Procedures: I.

Solution and Filtration

a) Results:

b) Results:

II.

Decolorization

Observation and Results:

III.

Crystallization

Observation and Results:

IV.

Sublimation

Observation and Results:

V.

Extraction

Observation and Results:

Observation and Results:

VI. Results:

Paper Chromatography

Questions: 1. Define dialysis, Chromatography and electrophoresis. Give the principle involved in each.

2. What is the role of boneblack in decolorization? Give the principle involved in decolorization.

3. Give the principle involved in crystallization. How are the impurities removed by this method? Give the qualities of a good solvent used in this method.

4. Which is more effective extractions, using single extraction with a large volume of solvent or several extractions with smaller volumes of solvent? Prove this by solving the following problem. a) Calculate the amount of solute extracted from a solution containing 5 grams of solute in 100 mL of water, using 35 mL of ether. The distribution coefficient of the above sample is 4.

b) Calculate the amount of solute from solution in (a) with 20 mL and 15 mL portions of ether. Compute also for the percentage recovery in both cases.

5. What is the law of partition?

6. How is the extraction process involving immiscible solvents?

Experiment Number 1
Name: AL-Ramahi, Victoria Hend Sharmila C. Date started: 04-19-10 Date finished: 04-20-10

DATA AND RESULTS

Complete the Table

Method of Purification Solution and Filtration Crystallization Decolorization Extraction Sublimation Chromatography Distillation Electrophoresis Dialysis

Principle Involved

Practical Application

Example of The process

Answer to Questions: