5711800084

1
1. 1

1 TG-DTA
1
(Thermogravimetric analysis; TGA)
(Differential thermal analysis; DTA)
SDT Q600 TA instrument

- TGA

(Thermogram)
(mg) (C)
- DTA

(mW)

 5711800084
(C)


SDT Q600
1000 C 10
C 1 TG
800C
3 230 C

DTA
230 C
400 C
DTA
(exothermic)

800 C
TG
500-800 C
2. (TiO2)
3
D

m
V

D (g/cm3)
m (g)

V (cm3)

 5711800084
1)

1.1)
4
8
6.02 10 23 47.99
4

4 47.867
3.18 10 22
23
6.02 10

6.02 10 23 15.99
8

8 15.99
2.12 10 22
23
6.02 10

3.18 2.12 10 22 5.30 10 22

1.2)

a b 3.776 3.8 10 8 cm c 9.486 9.486 10 8 cm

V a b c 3.776 10 8 3.776 10 8 9.48610 8 cm3

1.372 10 22 cm3

 5711800084
D

m
V
5.30 10 22
3.863 g/cm3
D
22
1.372 10

2)

2.1)
2
4
6.02 10 23 47.867
2

2 47.867
1.59 10 22
23
6.02 10

6.02 10 23 15.99
4

4 15.99
1.06 10 22
23
6.02 10

1.59 1.06 10 22 2.6510 22

2.2)

 5711800084
a b 4.954 4.594 10 8 cm c 2.959 2.959 10 8 cm

V a b c 4.594 10 8 4.594 10 8 2.95910 8 cm3

0.624 10 22 cm3

m
V
2.65 10 22
4.240 g/cm3
D
22
0.625 10

3)

3.1)
8
16
6.02 10 23 47.867
8

8 47.867
6.36 10 22
23
6.02 10

6.02 10 23 15.99
16

16 15.99
4.25 10 22
23
6.02 10

 5711800084

6.361 4.25 10 22 10.6110 22

3.2)

a 9.166 9.166 10 8 cm b 5.436 5.436 10 8 cm c 5.135

5.13510 8 cm
V a b c 9.166 10 8 5.436 10 8 5.13510 8 cm3

2.559 10 22 cm3
D

m
V
10.61 10 22
4.146 g/cm3
D
22
2.559 10