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Isophorone: "ISOPHORONE" is a α, β unsaturated cyclic ketone, colourless to
Isophorone: "ISOPHORONE" is a α, β unsaturated cyclic ketone, colourless to
PROPERTIES:
Mol. Formula
: C9H14O
Mol. weight
: 138.21
Boiling point
: 215C
: 0.1 mmHg
Density at 20C
: 7.70 lb/gal
Specific Gravity
: 0.9229
Viscosity at 20C
: 2.6 cP
Melting point
: -8.1C
Solubility
: 1.2 g/100ml
RAW MATERIAL:
ACETONE
CAUSTIC (CATALYST)
OVERALL REACTION:
FLOWSHEET:
PROCESS:
Raw materials acetone and caustic (50% conc.) are fed to storage tank.
Caustic is diluted to 10% and along with acetone and water in the
reaction column.
In the reaction column, conversion is 6-8%which is increased by adding
the same to hydrolysing column.
In the hydrolysing column, steam is sparged with caustic (50% conc.)
from storage tank. From hydrolysing column steam and some
unconverted product is again fed to the reaction column.
The product from hydrolysing column is first cooled and then sent to
decanter unit.
From the 1st decanter 80% hydrocarbons are separated and remaining
20% sent to 2nd decanter where further separation is done and almost 8587% hydrocarbons are separated and water is removed.
The separated products from decanter are sent to distillation where both
columns (heading and pure column) are operated under vacuum.
From heading column lightens are removed. Heavys and isophorone
obtained as bottom products of heading column are fed to pure column
where heavys are removed from bottom and required product
isophorone is collected from top of pure column.
Uses: