KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:

BI 1: CN BNG LNG LNG H HAI CU T

Kt qu th nghim
1. Bng cc gi tr ghi nhn c:
ng s
TTphenol
TT nc
Nhit
bt u
trong 0C
Nhit
bt u
c 0C

ml
ml
Ln 1
Ln 2
Ln 3
Ln 1
Ln 2
Ln 3

1
0.6
5.4

2
0.9
5.1

3
1.2
4.8

4
1.5
4.5

5
1.8
4.2

6
2.1
3.9

7
2.4
3.6

8
2.7
3.3

9
3.0
3.0

10
3.3
2.7

10

11

2. Bng tnh phn trm khi lng cc cht trong hn hp:

Dng cng thc:
%KLphenol =
%KLnc =
ng
%phenol
%H2O

11
3.6
2.4

 th nhit thnh phn khi lng ca h phenol nc

Vy: Nhit ti hn ca h:
Thnh phn ha tan ti hn ca h:
TR LI CU HI.

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:

BI 2: CN BNG LNG RN
Kt qu th nghim.

Kt qu th (ch nh du im bt u kt tinh):
ng
Naphtalen
Diphenylamin
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25

1
10
0

2
8
2

3
6
4

4
4.5
5.5

5
3
7

6
2.5
7.5

7
1
9

8
0
10

Kt qu tinh:
Bng tnh phn trm khi lng Naphtalen Diphenylamin
ng
%Nap
%Diphe

Gin nhit - thi gian t suy ra gin nhit - thnh phn

TR LI CU HI

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:
BI 3: XC NH BC PHN NG
Kt qu th:
1. Xc nh bc phn ng theo Na2S2O3:
Th nghim s

Thi gian (giy)

2. Xc nh bc phn ng theo H2SO4:
Th nghim s

Thi gian (giy)

Kt qu tnh:
1. Bc phn ng theo Na2S2O3:

2. Bc phn ng theo H2SO4

Vy bc tng qut ca phn ng:

TR LI CU HI:

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:
BI 4: THY PHN ESTER BNG KIM.
1. Kt qu th:
Phn ng: CH3COOC2H5 + NaOH

CH3COONa

+ C2H5OH

Bng ghi tr s th tch NaOH dng chun HCl d

Thi im (Pht)/
Nhit
T1(phng 300C)
T2 ( 400C )

10

20

30

40

50

2. Kt qu tinh:
V1: th tch NaOH chun HCl d (ml)
V2: Th tch NaOH c trong 25ml mu th nt (ml)
Bng kt qu:
Nhit
300C

Nhit

400C

Thi im
5
10
20
30
40
50

V1

V2

nt-n

kT1

Thi im
5
10
20
30
40
50

V1

V2

nt-n

kT2

Nh vy gi tr k trung bnh:
kT1 = 4.561 (1/pht)
kT2 = 8.254 (1/pht)
Tnh nng lng hot ha ca phn ng:

TR LI CU HI :
:

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:

BI 5 PHN NG IOD HA ACETON T XC TC

KT QU TH NGHIM
Phn ng:CH3COCH3 + I2
CH3COCH2I + HI
a = 0.026 mol
b =0.025mol
Mu
Thi im
Vt
x =(V0-Vt)C10-3
k
-3
0
2.50
0.250 x10
10
2.35
0.015 x10-3
0.576 x10-3
15
2.25
0.020 x10-3
0.512x10-3
-3
30
2.00
0.050 x10
0.640 x10-3
45
1.80
0.070 x10-3
0.597x10-3
60
1.45
0.105 x10-3
0.672x10-3
90
1.15
0.135 x10-3
0.576x10-3
120
0.65
0.185 x10-3
0.592 x10-3
ng biu din tc theo thi gian

TR LI CU HI
1. Tnh thi gian cn iod ha 50%, 80%, 90% aceton
Khi iod ha 50% aceton tc l x = 50%.x0 =0.125 x10-3 khong 80 pht mi iod ha
c 50%
Khi iod ha 80% aceton tc l x = 80%.x0 =0.200 x10-3 phi hn 120 pht mi iod
ha c 80%
Khi iod ha 90% aceton tc l x = 90%.x0 =0.225 x10-3 phi hn 120 pht mi iod
ha c 90%
2. Mun tnh nng lng hot ng ha ca phn ng iod ha aceton, ngi ta c phi
lm thm th nghim g khng? Cch tin hnh th nghim nh th no?
Ta phi tin hnh th nghim nhit khc.

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:

BI 6: PHN NG XC TC NG TH PHN NG PHN HY H 2O2

KT QU TH NGHIM
Phn ng: 2H2O2

2H2O +

O2

Thi im t
0
5
10
15
20
30

CA-Cx

CA

k30

Thi im t
0
5
10
15
20
30

CA -Cx

CA

k40

Vy k30 =
k40 =
Nng lng hot ha ca phn ng E:

Tnh chu k bn hy 1/2 300C:

Tnh chu k bn hy 1/2 400C:
TR LI CU HI

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:
BI 7: HP PH TRONG DUNG DCH TRN B MT
CHT HP PH RN
KT QU TH NGHIM
Bnh
VNaOH 0.1N

(mol)

log

C/

Kt qu tnh
Bnh

C0 (mol/l)

1
2
3
4
5
6
th log theo logC

C (mol/l)

logC

Suy ra:

lgk =
1/n =
th C/ theo C

Suy ra

k =
=
Tnh b mt ring S0 ca than hot tnh (m2/g):
S0 =

TR LI CU HI:

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:
BI 8: X L LM SCH B MT KIM LOI BNG PHNG PHP HA
HC V PHNG PHP IN HA
Kt qu th nghim:
1. Ty g ha hc:
STT

Tnh cht b
mt trc ty

Thi gian ty
(pht)

Tnh cht b mt
sau ty

Ghi ch

Tnh cht b mt
vt ty

Ghi ch

Nhn xt th nghim:

Cc phn ng trn b mt vt ty:

2. Ty g in ha:
STT Ia(A/dm2) Ic(A/dm2) Thi gian

Nhn xt th nghim:

Cc phn ng trn in cc:

3. Ty du ha hc:
STT

Tnh cht b
mt trc ty

Thi gian ty
(pht)

Tnh cht b mt
sau ty

Ghi ch

Tnh cht b mt
vt ty

Ghi ch

Nhn xt th nghim:

Cc phn ng trn b mt vt ty:

4. Ty du in ha:
STT Ia(A/dm2) Ic(A/dm2) Thi gian

Nhn xt th nghim:

Cc phn ng trn in cc:

Tr li cu hi:

KHOA CNG NGH HA HC & THC PHM

BO CO TH NGHIM HA L
H Tn SV: ............................................. ......................MSSV: ..........................................
Lp: Nhm T

im:

Ngy TN Bui
GVHD:
BI 9: M NIKEL (Ni)
Kt qu th nghim:
Ln TN

I(A)
m
ms
Kt qu tnh:
STT

I(A)

Ic
Thi gian
2
(A/dm ) m (pht)

Tr li cu hi:

mtt(g)

lt(g)

H(%)

d()

Ghi ch