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IS 5760 (1998): Argon, compressed and liquid [CHD 6:

Industrial Gases]

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IS 5760 : 1998

Indian Standard
ARGON, COMPRESSED AND LIQUID
SPECIFICATION
( Second Revision )

ICS

71.100.20

BIS 1998

BUREAU OF INDIAN STANDARDS

MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
May 1998

Price Group

Industrial Gases Sectional Committee, CHD 006

FOREWORD
This Indian Standard (Second Revision) was adopted by the Bureau of Indian Standards, after the draft finalized
by the Industrial Gases Sectional Committee had been approved by the Chemical Division Council.
This standard was originally published in 1969 and covered only argon used for welding and other metallurgical
operations. In the first revision of this standard in 1983, another grade of argon was incorporated to cover high
purity argon for use in lamp industry and in direct reading vacuum spectrograph. Since then, other industrial
uses of high purity argon have grown tremendously, particularly, the use of ultra high purity argon in electronics
industry This second revision of the standard has been undertaken to incorporate another grade of argon, that
is, ultra high purity grade argon for use in electronics industry.
At present, argon is being manufactured and marketed in three grades, namely, Grade 1 Ultra high purity argon
for use in electronics and allied industries, Grade 2 High purity argon for use in lamp industry, and Grade 3
Argon for use in welding and for other metallurgical processes. Commercial/industrial users are also
accustomed to these grades.
As stringent limits of impurities have been prescribed for ultra high purity argon (Grade 1) and high purity argon
(Grade 2) the analysis of these grades of argon demands the employment of sophisticated modern instruments
having high degree of sensitivity and precision. In view of this, the conventional forms of glass test sets and
apparatus have not been prescribed for Grade 1 and Grade 2 argon. The equipment and the instruments prescribed
tor analysis are amongst the latest in the field.
The Committee responsible for formulation of this standard is given in Annex C.
For the purpose of deciding whether a particular requirement of this standard is complied with, the final value,
observed or calculated, expressing the result of a test or analysis, shall be rounded off in accordance with
IS 2 : 1960 'Rules for rounding off numerical values (revised)'. The number of significant places retained in the
rounded off value should be the same as that of the specified value in this standard.

AMENDMENT NO. 1 DECEMBER 2008

TO
IS 5760 : 1998 ARGON, COMPRESSED AND
LIQUID SPECIFICATION
( Second Revision )
(Page 5, Annex B, Table 2) Substitute the following for the existing:
Table 2 Number of Cylinders to be Selected
(Clause B-1.2)
Lot Size
N
(1)
Up to 25
26 to 50
51 to 100
101 to 200
201 to 300
301 and above

Number of Cylinders to be Selected

n
(2)
3
5
8
15
20
25

(CHD 6)
Reprography Unit, BIS, New Delhi, India

IS 5760 : 1998

Indian Standard
ARGON, COMPRESSED AND LIQUID
SPECIFICATION
( Second Revision )
1 SCOPE

5.2 The material shall comply with the requirements

prescribed in Table 1 when tested in accordance with
the methods prescribed in Annex A. Reference to the
relevant clauses of Annex A is given in col 6 of
Table 1.

This standard prescribes requirements and methods of

sampling and test for argon, liquid and compressed.
2 REFERENCES

6 PACKING AND MARKING

The Indian Standards listed below contain provisions

which through reference in this text, constitute
provisions of this Indian Standard. At the time of
publication, the editions indicated were valid. All
standards are subject to revision, and parties to
agreements based on this Indian Standard are
encouraged to investigate the possibility of applying
the most recent editions of the standards indicated
below:
IS No.

Title

4905 : 1968

Methods for random sampling

7062 : 1973

Glossary of terms used in gas

industry

6.1 The gas shall be supplied compressed in cylinders

or liquid argon tanks. The design of cylinders or liquid
argon tanks, the maximum pressure of argon in them.
and packing, marking, painting, labelling and transport
of cylinders tanks shall be in conformity with the Gas
Cylinder Rules, 1981 of the Government of India with
modifications as may be ordered from lime to time by
the Chief Controller of Explosives or any other
authority duly constituted by the Government of India.
Table 1 Requirements for Argon, Compressed
and Liquid
(Clauses 5.2 and B-3)
Sl
No.

3 TERMINOLOGY

Characteristic

Grade Grade
2
1
(3)
(4)
05
50
2 0 10 0
10
20
05
40

For the purpose of this standard, the definitions given

in IS 7062 shall apply.

(2)
(1)
i) Oxygen, ppm, Max
ii) Nitrogen, ppm, Max
iii) Hydrogen, ppm, Max
iv) Water vapours, ppm,
Max
05
v) Carbon dioxide, ppm,
Max
0.5
vi) Carbon monoxide, ppm,
Max
Hydrocarbons, ppm, Max 0 2
vii)

4 GRADES
There shall be three grades of argon, namely:
Grade 1 Ultra high purity argon for use in
electronics and allied industries and in
direct redding vacuum spectrograph,
Grade 2 High purity argon for use in lamp and
allied industries, and
Grade 3 Commercial grade argon for use in
w e l d i n g industry and for other
metallurgical operations.

Method of
Test (Ref
to Cl No.
Grade
in Annex A)
3
(6)
(5)
A-2, A 3
10 0
A-2, A 4
300
50
A-2
A-5
70

Requirement
4

05

30

A-2, A-6

05

20

A-2, A-7

05

A-2, A-8

7 SAMPLING
The method of drawing representative samples from a
lot, number of tests to be performed and the criteria for
conformity of the material to the requirements of this
specification shall be as prescribed in Annex B.

5 REQUIREMENTS
5.1 The material shall be compressed gas or liquid for
vaporization.

IS 5760 : 1998

ANNEX A
(Clause 5.2)
METHODS OF TEST FOR ANALYSIS OF ARGON, COMPRESSED AND LIQUID
passes through the detector chamber, is subjected to a
strong electromagnetic field maintained between two
electrodes by a high frequency generator. The
resulting luminescense is modified subsequently by
any other element passing through the chamber.

A-1 GENERAL
Only instrumental methods of test have been
prescribed for analysis of argon, compressed and
liquid.
A-2 D E T E R M I N A T I O N O F O X Y G E N ,
NITROGEN, HYDROGEN, WATER VAPOUR,
CARBON DIOXIDE, CARBON MONOXIDE
AND HYDROCARBONS

The high frequency generator is operated on a

stabilized voltage. The luminous intensity of the gas
discharge tube is measured by means of a photoresistive cell, which is one of the branches of the bridge
whose unbalanced voltage is the output signal for
recording or integrating.

A-2.1 Gas Chromatographic Method

A-2.1.1 Principle
Chromatography is a process of separation achieved
by means of a partition between a stationary phase and
a moving phase. A suitable synthetic zeolite and
suitable detector are used in chromatography.

A-2.1.2 Procedure
Calibrate the instrument against calibration gas of
known composition by measuring the peak heights or
areas under various peaks of the chromatograph
following the instructions of the manufacturer. Carry
out the test according to the manufacturer's
instructions and compute the concentration of the
various impurities by comparing the peaks or the areas
under peaks with that of the calibration gas.

When the accuracy of analysis is to be achieved at the

level of 1 vpm, the results obtained are always relative
to the impurities of carrier gas and are not absolute
values. Hence, the ultra high purity carrier gas, that is,
Grade 1 argon is to be purified further by a suitable
rare gas purifier to achieve zero impurity carrier gas.

The nature of chromatograph of a calibration gas

mixture in argon is depicted in Fig. 1.

The purifier system consists of titanium granules at

700C for removal of nitrogen and oxygen, a copper
oxide furnace for removal of hydrogen and carbon
monoxide, and molecular sieve to remove carbon
dioxide and moisture.

A-3 DETERMINATION OF OXYGEN

A-3.1 General
Two methods have been prescribed, namely
electrochemical analyser method and gas
chromatrographic method.

The construction of the gas chromatograph is the same

as that of any gas chromatograph with a gas sampling
value and a loop of known volume. The column
material is molecular sieve 5 A filled in stainless steel
column of 4 m length and 4.6 mm internal diameter.
The column is regenerated at 250C in a stream of
argon for about 4 h. The detector is the most important
part of the whole assembly and is called argon
discharge detector. Purified carrier argon gas, which

A-3.1.1

Electrochemical Analyser Method

A-3.1.1.1 Principle
The oxygen detection element consists of a number of
silver disc arranged around a central helix to form a
spiral through which the test gas passes. The spiral is
contained within a porous vyon tube immersed in a

CONCENTRATION IN pprn BY VOLUME

FIG. 1 CALIBRATION GAS

IS 5760 : 1998
pool of potassium hydroxide electrolyte to keep the
tube moist. The silver acts as the cathode of the cell.
Where oxygen molecules in the test gas are absorbed
on its surface and go into the solution in the electrolytes
as hydroxyl ions. These ions migrate through the
electrolyte to the cadmium anode which is oxidized to
cadmium hydroxide, the ions having given up their
negative charge causing a current to flow in the
external circuit consisting of a galvanometer connected
across the electrodes. The magnitude of the current is
a measure of the amount of oxygen in the gas.

A-4.1.2 Gas Chromatographic Method

The procedure for carrying out the determination shall
be the same as prescribed under A-2.
A-5 DETERMINATION OF WATER VAPOUR
A-5.1 General
Four methods have been prescribed. Three methods
are instrumental namely, electrolytic hygrometer, frost
or dew point hygrometer and capacitance hygrometer.
Fourth one is absorption method. For routine analysis
any of the methods may be employed. However, in
case of any dispute in the determination of water
vapour, absorption method shall be used as a referee
method.

A-3.1.1.2 Apparatus
The instrument should be capable of determining
oxygen in the range of 0 to 1 vpm, 0 to 10 vpm, 0 to
100 vpm and 0 to 1 000 vpm.
A-3.1.1.3 Procedure

A-5.1.1 Electrolytic Hygrometer

The procedure to be followed for the determination

shall depend on the type of analyser used. The
manufacturer's instructions in this regard shall be
followed.

The procedure for carrying out the determination shall

be the same as prescribed under A-2.

The method is based on the absorption and electrolysis

of the water vapour present in the sample gas. The
electrolytic current gives a direct measurement of
water vapour present in the gas flowing through the
instrument at a steady rate. The exact procedure to be
followed shall depend on the type of apparatus to be
used. The instrument manufacturer's instructions in
this regard shall be followed.

A-4 DETERMINATION OF NITROGEN

A-5.1.2 Frost or Dew Point Hygrometer

A-4.1 General

A metal surface on the hygrometer is cooled so that

dew or frost is formed from the water vapour content
of the gas at a particular pressure which may be
observed optically in the apparatus. The temperature
at which the dew or frost is formed is a measure of
water vapour content of the gas. The exact procedure
to be followed shall depend upon the type of apparatus
to be used. The instrument manufacturer's instructions
in this regard shall be followed.

A-3.1.2 Gas Chromatographic Method

Two methods have been prescribed, namely, gas

chromatographic method and spectra analysis method.
A-4.1.1 Spectra Analysis Method
A-4.1.1.1 Principle
The spectra analyser determines nitrogen in argon in
the range of 0 to 100 vpm. The analyser is based around
a pyrex/quartz cell through which the test gas is passed.
A high a.c. Voltage is applied to this cell which causes
ionization of the gas and consequent emission of light.
A particular and proportionate fraction of this light
results from the ionization of nitrogen which is present
in the sample. The intensity of emission of light is
proportional to the nitrogen concentration. The
emitted light through a chopper and narrow band
interference filter. The transmitted light, which is
proportional to the nitrogen present in the test gas, is
detected by a photo-multiplier tube and converted into
electrical signal. The signal is pre-amplified and
measured. The analyser is to be calibrated by a
standard gas mixture.

A-5.1.3 Capacitance Hygrometer

The method is based on the change of capacitance of
the sensor when a sample gas containing water vapour
passes through it. The change in capacitance gives a
direct measurement of water vapour present in the gas.
The procedure to be followed shall depend upon the
type of apparatus to be used. The instrument
manufacturer's instructions in this regard shall be
followed.
A-5.1.4 Absorption Method
A-5.1.4.1 Apparatus
The apparatus consists of the following parts
assembled as shown in Fig. 2.

A-4.1.1.2 Procedure

A-5.1.4.1.1 Gas meter accurate to I percent

It shall depend on the type of analyser used. The

instrument manufacturer's instructions in this regard
shall be followed.

A-5.1.4.1.2 Absorption train

Three U-tubes containing phosphorus pentoxide
connected in series to the gas meter. The one near to
3

IS 5760 : 1998

FIG. 2 ASSEMBLY OF APPARATUS FOR THE DETERMINATION OF MOISTURE

the gas meter will serve as a guard to prevent moisture

from backing into the first two tubes.

gases absorb energy at characteristic wavelengths

when subjected to infra-red radiation. The procedure
to be followed for determining the impurities shall
depend on the type of apparatus to be used. The
instrument manufacturer's instructions in this regard
shall be followed.

A-5.1.4.2 Procedure
Connect the 3 tubes in series to the inlet of the gas
meter and connect the free end of U-tubes to the gas
sample. Allow the gas to flow through the train for a
while to saturate the water in the gas meter with the
gas as well as replacing the air in the first two U-tubes.
Stop the gas flow, close the stopcocks of the U-tubes
and weigh the first two U-tubes. Connect again,
record the meter reading. Pass the gas through the train
at the rate of 10 litres per hour for 4 to 5 h. Close the
gas supply and record the meter reading. Remove the
first two U-tubes and weigh.

A-6.1.2 Electrochemical Method

When a gas containing carbon dioxide passes through
a reactive liquid, the electrical conductivity of the
liquid changes depending on the carbon dioxide
content. The measurement of the change in electrical
conductivity gives a direct measurement of the carbon
dioxide content. The procedure to be followed shall
depend upon the type of apparatus to be used. The
instrument manufacturer's instructions in this regard
shall be followed.

A-5.1.4.3 Calculation
Convert the volume of gas taken for the test to normal
temperature and pressure. From the increase in weight,
calculate the volume of water vapour present on the
basis that 1 g of water is equivalent to 1.244 litres of
water vapour at normal temperature and pressure and
express the result as percentage by volume.

A-6.1.3 Gas Chromatographic Method

The procedure for carrying out the determination shall
be the same as prescribed under A-2.
A-7 DETERMINATION OF CARBON
MONOXIDE

A-6 DETERMINATION OF CARBON

DIOXIDE

A-7.1 General

A-6.1 General
Three methods have been prescribed, namely,
infra-red analyser, electrochemical method and gas
chromatographic method.

Two methods have been prescribed namely, gas

chromatographic method and infra-red analyser
method.

A-6.1.1

A-7.1.1 Gas Chromatographic Method

Infra-Red Analyser

The infra-red analysers are used for determining

impurities of hetro-atomic gases. The hetro-atomic

The procedure for carrying out the determination shall

be the same as prescribed under A-2.
4

IS 5760 : 1998
A-7.1.2 Infra-Red Analyser Method

A-8.1.3 Total Hydrocarbon Analyser Method

The procedure for carrying out the determination shall

be the same as prescribed under A-6.1.1.

A-8.1.3.1 Principle
The sample containing hydrocarbon impurities is
burnt in a jet of hydrogen in the flame ionization
detector and the organic component present in the
sample gas provide the source of ions. Concentration
of ions is proportional to the concentration of
organic components. Electrodes having considerable
potential differnce between them are used to measure
the current produced due to ionization and the
instrument is calibrated in the terms of concentration
of hydrocarbons.

A-8 DETERMINATION OF HYDROCARBONS

A-8.1 General
Three methods have been prescribed, namely, gas
chromatographic method, infra-red analyser method
and total hydrocarbon analyser method.
A-8.1.1 Gas Chromatographic Method
The procedure for carrying out the determination shall
be the same as prescribed under A-2.

A-8.1.3.2 Procedure
Calibrate the instrument against calibration gas of
known concentration of hydrocarbon following the
instructions of the manufacturer. Then carry out the
test according to the manufacturers instructions.

A-8.1.2 Infra-Red Analyser Method

The procedure for carrying out the determination shall
be the same as prescribed under A-6.1.1.

ANNEX B
(Clause 7)
SAMPLING OF COMPRESSED ARGON
B-1 SCALE OF SAMPLING

Table 2 Number of Cylinders to be Selected

(Clause B-1.2)

B-1.1 Lot
In any consignment, all cylinders charged at a time
from one charging manifold shall constitute a lot.

Lot Size

B-1.2 The number of cylinders (n) to be selected

from a lot shall depend on the size of the lot (N) and
shall be in accordance with col 1 and 2 of Table 2.

(1)
Up to 50
51 to 100
101 to 150
151 to 300

(N)

B-1.2.1 The cylinders shall be selected at random and

in order to ensure the randomness of selection, a
random number table (see IS 4905) shall be used. In
case such a table is not available, the following
procedure shall be followed:

301 and above

Number of Cylinders
to be Selected
(n)
(2)
5
8
15
20
25

B-3 NUMBER OF TESTS

All the individual test samples in B-2 shall be tested
separately for the requirements given in Table 1.

Starting from any cylinder in the lot, count them in

one order as 1, 2, 3
up to r and soon, where
r is the integral part of N/n. Every rth cylinder thus
counted shall be withdrawn to give the sample for
test.

B-4 CRITERIA FOR CONFORMITY

A lot shall be declared as conforming to the
requirements of this specification if all individual
samples tested, pass the requirements prescribed
in 5.2.

B-2 TEST SAMPLES

A sample of gas shall be drawn from each cylinder
selected as in B-1.2 and shall be the individual test
sample from each cylinder.

IS 5760 : 1998

ANNEX C
(Foreword)
COMMITTEE COMPOSITION
Industrial Gases Sectional Committee, CHD 006
Chairman
SHRI I MOOKHERJEE
Praxair India Private Limited, Raheja Towers,
6th Floor, East Wing, 26-27, M G Road, Bangalore 560001
Members
SHRI A K AGARWALA

Representing
Hindustan Gas and Industries Ltd, 24 Parganas (WB)

SHRI I B PRASAD ( Alternate )

SHRI A K ANEJA
SHRI M P DHANUKA ( Alternate )
SHRI D BANDHYOPADHYAY

Steel Authority of India Ltd, New Delhi

SHRI S G K MURTHY ( Alternate )

SHRI SHAISH KUMAR

Department of Industrial Policy and Promotion, New Delhi

SHRI B B SHARMA (Alternate)

SHRI H P DUBEY

National Test House, Calcutta

Asiatic Oxygen Ltd, Calcutta

DR B B PAI ( Alternate )
SHRI T GARG

Industnal Gases Ltd, Calcutta

SHRI N K RAI ( Alternate I )

SHRI L R GARG ( Alternate II )
SHRI D R GHOSAI

Rashtnya Chemicals and Fertilizers Ltd, Mumbai

SHRI M KALYANARAMAN( Alternate )

REPRESENTATIVF
SHRI P R NARASIMHAN
SHRI R P KATHOR
DR K N NINAN

IOL Ltd, Calcutta

Bharal Electronics Ltd, Bangalore
Bombay Oxygen Ltd, Mumbai
Vikram Sarabhai Space Centre, Thiruvanathapuram

SHRI A K MUKHOPADHYAY ( Alternate )

DR U C PANDEY
SHRI S S N PRASAD
DR BADRI PRASAD

Department of Electronics, New Delhi

Semi Conductor Complex Ltd, Punjab
Central Revenues Control Laboratory, New Delhi

DEPUTY CHIEF CHEMIST ( Alternate )

SHRI H N SINHA
SHRI N V S RAMANI

Asiatic Oxygen and Acetate Co Ltd, Calcutta

Bharat Heavy Electncals Ltd, Hyderabad

SHRI K P JAFFAR ALI ( Alternate )

SHRI M I ALAM
SHRI A S GHOSHAL

Central Electronics Ltd, Ghaziabad

Chief Controller of Explosives, Nagpur

SHRI S K BHARDWAJ ( Alternate )

SHRI P K JAIN
SHRI R S SAIGAI

Industrial Oxygen Co Ltd, Mumbai

All India Industnal Gas Manufacturers Association, New Delhi

DR P L BHATIA ( Alternate )
SHRI B D REHANI

Gujarat State Fertilizer Corporation, Vadodara

SHRI R N CHOKHSI ( Alternate )

SHRI S K KAPOOR

Laxman Sylvanu Ltd, New Delhi

SHRI N SIKKA ( Alternate )

SHRI S K SRIVASTAVA
SHRI S P SINGH ( Alternate )
DR V N SINGH
DR R S RAJAGOPALAN,

Ministry of Defence (DGQA), New Delhi

Ordinance Factory, Bhandara
Director General, BIS (Ex officio Member)

Director (Chem)
Member Secretary
SIIRI S MAJUMDER
JOINT DIRECTOR (Chem), BIS

( Continued on page 7 )

IS 5760 : 1998
( Continued from page 6 )

Oxygen, Argon, Acetylene, Hydrogen, Nitrogen, Carbon Dioxide, Helium Subcommittee, CHD 006 01
Convener
SHRI 1 MOOKHERJEE

Praxair India Private Limited, Raheja Towers,

6th Floor, East Wing, 26-27, M G Road, Bangalore 560001
Members
SHRI R C

AGGARWAL

Representing
Asiatic Oxygen Ltd, Calcutta

SHRI M P DHANUKA (Alternate)

SHRI M

BANDOPADHYAY

Electric Lamp Mfrs (I) Ltd, Calcutta

SHRI S B BHATTACHARYA (Alternate)

SHRI F L

DADABHOY

South India Carbonic Gas Industries Ltd, Chennai

SHRI T JAGDEESAN ( Alternate )

SHRI H

P DUBEY

National Test House, Calcutta

DR S RAHUT ( Alternate )
SHRI T GARG

Industrial Gases Ltd, Calcutta

SHRI N K PAI ( Alternate I )

SHRI RAM SINGH ( Alternate II )
SHRI D
DR E

R GHOSAL
R JAYNARAYANA

SHRI M

PATEL

Rashtriya Chemicals Fertilizers Ltd, Calcutta

Mohan Meakins Ltd, Mohan Nagar
Gujarat State Fertilizer Corporation, Vadodara

SHRI JASALPURA ( Alternate )

REPRESENTATIVE
REPRESENTATIVE
SHRI S L ROY

Laxman Sylvania Ltd, New Delhi

RDSO, Lucknow
Kamrup Industnal Gases Ltd, Calcutta

SHRI D K GARG ( Alternate )

SHRI R S SAIGAL

All India Industrial Gas Manufacturers Association, New Delhi

DR P L BHATIA( Alternate )
SHRI V

K SHARMA

Hindustan Lever Ltd, Mumbai

SHRI R J A PAI ( Alternate )

SHRI P K VERMA

National Thermal Power Corporation, New Delhi

SHRI P K BANERJEE ( Alternate )

Bureau of Indian Standards

BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods
and attending to connected matters in the country
Copyright
BIS has the copyright of all its publications No
without the prior permission in writing ot BIS
implementing the standard, of necessary details,
Enquiries relating to copyright be addressed to

part of these publications may be reproduced in any form

This does not preclude the tree use, in the course of
such as symbols and sizes, type or grade designations
the Director (Publications), BIS

Review of Indian Standards

Amendments are issued to standards as the need arises on the basis of comments Standards are also
reviewed periodically, a standard along with amendments is reaffirmed when such review indicates that
no changes are needed, if the review indicates that changes are needed, it is taken up for revision Users
of Indian Standards should ascertain that they are in possession of the latest amendments or edition by
referring to the latest issue of 'BIS Handbook' and 'Standards Monthly Additions'
This Indian Standard has been developed from Doc

No

CHD 6 ( 2 5 8 )

Amendments Issued Since Publication

Amend No

Date of Issue

Text Affected

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