B CNG THNG

TRNG I HC CNG NGHIP THC PHM KHOA CNG NGH THC PHM

Gii thiu my AAS v ng dng

Nhm: 7 Lp : 04CDNKN2 Mn : Phn tch nc GVHD : Mc Xun Ha

Danh sch nhm

Nguyn Th Ngc Nhung Trng Minh Nht L Th Hng Phng Phng Thin Tm Nguyn Th L Thu Thch Th Tuyt Phng 3305110468 3305110479 3305110516 3305110568 3305110653 3305110925

L ng

3305110943

1. Nguyn tc:
Xc nh mu da vo s hp th nh sng ca hp cht mu c trong dung dch.

2. Dng c, thit b v ha cht

2.1 Dng c, thit b:

My Spectrophotometer Pipet 10 ml, 1 ml ng ly tm My ly tm Bnh tam gic 100 ml Phu thy tinh Bnh nh mc 100 ml, 1000 ml

2.2 Ha cht
- Dung dch mu chun (A): cn 0.0875g K2Cr2O7, 2g CoSO4 trn vi 1 ml H2SO4 m c thm nc ct ha tan hon ton sau chuyn vo bnh nh mc 1 lt v nh mc ti vch. - Dung dch H2SO4 long (B): ha tan 1 ml H2SO4 m c thnh 1 lt.

3. Cch tin hnh

3.1 Lp ng chun

Pha long dung dch mu chun c thang mu chun t 0-250 n v mu Pt-Co, dung dch c pha ln lt theo bng sau:

Ln lt o hp th OD cc mu t 0-250 trn my quang ph hp thu bc sng 455nm Lp th biu din mi tng quan gia mu v hp thu OD

3.2 o hp thu o hp thu ca mu trn my quang ph hp thu bc sng 455nm. Ly tm mu cho n khi loi b hon ton cc ht huyn ph. o hp thu ca mu nc sau khi ly tm.

4. Tnh kt qu
T gi tr OD thu c ca mu, kt hp vi th xc nh mu ca mu. Nu tr s OD ca mu vt qu cc tr s ca dung dch chun th phi pha long mu n nng thch hp.

5. Lu
- c nh hng n vic xc nh mu. - Ngoi ra mu cn ty thuc v pH ca nc, do trong bng kt qu cn ghi r pH lc xc nh mu.