: UOP874-88 ( ASTM )

:
,(),, 1 200 ,
QUANTACHROME AUTOSORB-1 AUTOSORB-6B/3B

20
/

27mm SARTORIUS R300S

6mm 9mm
0.1MPa
0.1MPa
AUTOSORB-1 AUTOSORB-6B 1 6
6mm 9mm

99.995
99.997

AUTOSORB

51
0.1mg

20 50 m2
0.200.02g

300 300

1.
2.
3. 90 101
4. 100 10
5. 110 3
6. 300 150 2-4
2 4

( 2mtorr/min)

Remove

0.1mg

( Po )
AS 60

/
Physisorption Analysis Menu 1
Analysis Menu
(Sample ID), (Operator), (Adsorbate Gas, N2)(Weight),
(Outgas time); (Outgas Temp); (Evacuation);
Coase() Fine ()Select P/Po
2

30

P/Po 3

 BET5 BET7 BET11 BET10/10 20/20 40/40

Equilibration time
(1 5 ) (Tolerance)
( 0) 3

( P/Po 0.001 ) Tolerance = 0

OKStartOK
//

1.
2.
3.
4. O
5. ()
6. ()

/ Edit Raw Data

and Tags()
Multi-point BET( BET) Single point BET ( BET) Satistical Thickness( ) Pore
Volume()Langmuir Data()Pore Size Distribution()DR and Fractal(DR
)
(1) /FileOpenFile nameOK
(2) Edit Raw Data and Tags
P/Po
1 Switch ON
2 P/Po
Set selectedFlags (
Switch Off Set Selected)
3 OK
(3)
1 BET
BET 0.3
BET BET
1
00.3 P/Po Set Selected
OKGraphics PlotsBET Plot BET
Edit Raw Data and
Tags MultiPoint BET Switch Off

 Set Selected OK Graphics Plots BET Plot

BET
Tabular Data MultiPoint BET BET
Area BET m2/g
Slope: BET
Y intercept: BET
Correlation Coefficient:
C
2 BET
BET P/Po=0.3 Tabular Data Single Point BET

3
Pore volume P/Po=1
Pore Size Distribution P/Po 0.31 ()
DR and Fractal P/Po 0.4 ( BET
P/Po DR Plot FHH )
BJH DH MP HK SF
DA DFT
Graphics Plots
Graphics Plots BJH Adsorption BJH Adsorption Pore Volume BJH

Tabular Data Tabular Data BJH
Pore Size DistributionAdsorption
DR HK
20A Tabular DataDR Plot
DR
Tabular Data DR Method Micropore Analysis
Graphics Plots HK Cumulative Pore Volume
HK
Tabular Data HK Method Cumulative Pore Volume
Tabular Data Area-Volume-Pore Size Summary