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    APM-7

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
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    241 views26 pages

    Manual Equipo Flash Point APM-7

    Uploaded by

    Alberto Salud Sarabia
    APM-7

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
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    Pensky-Martens Closed Cup Automatic Flash Point Tester Model APM-7 with Data Memory Instruction Manual Rev.3.2F-$ 050711 IMPORTANT: *This Manual contains important technical information as wall as safety information, *Read this Manual thoroughly before use, and cep it for later u: TANAKA SCIENTIFIC LIMITED FORWARD... INTENDED READER OF THIS MANUAL «s+... REVISIONS .sccssssseoe SAFE OPERATION ...... WARNING 1, Overview of Model APM-7 2. Installation ....... 2.1 Installation Site 2.2 Electric Connections ssssssse 2.3 Gas Connection 3. Operation ... 3.1 Power ON . 3.2 Entering a Barometr 3.3 Select Test Procedure and Mode.. 1 ASTM Mode 10 3.3.3 User’s Custom Mode ...... seevoe 0 10 3.4 Test Procedure in ASTM Mode 3.4.1 Setting of Expected Flash Point .. 3.4.2 Preparation of Test Cup and Sample 3.4.3 Test Start vsssoossscesceceeeeseersnnsnnne 3.44 Start of Ignition Source Application 3.4.5 Flash Detection 3.4.6 Completion of a Test 3.5 Test by Special Mode .. 4, Data Storage Function ..... 5. In Case of Abnormal Operation or Trouble 6. Safety esse 6.1 Gas Piping (When Gas Ignition is used) 6.2 Prevention of Sample from Catching Fire ....sssssssssssees 7. Post-sales Servicing ......ss 8, Precaution in Case of Loss of Instruction Manual . g This Tester ... 9, Caution when Transfer: 10. Specifications ......osse0 FOREWORD ‘Thank you for purchasing model APM-7. ‘This Instruction Manual includes necessary information for the installation/operation of APM-7. Please read this Manual thoroughly to understand the contents before installation and operation. While all our products have been adjusted and inspected to our specification prior to shipment, should any quality or specification concer arise, please contact Tanaka or its authorized distributor. INTENDED READER OF THIS MANUAL This Manual has been intended to be read and understood by all those who operate APM-7. Also, itis assumed that the user have knowledge of handling of dangerous goods as ‘well as related industrial standard such as ASTM. REVISIONS ‘The contents of this Manual may be subject to change without prior notice. SAFE OPERATION ‘The following nomenclature to indicate the safety precaution have been used in this Manual, AXWARNING : Indicates a potentially hazardous situation which, if not avoided, could result in death or serious bodily injury. AXCAUTION : Indicates a potentially hazardous situation which, ifnot avoided, may result in minor or moderate bodily injury and/or property damages. And also the WARNING LABELS are put on the body of APM-7. The meaning of these labels is as follows. Z\ : GENERAL WARNIN A : HOT Z\ WARNING Installation Site: Install the Tester on a solid horizontal work bench with a provision of ventilation Nearby or inside a fume hood. The Tester needs to be placed at least 20cm away from other objects ‘Ambient temperature to be 10-30°C and humidity to be less than 90% (no condensation), Power Source Voltage: ‘Supply a specified power source voltage. Turn the power on after all electric connection are made, Alteration: Do not make any modification to the Tester, in whole or a part, or add any unauthorized accessories to the Tester without prior consent by Tanaka Scientific Limited(hereinafter referred to as Tanaka). We can not take any responsibilities for damages, including but not limited to property and/or bodily damages, associated with the alteration of Tester. Maintenance: Any repair on the Tester should be made by an authorized service technician appointed by Tanaka. For consumable, use only Tanaka genuine parts. Use of This Tester for Other Purposes: Use this Tester solely for its intended use of performing determination of the flash point of petroleum products subscribed in such test standard as ISO 2719, ASTM D983 and IP 34. Unattended Operation: The specimen may catch a fire and blaze up. For the safety, itis essential that at least one trained personnel be present in your test room, lab, etc. when testing. In Case of abnormality: Should any abnormality including abnormal noise or movement be observed, tum the power off and contact Tanaka or its authorized distributor. 1. Overview of Model APM-7 Heater Output Indicator lest ignitor Test Cover Electric Ipnitor Release Buon Tein Needle Valve for Test Flame Test Flame ‘Temperature a Sensor Display Panel Sheet Switeh Windscreen Flame Size Comparison Bead Stove Section MAIN Switeh (Heit a (eat Noni ed Control Unit Fig. 1 External View of Model APM-7 MAIN Switch: Used for switching power source to the Tester. Panel Sheet Switch: Consists of START, COOL, RESET switches as well as switches for changing test parameters, Display: splays test status and result as well as test parameters Flash Detector: Detects flash by monitoring the change in temperature before and after the ignition source application. ‘Temperature Sensor: Senses specimen temperature, Needle Valve for Test Flame: Adjusts test flame size. Windscreen: Shields to insure flame integrity during test. Test Cover Release Button: Release from lock of arm. Arm: Lift this arm up and hold the handle when you set the test cup. Heater Output Indicator: Blinks when the heater is tuned on. Electric Ignitor Terminal: Push the center of this termi nal to release the Electric Ignitor wires. Electric Ignitor: Ignitor uses a platinum coil, It will be as a pilot when “Ges ignition model”, and as a Ignition source when “Electric ignition model”, Stove Sect Houses the heater block assembly for specimen heating inside. Thermofuse: Detects blaze up of specimen, Flame Size Comparison Bead: Adjust the test-flame to-the size of this bead- ott @ 2 pP at) ¥ ae i e119) 5869 9 Geb ft @ © Mm ® o Fig. 2 Operation Panel and Display of Control Unit (2) Fluorescent Displa Displays test mode, specimen temperature, flash point (when blinking), expected flash point, trouble message, etc... Q) RUN Lamp: Illuminates when a test process is in progress, @) COOL Lamp: Illuminates when cooling, (4) MODE Switch: ‘Changes the test mode, (5) START Switch: Starts a test, (© COOL/WARM Switch: This key have only function of cool, used for manual cooling (1) RESET Switch: Used for returning stand-by status. (e.g. stopping a test, stopping a cooling) (8) CHECK Switch: Used for manually applying the ignition source. (0) Left-Right Keys: Used for moving cursor. (10) Up-Down Keys: Used for increasing/decreasing numeric figures. ‘1 FUNCTION Key: Used for changing screen, 2. Installation 2.1 Installation Site Install the Tester on a draft-free, level and stable table. The Tester needs to be placed at least 20em away from other objects. ‘The following locations should be avoided as the installation site: ~ An area with high temperature and/or high humidity ~ An area exposed to direct the sun ~ An area with poor ventilation and/or dusty air ~ An area subject to rapid changes in ambient temperature 2.2 Electric Connections (Fig. 3) ‘A, | WARNING | To prevent electric shock hazard, be sure the groun connected. Do not ground to gas pipe; fire or explosion may result. The grounding wire may be connected to one of the following: - The ground terminal of the power outlet - Copper wire buried at least 6Sem deep in the earth - Metallic water pipe line appropriate for use as electric grounding 2 Wi (1)Confirm the voltage of the serial number label located left side of Control Unit ‘and your electrie source. (2)Connect the Control Unit and the Test Unit with Signal Connecting Cable. (3)Connect the power connecting cable of Control Unit to the Test Unit, (4)Plug in the AC power code of the Control Unit to an electric outlet. Be sure to get ‘grounding to prevent an accident. 2.3 Gas Connection (When Gas Ignition is Used) A, [WARNING | The maximum gas pressure should be lower than 9.8 kPa. Using the rubber hose supplied for gas, connect the gas source (LP gas or Natural gas) and the gas inlet nipple on the rear panel of the Test Unit. Then fasten both ends with hose bands. See Fig. 3. ‘The APM-7 is shipping os “Gas Ignition Configuration’, if the customer want to change ignition source, please see APM-7 maintenance manual Control Unit RS-232C Connector Power Connecting Cable AC Power Cond — Fig. 3 Rear View and Electric Connection > Signal Connecting Coble Oat caste AC Outlet ©O© 3. Operation 3.1 Power ON ‘Turn the MAIN switch ON. A message sereen as illustrated in Fig. 4 appears on the control Unit display. Model Type Ignition Source (appear when electric configuration only) APM TEMP EXP. FP aay |__ Expected Electric 2207-ernt 23.4 Procedure & Mode Specimen Temperature Fig. 4 Main Sereen 3.2 Entering a Barometric Pressure Value (not necessary when buil sensor is equipped) APM-7 is capable of making automatic correction for barometric pressure by entering the barometric pressure reading through the control panel. Enter the barometric pressure before a flash point test starts as follows: (1) Press FUNCTION key, The display shows Baro set screen as illustrated in Fi appears. (If the temperature unit is selected °F, (mmHg) will appear instead of (hPa). (2) Press Left or Right key to appear the cursor under the barometric pressure value, G) Enter the barometric pressure reading that was obtained from a calibrated barometer using the four arrow keys (Left-Right, Up-Down keys). in pressure APM Baro set (hPa) 1013 Prev. FP 137.0 Fig. 5 Barometric Pressure Entering Screen 3.3 Select Test Procedure and Mode APM-7 has 6 kinds of test mode. ASTM A mode, ASTM B. ‘mode, Special A mode, Special B mode, User's Custom and Simulated TAG mode. Each of B modes, User's Custom and Simulated TAG mode are invalid when shipping. (See APM-7 Maintenance Manual.) Press the MODE switch to select test procedure and mode. Display Provedure & Mode AR ASTM A mode -B- ASTM B mode =A ‘ASTM A Special (Fast Search) SPE mode ~B- ‘ASTM B Special (Fast Search) SPE mode User User’s Custom mode [___ S_TAG Simulated TAG mode 3.3.1 ASTM Mode In this mode, the test proceeds until flash detection in accordance with ASTM D93. Select procedure A or B. 3.3.2 Special Mode This mode is used for measuring the approximate flash point of a sample of unknown expected flash point. This mode is more quickly than the method of prescribed in ASTM D93. With a faster temperature rise speed, the mode starts the ignition source application from the test start. This is different from the ASTM mode. 3.33 User’s Custom Mode In this mode, heating rate, stirring speed, application interval and its start temperature can be changed by operator. 3.3.4 Simulated TAG mode ‘The test sequence of this mode is the same as ASTM DS6. The stirrer does not work in this mode. Note that obtained result using this mode may be different from original DS6’s result. 3.4 Test Procedure in ASTM Mode 3.4.1 Setting of Expected Flash Point A | WARNING | The sample may eatch a fire, if'an erroneous expected flash point was set. | ‘The expected flash point is displayed in a three-digit figure below the EXP. F.P on the right end of the display. When altering the expected flash point, press the Right-Left Key to move the cursor, and after that, operate the Up-Down keys, No numeric figures above 370 (700 in °F) can be set. 10 3.4.2 Preparation of Test Cup and Sample A | CAUTION | Do not bend the tip of the flash detector when cleaning test cover. If the tip of the fash detector is bent, sensitivity deteriorates and thus flash detection may be missed. (1) Before using the test cup and the test cover, clean them with suitable solvent and dry them, When cleaning the test cover, use solvent and soft material such as cotton swab. Care should be taken not to damage the tip of the flash detector. (2) When testing samples of very viscous materials and containing dissolved or free water, follow Sampling section of ASTM D93, (3) After pressing the test cover release button (the latch is disengaged), push up the arm handle. ‘The arm will finally stop slightly below the original stopping position. (4) Fill the test cup with the test specimen to the filling mark inside of the test cup. Set the test cup in the stove section, (S) Lift the arm a little above its stopping position and lower the arm gently. Put it on the test cup. By pushing it downward further, the latch is engaged and the test cover is contacted closely to the test cup and secured. Now you have completed the preparation for the test. 3.4.3 Test Start A. | WARNING | Toxic gas may generate as a result of decomposition of specimen in the course of heating. Provide adequate ventilation. Specimen may catch fire in the course of a test. Place a fire extinguisher near the Tester. Also, do not leave the Tester unattended, Press the START switch; RUN lamp illuminates, and the test starts, The expected flash point (#1) and filament output value is displayed for 5 seconds, the ignition coil lights up and specimen heating starts. When gas ignition is used, test flame is ignited by ignition coil automatically. Adjust the test flame to 4mm in diameter (the flame size comparison bead size, see Fig.1) by needle valve. The test proceeds automatically hereafter, “1: The setting of the expected flash point is changeable even during the test. After changing in accordance with Section 3.4.1, re-press the START switch. Also inthis case, the newly set expected flash point appears in the center of the display for 5 seconds. 3.4.4 Start of Ignition Source Application After the test starts, the specimen temperature rises ata rate of $ to 6°C /min (9 to 11 °F /min) in Procedure-A, at 1 to 1.5°C /min (2 to 3 °F /min) in Procedure-B. The ignition source begins to apply when the temperature becomes 22°C (40 °F) (*2) below the expected flash point. After that, the application operation is repeated at each 1°C (2 °F) for an expected flash point at/below 110°C (230 °F), and each 2°C (5 °F) for above 110 °C.230°F). rl *2: Application starting temperature is adjustable, For changing temperature, consult Tanaka authorized distributor, 3.4.5 Flash Detection (1) When the flash is detected, the displayed temperature value (*3, recorded flash point) is locked and then starts flashing, See Fig. 6. At the same time buzzer beeps intermittently for 8 seconds. Furthermore, the solenoid valve for gas is closed, the test flame goes out (when gas ignition is used) and electtic ignitor goes off and the stove section starts cooling down. (The COOL lamp lights up.) Appears when corrected FP is different from observed FP APM — FLASH P EXP. FP Electric BARO CORR 270 270. 5x Flash Point (flashing) Fig. 6 Flash Point is Detected Normally +3: The corrected flash point (Fe) is computed automatically by using the following formula, rounded to the nearest 0.5 °C (1 °F) and then displayed. Fe=C+0.025(1013-K) or Fe=F+0.06(760-P) where Fe: Corrected flash point C : Observed flash point, °C F : Observed flash point, °F K_: Entered (detected) barometric pressure value (hPa) P_: Entered (detected) barometric pressure value (mmHg). Also, if Fe, BARO CORR is shown under FLASH POINT in the display and observed flash point can be seen by pressing FUNCTION key. In case a wrong pressure valuc has been entered, enter the right value and then press FUNCTION key; recalculated flash point will be shown, 1 (2) When a flash point is detected at first application of the ignition source, NG Ist appears right side of flash point. See Fig. 7. In this case, alter the expected flash point and restart the tost, APM — FLASH P EXP. FP Electric 270 248. Oc nese Fig. 7 Flash Point is Detected at First Application ‘When a flash point is detected at a temperature which is greater than 28°C (50 °F) above the temperature of the first application of the ignition source, or when a flash point is detected at a temperature witch is less than 18°C (32 °F) above the temperature of the first application of the ignition source, NG and “Temperature fom the first application of the ignition source” appears right side of flash point. See Fig. 8. In this case, alter the expected flash point and restart the test. APM _ FLASH P EXP. FP Electri 270 278. Oc ns Fig. 8 Flash Point is Detected out of the ASTM range | NG appears (4) If the flash point has not been detected when the safety cut temperature (expected flash point +20°C (+40 °F) or 370°C (700°F)) is reached, the display will be as Fig. 9, indicating the safety cut temperature. ‘Then, the heating will stop to start cooling. APM TROUBLE FLASH POINT > 290°C Temp 300.0 Fig. 9 Safety Cut Sereen 3.4.6 Completion of a Test B ‘A | WARNING | If test cup and test cover are still hot after cooling is finished, do not touch except arm handle without wearing gloves. Be careful when handling the hot specimen, It may flash or explode, if you disposed it to waste tank containing waste with low flash point. The cooling fan stops (the COOL lamp goes off) in 10 minutes (*4) after the flame detection. One cycle of a testis completed at this moment and you can start the next test. When further cooling is required, press the COOL switch. Cooling is available for another 10 minutes (*4). The temperature display (flash point) is held until the RESET or START switch is pressed. *4: Cooling time is adjustable. For changing cooling time, consult Tanaka authorized distributor. 3.5 Test by Special (Fast Search) Mode ‘This mode is used for measuring an approximate flash point of a specimen of unknown expected flash point. With a faster temperature rise speed, the mode starts the ignition source application from the test start Other than the temperature rise speed and the ignition source application, all the rest of the test procedure is the same as the standard ASTM test mode’s. ‘The following shows only differences from ASTM mode. See Section 3.4.1 to 3.4.6 also. (1) The temperature rises at 14 o 17°C /min (25 to 30°F /min) in Procedure-A, at 6.5 to 7.5°C /min (12 to 14°F /min) in Procedure-B up to 50°C (90 °F) below the expected flash point, and after that, at 5 to 6°C /min (9 t0 11°F /min) in Procedure-A, at 1 to 1.5°C /min (2 to 3 °F /min) in Procedure-B. (2) Immediately after the test starts, the ignition source application starts at each 1°C (2 °F) (incase the expected flash at/below 110°C (230°F)) or 2°C (5 °F) (above 110°C (230 °F)). 4. Data Storage Function (use this function with optional Built-in Clock Board) APM-7 has a data storage function. Up to 50 successive data can be memorized. (#5) After APM-7 detects a flash point, the data will be stored automatically. If Built-in Clock Board is not installed, actual date will not be memorized in DATE column. The recalling procedure is as follows. Press the MODE switch and RESET switch, then consecutively release the RESET switch and then the MODE switch. The following screen will appear: APM DATE SAMPLE ID FLASH. P 01 (New Data) 02 t 03 (Old Data) Fig. 8 Data Recall Screen By pressing Up-Down key, the screen will be setolled. Ifneeded, press FUNCTION key to print out all data, (when optional printer is, connected) *5: Following data will not be stored, = used special mode, simulated TAG mode and user custom mode = flash is detected at first application is detected by manual application is detected at a temperature which is greater than 28°C (50°F) above the temperature of the first application of the ignition source, or when a flash point is detected at a temperature witch is less than 18°C (32 °F) above the temperature of the first application of the ignition source. ' 5, In Case of Abnormal Operation or Trouble | A | CAUTION | If even a “minor” abnormality is detected, stop using the Tester immediately and consult Tanaka authorized distributor. When a problem occurs on the Tester, a buzzer will sound and one of the trouble messages in Tab. 1 will be shown. When one of these events occurs, all outputs will be shut off. For troubleshooting, consult Tanaka authorized distributor. Tab. 1 Trouble Messages Trouble, [_ Message on Display Control computer nae runs away ‘Temperature sensor TROUBLE | Beeps intermittently for is found defective TEMP SENSOR eight (8) seconds Flash detector is TROUBLE | Beeps intermittently for found defective FLASH DETECTOR ight (8) seconds i Flash detector detects TROUBLE _| Beeps intermittently for | “Fire” FIRE? (by detector) | eight (8) seconds | Electric ignitor is TROUBLE | Beeps intermittently for i found defective FILAMENT BREAK _ | eight (8) seconds | Built-in battery has TROUBLE Beeps intermittently for | expired REPLACE BATTERY _| cight (8) seconds ‘Arm is not set in TROUBLE __| Beeps intermittently for | place ARM POSITION | eight (8) seconds | Stirring motor is TROUBLE Beeps intermittently for stopped (*6) MOTOR OVERLOAD _| eight (8) seconds ‘Thermofuse is blown TROUBLE Beeps big sound THERMOFUSE BLOWN | continuously *6: When this trouble occurs, press START switch while this trouble mess in the display. Specimen will be heated without stitting, This function is useful to be lower the viscosity of specimen. 6. Safety 6.1 Gas Piping (When Gas Ignition is used) Gas piping inside the Test Unit is made of nylon tube; outside, viton tube. Gas is very dangerous if it leaks. Consult the Tanaka authorized distributor for periodical gas leakage check. THE TESTER IS NOT EQUIPPED WITH A GAS LEAKAGE, DETECTOR. 6.2 Prevention of Sample from Catching Fire In case the temperature at which the first test flame application is made is above the fire point of the specimen, there is a danger: the specimen catches a fire to blaze up. fe So.as to prevent such a danger in advance, for testing a sample of unknown flash point, use the Special mode in Section 3.8. Be sure to arrange at least one proper person in your test room, lab, etc., when testing, to cope with possible accidents. 7. Post-sales Servicing For ordering consumable items or parts or to request servicing, please contact Tanaka, authorized distributor. Please note that spare parts that are necessary to maintain/regain the function of this ‘Tester is kept in inventory for a minimum of 5 years after the delivery of this Tester. 8, Precaution in Case of Loss of Instruction Manual The Instruction Manual is a part of this instrument. In case itis lost, please request a new copy to Tanaka authorized distributor. Allso, itis highly recommended that the address and telephone number of Tanaka and/or its authorized distributor be kept separately from this Manual. 9, Caution when Transferring This Tester If this Tester is transferred or sold to a third party, please inform Tanaka or its authorized distributor. Wrong source voltage and/or AC frequency could cause damages or malfunctioning, In case of transferring this Tester, make sure to attach this Instruction Manual. 10, Specifications (1) Conforming standard: ISO 2719, ASTM D93, IP 34 (2) Measuring Range: Ambient to 370°C (700 °F) (3) Test Modes: ASTM D93 (ISO 2719, IP 34) A + B, Special (Fast Search), Simulated TAG (Optional), User’s Custom (Optional) (4) Display: Fluorescent display tube (VFD module) (5) Temperature Sensor: PT-100 in stainless steel sheath (6) Flash Detector: CRC Thermocouple (7) Heater: Band type heater 400W@100V or 400w@220V (8) _ Ignition Source: Gas ignition with automatic lighting or electric ignition, Interchangeable (9) Cooling Device: Forced air cooling by siroceo fan (10) Barometric Correction: By entering the barometric pressure reading through the control panel, or by optional barometric pressure sensor (11) Safety Mechanism: Automatically shuts off and the problem is reported by buzzer and display in case: (a) EFP+20°C (+40 °F) or 370°C (700 °F) is reached, (b) temperature sensor is found defective, ©) flash detector is found defective, (@) thermofuse is blown, (©) electric ignitor is blown, (D stirring motor is stopped, (g) built-in battery has expired, (h) test cover is not set im place; or ( control computer runs away (buzzer only) W a2 as) aa (sy 16) (7) Dimensions & Weight: Control unit: 230W x 455D x LOH(mm), 6.0kg Test Unit: 230W x 480D x 275H(mm), 18.0kg Installation Site: Ambient temperature: 10-30°C (50-86 °F) Humidity: less than 90% Utility: Power Supply: AC100/120V or 220/240V, 50/60FIz (set atthe factory), 0.7kW (max.) Gas Supply (When Gas ignition is used): LP gas or natural gas (Max. pressure<9.8kPa) Standard Accessories: Description ‘Test Cup Assembly Power Connecting Cable, 0.6m Ipe ‘Signal Connecting Cable, 0.6m Ipe AC Power Cord, 2.5m (

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