B NNG NGHIP

V PHT TRIN NNG

THN

CNG HA X HI CH NGHA VIT NAM

c lp - T do - Hnh phc

DANH MC PHP TH

Ch nh b sung php th cho Phng th nghim thuc

Trung tm Kim nghim Thuc th y Trung ng I
(Ban hnh km theo Quyt nh s 1897 /Q-BNN-KHCN ngy 10 thng 8
nm 2012 ca B trng Nng Nng nghip v PTNT)
STT

Tn php th

i tng
php th

Gii hn pht
hin /Phm vi
o (nu c)

Phng php th

Lnh vc Thuc th y

1. Kim nghim hm lng nhm

-lactam v Cephalosporine
(Amoxicilline, Ampicilline,
Cephalexin, Ceftiofur,
Cephalothin, Cloxacillin,
Penicillin)

Thc n chn
nui

10 ppb

AOAC 979.14;
982.16;

2. Kim nghim hm lng nhm

Tetracycline
(Chlotetracylin, Doxycyclin,
Tetracyclin, Oxytetracyclin)

Thc n chn
nui

10 ppb

AOAC 995.09

3. Kim nghim hm lng nhm

Fenicol (Chloramphenicol,
Florfenicol, Thiamphenicol)

Thc n chn
nui

0,1 ppb

ISO 13493
FDA LIB # 4306,
2003

4. Kim nghim hm lng nhm

Quinolone (Danofloxacin,
Flumequine, Marbofloxacin,
Enrofloxacin, Norfloxacin,
Difloxacin, Ciprofloxacin,
Ofloxacin)

Thc n chn
nui

0.6 ppb

FDA LIB # 4298,

2003

5. Kim nghim hm lng

nhm Sulfamide (Sulfadiazin,
Sulfadimidin, Sulfaguanidin,
Sulfamethoxazol,
Sulfamethoxypirydazin,
Sulfaquinoxalin,
Sulfachloropyrazin,
Sulfachloropyridazin,
Sulfaclozin, Sulfamethoxin,
Trimethoprim, Omethoprim)

Thc n chn
nui

10 ppb

AOAC 993.32
DVN4
BP2007

STT

Tn php th

i tng
php th

Gii hn pht
hin /Phm vi
o (nu c)

Phng php th

6. Kim nghim hm lng vitamin

A, vitamin D3, vitamin E

Thc n chn
nui

10 ppm

AOAC 992.03;
992.06;

7. Kim nghim hm lng vitamin

nhm B tan trong nc (Vitamin
B1, Vitamin B2, Vitamin B6,
Vitamin PP, Vitamin C)

Thc n chn
nui

100 ppm

DVN4

8. Kim nghi m hm lng nhm

acid amin (Methionine, Lysin,
Leucin, Isoleusin, Arginin,
Histidin, Phenylalanin,
Trytophan, Tyrosin, Valin)

Thc n chn
nui

1 ppm

AOAC 2005,
Ch4,p.8-24

Thc n chn
nui

0,01%

AOAC 2005.
Ch.33.p.28

HC dng trong
thy sn

0,01%

Tiu chun c s

Thc n chn
nui

1ppm

J. AOAC Internationa
l, 78(2), 343-352

1ppm

AOAC 967.40.
AOAC 967.40
Journal of
Pharmaceutical and
Biomedical Analysis
40 (2006) 981986

Thc n chn
nui

1ppm

AOAC
INTERNATIONAL
VOL. 83, NO. 6,
2000

14. Kim nghi m hm lng

erythromycin

Thc n chn
nui

0,01 ppm

AOAC2005., Ch5,
p.48

15. Kim nghi m hm lng tylosin

tatrate , tylosin photphat

Thc n chn
nui

0,1 ppm

AOAC 975.09

16. Kim nghi m hm lng

roxasone

Thc n chn
nui

0,1 ppm

AOAC 971.47

17. Xac inh hm lng khoang

cht:
- Nhm kim loai n ng: Thy
ngn (Hg), Ch (Pb), Cadimi
(Cd), Asen (As)
- Nhm kim loai kim th: Ca;
Mg; Bo
- Nhm khac: Natri (Na), Kali
(K) tng v Kali hu hi u, ng

Thc n chn
nui

0,1 ppb- 0,5

ppm

Ha cht dng
trong nui trng
thy sn

0,1 ppb- 0,5

ppm

As: TCVN 957.22

Pb:TCVN 7602-2007
Hg:TCVN 7604-2007
Cd:TCVN 7603-2007

9. Kim nghim hm lng nhm

acid hu c (acetic acid, citric
acid, formic acid, fumaric acid,
15lactic acid, malic acid,
propionic acid)
11. Kim nghim hm lng colistin
12. Kim nghim hm lng
Lincomycin

Thc n chn
nui

13. Kim nghim hm lng

Tiamulin

Nc v iu
ki n mi
trng
2

0,1 ppb- 0,5

ppm

SMEWW 3500 :
2005

STT

Tn php th

(Cu), Km (Zn), St (Fe),

Mangan (Mn), Niken (Ni),
20. Xac inh hm lng tro th

i tng
php th

Gii hn pht
hin /Phm vi
o (nu c)

Thc n
chn nui

Phng php th

TCVN 4327:2007
ISO 5984

21. Xac inh hm lng x th

Thc n
chn nui

0,01%

TCVN 4329:2007
ISO 6865:2001

22. Xac inh hm lng NaCl

Thc n
chn nui

0,001%

TCVN 4806:2007

23. Xac inh hm lng cht beo

Thc n
chn nui

24. Xac inh m v hm lng

cht bay hi khac

Thc n
chn nui

1 mg / 100 g

TCVN 4326:2001

Thuc thu y

10ppb

Tiu chun c s
(GCMS)

26. Xac inh hm lng Phospho,

P2O5 tng s

Thc n chn
nui

0, 62 ppm

TCVN 1525:2001

27. Xac inh hm lng Nit tng

s

Thc n chn
nui

1 mg/ 100g

TCVN 4328:2001

28. Xac inh hm lng Arsanilic

acid

Thc n
chn nui

0,1 ppm

AOAC 954.17

29. Xac inh hm lng Bacitracin

Zinc

Thc n
chn nui

0,1 ppm

30. Xac inh hm lng Amprolium

Thc n
chn nui

0,1 ppm

31. Xac inh hm lng Tylosin

Thc n
chn nui

0,04 ppm

25. Xac inh hm lng -agonist

Clenbuterol, Salbutamol,
Ractopamin

32.

AOAC 920.39

Xac inh hm lng

Aflatoxin tng s

Thc n
chn nui

Aflatoxin B1

Thc n
chn nui

0, 1 ppb

Thc n
chn nui

0,01 ppm

34.
Xac inh hm lng Zoalene

AOAC 982.44
AOAC 961.24
AOAC 962.26
TCVN 7596-2007

0, 1 ppb
TCVN 6953-2001
AOAC 961.26
EN 15792:2009

STT

Tn php th

i tng
php th

Gii hn pht
hin /Phm vi
o (nu c)

Phng php th

35. Xac inh hm lng

Salinomycin

Thc n
chn nui

0,01 ppm

36. Xac inh hm lng Monensin,

Narasin

Thc n
chn nui

0,01 ppm

37. Xac inh hm lng Roxarsone

Thc n
chn nui

0,01 ppm

38. Xac inh hm lng

Sulfadimethoxin v Ormetoprim

Thc n
chn nui

0,02 ppm

39. Xac inh hm lng Clopidol

Thc n
chn nui

0,1 ppm

40. Xac inh hm lng Nitrofural

v cac dn xut

Thc n chn
nui

0,5 ppb

ISO 14797:1999

41. Xac inh hm lng sodium

thiosulfate

Ha cht dng
trong nui trng
thy sn

0,01%

DVN4

42. Kim nghi m cac chi tiu v t ly

(pH, ty trong, m)

Nc v iu
kin mi trng

43. Xac inh hm lng saponin

Ha cht dng
trong nui trng
thy sn

0,01%

DVN4

44. Xac inh hm lng oxygen

hoat tnh

Ha cht dng
trong nui trng
thy sn

0,01%

AOAC 973.45

45. Xac inh hm lng chlorine

hoat tnh

Ha cht dng
trong nui trng
thy sn

0,01%

TCVN 6225-3:2011
DVN II
DTQ 2005

46. Xac inh hm lng sodium

lauryl sulfate

Ha cht dng
trong nui trng
thy sn

0,01%

AOAC 968.18

Ha cht dng
trong nui trng
thy sn

0,01%

BP 2007

48. Xac inh cng

Nc v nc
thi

1 ppm

SMEWW 2340 C :
2005

49. Xac inh hm lng H2S, Flo

(F), Clo d (Cl2), Cloride (Cl-),
Phospho tng (P), Phosphate
(PO43-), Sulfat (SO42-), Nitrat

Nc v nc
thi

47. Xac inh hm lng

benzalkonium, myristal
benzalkonium chloride,
tetradecyl trimethyl ammonium
bromide

ISO 14183:2005
ISO 14183:2005
AOAC 971.47
AOAC 970.88
AOAC 974.45

TCVN 6492 : 1999

1 ppm

SMEWW 4500 :
2005

STT

Tn php th

i tng
php th

Gii hn pht
hin /Phm vi
o (nu c)

Phng php th

(NO3-)
50. Xac inh hm lng Nit tng

Nc v nc
thi

1 mg/100ml

51. Xac inh hm lng Nitrit

(NO2-)

Nc v nc
thi

0,2 ppm

52. Xac inh hm lng Carbonate

(CO32-)

Nc v nc
thi

1 ppm

53. Xac inh hm lng Sulfua (S2-)

Nc v nc
thi

2 ppm

54. Xac inh hm lng tng carbon

hu c TOC

Nc v nc
thi

1 ppm

55. Kim nghim vc xin Gan thn

m (Edwardsiella ictaluri) trn
ca
56. Kim nghim vc xin
Streptococcus trn ca diu hng
II

TCVN 5987 : 1995

TCVN 6178 1996
AOAC 920.194
SMEWW 2320 B
TCVN 4567 : 1988

TCVN 6634 : 2000

Thuc thu y

Tiu chun c s

Thuc thu y

Tiu chun c s

Thc n chn
nui v sn
phm thit

TCVN 8730:2011

Lnh vc Vi sinh v t
57.

Xac inh tng s vi khun

Lactobacillus sp
Lactobacillus acidophilus

59.
Xac inh tng s vi khun hiu
kh

Thuc thu y
Thc n chn
nui v sn
phm thit

TCVN 5165-90

Thuc thu y
61.
Xac inh tng s nm men, nm
mc

Thc n chn
nui v sn
phm thit

TCVN 5166-1990

Thuc thu y
63. Xac inh tng s vi khun
Bacillus sp
Bacillus subtilis
Bacillus cereus..

Thc n chn
nui v sn
phm thit

65.

Thc n chn
nui v sn
phm thit

Xac inh vi khun Salmonella

TCVN 8736:2011

Thuc thu y
TCVN 4829-05

Thuc thu y
67. Xac inh vi khun E.coli

Thc n chn
nui v sn
5

TCVN 6848-07

STT

Tn php th

i tng
php th

Gii hn pht
hin /Phm vi
o (nu c)

Phng php th

phm thit
Thuc thu y
69.

Xac inh vi khun

Rhodopseudomonas sp

70.
Xac inh vi khun coliform

Thc n chn
nui v sn
phm thit

TCCS

Thc n chn
nui v sn
phm thit

TCVN 4882-07

Thuc thu y
72.
Xac inh vi khun
Staphyloccocus aureus

Thc n chn
nui v sn
phm thit

TCVN 5156-90

Thuc thu y
74.
Xac inh vi khun
Campylobacter sp

Thc n chn
nui v sn
phm thit
Thuc thu y

ISO 10272 -1:2006