CALIBRATION REPORT FOR PRT & READOUT Prepared for: SAMPLE CUSTOMER S/N: 678910 SIN: 12345 Report Number: W185901ICL CALIBRATION LABORATORIES, INC. =e ISO/EC 17025 and ANSI/NCSL 2540-1 accredited 1501 Decker Avenue Suite 118 Stuart, FL 34904 USA The specialists in ASTM and laboratory thermometers & hydrometers Tel. 772 286 7710 1-800-713-6847 Miele: Rn WALT ee” Aer coma Fax: 772 286 6737 E-mail ssles@icicalbration com Setting new standards m calibration excellence Internet san iciads com Roport No, Wias901 So: 123456 Chiont! SAMfPLe CUSTOMER’ Date report issued: 09-26-2019, Page T of 3 CALIBRATION REPORT FOR PRT & READOUT The instrument identified herein was exemined and calibrated in (CL's calibration laboratory. using NIST traceable standards, folowing the caubration procedure referenced below. ‘This cafbration fulfils the requienvonts of SONEC. 17025-2005, ‘General Requirements, for the Compotonce of Testing and Callretion Laboratories” and ANISIINCSL 2640.1-1994, Caltyatin Laboratories and Measuring and Test Eavioment Goneral Requirements CuENT SAMPLE CUSTOMER STREET ADDRESS etry. stare ae Purchase order number: NOT AVAILABLE Submitted by: SAMPLE COMPANY DATES Date report issved: 09-25-2013, ‘Noxt due (specified by client): September 25, 2014 UUT (Unit Under Test) INFORMATION Sensor information: Manufacturar: HART SCIENTIFIC ‘Mode! fo: 5614 Sorin! No: 12345 Description: 4 wire 100 Oly secondary standard PAT Temperature range: 198/420 Aecuracy tolerance: 4. SEE BELOW Sensor immersion: Minimum 6 inches recommended Readout device information: Monufactoror: HART SCIENTIFIC ‘Mode! fe: 15024 ‘Serta! No: 678910 Readout resolution: 0,001°C Accuracy tolerance: +7 SEE BELOW. “AS FOUND" READOUT CALIBRATION CONSTANTS: Cal0: 0.0002 Ca/100: 0.0009 Cal400: 0.0011 ‘No chenges ware mado fo these constants NOTE: The accuracy tolerance for this system calloatin (sensor and readout) Is the rootsumm-square of the accuracy tolerance Of the sensor and tho acouracy toloranee of the readout device. Enginaering units: °C RESULTS OF PHYSICAL EXAMINATION The condition ofthis device was satisfactory with no visually apparent defects, unless noted below. CALIBRATION PROCEDURE USED ICL Procedure 05, which is dravn from ASTM E77, ASTM E644 and ASTM E1137, LABORATORY ENVIRONMENTAL CONDITIONS Temperature: 23°C +/- 2°C Relative humidity: between 30% 70%ICL CALIBRATION LABORATORIES. INC. Report No. 185901. SO: 123486. Gilont: Saudple CUSTOMER Bate report issued: 09-26-2013 Page 2 of 3 RESULTS OF CALIBRATION Note: the ’As Found! readings were observed using coofiicionts resident in tho non-volatile memory of he device, which were: RIPW: 100.027 c -7.52605E-04 bod: -3.021126-05 a8: -7.44288E-04 b8:-8.802128-05 "AS FOUND" VALUES: Tolerant 5 mi in o.010¢¢ o.g10:¢ | o.01s"c © -0.009°¢ 0.0167 © 0.0160°C PASS 0.003" 400:000°¢ © 3991996°C duo 028°C © “0:032°¢ © O038°C © 00287°C © MARGSY © 0.024"c 2ooro00-e ——«199:996°C 200-010" © “or014e¢ ©—«0:023°C © OrnaBrc = MARCY © 0.024"C S3alesace —-381833°¢ | -381825°C —-0.008°C ©~—«004s"c¢ ©—OoddL"c © PASS = 0-012°C -iseloooe —-issieds-c | -i98.653"¢ —0.0oe"c © o026"¢ = OLoza"c © PASS 0-010" ocon0°e foloi0"e © Oco1s"c © -0L008°¢ © -0e°c © O-o1eD°C © PASS = .003"C As can be determined from the information presented in the table above, one of more of the ‘As Found” readings of this device tere ether beyond the ‘hecept Limit. resulting in declaration of ‘Margina..2r were beyond the actual roleranc® Accordngly, an adjustment was undertaken. ‘The new resistance atthe tiple point of water (TPW) value cbsorved was entered into the device, and the calibration was ‘repeated fo obtain the ‘As Lett values shown in the folowing table, ‘Now RTPWY (resistance atthe triple point of water) valve: 100.0305, Revised cootcionts used for ‘As Loft values: <7 AKQBBE-04 8: -8.80212-05 ooore o1gorc pass 0. 003"¢ bose 2s7°c PASS (02a 002°6 ieee = PASS (oar ‘002°e ole PASS 226 -issleasre 0076 240°C PASS 20°C Oc010°e renee roleore BASS are “ACCEPT LIMITIs) The seceptance limits) shown above represent a statistical evelustan ofthe instrument's tolerance relative tothe Uncertainty of the measurement If requited, the acceptance limit is set to.8 value smaller than the tolerance. The diference betwaen the tolerance and the acceptance limit the “guard band” The guard band i imposed to reduce the probabilty of 2 false sceeprence PFA), ‘ra fais faiure, to lee than 23% PINE Accordingly, there are thee possible calibration outcomes for any given test point: 1. PASS The calibration result falls within the interval described by the test point + or - (the tolerance MINUS tho guard band). 2, MaRG*"" marginal The coloration result 2 bordering” or indeterminate, It's therefore statistically ond metrologicaly imprudent {9 declare that the intrumant ie detintively ether ‘intolerance’ or out-of tolerance’ 5. “Fall The calbration result fells outside the interval described by the test point + oF - (the tolerance PLUS the guard band) The methodology and equations used for determination of guard bands and acceptance limits comply with the requirements of ANSINCSL 2840.2 LIMITATIONS OF USE This i¢ 2 full slo coibration and no limitations of use are imposed on this instrument. (MEASUREMENT UNCERTAINTY The measurement uncertainty reported isthe expanded uncertainty st 2 sigma (k=21, to provide » confidence love of approximately 95% The uncertainty is celeulated considering Type A contibuters including the standard deviation of the mecsuroment process trom check standard ontrol charts the standard devioton of monthly Triple Point of Water calibrations of the standard, ond UUT varibiity observed during the albration, as’ wel’es Type 8 contrbutors, which include comparator uniformity, uncertainty of the Callretion of the stenderd, stem conduction ‘and other immersion effects, the sensituity and accuracy of the standard thermometer’ readout, and resolution of the standard and UUT. The Type A and B contnbutors are combined using the ot sum square method to obtain the standard uncertainty at 1 sigma, The standard uncertainty is then multpied by 2 to obtain the expanded uncertainty at 2 sigma (k= 2) The expanded uncertinty prasented i this report was calevated using methodology consistent with the ISO Guide to the Expression of Uncertainty in Measurement (the 'GUM') and NIST Techrice! Note 1297. The expanded uncertantesik =2) reported here do not contain estimates for (1) any effects that may be introduced by tensportation OF the msirament between ICL and the user's faciy. (2) drift of the instrument. 13) hysteresis ofthe instrument, oF () any measurement Uncertain Introduced By the user.ICL CALIBRATION LABORA TORIES, INC. Report io. 18590! $0: 123456 Gient: SAMPLE CUSTOMER Date repert issued: 08-25:2013 Page 3 of 8 NOTES AND SUPPLEMENTAL INFORMATION All temperotures given inthis report are those defined by the International Temperature Scale of 1990 (ITS-90) TRACEABILITY INFORMATION This caliration ie traceable to NIST through an unbroken chain of comparisons. The reference standard is used to caliirate the transfor Standerd, which in turn s used to callarata the clent's instrument. Every step in the chen is fuly documented, end measurement Lncertainy has been calculated ai each step. ur NIST primary reference thermometer from -196 t0 420C is @ Resemount model 162CE 26.5 Ohm SPRY, serial no. 8058, ‘albroted by NIST on August 17, 2012. NIST GMP.11 recommends 0 36 manth calibration cycle far SPRTs. PRT transfer stondords Sand ASTM hauidin glass tonsfer standards ore calibrated ennually apeinst this SPAT, per NIST GMP17 recommendations. [COMPARATORS USED IN PERFORMANCE OF THIS CALIBRATION Nominal Temp Comparator MTree ‘Manufacturer 0.010°C TPM Maint bath a Hart Sofentific 00°C | GOSoN Sat bath = 239, Hart Soientseie 00°C | GOS0H Gale bath © 240, Hart Soientific 34°C 7361 ale bath 255 Hart Scientific 00° LN comparator 330 Hart Scientific Too" Hw vaune bach 3 Hart Scientific TRANSFER AND CHECK STANDARDS USED IN PERFORMANCE OF THIS CALIBRATION Nominal Temp Transfer Stanctarc ree Manufacturer Next Due Posifon 0.010% TPH cell Ba2427 346 Hart /Piuke 05/23/14 standard 400:000°¢ | $620-35 PRI 0992 252, Hart Selentigte 09/07/14 Standard Se2e-as Per 1208 263 Mart Scientific 09/07/14 Check. standard 2oo.co0% Se28-i5 PRI 0992252 Hart Scientific 09/07/14 Standard’ Se2e-is pet 1208 269 Hart Scientific 09/07/14 Check standard -3e.esecc 5628-15 PRT 1755 306 Hart Scientific 09/07/14 Standard 3628-15 PRE 1751305 Hart Scientific 09/07/14 Check standard s1s6.o00"c | $628-15 PRI 1729307 Mart Scientific 09/07/14 Standard. Seae-as per 1726 308 Hart Scientific 09/07/14 Check. standard o.o1o’c Tp Gell BG2427, B46 Hart/Piuke 05/23/14 Standard THERMOMETER READOUT(S) USED TO READ THIS UUT All readings of this sonsor wore observed using customer's readout s/n: 678910 TECHNICIAN: J. JEFF KELLY ICL CALIBRATION LABORATORIES, INC. \ J WS Ray lt J rea fb Approved by: / waa Reviewed by: £ a ns J eff Ky, Tecnica! Director Karon Mangokd Betorah tt Veber Guaity epuy ‘his roportdocomant was propered by LORI PARR Date coltrated: 09-26-2019 ‘Rocetraton date speci by eflent: September 26, 2014 MST GMP-11 (Mar 03), "Good Measurement Practice for Assignment and Adjustment of Callration Intorvals for Standards cauiions thet “Temperature standerde are dynamic with use. ‘Shock, contarmination and other factors can cause Unit fram accepted values Table 4 of GHP-T recommends recalibration of lauid in-olags thermometers, standard thermistors and PAs at 12 manth laterals, Liguiésngtass thermometers used Yor "Temperature Culical Parameters’ should be recalbrated at 6 manth itervais. NIST GMP-11 is valle for dovnload in Adebe OF format on Our website at www. fellabs.com Follow the ink for Downloads ‘The user should bo aware that any number of factors may cause this instrument to drift out of calitration before the specilied calration interval has expired. This calration report may not be reproduced except in ful without the express written permission of ICL Calibration Laboratories, Inc This report applies only tothe item calibrated. This calibration report shall net be used to claim product endorsement by the A2LA,Report No. W185901 $0: 129456 Ghent: SAMPLE CUSTOMER Date report issued: 09-28-2013 SUPPLEMENTAL INFORMATION ADDENDUM "AS LEFT VAWUES Nomwat TesT — acTuAL TEST READING RESISTANCE, TEMPERATURE TEMPERATURE or uur ‘Onns" 9.o20°c 9.010°¢ o.010°%¢ 100.032 400:000'C —398:995°C — g00:005°C © 249.989 200:000%C + 199:396°¢ = 1991394ec = 177354 S3el34eC © =381834°C = 38183290 842453 -196:000°C | -1356a5°C — -135 652°C ial3ia O:o10°C. 02010°¢ 0:508°¢ = 100030 ‘Measurement uncertainty forthe tempereture values displayed above are found on Page 2 ofthis report ‘he temperature and resistance values provided were obtained using the readout specitied on Page 3 of this report.eb0zisZi6. rea ‘OL6829 us LAN LO6SSLM. ‘ou yedey z00'- S34 990000- ‘o000'0sz seess ere ose roo" S3X9z0000- ‘0s00'002 Lv00' 007 oz Loo 3A z0000 oz66'6r1 zzz66'6bL ost z00'0- S3A _$90000- ‘0400'001, se0o0'oo! 00k 000 S3\ _¥10000- ‘9966'67 97866 6 0s L000 S3k £0000 2960°6 11656'6 on ‘9 sBap ‘foeinaoe swuio eT sypuned sy swyo ‘uode: ——eouejisous uojeda §—geouesoo, ul “eousaYIC ‘inn sul [eoUloy senjen ——[eUILON 02000 8100 osz 200% 1 ‘Sul "SaUdJesOge] UOREIQ'IED 191) Lv00'0 zL00 dt 2007 Lv seo00 6000 eet 001 Ly PaulWuayep ueeq jou} £z00'0 900'0 ool 30 Lv ‘se4 e}ep sitp Jo} AuleueouN juewainseay “Aju ASeUNCO|| 9100°0 ‘7000 18 ‘90S: LY 24} 0} papinord 51 jeaysyi0%m si. 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