Ketones - NIOSH Methods 1300-1301

Column:
J&W P/N: Carrier: Oven: Injector: Detector:

DB -WAX
TM

30 m x 0.32 mm I.D., 0.5 m 123-7033 Helium at 35 cm/sec, measured at 40C 40C for 5 min 40-170C at 10/min Split 1:100, 250C 1 L of 5 g/L standard in CS2 FID, 300C Nitrogen makeup gas at 30 mL/min

6 7 8 5

10 12 9 11

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12.

Acetone Methyl ethyl ketone (2-butanone; MEK) 2-Pentanone Methyl isobutyl ketone (4-methyl-2-pentanone; MIBK) 2-Hexanone Mesityl oxide (4-methyl-3-penten-2-one) 2 Ethyl butyl ketone (3-heptanone) Diisobutyl ketone 1 (2,6-dimethyl-4-heptanone) Methyl amyl ketone (2-heptanone) Ethyl amyl ketone (5-methyl-3-heptanone) Cyclohexanone Camphor

0 C228

8 Time (min)

10

12

14

16

1`8