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Vacuum Distillation Guide

The document provides an overview of a crude vacuum distillation unit (VDU). The VDU takes long residuum from an atmospheric distillation unit and separates it into lighter end products like vacuum gas oils, vacuum distillate, slop wax, and residue using reduced pressure and high temperatures. It describes the feed, products, different types of vacuum distillation processes, key components like the vacuum heater, vacuum tower, and vacuum system including ejectors and condensers.

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100% found this document useful (2 votes)
948 views17 pages

Vacuum Distillation Guide

The document provides an overview of a crude vacuum distillation unit (VDU). The VDU takes long residuum from an atmospheric distillation unit and separates it into lighter end products like vacuum gas oils, vacuum distillate, slop wax, and residue using reduced pressure and high temperatures. It describes the feed, products, different types of vacuum distillation processes, key components like the vacuum heater, vacuum tower, and vacuum system including ejectors and condensers.

Uploaded by

chikukotwal
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
  • Introduction: Describes the purpose and function of the crude vacuum distillation unit, including feed and product information.
  • Different Types of Vacuum Distillation: Outlines the different types of vacuum distillation methods with their characteristics and pressure profiles.
  • VDU Flow Diagram: Presents the flow diagram of the vacuum distillation unit, detailing the process and components in the system.
  • Vacuum Heater: Explains the structure and functionality of the vacuum heater with a diagram and operational details.
  • Vacuum Tower: Illustrates the vacuum tower and explains its structure, sections, and types of trays used.
  • Vacuum System: Details the components and operating principles of the vacuum system with diagrams.
  • Thank You: Concludes the presentation with a closing note.

Crude Vacuum Distillation Unit

Prepared by

Rohan S. Sule

Confidential & Proprietary

Confidential & Proprietary

Topics
Introduction VDU Feed/Products Different Types Of Vacuum Distillation VDU Flow Diagram Process Equipments
!eater Vacuum Tower Vacuum "ystem

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Crude Vacuum Distillation Unit


Objective
To distill t#e long residuum crude from t#e atmosp#eric tower at #ig#er temperatures and reduced pressure$ T#e VDU ta%es t#e long residuum from t#e &DU '&tmosp#eric Distillation Unit( and separates t#e #ea)ier end products suc# as )acuum gas oils* )acuum distillate* slop wa+* and residue at reduced pressure and #ig# temperature$

Feed
,ong -esiduum '-educed .rude( from .DU

Products
,ig#t Vacuum /as Oil* !ea)y Vacuum /as Oil* -esiduum* "lop wa+* &sp#alt$

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Different Types Of Vacuum Distillation


Dry Vacuum Distillation
,ow energy consumption* applica0le to fuel type )acuum towers$ Do not utili1e stripping steam$ Pressure profile Flas# 1one2 34 mm !g a0s Top of tower2 5 l5 mm !g a0s 6

et Vacuum Distillation
!ig# product quality* applica0le to lu0e type )acuum towers and utili1e stripping steam$ Pressure profile Flas# 1one2 75 85 mm !g a0s Top of tower2 54 75 mm !g a0s 6

Damp Vacuum Distillation


,ow energy consumption and #ig# product quality$ "tripping steam is apprecia0ly reduced and t#e e9ector system is a t#ree stage system$ Pressure profile Flas# 1one2 :5 mm !g a0s Top of tower2 ;5 35 mm !g a0s

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VDU Flo! Dia"ram

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Vacuum #eater

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Vacuum #eater
Vacuum #eater
Vacuum #eater is a cylindrical furnace #a)ing con)ection 1one and radiation 1one$ T#e #eater operates at outlet temperature of 854F$ T#e furnace is fired 0y fuel gas and pilot gas$

6 Co$e %ormation 6 Reason&


.onditions in t#e radiant tu0es cause t#e reduced crude to t#ermally decompose to co%e and gas$

6 'voidin" co$e %ormation&


<y minimi1ing oil film temperature$ <y reducing t#e residence time of t#e oil in t#e tu0es of t#e radiant section$ "team can 0e used to lower oil residence time$ 6 6

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Vacuum To!er

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Vacuum To!er
Sections&
T#ree different section of different diameter and #eig#t ,arge diameter columns are used to maintain compara0le )apor )elocities at t#e reduced pressures$

Type o% Trays and Pac$ed beds&


T#ree pac%ed 0eds for t#ree draw off cuts and t#ree draw off trays are used Pac$ed bed ( "tructural pac%ing

Tray ( .#imney type for draw off trays

( "ie)e trays for t#e 0ottom section

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Vacuum System

Typical Vacuum system


"team E9ectors .ondensers .ondensate recei)er

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Vacuum System Steam )jectors

Steam )jectors consist o% %ollo!in" parts&


"team inlet "team no11le =i+ing c#am0er .on)erging inlet diffuser Diffuser t#roat Di)erging outlet diffuser
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Vacuum System
Operatin" principle
To con)ert pressure energy of #ig# pressure moti)e steam into )elocity$ =oti)e steam e+pands to a pressure 0elow t#e suction fluid pressure creating t#e dri)ing force to 0ring suction fluid into an e9ector$ !ig# )elocity moti)e steam entrains and mi+es wit# t#e suction fluid$ T#e resulting mi+ture is supersonic$ T#en t#e mi+ture passes t#roug# t#e con)erging* t#roat* and di)erging sections of a diffuser* #ig# )elocity is con)erted 0ac% into pressure$ In t#e diffuser>s di)erging section* cross sectional flow area is increased and )elocity is furt#er con)erted to pressure$

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Vacuum System
)jector System %or di%%erent types o% to!ers

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Vacuum System
Vacuum Condensers
T#e primary purpose of a condensers in an e9ector system is to condense as muc# steam and #ydrocar0ons as possi0le$ <y condensing steam and #ydrocar0on )apors* t#e load #andled 0y a downstream e9ector is reduced$ T#is maintains energy usage 'moti)e steam consumption( for dri)ing t#e e9ectors* to a minimum$

Confidential & Proprietary

Vacuum Condensers

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Thank You

Confidential & Proprietary

 
 
Confidential & Proprietary
Crude Vacuum Distillation Unit
Prepared by
Rohan S. Sule
 
 
Confidential & Proprietary
Confidential & Proprietary
   Topics
• Introduction
• VDU Feed/Products
• Different Types Of Vacuum Distillation
• VDU Fl
Confidential & Proprietary
Crude Vacuum Distillation Unit
•Objective
To distill the long residuum crude from the atmosphe
Confidential & Proprietary
Different Types Of Vacuum Distillation
Dry Vacuum Distillation
Low energy consumption, applica
 
 
Confidential & Proprietary
VDU Flow Diagram
 
 
Confidential & Proprietary
Vacuum Heater
Confidential & Proprietary
Vacuum Heater
•Vacuum heater is a cylindrical furnace having convection zone and radiation zon
 
 
Confidential & Proprietary
Vacuum Tower
Confidential & Proprietary
Vacuum Tower
Sections: 
•Three different section of different diameter and height
•Large diame

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