Professional Documents
Culture Documents
( Reaffirmed 1997 )
Indian Standard
METHODS FOR TEST SIEVING
( First Revision )
Fourth Reprint DECEMBER 1996
UDC 621.928.2:620.168.32
@ CoPyright 1977,
Gi 4
3uly 1977
kS: 1607- 19%
Indian Standard
METHODS FOR TEST SIEVING
( f?irst Revision J
Sieves, Sieving and Other Sizing Methods Sectional Committee, BDC IL’
Chairman Representing
DR M. PANCHOLY National Physical Laboratory ( CSIR ), New Delhi
Members
DR P. T. JOHN (Alternate to
Dr M. Pancholy )
SHRI V. K. AGARWAL Ministry of Railways
SHRI A. K. MUKHER~EE( Alternate )
SHRI P. N. ARORA ” ’ All India Wire Netting Manufacturer Association
SHRI S. N. ARORA Shalimar Wires & Industries Ltd, Distt Hooghly
SHRI S. KUMAR ( Alternate )
SHRI S. K. BAJORIA Krishanlal Thirani & Co Ltd, Calcutta
SHRI S. K. GANDHI ( Alternate )
SHRI R. K. CHOURARIA Jeetmul Jaicbandlall, Calcutta
DR R. K. DATTA Cent;~or3e~lding Research Institute ( CSIR ),
@ Copvrignt 1977
BUREAU OF INDIAN STANDARDS
This publication is rotected under the Indian Copyright Act (XIV of 1957 ) and
reproduction in who Pe or in part by any means except with written permission of the
publisher shall be deemed to be an infringement of copyright under the said Act.
-1.
.-
IS : 1607 I 197)
( Continuedfrompage1 )
Members &resenting
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1s:1607- 1977
Pndim Standard
METHODS FOR TEST SIEVING
( First Revision )
0. FOREWORD
0.1 This Indian Standard ( First Revision ) was adopted by the Indian
Standards Institution on 28 February 1977, after the draft finalized by the
Sieves, Sieving and Other Sizing Methods Sectional Committee had been
approved by the Civil Engineering Division Council.
0.2 Sieve analysis is one of the quality requirements specified for many raw
materials and finished products and in order to be able to produce
comparable and reproducible results, it is important that uniformity should
be observed in the procedure adopted for sieving. This standard aims at
establishing uniformity by laying down definite instructions regarding the
method of sieving, etc.
0.2.1 The standard was published in 1960. In this revision the proce-
dure with respect to wet sieving has been incorporated. The revision also
lists out the various physical and chemical properties of materials which
should necessarily be taken into account, while specifying the appropriate
sieving method ‘to be selected based on the physical and chemical properties
of the material to be sieved. Further the procedures for test sieving have
been suitably modified to make them more precise.
0.3 In the formulation of this standard due weightage has been given to
international co-ordination among the standards and practices prevailing
in different countries in addition to relating it to the practices in the field
in this country and this has been met by basing the standard on IS0 : 2591
Test Sieving.
1. SCOPE
1.1 This standard discusses the main factors affecting test sieving and the
results obtained, and specifies general principles to’be followed concerning
apparatus, procedure and presentation,ofsresults.
2. MATERIALS TO BE SIEVED
2.0 Materials to be test sieved range from very coarse lumps, such as stone
and coal to very fine materials, such as pigments and clay, and vary in
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IS t 1607- 1979
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L..__....I._.._. “__,.._ _...._.______._“_______..
- _,._. “,______“” .
IS : 1607 - 1977
2.1 .lO Chemical Reactivity - Certain materials may react with the
atmosphere or with the material of the sieves. This aspect should be
considered in choosing the sieve and in conducting the test.
3. SAMPLING
3.1.1 The method of sampling used should be such that the sample (see
IS : 5421-1969* ) taken for sieving is truly representative of the material
from which it has been drawn. The most suitable method will depend
both on the material and on the form in which it is presented, for example,-
whether it is in bags, in a heap or flowing as a continuous stream. It is
not possible to specify one method that is apphcable to all materials, and
precise sampling methods should be specified for particular materials and
circumqiances. As a guide methods specified in IS: 4879-1968t may be
considered.
3.2 Storage of Samples and Test Samples - Samples and test samples
should be stored in such a way that they are not liable to be contaminated
or affected in any other way.
4. APPARATUS
4.1 Test Sieves -Test sieving is carried out with a single test sieve or
with a series of test sieves with different nominal aperture sizes. A lid and
a receiver pan shall be included in both cases where appropriate. The
number of sieves used in the test should be sufficient to give the requisite
information about the material, and to avoid excessive wear or blinding.
Test sieves conforming to IS : 460-1962” should be used.
4.2 Preparation and Maintenance of Test Sieves
4.2.1 Variations in the sieving analysis are likely to occur;if the sieves
arc not properly cleaned and some of the openings are clogged. It is
necessary, therefore, that the sieves be cleaned either by a hard bristle
brush or by a jet of compressed air. The sieves may also be first washed
with a hot soap solution, then rinsed with water and finally dried with
alcohol. The cleaning of the sieves with very dilute hydrochloric acid is
also recommended in the case of sieves having aperture widths 200 pm or
less. Cleaning of the sieve with hydrochloric acid affects the aperture
widths and should be resorted to only when unavoidable. Another
cffcctive method of cleaning the test sieves is by ultrasonics.
4.2.2 The accuracy of the sieving ;;nediurn in the test sieve shall be
verified initially, and subsequently reverified in course of use ( see IS : 460-
1962* ). Factors, such as the frequency of use and type of material
sieved will influence the frequency of the verifications. It is desirable,
therefore, to have a record card for each test sieve.
4.2.2.1 One method of verification is to compare the performance of
the sieve with the performance of a reference sieve, using a sample
material similar to the one for which the test sieve is to be used.
4.3 Accessories - Depending on the material characteristics and the
particle size distribution of the sample to bettested, the following auxiliary
apparatus may be necessary:
a) For dry sieving- A soft brush, for .example, a paint brush, to clean
the underside of the sieving medium from time to time, and
b) For wet sieving -An installation with liquid reservoir, regulating
valve and collecting tank.
4.3.1 For test sieving, sieving aids, such as balls and chains added to the
material is not permissible.
5. PROCEDURE
5.1 General Considerations - Test sieving can be carried out by hand
or with the aid of sieve shaker. If sieve shaker is used, it shall be so
constructed and operated that the sieving results conform within agreed
tolerances to those obtained by hand sieving. The reference method shall
always be hand sieving, performed under specified conditions.
5 .l.l The following conditions should be laid down beforehand:
a) Method of sieving - dry, wet or a combination.of both; and
b) Number of sieves to be used and their aperture sizes.
5.1.2 For special cases when only machine test sieving is carried out, the
machine and method of operation shall be stated in the test report.
5.2 Procedure for Hand Sieving
5.2.1 Test sieving by hand should normally be performed on the whole
test sample with slcvcs up to 25 mm aperture siie. Above 25 mm the
particles can be prcsentcd individually by hand to the apertures.
5.2.2 The tc$ sample may be divided into fractions by a preliminary
sieving into the following particle six ranges:
a) larger than 25 mm,
b) 25 to 4 mm,
c) smaller then 4 and up to I mm, and
d) smaller than 1 mm.
5.2.3 The test sieving procedures for materials within these differentxize
ranges are given in 5.7.
5.2.4 The charges should be taken by sub-dividing the fractions obtain-
ed by the preliminary sieving. If, however, the charges do not ensure a
representative sample, the whole fraction in the size range under considera-
tion shall be tested.
5.2.5 If test sieving over more than one of the above size ranges is
required, the individual fractions shall be recorded in mass percentages of
these ranges, and in the final evaluation converted to mass percentages of
the sum of all the fractions collected.
5.2.6 The procedure consists in gently placing the material to be sieved
on the test sieve with a specified nominal aperture size and separating the
material by shaking, tapping or washing into oversize, aud undersize. In
sieving successively with test sieves of different aperture sizes the test sample
is separated into size fractions designated by the aperture sizes of the test
sieves used.
5.2.7 For hand test sieving the fo!lowing procedures are known:
a) Dry sieving - by shaking and tapping (the procedure suitable
for most materials ), and
b) Wet sieving - by washing i for materials which tend to
agglomerate ).
.I
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IS : 1607 - 1977
5.2.8 The hand sieving process may be adapted to the sieving charac-
teristics of the sample concerned by choosing from the following
alternatives:
a) The sieving of particles smaller than 1 mm may be facilitated by
starting with the finest test sieve, so that the coarse particles in
the charge may aid the sieving process. As is well. known, the
sieving of fine particles on a fine test sieve can be difficult owing
to the tendency of the apertures to blind. Care shall be taken,
however, to avoid the presence of excessively coarse particles as
these may easily damage the sieve.
b) Extremely fine particles ( such as those encountered in the deter-
mination of the grit content in soot) or particles which charge
themselves with static electricity (for. example, some plastics
powders ), or damp dust which cannot be dispersed, shall be
sieved wet.
5.2.9 The effectiveness of dry test sieving depends on:
5.5.1 .l The quantity should be’that indicated for the sieve correspond-
ing to the dominant size fraction of the sample, .providing that the size
distribution does not cause excess volume on any of the sieves in the set as
indicated in Table 1, co1 3.
5.5.1.2 The values given in Table 1 apply equally to single sieves and
tests of sieves, and to hand sieving and machine sieving.
5.5.2 Charge
10 IV”’ mm
where
W F the nominal aperture size in mm,
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IS I 1607 - 1977
Examples:
(2)
mm cm*
1 600 800
1 000 500
800 400
500 250
58-6 400 200
4 350 150
240 120
Ze8 200 100
l-4 160 80
1 140 70
w
710 120 60
500 100 50
355 80 40
250
180
125
ii
50
3”:
25
zs
45
40
zi
20
:3
*When using test sieves of different shapes and sizes, the values should be modified
accordingly.
iMasses of materials can be determined by multiplying the values in co1 2 and 3 by
the apparent bulk density (g/cm* ) of the material to be sieved.
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IS t 1607 - 1977
b) Place the charge on the sieve with the smallest aperture size in
the chosen range. After sieving, place the oversize material on
the next coarser sieve and repeat the process until all the sieves in
the chosen range have been used. This sequence has the
advantage that the coarser particles assist the sieving process on
the finer test sieves.
5.7.3.1 The test sieve, or nest of test sieves, is taken in one hand or if
too heavy, cradled loosely in the crook of the arm and tapped approxi-
mately 120 times per minute with the other hand at an inclination of 10 to
20”, the grasped point having the lower position. After 30 taps, that is
four times per minute, the test sieve is put into the horizontal position,
turned through 90” and given a hard tap by hand against the sieve frame.
A periodical vertical shake may also be given.
5.7.3.2 If particles are difficult to sieve, or when using fine test sieves,
the underside part of the sieving medium may be cleaned gently with a
soft brush ( see 4.3 ) when necessary. The resulting dust is added to the
undersize material.
5.8 Wet Sieving
5.8.1 Materials which become electrostatically charged, or damp-
samples, are best sieved wet to facilitate dispersion of the primary particles.
5.8.2 The liquid shall not affect the particles in any other way. Wetting
agents may be added ( see IS : 528%1969* ).
5.8.3 Liquid should be added slowly, regularly and at a very low
pressure to avoid loss of material and damage to the sieving medium. For
this purpose the accessories listed in 4.3 may be used.
5i8.4 Before wet sieving, the test sample shall be wetted by mixing with
a small quantity of the liquid to avoid loss of dust.
5.8.4.1 The following two procedures are permissible:
4 If the test sample is sufficiently large, a number of individual
samples may be produced by sub-division so that a fresh charge
can be used on each test sieve in the chosen range. At the
completion of the test, the test sieves together with the retained
oversize material are dried at a suitably low temperature.
b) If only a limited quantity of material is available, the test sample
may be washed successively through a nest of sieves with the finest
at ‘the bottom of the nest. The suspension which washes through
the coarser test sieve is placed directly on the next sieve. The
oversize is dried and weighed as described above.
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IS t 1607 - 1977
5.9 End-Point
5.9.1 Factors Affecting Sieving Duration - Sieving, like any other separa-
tion process, does not produce an ideal separation. A few particles which
are smaller than the nominal aperture size always rarnailr in the sieve
residue, for example, by stickin g to, larger particles, because they have not
found a free aperture or have only encountered undersize aperture.
Similarly, owing to the presence of oversize apertures, particles which are
larger than the nominal aperture size are to be found in the passing
fraction. Because of these imprccisions, no fxcd time can be determined
-at which the sieving process would be completed. The end-point has to
be based on experience.
5.9.1.1 The sieving time is dependent on:
a) the characteristics of the material, ftir example, fineness, particle
shape, size distribution, and densuy;
b) the volume of the initial charge;
c) the rate of sieving;
d) the nominal aperture size of the test sieve;
e) the characteristics of the sieving medium; and
f) the humidity of the air.
5.9.1.2 Diy Sieving End-Point- For most non-friable materials, the
end-point of the sieving process may be taken when the quantity passing
through the sieve in 1 min is less than U.1 percent of the charge, if no other
instructions are given. For friable materials and certain special cases,
the end-point of the sieving process has to be determined by trial. The
concerned parties shall agree to use a specific sieving time as only in this
way will their results be comparable.
5.9.1.3 Wet Sieviy Etzd- Point -A wet sieving operation is considered
completed when the hquid used flows off practically clear.
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IS : 1607 - 1977
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tS : 1607- 1997
6.1.1 Useof Only One or Two Sieves - Analyses requiring the use of only
one or two sieves may be presented in the following simplified manner:
a) Using one sieve - The oversizd shall be recorded as a mask
percentage of the sum of the two fractions, oversize and undersize.
b) Using two sieves-They may be used either to determine the
proportions of material coarser and finer than the two sieves, or to
determine the proportion falling between the two limits.
6.1.1.1 The results to be given shall be the oversize on each of the
sieves and the undersize passing the finer sieve, as a percentage of the sum
of the fractions:
6.1.1.2 The proportions shall be recorded as mass percentages:
Example:
Particle Sire Mass in Fraction
( Percent of the Sum of the
Masses of the Fractions )
Larger than 2 mm ( oversize ) 5
Between 2 and 1 mm ( oversize ) 75
Smaller than 1 mm (final undersize ) 20