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Bo Co NGHIN CU TNG HP XC TC LAI TP DNG CHO PHN NG NG PHN Ha n-HEXAN

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ti: NGHIN CU TNG HP XC TC LAI TP DNG CHO PHN NG NG PHN Ha n-HEXAN Chuyn ngnh: Ha Hc Th loi: BO CO Gi: M s ti liu: 82641 nh gi: Np xu
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NGHIN CU TNG HP XC TC LAI TP DNG CHO PHN NG NG PHN Ha n-HEXAN n Ta son 19-7-2006 L THANH TNG, HOA HU THU B mn Ha hc du m, khoa Ha hc, tr*ng HKHTN-HQGHN SUMMARY A series of hybrid catalysts PtWZr/PtSZr, PtWZr/H-ZSM5 and PtWZr/HPA was been prepared. The structure and the surface property of the hybrid catalysts obtained were characterized by using different methods physical such as XRD, SEM, TEM, BET, NH3-TPD. Their catalytic activity in n-hexan isomerization was tested by MAT5000 showed that the conversion of this reation on catalysts is from 48,97% to 52,01%, selectivity is from 86,73% to 98,5% and that their stability of catalysts is high. I - Gii thiu Cht xc tc zirconia bin tnh, nh zirconia tungstate c hot ng xc tc cao cho phn ng ng phn ha v+ cracking n-parafin d i nhng iu kin m du [1]. Platin v+o c a h xc tc n+y nhm tng hot ng ca xc tc c bn v+ tng bn vng ca chng, c bit khi c mt hidro trong h thng phn ng gy ra hin t tr+n y (spillover) thc y ng qu trnh ng phn ho, gim thiu l cc ng to th+nh [2]. Trong qu trnh spillover H2 phn ly th+nh Hv+ H+ sau khi hp ph trn b mt Pt v+ hai loi ion n+y khuch tn v+o pha th hai y l+ PtSZr, H-ZSM5 v+ HPA v+ tip tc tham gia qu trnh ng phn ha n-ankan. Khi c mt ca W trong pha th nht nh PtWZr qu trnh

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to th+nh H+ v+ Hc th xy ra theo c ch sau [3, 4]: Pt-H + WO3 + H2WO3 Pt WO3 + H+ H+ Bn cnh khi zirconia bin tnh c bng W, bn, n nh ca xc tc tng ln r rt. Zirconia th tn ti hai dng th ng hnh l+ monoclinic v+ tetragonal trong dng tetragonal l+ dng bn v+ dng monoclinic l+ dng km bn d t tc vi cc cht khc. ng Khi dng monoclinic t tc s l+m cn bng ng tetragonal v+ monoclinic chuyn dch sang pha to th+nh monoclinic, l+m gim h+m l ng tetragonal tc l+m gim hot tnh cng nh bn ca xc tc. Mt khc, ng ta thy rng khi W v+o i a h xc tc vi h+m l 12,5%W, ZrO2 s tn ng ti ch yu d dng tetragonal l+m cho xc tc i n nh [5]. ng thi khi bin tnh zirconia bng cch sunfat ha cho ta xc tc zirconia sunfat (ZrO2.SO4 2) c tnh axit mnh hn H2SO4 100% c pH = -16,1 n -19. V th zirconia sunfat ha c hot tnh xc tc rt mnh thun li cho phn ng ng phn ha iu kin m du. Mt s axit rn c lc axit cao cng c nghin cu dng cho phn ng ng phn ha nh : zeolit H-ZSM5 [6], heteropolyaxit (NH4)2,5H0,5PW12O40 (HPA) [6]. Theo cc t+i liu [5, 6], cc hp phn ring bit trong th+nh phn xc tc lai tp c im u v+ nh im nh c : - PtWZr (Pt-WO3-ZrO2) c bn cao nh hot tnh ng phn ha n-hexan ca xc ng tc khng cao. - PtSZr (Pt-ZrO2-SO4 2), H-ZSM5, HPA

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TH C S Tng hp v phn tch tnh cht ha l ca xc tc trn c s Ni+Ca/A l2O3+SiO2 cho phn ng metan ha c trong k h giu H2 (80) N Tng hp cc mu xc tc Ni/C* v i hm lng Ni thay i nghin cu hot tnh cc mu xc tc cho qu trnh HDC pha k h thng qua phn ng chuy n ha... (79) LU N V N NGHIN CU A D NG DI TRUYN CA QU N TH N M Cory nespora cassiicola (Berk & Curt) Wei G Y BNH TRN C Y CA O SU (Hev ea brasiliensis Muell. A rg.) T I... (224) LU N V N La chn, xy dng v s dng h thng bi tp ha hc dng k im tra nh gi k in thc hc phn C s ha hc hu c 2 ca sinh v in trng cao... (277) TH C S Cc y u t thuc thnh phn nhn thc v cm xc tc ng n hnh v i mua ca k hch hng tiu dng Thnh ph H Ch Minh Trng hp: Sa tm... (527)

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