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Unexplained Glass Failure - Don’t jump
to inclusion conclusions Make an enquiry e
Tuesday 1 July 2014
Nicke| Sulphide (NiS) inclusions are a known Issue for toughened glass, resulting from
the presence of nickel contaminants in the glass melt reacting with sulphur, most likely}
from the furnace fuel. During thermal toughening, these inclusions undergo a
crystalline phase change to a smaller form and are fixed in place within the glass upon
‘cooling. Over time the inclusions grow and can eventually impart enough stress in the
glass to cause spontaneous failure. When toughened glass panels fail, Nickel Sulphide|
(Nis) inclusions are the “go to” culprit. Independent research and development,
consultancy and testing specialist, Glass Technology Services (GTS) is urging
property owners and insurers not to assume that a NiS inclusion is the cause of an
unexplained breakage.
GTS Glass Technologist, Or Richard Cave, comments: “It should never be assumed that the seemingly spontaneous failure
of a toughened glass panel is due to 2 NiS inclusion. Numerous other factors could be involved, such as non-NiS inclusions,
vandalism, design flaws, poor toughening, edge damage and damage due to contact with fitings and fixtures. Any
tunexplained failures of toughened panels should undergo analysis to determine the true cause of failure.”
Even where a ‘butterfly’ failure pattem is observed — something commonly associated with a ‘spontaneous’ NiS failure —a
Nis inclusion cannot be assumed. The three images below depict this same failure pattern, however, whilst one is due to a
INS inclusion the other two have resulted from a glassy inclusion within the glass and an impact,
Fancy winning an iPad Mini or a place on our Glass Appreciation Course this October? Simply tellus which of the
butterfly failure pattems below is caused by NiS for the chance to win. For more information follow us on twitter
@GlassTesting and look out for our #ButterflyCompetition announcement, alternatively subseribe to our newsletter to receive
elas in our next bulltin, Click here for ful competition tails and terms and conditions.
‘The GTS team works throughout the glass supply chain - from manufacturers, processors and installers through to
architects, consulting engineers, property owners insurers and loss-adjusters - to analyse glazing failures, This service can
be provided both on-site or in the laboratory
When a fully toughened panel fails, the failure origin must be analysed in order to determine the cause of failure — therefore
itis essential that the broken remains are retained for investigation. Once the origin is identified this is analysed using optical
microscopy, scanning electron mierocopy and energy dispersive x-ray spectroscopy, to identify the presence and nature of
inclusions (NIS or otherwise) or physical damage, Where inclusions aren't to blame, physical damage and residual material
‘can be analysed to determine likely contacting objects, whether ibe from an outside source or from interactions with
fixtures and fittings in the framing system,
‘These analytical capabilities and experience in glass enable the team to provide expert reports conceming a whole range of
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failures - ranging from external influences, such as vandalism and impacts, through to incorrect specification, interaction with
‘components, material processing and fabrication or the presence of manufacturing defects.
“The industry knows that thermally toughened glass has numerous benefits over annealed and heat-strengthened glass,
including better resistance to thermal changes, increased strength and safe breakage characteristics,” said Dr Cave, “Steps
have been taken to eliminate NiS from the production of float glass, with changes in raw materials, manufacturing methods
‘and processing techniques. The heat soaking process, introduced into manufacture by Pilkington in the late 60s, is also now
recommended for all glazing installed in critical locations such as barriers or overhead glazing. Whilst itis not guaranteed to
climinate NiS inclusions altogether, the likelihood of spontaneous failure due to NIS is significantly reduced when heat
‘soaking has been carried out,
“Bul NIS inclusion should never be assumed. Of the failed toughened panels examined by GTS in 2013, two thirds had
falled dus to the presence of NiS inclusions, with the remaining third a combination of impact damage, poor toughening,
detrimental interaction with fixtures and non-NiS inclusions.
“To highlight this, a property management firm recently sent several falled toughened units to GTS for analysis after
spontaneous failures had occurred throughout the building, Whilst analysis ofthe majority of the units identified the
presence of NiS inclusions, other units featured impact damage at the failure origin,
“Uttimately, architects, engineers and specifiers should consider the benefits and drawbacks ofall types of glazing before
installation and ensure that they adhere to all relevant building regulations and codes of practice. Installers should adhere to
the specifications and follow best practice to avoid unnecessary breakages.”
GTS is accredited to ISO 9001, ISO 14001 and ISO 17025 standards and is a Notified Body (number 2461) for the Initial
‘Type Testing (ITT) of glass products under the European Union's Construction Products Regulation (EU) No 305/2011
(CPR) in order to CE mark products for the European marketplace. The team provides analysis, consultancy, testing,
research and development suppor to glass manufacturers, processors, tougheners, designers, architects, consulting
‘engineers and specifiers across the UK and internationally.
See our newly launched website at www.glass-s.com/architecture-and-glazing; email eng
(0) 114 290 1801
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