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  • Iatronscan MK6 Catalogue - 06

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    Efrain Ramirez Chavez
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    Analisis SARA

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    Iatronscan MK6 Catalogue_06

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    Analisis SARA

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
    5 views6 pages

    Iatronscan MK6 Catalogue - 06

    Uploaded by

    Efrain Ramirez Chavez
    Analisis SARA

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
    of 6
    The first in the TLC World! IATROSCAN™ mounted FPD does break down preconceived idea on TLC. IATROSCAN became new. The new model [ATROSCAN MK-6 with PPD (flame photometric detector) detects the hetero-atoms such as phosphorous and sulfur selectively. Furthermore, the simultaneous measurement by both FPD and FID (ame ionization detector) is possible. Organic compounds on the thin-layer are surely captured by means of two eyes of FID (patented) and FPD (under patent application) without omission. ‘The addition of FPD to the former TLC-FID TATROSCAN with improved quan- tification and reproducibility enables to acquire a wealth of analytical informa tion much more than ever. —) Blank scan ‘The CHROMAROD can be "| Solvent removal cleaned and activated by hy- ZL) After development, the de drogen flame through the blank sean _yelopment solvent adsorbed on the CHROMARODG) is removed. fon JATROSC, ~)) Sample spotting | Approx. 111 of the sample solution is spotted on. the CHROMAROD by means of a micro- dispenser, Measurement After solvent removal, start measurement by pressing START key. Separation The components in the sam- ple on the CHROMAROD(S) are separated through development procedure in the development tank, ootabasS IATROCORDER TC-21 IATROCORDER C21 is an inte grator exclusively used for 1A- TROSCAN, which makes i¢ poss ble to get analytical reslts follow ing ils easy operational proce- dure provided, however, that it ad ditionally requires a print eicult board_of A/D converter (option) for dual measurement ‘The chromatograms, information fom peaks of components and theit quantitative analytical results can be stored for long period owing to the elear output recorded by inkjet printer plotter on the paper for ‘common use, Tt is easy to automat cally identify the measuring mode set by IATROSCAN in advance, and easily calelate the average of analytical results of plural rods as wel CHROMAROD™ ‘The CHROMAROD, developed exclu ly for the IATROSCAN, is thin layer in the form of thin quartz rod evenly ap plied and sintered inorganic binder and ausorbent on it Usually, the cleaning and activation of CHROMARODs ean be ach- ieved by Blank scan onthe [ATROSCAN, which enable CHROMARODs to be used repeatedly. The CHROMARODs give ex cellent separability of components and exhibit stable reproducibility. Special types of thinlayers, such as those suit- able for separating triglycerides in accor ddance with their unsaturation degrees or alyeeride isomers, can be easly prepared simply by immersing CHROMARODs in silver nitrate or borie acid solution ee. spectively WW tarene) Quartzrod ——_Adorbent IATROSCAN ean cove a ‘whole range of organic compounds’ ‘TIC analyses and is optimal especially for heavy oll type analysis, tracking organie synthetic reactions and so forth. It is also available with versatility for crude materials’ analyses under ‘open atmosphere, which are difficult to be done by GC and/or LC. Furthermore, the sample spotted on the CHROMAROD can be simply quantified without development. Heavy oil type analysis (FID/FPD:S) Lipids analysis (FIO/FPD:P) Serle Sersainme Fo. FPDP) Calibration curve of S-compound (FID/FPD:S) FPo(s) Glycerides analysis (FID) Simple quantification method (FID)... ie ‘Soper pte sar ie eats EA, Bimenen feo Zia sat S00 Goan) 1206 puma Stig (remand ‘Smee peat 2 Shy Siatty le Tasty Stag’ Bu {eum aay ‘Spas te dope Core Sloan cramer 8 ee oo Han ovt ‘Simple Operation ‘@pecdy detection of component(s) in a sample ‘@Easy to acquire related chromatogram(s) @NXo need for troublesome coloring procedure ‘required for conventional TLC after development ‘Not only the organie compounds analyzable by ‘TLC, but also the organic compounds with boiling points (oligomers, polymers, et.) hardly analyzed by GC and those difficult to be detected by LC (oils and fats, lipids, ete.) are analyzable. High efficiency @simultaneous development and detection of ‘components in a samples on ten (10) CHROMARODs mounted on one rod-holder are possible. ©The measuring time required for one sample is approx. 30 seconds, which is enable quite efficient analysis Cost effective CHROMAROD can be used repeatedly. Easy quantification Peak identification and quantification are easy since the analytical results are output to the ‘exclusive use integrator (option } or chromatogram processing, software package on PC basis (option), 4b rinciple.of Measuremen), A specially designed thin layer quartz rod (CHROMAROD™ ) traverses the hydrogen flame at constant speed after developing the sample and separating its components on it Each organic compound separated on the rod is ionized by the energy of hydrogen flame, which generates electric current on the FID electrodes in between. This electric current proportional to the amount of sub- stance in the flame is multiplied and there: by enables quantitative determination, Tn case the organic components on the rod contain phosphorous and/or sulfur elements, they emit their inherent lights during being burnt in the hydrogen flame. After spectro scopically separated by the interference fil ter, those lights are multiplied by the photo ier in order to detect phosphorous and/or sulfur selectively. Principle chart ammeter a | Data Processing Unit Ke | Interference itor “footecter eloctrode “oh Photomutiolior Ain Guiae Ai, Hyarogen IATROSCAN MK-6 ‘D000 TATROSCAV NIG - Components’ separation by tiiniayer chromatoaranhy using “aTROSCAN RB CHROMAROD (epecial thimiayer rod) (CHROMAROO-SIE Toe Fea hor S05 7 Detectors Hycrose ‘photometric detector FPO) w Tonization dtector (FID) and Flame ‘Develooment tenk OT TSO Power soiree? AG 100,120,220 & 240V,60/80H2 ‘Ron STS. © SD r Interference fitr for sufur t ateetion tie : 25, 30. 95. 40.50, 60se6, Interforence ft for phospho r Fiydrouen flow monitor electronic flow meter sitet leplan) ‘Spotting ude r Air flow monitor a ow mater (oat €yp8) ‘Mewaepenser 2k iow monitor Leif metar eet te) Hydrogen load a 2m od holder : available for loading 10 rods: ‘Tables (poner, signal earth Or ‘Measuring modes ! Normal scan / Blank scan 7 Orin ecan 7 Tweezers r Partial pyrolysis scan Fuse - r r i ‘poration waaval Power consumption approx, 50VA 57 aa Temperature / Hurisity requremanta: T0350 /20~BO% “iROSoAN Ss = ‘imensione ? 520(W)

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