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Sensor Do PH
Sensor Do PH
Sensor Do PH
80089
Sensor pHD
02/2010, xut bn ln th 1
Hng dn s dng
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
MC LC
Thng s k thut .................................................................................................................................. 4
Thng tin chung .................................................................................................................................... 5
Tng quan sn phm ............................................................................................................................ 7
L thuyt hot ng............................................................................................................................................ 7
Cu to sn phm .............................................................................................................................................. 7
Lp t ................................................................................................................................................................. 8
Lp t sensor ................................................................................................................................................ 8
Kt ni sensor vi gateway........................................................................................................................... 9
Vn hnh............................................................................................................................................. 13
Hng dn vn hnh.......................................................................................................................................13
S iu hng..................................................................................................................................................14
nh dng sensor .............................................................................................................................................14
Chn cc thng s nhit ............................................................................................................................14
La chn cc thng s pH ..............................................................................................................................14
Hiu chun sensor ...........................................................................................................................................15
i vi hiu chun sensor ..........................................................................................................................15
Quy trnh hiu chun nhit ....................................................................................................................15
Quy trnh hiu chun pH .................................................................................................................................16
Thit lp li hiu chun mc nh ..................................................................................................................19
Thay i cc ty chn hiu chun .................................................................................................................19
Ghi d liu (DATA LOG) .................................................................................................................................20
ng k MODBUS ............................................................................................................................................20
Bo dng .......................................................................................................................................... 21
Lch bo dng ................................................................................................................................................21
V sinh sensor ..................................................................................................................................................21
X l s c.......................................................................................................................................... 22
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
Thng s k thut
Cc thng s k thut c th b thay i m khng bo trc.
Thng s k thut
Chi tit
Thang o (pH)
2.5 n 12.5 pH
Thang o ( nhit )
-5 n 95 0C
phn gii
B tr nhit
n nh ( ch i vi b phn tch)
nhy
< 0.005pH
Tc dng chy ti a
3m/s
Ngun yu cu
Nhit hot ng
-5 n 95 C
6m, 5 conductor ( c 2 lp cch ly) cp vi
u cm XLPE (cross-linked polyethylene)
Chiu di cp/loi
914m
Ban u 2 im hiu chun s dng 2 dung
dch m v sau ty chn s dng 1 im
Giao din
Modbus t gateway
Thn Ryton (PVDF), vt liu cu mui ph
hp vi u ni Kynar, in cc u thy
Vt liu
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
Ch th tnh trng nguy c tim n c th gy thng vong hay thng tt nghim trng hoc lm hng
thit b.
Ch th tnh trng c th gy hng thit b nu khng trnh c. Thng tin yu cu nhn mnh ch
c bit.
Nhn cnh bo
c k cc thng tin nhn c dn trn thit b. Thng tt cho ngi hoc h hng thit b c th
xy ra nu khng quan st ch . Mt k hiu nu c ghi ch trn thit b s l tnh trng nguy him
(Danger) hoc thn trng (Caution) trong ti liu hng dn.
K hiu cnh bo an ton. Tun theo cc dng nhc nh v an ton m k hiu cho
php trnh c th b nguy him. Nu k hiu ny xut hin trn thit b, th tham
tho phn hng dn vn hnh v thng tin an ton.
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
L thuyt hot ng
pH l logarit m hot tnh ca ion H+ v o acid v kim trong mt dung dch.
pH thng c o vi in cc thy tinh v mt in cc tham chiu. in cc thy tinh hot ng
nh my bin nng bin i nng lng ha hc (hot tnh ion H+) sang nng lng in (o c
bng milivn, mV). Phn ng cn bng v dng in c khp kn bng dng ion t dung dch tham
chiu n dung dch c phn tch.
Dung dch tham chiu v in cc cng pht sinh mt in p (emf) c ln ph thuc vo loi in
cc tham chiu, cu trc bn trong ca in cc thy tinh, pH v nhit ca dung dch.
Cu to sn phm
Tham kho hnh 1 v chc chn tt c cc thnh phn ca my nhn . Nu bt k mt hng no
thiu hoc h hi, lin h nh sn xut hoc i din bn hng ngay lp tc.
Hnh 1 Cc thnh phn sensor
1. pHD sensor
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
Lp t
Nguy him nh hng ngi dng. Ch ngi c chuyn mn mi c thc hin cc bc c m
t trong phn ny ca hng dn.
Lp t sensor
sensor pH phi c ci t trong flow cell, c kt ni qua gateway v hiu chun trc khi s
dng. Sensor khng cn c x l ban u trc khi s dng. ci t sensor, tham kho cc
bc minh ha.
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
Kt ni sensor vi gateway
Nguy him in git. H thng dy in in p cao cho controller c thc hin pha sau hng ro
in p cao trong vng bao controller. Hng ro vn ng v tr ngoi tr khi lp t cc m un,
hoc khi chuyn vin k thut ang lp t in, r le hoc analog v network cards.
Nguy hi in git tim tng. Lun lun ngt ngun vi thit b kh thc hin cc kt ni
ngun in.
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
J4
GRN (TB1)
RED (TB2)
Pin
Tn hiu
Dy in sensor
WHT
-5 VDC
Trng
SHLD
Dy t
BLK
Nhit
en
YEL
Nhit +
Vng
Tham chiu
Xanh
Tham chiu
Hot ng/o c
Hot ng/o c
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
10
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
11
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
12
Vn hnh
Hng dn vn hnh
13
S iu hng
Tham kho ti liu controller cho m t bn phm v thng tin hng dn
nh dng sensor
S dng menu Configure ng nhp thng tin xc nh v mn hnh ty chn cho sensor v thay
i ty chn x l d liu v lu tr.
1. Nhn phm Menu v chn Sensor Setup, Configure.
Ty chn
M t
EDIT NAME
SELECT PARAM.
RESET DEFAULTS
LOG SETUP
M t
Chn n v nhit (0C hoc 0F )
Chn hng s thi gian tng n nh tn hiu. Hng s thi
gian tnh gi tr trung bnh trong mt khong thi gian o ch nh
no -0 (khng nh hng, mc nh) n 60 giy (trung bnh
cc tn hiu o c trong 60 giy). B lc tng thi gian cho tn
hiu sensor p ng s thay i ca h thng
Ci t khong cch thi gian cho event hoc cho data logging
i vi nng clo v tnh trng dng chy-10, 30 giy, 1, 5, 15
(mc nh), 60 pht
La chn cc thng s pH
1. Chn kiu Clo sensor c s dng- o clo tng hay o clo t do (total Cl2 hoc free Cl2)
2. Chn Yes
3. Chn DIFF PH
4. Chn pH
5. Ty chnh cc ty chn
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
14
Ty chn
DISPLAY FORMAT
FILTER
LOG SETUP
M t
Chn mt s thp phn c hin th trn mn hnh o XX.XX
hoc XX.X
Chn hng s thi gian tng n nh tn hiu. Hng s thi
gian tnh gi tr trung bnh trong mt khong thi gian o ch nh
no -0 (khng nh hng, mc nh) n 60 giy (trung bnh
cc tn hiu o c trong 60 giy). B lc tng thi gian cho tn
hiu sensor p ng s thay i ca h thng
Ci t khong cch thi gian cho event hoc cho data logging
i vi nng clo v tnh trng dng chy-10, 30 giy, 1, 5, 15
(mc nh), 60 pht
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
15
Ty chn
ACTIVE
M t
Thit b gi gi tr o c hin ti trong qu trnh hiu chun
HOLD
TRANSFER
6. o nhit ca mu hoc dung dch tham chiu vi thit b xc minh ph ( nh nhit k theo di
NIST)
7. S dng cc phm mi tn nhp gi tr c o v nhn ENTER.
8. Xem li kt qu hiu chun:
Passed (t)-sensor c hiu chun v sn sng o mu. Gi tr b tr s c hin th.
Failed (cha t)-b tr ng hiu chun nm ngoi gii hn chp nhn. Thc hin bo dng
sensor (tham kho phn Bo dng) v lp li hiu chun.
9. Nu hiu chun t, nhn ENTER tip tc.
10. Nu ty chn cho ID ngi dng c ci t YES trong menu Cailbcate Optoins, nhp ID ngi
dng.
Tham kho Thay i ty chn hiu chun.
11. Trn mn hnh New Sensor , chn sensor mi:
Ty chn
YES
M t
Sensor cha c hiu chun trc vi thit b ny. S ngy vn hnh
v cc ng hiu chun trc o cho sensor c ci t li
NO
16
2. Hiu chnh sensor pH trong flow cell, lp sensor pH vo flow cell v bt flow.
3. Nhn phm MENU v chn Sensor Setup, Calibcate, pH.
4. Chn kiu hiu chun:
Ty chn
M t
2 im m
1 im m
S dng 1 im m, v d pH 7. m phi t
b m c ch r trong Cal Options menu
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
17
M t
Thit b gi gi tr o c hin ti trong qu trnh hiu chun
HOLD
TRANSFER
7. Vi sensor trong dung dch tham chiu u tin hoc mu, nhn ENTER.
Gi tr pH v nhit o c hin th.
8. Ch n khi gi tr n nh v nhn ENTER1.
9. S dng mu, o gi tr pH vi thit b xc nh ph. S dng cc phm mi tn nhp gi tr
o v nhn ENTER.
Lu : Nu pH m khng c trong danh sch Cal Options menu c s dng, tham kho chai
m tm gi tr pH tng ng vi nhit ca m.
10. Cho 2 im hiu chun:
a. Nu s dng dung dch tham chiu, di chuyn sensor ra khi dung dch u tin v sc ra vi
nc sch.
b. t sensor trong dung dch tham chiu tip theo hoc mu v nhn ENTER.
Gi tr pH v nhit o c hin th
c. Ch gi tr ny n nh. Nhn ENTER1.
d. Nu dung dch ny l mu, o gi tr pH vi thit b xc nh khc. S dng cc phm mi tn
nhp gi tr o v nhn ENTER.
Lu : nu m pH khng c trong danh sch Cal Options menu c s dng, tham kho chai
m tm gi tr pH tng ng vi dung dch ca m.
11. Xem li kt qu hiu chun:
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
18
M t
Sensor cha c hiu chun trc vi thit b ny. S ngy vn hnh
v cc ng hiu chun trc o cho sensor c ci t li
NO
M t
i vi pH thay i b set dung dch m c ng nhn cho hiu
chun pH ) l 4.00, 7.00, 10.00 ( b mc nh) hoc or DIN 19267 (pH
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
19
CAL REMINDER
OP ID ON CAL
ng k MODBUS
Danh sch ng k MODBUS c sn trong phn giao tip mng. Tham kho trn a CD c thng
tin chi tit.
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
20
Bo dng
Cnh bo: Nguy hi nh hng ngi s dng. Ch ngi c chuyn mn c thc hin
cc thao tc c m t trong cc mc ca hng dn ny.
Lch bo dng
Cng vic thc hin
Lm sch v kim tra sensor
Tn sut
90 ngy
(pH sensor cn c lm sch ty thuc vo cht
lng nc)
3 6 thng.
4 5 nm
V sinh sensor
Cnh bo : nguy hi cht ha hc. Lun lun eo bo v an ton c nhn theo quy nh ca Bng
Thng s An ton ha cht c s dng.
Kim tra sensor c h hng, cc mnh v, hoc cn nh k .Lau sch sensor khi tng cc cn bn
hoc khi hot ng ca my b gim st.
Yu cu trc khi thc hin: Chun b mt dung dch x phng nh vi cht ty ra khng n mn,
khng cha lanolin. Lanolin l mt film trn b mt in cc, v th c th l suy gim hiu qu hot
ng ca sensor.
1. Tt dng chy
2. Ni lng kha vng v tho pH sensor ra khi flow cell.
3. Sc sensor vi nc m. nu cn mnh vn, chun thn lau ton b sensor vi vi sch di
chuyn cc cht bn ra. Sau sc ra sch bng nc.
4. Ngm sensor khong 2 -3 pht trong dung dch x phng.
5. S dng bn chi lng mm v lau chi ton b sensor , lau sch hon ton b mt in cc v
salt bridge.
6. Nu cn trn b mt vn cn, ngm sensor trong dung dch acid long, nh clohydric acid(HCl)
( hoc dung dch acid long khc), ti a l 5 pht.
Lu : Acid nn c pha long, khng qu 3% HCl. Thc t s xc nh acid s ng v thang
o pha long thch hp. Cc vt bm qu cht c th c lm sch bng cc tc nhn khc. Lin
h h tr k thut.
7. Ra vi nc v ngm trong dung dch nc x phng khong 2 3 pht trung ha acid cn
xt li.
8. Ra sensor vi nc sch.
9. Hiu chun sensor trong cc bng cch s dng dung dch tham chiu.
10. Lp pH sensor trong flow cell v vn cht kha vng.
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
21
X l s c
Kim tra sensor
Yu cu trc khi thc hin: 2 dung dch m (pH 7 v pH 4 hoc pH 10) v my o vn k.
Lu : Nu hiu chun li, ra sch sensor v thay i cu mui v dung dch chun bn trong in
cc ( standard cell solution) v sau lp li hiu chun. Ch kim tra sensor nu vn ny khng
khc phc khi bo dng.
1. t sensor trong dung dch m pH 7 v ch n khi nhit sensor v m bng nhit phng.
2. Ngt dy sensor vng v en khi gateway.
3. o in tr gia dy mu vng v mu en xc nh yu t nhit hot ng. in tr nn
nm gia 250 350 ohms xp x 25C.
Nu yu t nhit tt, kt ni li cc dy vo gateway.
4. Nhn phm MENU v chn Sensor Setup, Diag/Test, Signals. Kt qu pH nn nm trong khong
50 v + 50mV.
5. Ra sensor vi nc v t trong dung dch m pH 4 hoc pH 10. Ch n khi nhit sensor
v m t n nhit phng.
6. So snh kt qu c mV trong m pH 4 hoc pH 10 vi kt qu c trong m pH 7. Kt qu c
nn khc xp x 160mV.
Nu s sai khc thp hn 160mV, lin h h tr k thut.
CAL DAYS
CAL HISTORY
M t
Hin th thng tin phin bn ca phn do (firmware), s s-ri
v phin bn boot ca b iu khin v loi sensor c ni
vo controller
Hin th s ngy tri qua k t khi sensor c hiu chun
Hin th danh sch cc ln sensor c hiu chun. Nhn
ENTER di chuyn trong danh sch v xem tm tt cc s
liu hiu chun.
Ci t li calibration history. Cn phi nhp mt m
Hin th gi tr tn hiu o c theo mV
Hin th s ngy hot ng ca sensor
Ci t li s ngy sensor v s ngy hiu chun v ch
mc nh. Cn phi nhp mt m
Hin th gi tr dc, gi tr b (offset) cho clo v pH (nu c
dng sensor o pH). Hin th gi tr b tr (offset) cho nhit
(nu c dng sensor o pH).
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
22
pH TOO LOW
pH TOO HIGH
M t
Yu cu hiu chun clo hoc pH.
Gi tr o clo v pH thay i t mc
cnh bo t CAL WATCH. Tham
kho phn chn cc gi tr cnh bo
t Cal Watch.
Gi tr pH thp hn 0pH
Gi tr pH cao hn 14pH
pH SLOPE FAIL
dc vt ngoi thang o 45
n 65 mV/pH
pH OFFSET FAIL
Gi tr b tr vt ngoi khong
60 mV
TEMP FAIL
pH CAL RECD
M t
Yu cu hiu chun clo hoc pH c
khuyn khch. Gi tr o clo v pH thay i
t mc cnh bo t CAL WATCH. Tham
kho phn chn cc gi tr cnh bo t
Cal Watch.
Hiu chun pH c khuyn khch
D liu hiu chun pH khng c sn
( sensor vi d liu hiu chun mc nh)
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
23
PH CAL TO DO
TEMP CAL TO DO
PH MAINT RECD
PH MAINT RECD
T MAINT RECD
Event log
Controller cung cp mt Event log cho m sensor. Event log lu tr a dng cc s kin xut hin
trong thit b nh thc hin hiu chun, cc ty chn hiu chun c thay i mt danh sch
cc s kin c th xut hin c hin th Bng 5 pha di. Event log c th c c trong nh
dng CSV. c hng dn v vic ti cc log, tham kho hng dn s dng controller.
Bng 1 Event log
Event
Power On
M t
Ngun in c bt ln
Flash Failure
1pointpHCalibration_Start
Bt u hiu chun 1 im mu i vi pH
1pointpHCalibration_End
2pointpHCalibration_Start
Bt u hiu chun 2 im mu i vi pH
2pointpHCalibration_End
1pointBufferpHCalibration_Start
Bt u hiu chun 1 im m i vi pH
1pointBufferpHCalibration_End
2pointBufferpHCalibration_Start
Bt u hiu chun 2 im m i vi pH
2pointBufferpHCalibration_End
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
24
TempCalibration_Start
TempCalibration_End
pHCalSetDefault
TempCalSetDefault
AllCalSetDefault
pHCalOptionChanged
TempCalOptionChanged
SensorConfChanged
ResetpH CalHist
ResetTemp CalHist
ResetAllSensorsCalHist
ResetpHSensor
ResetTempSensor
ResetAllSensors
Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
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Hng dn s dng sensor pHD trong CLF10 v CLT10, dch bi Hach Vit Nam
26