first

Retention time in destillation column

Minimum allowable flow reactant
Maximum unit operation

Volume and retention time reactor

ket
CAPACITY
1500 L
RT min
2 minutes
RT Max
10 minutes
ans
Qmax
750 L/min
Qmin
150 L/min
Volume for pre-reactor
ket
Volume pre reactor
ans
RT min

750 L
5 minutes

range of pump rates

molar volume 30 C Jatropha
981.94 Ml/Mol
Volume Ratio
3:01
ans
Volume ratio
0.125
Pumping rate min
133.3333333 L/minutes methanol
Pumping rate max
666.6666667 L/minutes methanol
Pipe
10 mm
0.79 mm2
size of container
methanol n NaOH
Oil
mass NaOH

3 hour withut refill

120000 L
7992 L
7.9776 kg/min

8 mL/minutes oil
44.4 mL/minutes oil

1,5% dari masa oil

Q max

total

BIODESEL CALCULATION
hour

Reactor Volume
1000
1100
1200
1300
1400
1500
1600

Flow (L/min)
2
500
550
600
650
700
750
800

10
100
110
120
130
140
150
160

retention time (minute)

Volume for pre-reactor
Qmin (150 L/min)
Qmax (750 L/min)
500
3.333333333 0.666667
600
4
0.8
700
4.666666667 0.933333
750
5
1
800
5.333333333 1.066667
900
6
1.2
1000
6.666666667 1.333333
mL/minutes oil
mL/minutes oil

pumping rate oil & methanol

Flow
L/min
methanol
150
750
oil
150
750

Molar ratio
3:01 4,5:1
16.66667 23.94958
83.33333 119.7479
133.3333 126.0504
666.6667 630.2521

subtance
jatropha
glycerol
biodiesel
methanol

Volume Ratio methanol : oil

molar ratio volume (L)
methanol
3:01
0.125
4,5:1
0.19
6:01
0.25

6:01
30
150
120
600

mass flow rate each component entering to evaporator

component
Stoechiometric mass flow rate
kg/sKg/min flow rate L/min
Ratio Volume %
oil
methanol
biodiesel
glycerol
total

0.4
4.2
1.8
0.6

236.2667
91.24782
355.6221
37.51752

3.937778 285.6913 37.84637

1.520797
5.927034 433.6854 57.45159
0.625292 35.49434 4.70204
754.871

100

30
0.982
0.073
0.338
0.041

Molar volume (L/min)

60
92.5
1.014
1.052
0.075
0.075
0.343
0.348
0.042

110
1.073
0.076
0.351

130
1.098
0.076
0.355

ume Ratio methanol : oil

oil
1
1
1

Masa

Ratio Volume %
oil
methanol
biodiesel
glycerol

kg/m3 g/mol
886
870
782
5.64
859.7
291
808.2
92.1

Pada input reactor

stokiometri
0.4
4.2
1.8
0.6

Input evaporator

mass enter to reactor Molar flow mol/min

590.6667
678.9272

1000
1000
1000
1000

982
73
338
41

1014
75
343
42

1052
75
348

1073
76
351

1098
76
355