1827-1836, 2001.
[7] Evans A.G., Charles E.A.; Fracture toughness determination by indentation; J. Am.
Ceram. Soc., 59:371-372; 1976.
[8] Marshall D.B., Noma T., Evans A.G.; A simple method for determining elasticmodulus-to-hardness ratios using Knoop indentation measurements; Comm. Am.
Ceram. Soc., 65: C-175- C-176, 1982.
[9] Lesage J., Chicot D.; Models for hardness and adhesion of coatings; Surf. Eng., 15:
447-453, 1999.
[10] Lesage J., Staia M.H., Chicot D., Godoy C., De Miranda P.E.V.; Effect of
thermal treatments on adhesive properties of a NiCr thermal sprayed coating; Thin
Solid Films, 377-378: 681-686, 2000.
[11] Mohammadi Z., Ziaie-Moaied A. A., Mesgar A. S.; Grit Blasting of Ti-6Al-4V
alloy: optimization and its effect on adhesion strength of plasma-sprayed
hydroxyapatite coatings Submitted to J. Materials Processing Technology.
[12] Breme H. J., Biehl V., Helsen J.A.; Metals and implants: Metals as
Biomaterials; Wiley, New York, NY, 1998.
160
A1
A2
A3
B1
B2
B3
C1
C2
C3
)(kW
28
28
28
32/2
32/2
32/2
36/4
36/4
36/4
)(cm
14
11
11
14
11
14
-1
:d :a :c
60
8 cm
11 cm
40
30
38.5
36.4
34.3
32.2
30.1
28
)DOC at interface (%
14 cm
50
20
25.9
-2
161
400
8 cm
11 cm
14 cm
200
Vickers Hardness
300
100
0
36.4
28
32.2
)Spray pow er (kW
-3
0.115
8 cm
11 cm
14 cm
0.11
H/ E
0.105
0.1
0.095
36.4 38.5
28
0.09
25.9
-4
28
27
25
8 cm
11 cm
14 cm
)E (GPa
26
24
28
23
25.9
-5
162
1.2
K C (MPa m1/2)
8 cm
11 cm
14 cm
1.1
0.9
0.8
28
32.2
36.4
-6
(a)
(b)
5
3
B2
32.2 kW, 110 mm
ln (d/2) (d in microns)
ln (a) (a in microns)
PC = 0.415 N
1
-1.1
-0.1
0.9
1.9
2.9
ln (d/2)
3
A1
28 kW, 80 mm
PC = 0.190 N
1
1
-2.1
1
-2.1
3.9
-1.1
-0.1
0.9
1.9
2.9
3.9
ln P (P in N)
ln P (P in N)
(c)
5
ln (d/2)
3
C3
36.4 kW, 140 mm
ln (a) (a in microns)
ln (a)
ln (d/2) (d in microns)
ln (d/2) (d in microns)
ln (d/2)
PC = 0.227 N
1
-2.1
1
-1.1
-0.1
0.9
1.9
2.9
3.9
ln P (P in N)
-7
C3 :c B2 :b A1 :a
ln (a) (a in microns)
ln (a)
ln (a)
163
1.4
8 cm
11 cm
14 cm
1.3
1.1
)K Ca (MPa m1/2
1.2
0.9
36.4
28
32.2
)Spray pow er (kW
-8
1.4
1.3
1.1
)K Ca (MPa m1/2
1.2
1
0.9
55
50
45
40
35
30
25
)DOC at interface (%
-9 -