Scribd Logo
Upload

Welcome to Scribd!

  • Lamda Maks Standar + H2SO4: Analisis Crom (VI) Dengan Asam Sulfat

    Uploaded by

    aninnnn
    5 views8 pages
    This document discusses the analysis of chromium (VI) and phosphorus using UV-Vis spectroscopy. It determines the optimal wavelengths for chromium standards using sulfuric acid and hydrochloric acid. Calibration curves were constructed for chromium and phosphorus that showed good linearity. The effect of chromium (III) on the chromium (VI) analysis was also examined, showing little interference. Finally, the stability of the phosphorus complex over time was analyzed through monitoring its absorption over 60 minutes.

    Original Description:

    Original Title

    Analisis Crom.docx

    Copyright

    © © All Rights Reserved

    Available Formats

    DOCX, PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    This document discusses the analysis of chromium (VI) and phosphorus using UV-Vis spectroscopy. It determines the optimal wavelengths for chromium standards using sulfuric acid and hydrochloric acid. Calibration curves were constructed for chromium and phosphorus that showed good linearity. The effect of chromium (III) on the chromium (VI) analysis was also examined, showing little interference. Finally, the stability of the phosphorus complex over time was analyzed through monitoring its absorption over 60 minutes.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    5 views8 pages

    Lamda Maks Standar + H2SO4: Analisis Crom (VI) Dengan Asam Sulfat

    Uploaded by

    aninnnn
    This document discusses the analysis of chromium (VI) and phosphorus using UV-Vis spectroscopy. It determines the optimal wavelengths for chromium standards using sulfuric acid and hydrochloric acid. Calibration curves were constructed for chromium and phosphorus that showed good linearity. The effect of chromium (III) on the chromium (VI) analysis was also examined, showing little interference. Finally, the stability of the phosphorus complex over time was analyzed through monitoring its absorption over 60 minutes.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 8

    Analisis Crom (VI) dengan asam sulfat

    - Penentuan panjang gelombang optimal


    Kurva Kalibrasi larutan standar
    Lamd
    a
    500
    505
    510
    515
    520
    525
    530
    535
    540
    545
    550
    555
    560
    565
    570

    A
    0,081
    0,092
    0,1
    0,105
    0,116
    0,123
    0,129
    0,133
    0,132
    0,131
    0,132
    0,126
    0,122
    0,113
    0,104

    C
    (ppm)
    0

    0,1

    0,058

    0,2

    0,105

    0,3

    0,141

    0,4

    0,188

    0,5

    0,213

    Lamda Maks Standar + H2SO4


    0.15
    0.1
    A

    0.05
    0
    490

    500

    510

    520

    530

    540

    lamda

    550

    560

    570

    580

    Kurva Standar + H2SO4


    0.25
    0.2 f(x) = 0.43x + 0.01
    R = 0.99
    0.15
    A

    0.1
    0.05
    0
    0

    0.1

    0.2

    0.3

    0.4

    0.5

    0.6

    C (ppm)

    Analisis Crom (VI) dengan asam klorida


    - Penentuan panjang gelombang optimal
    larutan standar
    Lamd
    a
    500
    505
    510
    515
    520
    525
    530
    535
    540
    545
    550
    555
    560
    565
    570

    A
    0,08
    0,089
    0,098
    0,105
    0,112
    0,119
    0,124
    0,127
    0,131
    0,128
    0,127
    0,122
    0,117
    0,111
    0,103

    Kurva Kalibrasi

    C
    (ppm)
    0
    0,1
    0,2
    0,3
    0,4
    0,5

    A
    0
    0,063
    0,101
    0,13
    0,157
    0,181

    Lamda Maks + HCl


    0.15
    0.1
    A
    0.05
    0
    490

    500

    510

    520

    530

    540

    550

    560

    570

    580

    Lamda

    Kurva Standal + HCl


    0.2
    f(x) = 0.35x + 0.02
    0.15 R = 0.96
    A

    0.1
    0.05
    0
    0

    0.1

    0.2

    0.3

    0.4

    C (ppm)

    Penentuan Pengaruh Cr (III)

    C
    (ppm)
    0

    A
    0,141

    0,152

    0,155

    10

    0,151

    15

    0,153

    0.5

    0.6

    Grafik Uji Cr (III)


    0.16
    0.16
    0.15
    A 0.15
    0.14
    0.14
    0.13
    0

    10

    C (ppm)

    Analisis Fosfor
    - Penentuan Waktu Kestabilan Kompleks
    Waktu
    (menit)
    10
    15
    20
    25
    30

    A
    0,2560
    0,2549
    0,2536
    0,2529
    0,2518

    12

    14

    16

    35
    40
    45
    50
    55
    60

    0,2504
    0,2497
    0,2478
    0,2449
    0,2464
    0,2489

    Kurva waktu kestabilan kompleks


    0.26
    0.26
    0.25
    A

    0.25
    0.24
    0.24
    0

    10

    20

    30

    40

    t (menit)

    Kurva Kalibrasi

    C
    (ppm)
    0
    2
    4

    A
    0,002
    0,0887
    0,1921

    50

    60

    70

    6
    8
    10

    C
    A
    0,2558 (ppm)
    0
    0
    0,3472
    2 0,0867
    0,4232
    4 0,1901
    6 0,2538
    8 0,3452
    10 0,4212

    Kurva kalibrasi P
    0.45
    0.4 f(x) = 0.04x + 0.01
    0.35 R = 1
    0.3
    0.25
    A 0.2
    0.15
    0.1
    0.05
    0
    0
    2
    4

    6
    C (ppm)

    10

    12

    Lamda Maks + HCl


    0.15
    0.1
    A

    0.05
    0
    490 500 510 520 530 540 550 560 570 580
    Lamda

    Lamda Maks Standar + H2SO4


    0.15
    0.1
    A

    0.05
    0
    490 500 510 520 530 540 550 560 570 580
    lamda

    Grafik Uji Cr (III)


    0.16
    0.15
    A

    0.14
    0.13
    0

    C (ppm)

    10

    12

    14

    16

    Kurva waktu kestabilan kompleks


    0.26
    0.26
    0.25
    A 0.25
    0.24
    0.24
    0

    10

    20

    30

    40

    t (menit)

    50

    60

    70

    You might also like