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oc lap T do Hanh
phuc
O AN
= 1% phan khoi
Trang 1
Trang 2
LI M U
Trang 3
MUC LUC
Trang 4
Li m u.....................................................................................3
CHNG 1 : TNG QUAN ....................................................................................4
I.L thuyt v chng ct..........................................................................................................5
II.Gii thiu s b v nguyn liu............................................................................................7
CHNG 2 : QUY TRNH CNG NGH.............................................................9
CHNG 3 : CAN BANG VAT CHAT...............................10
Cac thong so ban au ............................................10
Xac nh suat lng san pham nh va san pham
ay thu c..............................................................10
III.
Xac nh t so hoan lu lam viec..........................11
IV.
Xac nh phng trnh ng lam viec So mam ly
thuyet........................................................................13
V.
Xac nh so mam thc te.......................................14
I.
II.
I.
II.
III.
IV.
V.
VI.
VII.
Ket luan........................................................................54
Tai lieu tham khao.......................................................54
Trang 5
Chng 1 :
TNG QUAN
I. L THUYT V CHNG CT :
1. Khi nim :
Trang 6
Trang 7
u
im
Nhc
im
Thp chm
Thp mm xuyn l
Thp chp
- Cu to kh n gin.
- Tr lc thp.
- Lm vic c vi cht lng bn
nu dng m cu c ca
cht lng.
- Do c hiu ng thnh hiu sut
truyn khi thp.
- n nh khng cao, kh vn
hnh.
- Do c hiu ng thnh khi tng
nng sut th hiu ng thnh tng
kh tng nng sut.
- Thit b kh nng n.
- Tr lc tng i thp.
- Hiu sut kh cao.
- Kh n nh.
- Hiu sut cao.
Vy :qua phn tch trn ta s dng thp mm chp chng ct h Benzen Toluen.
Trang 8
C6H6
CH3(CH2)4CH3
o Dehidro ha cc cycloankane
Cc cycloankane c th b dehidro ha nhit cao vi s c mt ca cc xc tc
kim loi chuyn tip to thnh benzen hay cc dn xut cu benzen
P t/ P d
C6H12 C6H6
o i t acetylen
un acetane trong s c mt cu ca xc tc l than hot tnh hay phc ca niken nh
Ni(CO)[(C6H5)P] s thu c benzen
3C2H2 x t C6H6
o T benzen ta c th iu ch c cc dn xut ca benzen nh toluen bng phn ng
Friedel-Crafts (phn ng ankyl ha benzen bng cc dn xut ankyl halide vi s c
mt cu xc tc AlCl3 khan
C6H6 + CH3- Cl Al C l C6H5-CH3
2. Hn hp benzen toluen :
Ta c bng thnh phn lng (x) hi (y) v nhit si ca hn hp Benzen
Toluen 760 mmHg.(Tham kho STT1)
Cr2O3 / Al2O3
x (% phn mol)
y (% phn mol)
t (oC)
0
0
110,6
5
11,8
108,3
10
21,4
106,1
20
38
102,2
30
51,1
98,6
40
61,9
95,2
50
71,2
92,1
60
79
89,4
70
85,4
86,8
80
91
84,4
90
95,9
82,3
100
100
80,2
Chng 2 :
Trang 9
(3). Dng nhp liu c gia nhit ti nhit si trong thit b truyn nhit ng chm. Sau
hn hp c a vo thp chng ct (6) a nhp liu v bt u qu trnh chng ct.
Lu lng dng nhp liu c kim sot qua lu lng k (14).
Trn a nhp liu, cht lng c trn vi phn lng t on luyn ca thp chy
xung. Trong thp, hi i di ln gp lng i t trn xung. y c s tip xc v trao i
gia hai pha vi nhau. Pha lng chuyn ng trong phn chng cng xung pha di cng
gim nng cc cu t d bay hi v b pha hi to nn t ni un (10) li cun cu t d
bay hi. Nhit cng ln trn cng thp, nn khi hi i qua cc a t di ln th cu t c
nhit si cao l toluen s ngng t li, cui cng trn nh thp ta thu c hn hp c cu
t benzen chim nhiu nht (nng 98% phn khi lng). Hi ny i vo thit b ngng t
(7) c ngng t hon ton. Mt phn cht lng ngng t i qua thit b lm ngui sn phm
nh (8), c lm ngui bng thit b trao i nhit ng lng ng(8) ri c a qua bn
cha sn phm nh (9). Phn cn li ca cht lng ngng t c hon lu v thp a trn
cng vi t s hon lu thch hp v c kim sot bng lu lng k(5). Cui cng y
thp ta thu c hn hp lng hu ht l cu t kh bay hi (Toluen). Hn hp lng y c
nng Toluene l 99% phn khi lng, cn li l Benzene. Dung dch lng y i ra khi
thp vo ni un (10). Trong ni un dung dch lng mt phn s bc hi cung cp li cho
thp tip tc lm vic, phn cn li ra khi ni un c cho qua thit b lm ngui sn
phm y (13) ri i vo thit b lm ngui sn phm y(13) sau vo bn cha sn phm
y(12).
H thng lm vic lin tc cho ra sn phm nh l Benzen, sn phm y l Toluen
Trang 10
Chng 3 :
CN BNG VT CHT
I.
CC THNG S BAN U :
Trang 11
= 815 kg/m3,
= 805 kg/m
=
xD
1 xD
D = 809 kg / m 3
D=M
= 2,07 kmol / h
F = D +W
F .xF = D.xD +W .xW
W =240 ,6kg / h
W =2,8kmol / h
F =402 .4kg / h
F =4,87 kmol / h
F = 402,4 kg/h
F = 4,87 kmol/h
D = 161,8 kg/h
D = 2,07 kmol/h
x F = 0.4
x D = 0,98
x F = 0.44
x D = 0,983
= 240,6 kg/h
W = 2,8 kmol/h
xW
xW
=0,01
= 0,012
Trang 12
4.5
3.5
2.5
Nlt
(R+1).
Nlt
12
13
14
16
15
15
18
72
71.5
70
72
60
52.5
54
Trang 13
(R+1).Nlt
2,48
0,983
R
x
x+
x+ D =
2,48 +1
2,48 +1
R +1
R +1
= 0,771.x + 0,284
R+ f
f 1
x xW =1,37x -0.0044
R +1
R +1
x D xW
0,983 0,012
vi f=
x F xW
Trang 14
3 . So a ly thuyet :
th xc nh s a l thuyt :
Trang 15
n D + nF + nW
3
Vi n D n F nW - ln lt l hiu sut a trn cng, hiu sut a nhp liu v hiu
sut a di cng
- Xc nh nD
ta c: T(nhit nh thp) = 800C, xD = 0,983 suy ra yD = 0,994 s dng bng I.101
trang 91 STT1 tra v ni suy cc gi tr nht B = 0,316.10-3 N.s/m2, T = 0,319.10-3
N.s/m2.
nht ca hn hp lg hh = xD.lg B (1- xD).lg T (theo cng thc I.12 trang 84
[5] ) hh = 0,316. 10-3 N.s/m2 (= 0.316cP)
tb
0.994
1 0.983
.
= 2,87
1 0.994
0.983
. hh = 2,87.0,316 = 0,905, theo hnh IX.11 trang 171 th nD = 0,53
- Xc nh nF , tng t nh trn ta c:
V bay hi tng i =
y 1 x
.
=
1y
x
TF(nhit a nhp liu) = 940C, xf = 0,44 suy ra yD = 0,643 s dng bng I.101 trang
91 [5] tra v ni suy cc gi tr nht B = 0,277.10-3 N.s/m2, T = 0,291.10-3 N.s/m2.
nht ca hn hp lg hh = xD.lg B (1- xD).lg T (theo cng thc I.12 trang 84
STT1) hh = 0,293. 10-3 N.s/m2 (= 0,293 cP)
0.643
1 0.44
.
= 2,29
1 0.643
0.44
. hh = 2,29.0,293 = 0,672, theo hnh IX.11 trang 171 th nD = 0,58
- Xc nh n w , tng t nh trn ta c:
V bay hi tng i =
y 1 x
.
=
1y
x
V bay hi tng i =
y 1 x
.
=
1 y
x
Suy ra s mm thc :
Nt = Nlt/ tb = 15/0,58 = 25,8 ly trn 26 mm
Chng 4 :
I.
4V tb
= 0,0188
.3600. tb
g tb
( y . y ) tb
(m)
g1 = G1 + D
(IV.1)
Vi:
G1 : lng long a th nhat cua oan cat .
r1 : an nhiet hoa hi cua hon hp hi i vao a th nhat
cua oan cat
rd : an nhiet hoa hi cua hon hp hi i ra nh thap .
* Tnh r1 : t1 = tFs = 94oC , tra bang I.212, trang 254, [5] ta co :
An nhiet hoa hi cua Benzen : rB1 = 383,1 kJ/kg.
An nhiet hoa hi cua Toluen : rT1 = 371,3 kJ/kg.
Suy ra : r1 = rB1.y1 + (1-y1).rT1 = 373,1y1 - 11,8y1
r1 = 373,1y1 - 11,8y1 kJ/kg
* Tnh rd : tD = 80 oC , tra bang I.212, trang 254, [5] ta co :
An nhiet hoa hi cua Benzen : rBd = 393,3 kJ/kg.
An nhiet hoa hi cua Toluen : rTd = 378,3 kJ/kg .
Suy ra : rD = rBd.yD + (1-yD).rTd = 393,3.0,99 + 378,3.0,01
rD = 393,15 kJ/kg
(vi xD = 0,983 suy ra yD theo phn khi lng l 0,99)
* x1 = xF = 0,4(ta coi n)
Giai he (IV.1) , ta c : G1 = 593,3 kg/h
y1 = 0,524 (phan khi lng benzen)
g1 = 755,1 kg/h
Trang 17
Vay : gtb =
( .w )
y
tb
Vi : xtb : khoi lng rieng trung bnh cua pha long kg/m3 .
ytb : khoi lng rieng trung bnh cua pha hi kg/m3 .
h: khong cch mm (chn h = 0,3 ng vi D = 0,6-1,2m)
[] : h s tnh n sc cng b mt
Xac nh ytb :
ytb =
= 89,5 oC
Suy ra :
Xac nh
=2,752 kg/m3.
xtb :
y1 + y D
=
2
t1 + t D 98 ,5 +80 ,5
=
2
2
ytb
xF + xD
2
0,44 + 0,983
=
2
78 .xtb
= 65,5 %.
78 .xtb + (1 xtb ). 92
ttb = 89,5oC , tra bang I.2, trang 9, [5], ta co :
benzen = 804 kg / m3
toluen = 798 kg / m3
Suy ra : xtb =
xtb
1 xtb
xtb
benzen toluen
xtb = 802 kg/m3
Xc nh [] : h s tnh n sc cng b mt
Ta c:
1
hh
1
1
+
hh = 10 ,7.10 3 N / m = 10 ,7 dyn / cm
3
3
21,3.10
21,5.10
Vi: B =21,3.10 N/m, T = 21,5.10-3 N/m (s liu tra t bng I.242 trang 300 STT1)
Ta thy hh < 20 theo STT2 tr184 chn [] = 0,8
-3
( .w )
y
y tb
D t = 0,0188
g tb
659 ,5
= 0,0188 .
= 0,419 m
( y . y ) tb
1,33
.w y ) tb
1,33
= 0,483 m / s
2,752
Trang 18
G = g + W
'
'
G 1 .x'1 = g 1 . yW + W .xW
g ' .r ' = g ' .r ' = g .r
1 1 n n 11
(IV.2)
G 1 = 1030,3 kg/h
g1 = 789,7kg/h
Vay : gtb =
789 ,7 + 755 ,1
= 772 ,4 kg/h
2
( .w )
y
tb
Vi : xtb : khoi lng rieng trung bnh cua pha long kg/m3 .
ytb : khoi lng rieng trung bnh cua pha hi kg/m3 .
h: khong cch mm (chn h = 0,3 ng vi D = 0,6-1,2m)
[] : h s tnh n sc cng b mt
Xac nh ytb :
ytb =
Trang 19
=2,96 kg/m3.
xtb :
y1 + y D
=
2
t1 + tW
98 ,5 +110
=
=
2
2
ytb
x F + xW
2
0,44 + 0,012
=
2
0,226
Suy ra : xtb =
78 .xtb
= 18,8 %.
78 .xtb + (1 xtb ). 92
t F + tW
93 +110
= 101,5oC , tra bang I.2, trang 9, [5] , ta
=
2
2
co :
benzen = 793 kg / m 3
toluen = 788 kg / m 3
ttb =
xtb
1 xtb
xtb
benzen toluen
Suy ra: xtb = 789 kg/m3
Xc nh [] : h s tnh n sc cng b mt
Ta c:
1
hh
[5] )
1
1
+
hh = 10 ,3.10 3 N / m = 10 ,3dyn / cm
3
18,8.10
21,5.10 3
Vi: B =18,8.10-3 N/m, T = 21,5.10-3 N/m (s liu tra t bng I.242 trang 300
( .w )
y
tb
D t = 0,0188
g tb
772 ,4
= 0,0188 .
= 0,444 m
( y . y ) tb
1,38
.w y ) tb
ytb
1,38
= 0,466 m / s
2,96
Trang 20
+ Phan chng :
III.
lv
0,0188 2.g tb
Dt . y tb
2
0,0188 2.772 ,4
= 0,369 m/s.
0,50 2.2,96
y .w 2 0
Trong : - h s tr lc, thng chn = 4,5 5( y ta chn = 5); y khi lng ring ca pha hi, kg/m3; w0 tc kh qua rnh chp, m/s
Vi khi lng ring pha hi i trong ton thp:
y =
2,752 + 2,96
= 2,856 kg / m 3
2
Suy ra: Pk
0,369 + 0.339 1 1
= 35 ,4m / s
2
10 10
y .w 2 0
2,586.35,4 2
=
= 5.
= 8045,3 N / m 2
2
2
Tr lc do sc cng b mt Ps , N/m2
4.
Ps =
, N/m2
d
t
Trang 21
4. f x 4.50
=
= 6,67 mm = 6,67 .10 3 m
30
4. 4.10 ,5.10 3
=
= 6,296 N / m 2 , vi
Vy Ps =
3
Suy ra: dt =
d t
6,67 .10
l sc cng b mt trung
Pt = b .g hb , N/m2
2
Trong b chiu cao khe chp, m; b - khi lng ring bt, kg/m3; hb chiu
cao ca lp bt trn a, m; g gia tc trng trng, m/s2
+ Khi lng ring bt b = 0,5 x = 0,5.795,5 = 379,75 kg/m3, vi x - khi
lng ring trung bnh pha lng phn chng v phn ct,
+ chung 789 + 802
x = ct
=
= 795,5kg / m 3
2
+ hb chiu cao lp bt ly bng hai ln chiu cao lp cht lng trn a, theo phn
tnh ton cho a th chiu cao lp cht lng trn a l 25mm, vy hb = 50mm
+b chiu cao khe chp, tnh ton phn chp ta c b = 10mm
Suy ra:
b
0,01
Tng tr lc ca 1 a:
Pd = Pk + Ps +
Pt = 8045,3 + 6,296 + 167,6 = 8219,2N/m2
Tr lc ca ton thp:
P = N tt .Pd = 25 .8219 ,2 =16438 ,39 N / m 2
Trang 22
CHNG 5:
II.
2,07.78,28
3600
Do o QF=1913,2.
4,87.86,4
3600
III.
110 + 35
=72,5oC . Tai nhiet o ny ta ni suy t bang I.153 TR1712
IV.
2,8. 91,86
.1952,31.(110-35)=11,86, kW
3600
Trang 23
V.
2,07 .86 ,4
.1877 .(80-35)=5,13 kW
3600
Trang 24
CHNG 6:
TNH TON C KH
I . THN THP :
1. Be day than :
V thiet b hoat ong ap suat thng nen ta thiet ke
than hnh tru bang phng phap han ho quang ien, kieu han
giap moi 2 pha. e am bao chat lng cua san pham va
kha nang an mon cua benzen oi vi thiet b, ta chon thiet
b than thiet b la thep khong g ma X18H10T. Thn thp c
ghp vi nhau bng mi ghp bch. V thp lm vic vi nhit ln hn 1000C nn cn
phi bc cch nhit cho thp.
Cac thong so can tra va chon phuc vu cho qua trnh tnh
toan:
Nhiet o tnh toan : t = tmax + 20 = 110 + 20 = 1300C
Ap suat tnh toan :
V thp hot ng p sut thng nn ta coi p sut tnh ton bng vi p sut thy tnh
ln nht tc dng ln y thp. iu kin nguy him nht chn tnh ton l thp
cha y Toluene nhit 300C khi khi lng ring ca Toluene T = 856,5
kg/m3
Nn: P = (Hthan + 2Hnap).g.T = (7,5 + 2.0,15).9,81.856,5 = 61328 N/m2
0,0613 N/mm2
Vi dung tch thp nh hn 30m3 ta chn theo bng 1.1 tr10- Tnh ton thit k chi tit thit
b ha cht du kh H L Vin th p sut tnh ton P = 0,01N/mm 2, nn ta chn p sut
tnh ton theo iu kin nguy him nht nh trn tnh.
vi Hnp = h + ht = 125 +25 =150 mm(tnh phn y np).
H s b sung do n mn ha hc ca mi trng:
Chn h s b sung do n mn ha hc Ca = 1 mm
Trang 25
S Ca
4 1
0,1
0,1 0,006 0,1 (thoa)
Dt
500
2[ ]h ( S C a ) 2 140 0,95 ( 4 1)
=
Nn: [ P ] =
= 1,586 > P = 0,061 N/mm2
Dt + ( S C a )
500 + (4 1)
: thoa
Vy kt lun: b dy thn thp S = 4mm, ng knh ngoi thp Dn = 500 + 2.4 =508 mm
iu kin:
2.3,5 2.2,8
= 0,0218 m, chn b = 25 mm
9,81 .790
140
Trang 26
Rt .P
+ Ca
2.[ k ].h
2
D
Trong S b dy y np, mm; Rt = t bn knh cong bn trong nh y(np),
4.ht
m;
h - h s bn mi hn (ly bng 0,95); [k ] - gii hn bn ko ca vt liu vi
X18H10T th [k] =540.106 N/m2; P p sut tnh ton N/m2; Ca h s n mn, mm
Rt .P
500 .0,105
S=
+ Ca =
+ 0,001 = 0,00105
2.[ k ].h
2.540 .10 6.0,95
Ta thy S Ca = 0,05 < 10mm nn ta cng thm 2 mm na cho b dy (theo hng dn
trg 386 STT2) suy ra S = 3,05 mm ly theo chun S = 4 mm
V y np tiu chun nn ta c: ht = 0,25 do Rt = Dt = 500 mm
Dt
V chn cc kch thc theo STT2 tr382:
+ ht =125 mm
+ Chieu cao g: hg = h = 25 mm
+Dien tch be mat trong: Say = 0,31 m2
+The tch cha cua ay(nap):Vay cha = 27,6.10-3 m3
S Ca 4 1
D = 500 = 0,006 < 0,125
t
Tnh kim tra bn:
2[ ] h ( S C a ) 2.140.0,95(4 1)
[ P] =
=
= 1,586 > P = 0,105
Rt + ( S C a )
500 + ( 4 1)
Vy tha iu kin bn. Kt lun chn kch thc y np:
+ ht =125 mm
+ Chieu cao g: hg = h = 25 mm
+Dien tch be mat trong: Say = 0,31m2
+The tch cha cua ay(nap):Vay cha = 27,6.10-3 m3
+ Rt = Dt = 500 mm
Mat bch la bo phan quan trong dung e noi cac phan cua
thiet b cung nh noi cac bo phan khac vi thiet b. Cac loai
mat bch thng s dung:
Bch lien: la bo phan noi lien vi thiet b (han, uc va
ren). Loai bch nay chu yeu dung thiet b lam viec vi
ap suat thap va ap suat trung bnh.
Bch t do: chu yeu dung noi ong dan lam viec nhiet
o cao, e noi cac bo bang kim loai mau va hp kim cua
chung, ac biet la khi can lam mat bch bang vat lieu
ben hn thiet b.
Bch ren: chu yeu dung cho thiet b lam viec ap suat
cao.
Chon bch c ghep than, ay va nap lam bang thep CT3,
cau tao cua bch la bch phng hn kiu 1 theo bng XIII.27 trg417 STT2.
Trang 27
Dt
Db
D1
Do
(mm)
500
630
580
550
511
22
Bu-long
db
Z
(cai)
20
16
Trs bng IX.5 trang 170 [6] ng vi ng knh trong 500mm ta chn s a gia hai bch
N
25
+ 1 = 6,25
l 4, vy tng s bch cn dng l N B = t + 1 =
4
4
Ta chn 7 bch ghp thn
o kn cua moi ghep bch chu yeu do vat em quyet nh.
em lam bang cac vat lieu mem hn so vi vat lieu bch. Khi
xiet bu long, em b bien dang va ien ay len cac cho go
ghe tren be mat cua bch. Vay, e am bao o kn cho thiet
b ta chon em la day amiang, co be day la 3 mm.
Tnh kim tra b dy ca bch theo cng thc 7.1 trg 148 Tnh ton cc chi tit thit b
ha cht v du kh -Ho Le Vien :
h = t = 0,61.d b .
[ ]b
K .[ ]bi
l
D
P
1 Z + 0,7.
( l )2
[ ]b d b
l2
580 500 4
= 38 mm
2
S b dy thit b, mm
P p sut ca mi trng trong thit b N/mm2
db ng knh ngoi ca bulong, mm
[]b - ng sut cho php ca vt liu lm bulong
[]bi - ng sut cho php ca vt liu lm bch
K, h s. Vi
K =1+
Dt
2.l 2
l
S
(1 2 2 ) + ( ) 2 1
Db
t
Dt
Trang 28
: h s
= (1
l1 Db 2.l 2 2
l
15 580 2.38 2
15
).(
) + 1 + 0,2 1 = (1 ).(
) + 1 + 0,2
= 1,19
l2
Dl
l2
38
550
38
Db
D1
Do
(mm)
500
630
580
550
511
22
Bu-long
db
Z
(cai)
20
16
Trang 29
Dy
Dn
Db
D1
25
32
100
mm
75
60
12
Bu long
db
10
cai
4
Dn
32
Db
D1
100
mm
75
60
12
Bu long
db
Z
cai
10
4
Trang 30
Dn
D1
mm
100
Bu long
db
Z
cai
12
4
40
45
130
80
12
4. ng dn hi vo y thp:
Nhit ti y thp l 1100C khi lng ring ca pha hi ti y thp
PM HW
1 91,86
HW =
=
= 2,92 kg / m 3
22
,
4
RTHW
(110 + 273)
273
Chon van toc hi vo y thap la vHD = 20 m/s.(theo bng 2.2 trg370
STT1)
ng knh trong ca ng ni
Vi lu lng hi i vo y thp g1 = 789,7kg/h = 0,22kg/s = 0,075m3/s
Suy ra Dy =
4.0,075
= 0,069 m = 69 mm
..
Trang 31
Chon van toc ca dng ny vo thp l v = 0,3 m/s. (theo bng 2.2 trg370
[5] )
Khoi lng rieng cua benzen : B = 813,46 kg/m3
Khoi lng rieng cua toluen : T = 806,56 kg/m3
1
x
1 xD 0,9765 1 0,9765
= D +
=
+
Nen:
D = 813,3 kg/m3
D B
T
813,46
806 ,56
ng knh trong cua ong noi:
4.G D .R
4.416 ,88
=
Dy =
= 0,023 m = 23 mm
3600 .D ..v
3600 .812 ,9..0,3
Dn
25
VI.
32
Db
D1
100
mm
75
60
12
Bulong
db
Z
cai
10
4
2
mbch = 8. D 2 Dt .h.CT 3 = 8. ( 0,630 2 0,500 2 ) 0,022 7850 = 159,3 kg
4
.(D2ng D2t).Hthan .
4
X18H10T
kg
Khoi lng cua ay (nap) thap:
may(nap) =2. Sbe mat . ay . X18H10T = 2.0,31 . 0,004 . 7900 = 19,9 kg
Khi lng mm, ta c 25 mm v thit b un si
Mmm = khi lng chp + khi lng a di chp + khi lng ng chy chuyn(bao
gm c phn g chy trn) + khi lng ng hi
Ta ly khi tng th ca mt mm bng 2 ln khi lng mm khng c l v ng chy
chuyn cng vi b dy mm l 4mm, suy ra:
Mmm = 2. . D2t. . X18H10T = 2. .0,52. 0,004 . 7900 = 12,4 kg
4
2
. D t. Ht .
4
toluene
Trang 32
Truc thiet b
T heo ay
thie t b
P mg
2142,2 9,81
=
=
= 0,5253.104 N
4
4
4
N/m2
0,29
B1
B2
110
80
95
110
H
mm
180
120
40
18
m
57,0
2
N/m2
0,44
90
65
75
140
mm
6
35
15
14
1,0
Trang 33
Chng 7 :
1
( t v + t r ) = 1 ( 30 + 40 ) = 35 0 C
2
2
Trang 34
(80 ,5 30 ) (80 ,5 40 )
80 ,5 30
= 45,32 K.
Ln
80 ,5 40
3. He so truyen nhiet:
He so truyen nhiet K c tnh theo cong thc:
K=
1
1
1
+ rt +
n
ngng
, W/m2.K
Vi:
n : he so cap nhiet cua dong nc lanh W/m2.K
ngng : he so cap nhiet cua dong hi ngng tu W/m2.K
rt : nhiet tr qua thanh ong va lp cau.
3.1. Xac nh he so cap nhiet cua nc i trong ong :
Nhiet o trung bnh cua dong nc
trong
ong:
tf =
1
( t v + t r ) = 1 ( 30 + 40 ) .
2
2
Trang 35
t w1 t w 2
rt
Trong o:
tw1 : nhiet o cua vach tiep xuc vi hi ngng tu, oC
tw2 : nhiet o cua vach tiep xuc vi nc lanh, oC
rt = t + r1 + r2
t
Be day thanh ong: t = 0,002 m
He so dan nhiet cua thep khong g: t = 16,3 W/mK
Nhiet tr lp ban trong ong: r1 = 1/5000 m2.K/W
Nhiet tr lp cau ngoai ong: r2 =1/5800 m2.K/W
Nen: rt = 0,0005 m2.K/W
3.3. Xac nh he so cap nhiet cua hi ngng tu ngoai ong :
ieu kien:
- Ngng tu hi bao hoa.
- Khong cha khong kh khong ngng.
- Hi ngng tu mat ngoai ong.
- Mang chat ngng tu chay tang.
- Ong nam ngang.
Ap dung cong thc (3.65), trang 120, [4] oi vi ong n
chiec nam ngang th:
r. 2 .g.3
1 = 0,725 4
.(t ngng - t W1 ).d n
Tra hnh V.20, trang 30, STQTTB Tp [6] he so phu thuoc vao
cach bo tr ong va so ong trong moi day thang ng la tb
= 0,7 (v xep xen ke va so ong trong moi day thang ng la
9)
He so cap nhiet trung bnh cua chum ong: ngng = tb 1 =
0,7 1
Dung phep lap: chon tW1 = 52 oC
Nhiet o trung bnh cua mang chat ngng tu: tm = (tngng + tW1)
= (80,5 + 52) = 66,25 oC
Tai nhiet o nay th:
Khoi lng rieng cua benzene : B = 828,92 kg/m3
Khoi lng rieng cua toluene : T = 820,34 kg/m3
1 xD 1 xD 0,9765 1 0,9765
=
+
=
+
Nen:
= 828,71 kg/m3
N
A
828,92
820,34
o nht cua benzene : B = 3,67.10-4 N.s/m2
o nht cua toluene : T = 3,51.10-4 N.s/m2
Nen: lg = xDlg B + (1 xD)lg T = 0,98.lg(3,67.10-4) + (1 0,98)lg(3,51.10-4)
= 3,67.10-4 N.s/m2
He so dan nhiet cua san pham nh : D = 0,1436 W/mK
Trang 36
qngng qn
qngng
100%
20183 ,7 33228 ,2
20183 ,7
100%
Hi Ngng t
Tnh
tngng
80.5
80.5
80.5
tw
1
6
0
6
1
5
9
t1
ngng
qngng
20.
70.25
5
1414.474
28996.7191
19.
70.75
5
1432.27
27929.2597
21.
69.75
5
1397.732
30051.234
tm
Ket luan: vy chn ln tnh lp li th nht vi: tw1 = 600C c sai s nh nht, v
tw2 = 45,60C
3.4. Xac nh he so truyen nhiet:
K=
1
1
1
= 646,742 W/m2K
+ 0,0005 +
2947 ,8
1414 ,474
Trang 37
D2 =
Q nt + Q W + Q D - Q F - Q f
r2
Q nt + Q W + Q D - Q F - Q f
65,32
=
= 0,0315 kg / s = 113,05kg / h
0,95.r2
0,95.2189 ,5
3. He so truyen nhiet:
Trang 38
1
1
1
+ rt +
n
S
,W/m2.K
Vi:
n : he so cap nhiet cua hi ot W/m2.K
S : he so cap nhiet cua san pham ay W/m2.K.
rt : nhiet tr qua thanh ong va lp cau.
3.1. Nhiet tai qua thanh ong va lp cau:
t t
qt = w1 w2 , W/m2.
rt
Trong o:
tw1 : nhiet o cua vach tiep xuc vi hi ot trong ong, oC
tw2 : nhiet o cua vach tiep xuc vi san pham ay
ngoai ong, oC
rt = t + r1 + r2
t
Be day thanh ong: t = 0,003 m
He so dan nhiet cua thep khong g: t = 16,3 W/mK
(Bang XII.7, trang 313, STQTTB [6] )
Nhiet tr lp ban trong ong: r1 = 1/5800 m2.K/W (Bang 31,
trang 419, [4])
Nhiet tr lp cau ngoai ong: r2 =1/5800 m2.K/W
Nen: rt = 5,289.10-4 m2.K/W
3.2. Xac nh he so cap nhiet cua dong san pham ay
ngoai ong:
Ap dung cong thc (V.89), trang 26, [6]:
0,033
0,333
.r
0,75.q0,7
.
. 0,45 0.117 0,37
S = 7,77 . 10 . h
.c
.Ts
h
Nhiet o soi trung bnh cua dong san pham ngoai ong:
t +t
110 ,2 + 110 ,6
t S = S1 S 2 =
= 110,4 (oC) tS = 110,4 + 273 = 383,4 K
2
2
Tai nhiet o soi trung bnh th:
Khoi lng rieng cua pha hi trong dong san pham
ngoai ong:
PM HW
1 92
h =
=
22,4
= 2,91 kg/m3
RTS
(110 ,4 + 273)
273
Khoi lng rieng cua benzen : B = 780,52 kg/m3
Khoi lng rieng cua toluen : T = 781,64 kg/m3
-2
Trang 39
1 xW 1 xW 0,00365 1 0,00365
=
+
=
+
= 0,00128
B
T
780,52
781,64
= 781,636
kg/m3
o nht cua toluen : T = 2,994.10-4 N.s/m2
o nht cua benzen : B = 2,71.10-4 N.s/m2
Nen: lg = xWlg B + (1 - xW)lg T = 0,0043.lg(2,71.10-4) + (1 0,0043)lg(2,994.10-4)
= 2,993.10-4 N.s/m2
He so dan nhiet cua hn hp : = 0,149 W/mK
Sc cang be mat cua benzen : B = 0,01755 N/m
Sc cang be mat cua toluen : T = 0,0183 N/m
B T
Nen: =
= 0,009 N/m
B +T
Nhiet dung rieng cua benzen : cB = 2157,45 J/kg.K
Nhiet dung rieng cua toluen : cT = 2108,19 J/kg.K
Nen: c = cN xW + cA. (1 - xW ) = 2108,37 J/kgK
Nhiet hoa hi cua Benzen: rB = 370636,47 J/kg
Nhiet hoa hi cua toluen : rT = 362262,87 J/kg
Nen: r = rN xW + rA. (1 - xW ) = 362293,45 J/kg
3.3. Xac nh he so cap nhiet cua hi ot trong ong:
Ap dung cong thc (3.65), trang 120, [4]: n = 0,7254
rn . 2n .g.3n
n .(tn - tW1).dtr
qn qS
qn
1
1
1
= 988,73 W/m2K
+ 5,289 .10 4 +
1849 ,76103
2481 ,544
Trang 40
Trang 41
Ftb =
,m2
1
1
1 ,W/m2.oK
+ rt +
N
D
vD =
GD
4
0,045
4
.
=
.
= 0,475 m/s.
D .( D 2 tr d 2 ng ). 837,91 .(0,022 0,0162 )
Trang 42
Nu D . D
83,01.0,149
3095,8
=
=
0 , 25
0 , 25
d td
Prw1 .0,004 Prw1
vN =
GN
4
0,102
4
.
=
.
= 0,798 (m/s).
2
N .d tr 994,4 .0,01282
Chuan so Reynolds :
v d .
0,798 .0,0128 .994 ,4
Re N = N . tr N =
= 13779 ,94 > 104 : che o
N
0,7371 .10 3
chay roi, cong thc xac nh chuan so Nusselt co
dang:
Pr
0 ,8
0 , 43
Nu N = 0,021 . l . Re N Pr N
.( N ) 0, 25
Pr w 2
Trong o:
Trang 43
Nu N . N 128,49.0,6242 5265,90
=
=
0 , 25
0 , 25
d tr
Prw 2 .0,0128 Prw 2
0,138
3095 ,8
.( 57 ,75 50 ,5) =14438 ,02 W/m2.
T (IV.9): qD =
5,84 0 , 25
Khi o : Prw1 =
qt
= 43,8oC
2155 ,9
5265 ,90
.( 43 ,8 34 ) =16650 ,7 W/m2.
3,95 0, 25
q N q D
qD
= 13,29% sai s ny
Khi o:
N =
Trang 44
Ftb =
5,13.10 3
810 ,05 .20 ,038
= 0,316 m2
0,316
= 6,99
0,016 + 0,0128
m
.
2
L
7,5
=
= 625 > 50 th
d tr
0,0128
= 1: thoa.
Q
11 ,86 .3600
= 180 ,17 113 ,13 = 636,8
hR hV
kg/h
2. Hieu so nhiet o trung bnh:
Chon kieu truyen nhiet ngc chieu, nen:
(110 ,2 43) (35 27 )
tlog =
110 ,2 43
= 27,82 K.
ln
35 27
3. He so truyen nhiet:
He so truyen nhiet K c tnh theo cong thc:
Trang 45
1
1
+ rt +
n
W
W/m2.K
Vi:
n : he so cap nhiet cua dong nc lanh W/m2.K
W : he so cap nhiet cua dong san pham ay W/m2.K
rt : nhiet tr qua thanh ong va lp cau.
3.1. Xac nh he so cap nhiet cua nc trong ong:
Kch thc cua ong trong:
ng knh ngoai: dn = 16 mm = 0,016 m
Be day ong: t = 1,6 mm = 0,0016 m
ng knh trong: dtr = 0,0128 m
Nhiet o trung bnh cua dong nc trong ong: tf = (tV + tR) =
35 oC
Tai nhiet o nay th:
Khoi lng rieng cua nc: n = 994 kg/m3
o nht cua nc: n = 7,23.10-7 m2/s
He so dan nhiet cua nc: n = 0,626 W/mK
Chuan so Prandtl: Prn = 4,9
Van toc nc i trong ong:
4Gn
4 636,8
vn =
=
= 1,383 m/s
2
3600 nd tr 3600 994 0,01282
Chuan so Reynolds :
v d
1,383 0,0128
Re n = n. tr =
= 24484.65 > 104 : che o chay roi
n
7,23 .10 7
Ap dung cong thc (11), trang 7, [6] cong thc xac nh
chuan so Nusselt:
0 , 25
0 ,8
0 , 43 Pr n
Nu n = 0,021 . l . Re n Prn .
Pr w 2
Trong o: 1 he so tnh en anh hng cua he so cap
nhiet theo ty le gia chieu dai L va ng knh d cua ong v Re,
ta chn 1 = 1 theo bng trang 7 - [6]
Nun . n
He so cap nhiet cua nc trong ong: n =
dtr
3.2. Nhiet tai qua thanh ong va lp cau:
t t
qt = w1 w2 , W/m2
rt
Trong o:
tw1 : nhiet o cua vach tiep xuc vi san pham ay (trong
ong trong), oC
tw2 : nhiet o cua vach tiep xuc vi nc lanh (ngoai
ong trong), oC
rt = t + r1 + r2
t
Trang 46
c
= 4,42
4F
= Dtr dn = 0,02 0,016 = 0,004 m
Chuan so Reynolds :
vd 0,73 0,004 814 ,224
Re = t =
= 7169,89 < 104 : che o chay chuyn
3,316 .10 4
tip
Ap dung cong thc (10), trang 6, [6] cong thc xac nh
chuan so Nusselt:
0 , 25
Nu W = C l . Pr
0 , 43
Pr
.
Pr
w1
Trang 47
0 , 25
Nu W = C l . Pr
0 , 43
Pr
.
Pr
w1
0 , 25
= 27 .1,9.4,88
0 , 43
4,9
.
4,71
= 69 ,74
Nu W . 101,03 .0.1189
=
= 2219 W/m 2 .K
d t
0,004
qW = W (tW tW1) = 2219 (76,2 60) = 25740,44 W/m2
qt = qW = 25740,44 W/m2 (xem nhiet tai mat mat la khong
ang ke)
tw2 = tw1 - qt rt = 41,2 oC
PrW2 = 4,31
Nun = 153,4
n = 4801,55 W/m2K
qn = n (tW2 tf) = 28809,33 W/m2
qW qn
qW
kt qu ny chp nhn c
Ket luan: tw1 = 60 oC va tw2 = 41oC
3.4. Xac nh he so truyen nhiet:
K =
1
1
1 = 798,62 W/m2K
+ 5,565 .10 4 +
4081 ,55
2219
11,86 1000
Trang 48
Kiem tra:
L
2,5
=
= 195 > 50
d tr
0,0128
= 1: thoa
t log =
8. He so truyen nhiet:
He so truyen nhiet K c tnh theo cong thc nh oi vi
tng phang:
K=
1
1
1
+ rt +
n
F
,W/m2.K
Vi:
n : he so cap nhiet cua hi ot W/m2.K
F : he so cap nhiet dng nhp liu W/m2.K.
rt : nhiet tr qua thanh ong va lp cau.
Trang 49
rt = t + r1 + r2
t
Be day thanh ong: t = 0,003 m
He so dan nhiet cua thep khong g: t = 16,3 W/mK
(Bang XII.7, trang 313, STQTTB [6] )
Nhiet tr lp ban trong ong: r1 = 1/5800 m2.K/W (Bang 31,
trang 419, [4])
Nhiet tr lp cau ngoai ong: r2 =1/5800 m2.K/W
Nen: rt = 5,289.10-4 m2.K/W
3.6. Xac nh he so cap nhiet cua dong nhp liu trong ng:
Tai nhiet o soi trung bnh th ca dng nhp liu tFtb = 620C:
Khoi lng rieng cua benzen : B = 836 kg/m3
Khoi lng rieng cua toluen : T = 828 kg/m3
1 x F 1 xF
0,4 1 0,4
=
+
=
+
= 0,0012 = 831,2 kg/m3
Nen:
B
T
836
828
o nht cua toluen : T = 3,81.10-4 N.s/m2
o nht cua benzen : B = 3,9.10-4 N.s/m2
Nen: lg = xFlg B + (1 xF)lg T = 0,4.lg(3,9.10-4) + (1 0,4)lg(3,81.10-4)
= 3,85.10-4 N.s/m2
He so dan nhiet cua hn hp : = 0,149 W/mK
Nhiet dung rieng cua benzen : cB = 2157,45 J/kg.K
Nhiet dung rieng cua toluen : cT = 2108,19 J/kg.K
Nen: c = cN x F + cA. (1 - x F ) = 2108,37 J/kgK
cF F
p dng cng thc (V.35), trang 12, [6] ]: PrF =
= 1,94
F
Vn tc dng nhp liu i trong ng:
4GF
4 402,4
vF =
=
= 0,167 m/s.
2
3600 d tr 3600 831,2 0,032 2
Chun s Reynolds :
v d
0,167 0,032 831,2
Re F = F tr F =
= 11534,71 > 104 : ch chy ri
F
3,85 .10 4
p dng cng thc (3.27), trang 110, [4] Cng thc xc nh chun s Nusselt:
0 , 25
0 ,8
0 , 43 Pr F
Nu F = 0,021 . l . Re F Pr F .
Pr F 2
Trong : 1 h s tnh n nh hng ca h s cp nhit theo t l chiu di v ng
knh ng.
3.7. Xc nh h s cp nhit ca hi nc i pha v :
Trang 50
rn . n2 .g.3n
n .(t n - t W1 ).d tr
Pr
Nu F = 0,021 . l . Re Pr . F = 704,56
Pr F 2
F = 2818,23 W/m2K (vi q = qt)
qF = F (tF2 tF) = 17134,8 W/m2
Kiem tra sai so:
0 ,8
F
0 , 43
F
qn qS
qn
1
1
1
= 1024,69 W/m2K
+ 5,289 .10 4 +
10849 ,76
2818 ,23
Trang 51
VI . BONCAO V :
Trang 52
100
+
d1 Re F
0,25
= 0,031
1.3. Xac nh tong he so ton that cuc bo :
Cho uon cong :
Tra bang II.16, trang 382, [5]: Chon dang ong uon cong 90o
co ban knh R vi R/d =2 th u1 (1 cho) = 0,15.
ng ong co 6 cho uon u1 = 0,15. 6 = 0,9
Van :
Tra bang 9.5, trang 94, [1]: Chon van cau vi o m hoan
toan th van (1 cai) = 10.
ng ong co 2 van cau van = 10. 2 = 20
Lu lng ke : l1 = 0 (coi nh khong ang ke).
Vao thap : thap = 1
Nen: 1 = u1 + van + ll = 21,9
Vay: h1 = 0,031
30
0,114 2
+ 21,9 .
= 0,022 m
0,08
2 9,81
P2 P1 v2 v1
+
z1 = z2 +
+hf1-2
F .g
2.g
Trong o:
z1: o cao mat thoang (1-1) so vi mat at, hay xem nh la
chieu cao bon cao v Hcv = z1.
z2: o cao mat thoang (2-2) so vi mat at, hay xem nh la
chieu cao t mat at en v tr nhap lieu:
z2 = hchan + hay + (nttC 1) h + 0,4
= 0,18 + 0,150 + (14 1)0,25 + 0,4 = 3,98 m
Trang 53
= 3,98 +
24485
0,32 2 0
+
+ 0,662
9,81 .832
2 9,81
= 8,78 m
Chon Hcv = 10 m.
VII . BM :
1. Nang suat:
Nhiet o dong nhap lieu la tF = 30oC.
Tai nhiet o nay th:
Khoi lng rieng cua benzen : B = 869,25 (kg/m3)
Khoi lng rieng cua toluen : T = 855,39 (kg/m3)
1
x
1 xF 0,2665 1 0,2665
= F +
=
+
Nen:
F = 858,78 (kg/m3)
F N
A
869,25
855,39
o nht cua benzen : B = 5,91.10-4 (N.s/m2)
o nht cua toluen : T = 5,39.10-3 (N.s/m2)
Nen: lg F = xFlg B + (1 xF)lg T
F = 5,541.10-4 (N.s/m2)
Suat lng the tch cua dong nhap lieu i trong ong:
3
Q = 402 ,4kg / h = 0,5 m /h
F
2. Cot ap:
Chon :
Mat cat (1-1) la mat thoang chat long trong bon cha
nguyen lieu.
Mat cat (2-2) la mat thoang chat long trong bon cao v.
Ap dung phng trnh Bernoulli cho (1-1) va (2-2):
2
2
P1
P2
v1
v2
z1 +
+
+ Hb = z2 +
+
+hf1-2
F .g
F .g
2.g
2.g
Trong o:
z1: o cao mat thoang (1-1) so vi mat at, chon z1 = 1m.
z2: o cao mat thoang (2-2) so vi mat at, z2 = Hcv = 10m.
P1 : ap suat tai mat thoang (1-1), chon P1 = 1 at.
P2 : ap suat tai mat thoang (2-2), chon P2 = 1 at.
v1,v2 : van toc tai mat thoang (1-1) va(2-2), xem v1= v2 = 0
m/s.
Trang 54
2.1.
Tnh tong tr lc trong ong:
Chon ng knh trong cua ong hut va ong ay bang nhau:
dtr = 50 mm
Tra bang II.15, trang 381, [5] o nham cua ong: = 0,2 mm
= 0,0002 m (an mon t)
Tong tr lc trong ong hut va ong ay
lh + l
vF 2
+ h + .
hf1-2 =
d
tr
2g
Trong o:
lh : chieu dai ong hut.
Chieu cao hut cua bm: Tra bang II.34, trang 441, [5] hh = 4,3
m
Chon lh = 6 m.
l : chieu dai ong ay, chon l = 15 m.
h : tong ton that cuc bo trong ong hut.
: tong ton that cuc bo trong ong ay.
: he so ma sat trong ong hut va ong ay.
vF : van toc dong nhap lieu trong ong hut va ong ay
m/s.
4Qb
4 2,5
vF =
=
= 0,36 m/s
2
3600d tr 3600 0,0502
Xac nh he so ma sat trong ong hut va ong ay :
Chuan so Reynolds :
v d
0,36 0,05 858,78
Re F = F tr F =
= 27122,63 > 4000 : che o chay
F
5,541 .10 4
roi
Chuan so Reynolds ti han: Regh = 6(dtr/ )8/7 = 3301,065
Chuan so Reynolds khi bat au xuat hien vung nham: Ren =
220(dtr/ )9/8 = 109674,381
V Regh < ReF < Ren che o chay roi ng vi khu vc qua
o.
100
+
Ap dung cong thc (II.64), trang 379, [5]: = 0,1.1,46.
dtr Re F
0,25
= 0,03124
Xac nh tong ton that cuc bo trong ong hut :
Cho uon cong :
Tra bang II.16, trang 382, [5]: Chon dang ong uon cong 90o co
ban knh R vi R/d = 2 th u1 (1 cho) = 0,15.
Ong hut co 2 cho uon u1 = 0,15. 2 = 0,3
Van :
Tra bang 9.5, trang 94, [1]: Chon van cau vi o m hoan
toan th v1 (1 cai) = 10.
Trang 55
v1
= 10
6 + 20
0,32 2
+10 ,3 +11,6 .
= 0,2 m
0,05
2 9,81
2.2.
Tnh cot ap cua bm:
Hb = (z2 z1) + hf1-2 = (10 1) + 0,2 = 9,2 m
3. Cong suat:
Chon hieu suat cua bm:
= 0,8.
Qb H b F .g 0,5 9,2 858 ,78 9,81
=
Cong suat thc te cua bm: Nb =
3600 .b
3600 0,8
= 13,45 W
Ket luan: e am bao thap hoat ong lien tuc ta chon 2
bm li tam loai XM, co:
- Nang suat: Qb = 0,5 m3/h
- Cot ap: Hb = 9,2 m
- Cong suat: Nb = 13,45 W
b
KET LUAN
Vi quy trnh cng ngh tnh ton trn ta thy rng mt lng nhit ng
k cn gii l ngng t sn nh, gii nhit sn phm nh v gii nhit cho sn
phm y cha c tn dng gia nhit cho dng nhp liu. Nhng trong qu
trnh tnh ton gia nhit cho dng nhp liu ti trng thi lng si nu tn
dng nhit th cha gia nhit ti lng si trong khi phi tn thm thit
b, ng ng lm tng chi ph ca phn xng. Vn tn dng nhit l mt
vn thc t rt c quan tm, n nh l mt gii php nng cao hiu qu
ca qu trnh v tit kim nng lng, nhng trong gii hn v thi gian, kh
nng v kinh nghim thc t nn em cha phn tch tnh ton nh gi ng
mc cc qu trnh. n mn hc l mt mn hc tng hp v n mang li
cho em nhiu kinh nghim tnh ton thit k hon chnh mt qu trnh trong
sn xut.
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