TOXICOLOGY TRAINING CHECKLIST OPIATES BY GC/MS Trainee: ____________________________________________ (Print) Instructor: __________________________________________ (Print) As each area of training is covered,

that area will be checked off and the trainee and instructor will initial and date below. The areas to be covered are as follows: Trainee Initials Instructor

Date

___Read Selective Ion Monitoring _____ _____ ______ ___Read Opiate by GC/MS and training literature _____ _____ ______ ___Read Handbook of Derivatives for Chromatography _____ _____ ______ Section 4.4.1 page 57-58 ___Read Gas Chromatography Derivatization in the _____ _____ ______ Pierce Catalog and Handbook, page T-231-238 Trainee will spend approximately 1 week with instructor covering all areas of analysis listed below. Instructor and trainee will initial and date the individual areas when trainee demonstrates proficiency. ___ Generation of Sample Work List _____ _____ ______ ___ Preparation of Standards ___ Preparation of Calibrators ___ Preparation of Controls ___ Preparation of Reagents ___ Derivatization Procedure ___ GC / MS Operation ___ Instrument Parameters ___ SIM Parameters ___ Data Analysis ___ Successful Quality Control Run 10 quality control samples 15 repeat samples where available 3 supervised runs _____ _____ _____ _____ _____ _____ _____ _____ _____ _____ _____ _____ ______ ______ ______ ______ _____ ______

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Dallas County Institute of Forensic Sciences Toxicology Training Manual

Opiates by GC/MS Version 2.0

When all the areas have been checked off and initialed, the trainee, supervisor, and section chief will sign and date this form. This form will then be placed in the analysts training folder that is kept by the Quality Manager. Trainee: Supervisor: Section Chief: Date: Date: Date:

Dallas County Institute of Forensic Sciences Toxicology Training Manual

Opiates by GC/MS Version 2.0