A

1
2
3

LD.1 Perhitungan Densitas, Viskositas, dan Kadar Formaldehid Bebas

5 Berat piknometer kosong
6 Berat piknometer + air
7 Volume sampel
8 Densitas air
9 Molaritas HCl
10 Volume titrasi blanko
11 Berat air
4

13.8 gram
18.6 gram
5 ml
0.99568 g/ml
0.7 N
0 ml
4.78 gram

12
13
14
15
16
17
18
19
20
21

No
0
1
2
3
4
5
6

Waktu
(menit)
0
0
8
16
24
32
40

Berat piknometer + Sampel

(gram)
19.54
20.53
19.54
18.88
19.06
19.46
19.69

Berat Sampel
(gram)
5.77
6.76
5.77
5.11
5.29
5.69
5.92

22
23
24

LD.2 Perhitungan Konstanta Reaksi dan Orde Reaksi

Massa urea
27 Massa formaldehid
28 Volume formaldehid
29 BM formaldehid
25
26

61.52175 gram
82.029 gram
200 ml
30.02 g/mol

Densitas
(g/ml)
1.2019
1.4081
1.2019
1.0644
1.1019
1.1852
1.2331

pH
10
10
10
10
10
10
10

BM urea
Formaldehid (A) : Urea (B)
32 Mol B : Mol A
33 CA0

31

34

60.06 g/mol
8:6

30

CB0

3/ 8
13.66

5.12

35
36
37
38
39
40
41
42
43
44
45
46

No
0
1
2
3
4
5
6

Waktu

Kadar Formaldehid

(menit)
0
0
8
16
24
32
40

Bebas
4.2000
3.3600
3.1500
2.9400
2.5200
2.5200
2.5200

CA
(M)
0.6995
0.5596
0.5247
0.4897
0.4197
0.4197
0.4197
JUMLAH

CB
(M)
0.2622
0.2098
0.1967
0.1836
0.1573
0.1573
0.1573

XA
0.9488
0.9590
0.9616
0.9642
0.9693
0.9693
0.9693

LAMPIRAN D
HASIL PROGRAM KOMPUTER

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29

Volume HCl
(ml)
10.0
8.0
7.5
7.0
6.0
6.0
6.0

Kadar Formaldehid Bebas

(g/ml larutan)
4.2000
3.3600
3.1500
2.9400
2.5200
2.5200
2.5200

30
31
32
33

rA

k CA

CB

34
35
36

(-rA)

37

(mol/ml.menit)
0.0000
0.0000
1.6422
0.8233
0.5518
0.4138
0.3311

38
39
40
41
42
43
44
45
46

y
log(-rA)
0.0000
0.0000
0.2154
-0.0844
-0.2582
-0.3832
-0.4801
-0.9905

x1

x2

log(CA)
-0.1552
-0.2521
-0.2801
-0.3101
-0.3770
-0.3770
-0.3770
-2.1286

log(CB)
-0.5813
-0.6782
-0.7062
-0.7362
-0.8032
-0.8032
-0.8032
-5.1114

y.x1
0.0000
0.0000
-0.0603
0.0262
0.0974
0.1445
0.1810
0.3887

L
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29

x12

x1.x2

y.x2

x22

0.0241
0.0636
0.0785
0.0962
0.1422
0.1422
0.1422
0.6887

0.0902
0.1710
0.1978
0.2283
0.3028
0.3028
0.3028
1.5958

0.0000
0.0000
-0.1521
0.0622
0.2074
0.3077
0.3856
0.8108

0.3379
0.4600
0.4988
0.5420
0.6451
0.6451
0.6451
3.7738

30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46