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  • Temperature vs Time DSC and TG Analysis Graphs

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    Narasimhan Suseendran
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    The document contains data from a differential scanning calorimetry (DSC) experiment measuring temperature, time, DSC signal in μV/mg, thermogravimetric (TG) weight change in %, sensitivity in μV/mW, and segment over a range of temperatures from 39.3 to 479.3°C. The data shows the change in DSC signal and TG weight as the temperature increases over time during the experiment.

    Original Description:

    Thermogravemetric Studies in HTPB. This is used in Digital Scanning Calorimetery

    Original Title

    TG and DSC.xlsx

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    © Attribution Non-Commercial (BY-NC)

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    The document contains data from a differential scanning calorimetry (DSC) experiment measuring temperature, time, DSC signal in μV/mg, thermogravimetric (TG) weight change in %, sensitivity in μV/mW, and segment over a range of temperatures from 39.3 to 479.3°C. The data shows the change in DSC signal and TG weight as the temperature increases over time during the experiment.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLSX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    5 views6 pages

    Temperature vs Time DSC and TG Analysis Graphs

    Uploaded by

    Narasimhan Suseendran
    The document contains data from a differential scanning calorimetry (DSC) experiment measuring temperature, time, DSC signal in μV/mg, thermogravimetric (TG) weight change in %, sensitivity in μV/mW, and segment over a range of temperatures from 39.3 to 479.3°C. The data shows the change in DSC signal and TG weight as the temperature increases over time during the experiment.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLSX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 6

    Temperature

    Time
    min

    39.3
    49.3
    59.3
    69.3
    79.3
    89.3
    99.3
    109.3
    119.3
    129.3
    139.3
    149.3
    159.3
    169.3
    179.3
    189.3
    199.3
    209.3
    219.3
    229.3
    239.3
    249.3
    259.3
    269.3
    279.3
    289.3
    299.3
    309.3
    319.3
    329.3
    339.3
    349.3
    359.3
    369.3
    379.3
    389.3
    399.3
    409.3
    419.3
    429.3
    439.3
    449.3
    459.3
    469.3
    479.3

    17.9
    21.2
    22.7
    24.0
    25.2
    26.4
    27.5
    28.6
    29.7
    30.8
    31.9
    32.9
    34.0
    35.0
    36.1
    37.1
    38.2
    39.2
    40.3
    41.3
    42.4
    43.4
    44.5
    45.6
    46.6
    47.7
    48.7
    49.8
    50.8
    51.8
    52.9
    53.9
    55.0
    56.0
    57.1
    58.2
    59.3
    60.5
    61.6
    62.7
    63.8
    64.9
    66.0
    67.1
    68.2

    DSC
    V/mg
    0.000084593
    -0.24611
    -0.31602
    -0.28372
    -0.29417
    -0.31114
    -0.32583
    -0.33741
    -0.3474
    -0.35504
    -0.36207
    -0.37056
    -0.37507
    -0.3763
    -0.37472
    -0.36914
    -0.36644
    -0.36299
    -0.3603
    -0.35866
    -0.35818
    -0.35664
    -0.35077
    -0.32994
    -0.25445
    -0.19708
    -0.092217
    0.034295
    0.13136
    0.29843
    0.50763
    0.73128
    0.92496
    0.97876
    0.8363
    0.58269
    0.34321
    0.1695
    0.051336
    -0.047762
    -0.14931
    -0.2575
    -0.77909
    -0.8073
    -0.74455

    TG
    %
    100.05
    100.07
    100.09
    100.10
    100.10
    100.10
    100.10
    100.10
    100.11
    100.11
    100.11
    100.11
    100.11
    100.10
    100.10
    100.10
    100.09
    100.08
    100.05
    100.02
    99.99
    99.94
    99.87
    99.78
    99.34
    98.70
    97.42
    95.56
    93.39
    91.15
    89.75
    88.74
    85.25
    85.34
    82.84
    81.07
    79.03
    76.62
    73.64
    69.44
    63.46
    54.14
    39.95
    26.50
    13.90

    Column1
    Temperature
    o

    Column2
    Time
    min

    39.3
    49.3
    59.3
    69.3
    79.3
    89.3
    99.3
    109.3
    119.3
    129.3
    139.3
    149.3
    159.3
    169.3
    179.3
    189.3
    199.3
    209.3
    219.3
    229.3
    239.3
    249.3
    259.3
    269.3
    279.3
    289.3
    299.3
    309.3
    319.3
    329.3
    339.3
    349.3
    359.3
    369.3
    379.3
    389.3
    399.3
    409.3
    419.3
    429.3
    439.3
    449.3
    459.3
    469.3
    479.3

    17.9
    21.2
    22.7
    24.0
    25.2
    26.4
    27.5
    28.6
    29.7
    30.8
    31.9
    32.9
    34.0
    35.0
    36.1
    37.1
    38.2
    39.2
    40.3
    41.3
    42.4
    43.4
    44.5
    45.6
    46.6
    47.7
    48.7
    49.8
    50.8
    51.8
    52.9
    53.9
    55.0
    56.0
    57.1
    58.2
    59.3
    60.5
    61.6
    62.7
    63.8
    64.9
    66.0
    67.1
    68.2

    Column3
    DSC
    V/mg
    0.000084593
    -0.24611
    -0.31602
    -0.28372
    -0.29417
    -0.31114
    -0.32583
    -0.33741
    -0.3474
    -0.35504
    -0.36207
    -0.37056
    -0.37507
    -0.3763
    -0.37472
    -0.36914
    -0.36644
    -0.36299
    -0.3603
    -0.35866
    -0.35818
    -0.35664
    -0.35077
    -0.32994
    -0.25445
    -0.19708
    -0.092217
    0.034295
    0.13136
    0.29843
    0.50763
    0.73128
    0.92496
    0.97876
    0.8363
    0.58269
    0.34321
    0.1695
    0.051336
    -0.047762
    -0.14931
    -0.2575
    -0.77909
    -0.8073
    -0.74455

    Column4
    TG
    %
    100.05
    100.07
    100.09
    100.10
    100.10
    100.10
    100.10
    100.10
    100.11
    100.11
    100.11
    100.11
    100.11
    100.10
    100.10
    100.10
    100.09
    100.08
    100.05
    100.02
    99.99
    99.94
    99.87
    99.78
    99.34
    98.70
    97.42
    95.56
    93.39
    91.15
    89.75
    88.74
    85.25
    85.34
    82.84
    81.07
    79.03
    76.62
    73.64
    69.44
    63.46
    54.14
    39.95
    26.50
    13.90

    Segment

    DSC Vs Temperat
    1.200
    1.000
    0.800

    V/mg

    0.600

    DSC

    0
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1

    0.400
    0.200
    0.000
    0

    50

    100

    150

    200

    250

    -0.200
    -0.400
    -0.600
    -0.800

    Temperatue
    -1.000

    110

    TG Vs Temperatu

    100
    90
    80
    70

    V/mW
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00

    60

    TG

    Sensitivity

    50
    40
    30
    20
    10

    Temperatue

    Temperatue

    0
    0

    Column5
    Sensitivity
    V/mW
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00
    1.00

    Column6
    Segment
    0
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1
    1

    50

    100

    150

    200

    250

    DSC Vs Temperature

    DSC Vs Temperature
    300

    Temperatue

    350

    400

    450

    500

    550

    oC

    TG Vs Temperature

    TG Vs Temperature

    Temperatue

    oC

    Temperatue

    oC

    300

    350

    400

    450

    500

    550

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