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P/M Parts

(a)

(b)

FIGURE 11.1 (a) Examples of typical parts made by powder-metallurgy processes. (b) Upper trip lever for a
commercial irrigation sprinkler, made by P/M. Made of unleaded brass alloy, it replaces a die-cast part, at a 60%
cost savings. Source: Courtesy of Metal Powder Industries Federation.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Particle Shapes
Acicular (chemical
decomposition)

Irregular rodlike
(chemical decomposition,
mechanical comminution)

(a) One-dimensional

Spherical
(atomization,
carbonyl (Fe),
precipitation
from a liquid)

Flake (mechanical
comminution)

Dendritic
(electrolytic)

(b) Two-dimensional

Irregular
(atomization,
chemical
decomposition)

Rounded
(atomization,
chemical
decomposition)

Porous
(reduction
of oxides)

Angular
(mechanical
disintegration,
carbonyl (Ni ))

(c) Three-dimensional

FIGURE 11.2 Particle shapes and characteristics of metal powders and the processes by which they are produced.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Powder Production
Ladle
Molten metal

Tundish

Tundish

High-pressure
water manifold

Atomizing
gas spray

Atomization tank

Atomizing chamber
Metal particles

Water
atomization

Dewatering

(b)

(a)

Inert gas
Vacuum

Ladle

Rotating consumable
electrode

Molten metal
Tundish

Spindle
Liquid metal
Nonrotating
tungsten electrode

Metal particles

Collection port

Spinning disk
(c)

(d)

FIGURE 11.3 Methods of metal-powder production by atomization: (a) gas atomization; (b) water
atomization; (c) atomization with a rotating consumable electrode; and (d) centrifugal atomization
with a spinning disk or cup.
Manufacturing Processes for Engineering Materials, 5th ed.
Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Particle Size Distribution


Cumulative weight finer (%)

20

Weight (%)

15
10
5
0
10

100
Particle size (m)

1000

(a)

100
75
50
25
0
10

100
Particle size (m)

1000

(b)

FIGURE 11.4 (a) Distribution of particle size, given as weight percentage; note that the highest
percentage of particles have a size between 75 and 90 m. (b) Cumulative particle-size distribution as a
function of weight. Source: After R.M. German.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Compaction
Upper punch
Compacted
shape
(green)

Powder
Feed
Shoe
Die
Lower punch

1.

2.

3.
Ejector

4.

(a)

Upper punch
P/M spur gear
(green)
Die
Core rod

Lower punch

(b)
Manufacturing Processes for Engineering Materials, 5th ed.
Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

FIGURE 11.5 (a) Compaction of metal powder to produce a


bushing. (b) A typical tool and die set for compacting a spur
gear. Source: Courtesy of Metal Powder Industries Federation.

Density vs. Compacting Pressure


1000 1200

0.29
0.3

s
Ten

200

Copper powder, coarse


Copper powder, fine
Iron powder, coarse
Iron powder, fine

2
1
0
0

20
40
60
80
Compacting pressure (tons/in2)

0.1

100
0
100

(a)

y
vit

t io

20

40

100

35

95

30

ga

Apparent
Density
3.49 g/cm3
1.44
2.75
1.40

150

nd

g th

on

Co

ti
uc

il e

n
s tr e

0.32

El

0.2

25
psi x 103

Density
of copper

Density
of iron

lb/in3

0.31

30

7
Density (g/cm3)

0.30

15

10

8.0

8.2
8.4
8.6
8.8
Sintered density (g/cm3)

90

25

85

20

80

Electrical conductivity (% IACS)

400

Elongation (%)

200

lb/in3

Tensile strength (MPa)

MPa
600
800

(b)

FIGURE 11.6 (a) Density of copper- and iron-powder compacts as a function of compacting pressure. Density greatly influences
the mechanical and physical properties of P/M parts. Source: After F.V. Lenel. (b) Effect of density on tensile strength, elongation,
and electrical conductivity of copper powder. (IACS is International Annealed Copper Standard for electrical conductivity.)

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Mechanics of Compaction
L/D = 1.66
700 MPa
600
500
400
300

200
100

(a)

(b)

(c)

(d)

D/ 2
C
L
(e)

p0

px

!r

dx

FIGURE 11.7 Density variation in compacting


metal powders in different dies: (a) and (c) singleaction press; (b) and (d) double-action press,
where the punches have separate movements.
Note the greater uniformity of density in (d) as
compared with (c). Generally, uniformity of
density is preferred, although there are situations
in which density variation, and hence variation of
properties, within a part may be desirable. (e)
Pressure contours in compacted copper powder
in a single-action press. Source: After P. Duwez
and L. Zwell.

Resultant pressure distribution:

!r
px + d p x

FIGURE 11.8 Coordinate system and stresses acting on an element in


compaction of powders. The pressure is assumed to be uniform across the
cross-section. (See also Fig. 6.4.)
Manufacturing Processes for Engineering Materials, 5th ed.
Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

px = poe4kx/D

Cold Isostatic Pressing


Upper cover
Cover

Wire
mesh basket

Pressure
vessel

Mold
seal plate

Metal
mandrel

Rubber
mold (bag)

Fluid

Pressure
vessel
Rubber
diaphragm

Pressing
rubber mold
Forming
rubber mold

Fluid

Powder

Powder
Pressure
source

Pressure
source

Lower
outside cover

Lower inside
cover
(a)

(b)

FIGURE 11.9 Schematic illustration of cold isostatic pressing in compaction of a tube. (a) The wet-bag process, where the rubber
mold is inserted into a fluid that is subsequently pressurized. In the arrangement shown, the powder is enclosed in a flexible
container around a solid core rod. (b) The dry bag process, where the rubber mold does not contact the fluid, but instead is
pressurized through a diaphragm. Source: After R.M. German.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Pressures and Capabilities


30
HIP
0.6
CIP
0.4

in.

Size (m)

20

P/F
0.2

10
P/M
PIM

1
2
3
4
5
Relative shape complexity

FIGURE 11.10 Process capabilities of part size


and shape complexity for various P/M
operations; P/F is powder forging. Source: Metal
Powder Industries Federation.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Metal
Aluminum
Brass
Bronze
Iron
Tantalum
Tungsten
Other Materials
Auminum oxide
Carbon
Cemented carbides
Ferrites

Pressure
MPa
psi 103
70275
400700
200275
350800
70140
70140

1040
60100
3040
50120
1020
1020

110140
140165
140400
110165

1620
2024
2060
1624

TABLE 11.1 Compacting Pressures for Various


Metal Powders

Hot Isostatic Pressing


Gas inlet

End cap
Pressure

Insulation
Heating coils
Workpiece

Temperature
Time

High-pressure
cylinder

Part

End cap
1. Fill can

2. Vacuum
bakeout

3. Hot isostatic press

4. Remove can

FIGURE 11.11 Schematic illustration of the sequence of steps in hot isostatic pressing. Diagram (4)
shows the pressure and temperature variation versus time.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Powder Rolling
Metal powder supply

Direction baffles

Hopper

Powder

Green sheet
Hot rolls

Shaping rolls

Coiler

Sintering furnace
Cooling

FIGURE 11.12 An example of powder rolling. The purpose of direction baffles in the
hopper is to ensure uniform distribution of powder across the width of the strip.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Spray Casting
Induction-heated
ladle
Atomizer
(nitrogen gas)

Particle injector
(optional)

Recipient
substrate
Tube
Deposition
chamber

FIGURE 11.13 Spray casting (Osprey process) in which molten metal is sprayed over a
rotating mandrel to produce seamless tubing and pipe.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Sintering
1.
R

1.
Neck formation
by vapor-phase
material transport

Neck formation
by diffusion
2.

2.
R
Distance between
particle centers
decreased, particles
bonded

3.

3.

(a)

(b)

TABLE 11.2 Sintering temperature and


time for various metal powders.
Manufacturing Processes for Engineering Materials, 5th ed.
Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Particles bonded,
no shrinkage (center
distances constant)

FIGURE 11.14 Schematic illustration of two


basic mechanisms in sintering metal powders:
(a) solid-state material transport and (b)
liquid-phase material transport. R=particle
radius, r=neck radius, and =neck profile
radius.

Material
Copper, brass, and bronze
Iron and iron graphite
Nickel
Stainless steels
Alnico alloys (for permanent magnets)
Ferrites
Tungsten carbide
Molybdenum
Tungsten
Tantalum

Temperature ( C)
760900
10001150
10001150
11001290
12001300
12001500
14301500
2050
2350
2400

Time (min)
1045
845
3045
3060
120150
10600
2030
120
480
480

Effect of Temperature and Time


40

20
1

Elongation (%)

30

31

C
5

0
23

C(

0
5
2
2

C (2 0

0
2
11

10

4
(2

F
0

F)

5 0 F)

30
60
90
120
Sintering time (min)
(a)

150

112
0C
(205
0F)

20.4

12
30
C

20.8

21.2

15
13

Dimensional change from die size (%)

21.6

(22
50
F)

(2
40
0
F)

30
60
90
120
Sintering time (min)

150

(b)

FIGURE 11.5 Effect of sintering temperature and time on (a) elongation and (b) dimensional
change during sintering of type 316L stainless steel. Source: ASM International.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Mechanical Properties of P/M Materials


Designation
Ferrous
FC-0208

MPIF
type
N
R
S

FN-0405

S
T

Aluminum
601 AB
pressed bar
Brass
CZP-0220

T
U
W

Condition

Ultimate
Tensile
Strength
(MPa)

Yield
Strength
(MPa)

AS
HT
AS
HT
AS
HT
AS
HT
AS
HT

225
295
415
550
550
690
425
1060
510
1240

205

330

395
655
240
880
295
1060

45
95
70
35
80
40
72
39
80
44

AS
HT

110
252

48
241

165
193
221

76
89
103

Elongation
in 25 mm
(%)

Elastic
Modulus
(GPa)

< 0.5
< 0.5
1
< 0.5
1.5
< 0.5
4.5
1
6
1.5

70
70
110
110
130
130
145
145
160
160

60 HRH
75 HRH

6
2

55 HRH
68 HRH
75 HRH

13
19
23

Hardness
HRB
HRB
HRB
HRC
HRB
HRC
HRB
HRC
HRB
HRC

Titanium
Ti-6AI-4V
HIP
917
827

13
Superalloys
Stellite 19

1035

49 HRC
<1
Note: MPIF=Metal Powder Industries Federation; AS=as sintered; HT=heat treated;
HIP=hot isostatically pressed.

TABLE 11.3 Typical mechanical properties of selected P/M materials.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Titanium Property Comparison


Density
(%)
100
100

Yield Stress
(MPa)
840
875

Ultimate Tensile
Strength (MPa)
930
965

Elongation
(%)
7
14

Reduction of
Area (%)
15
40

875
875
975

8
9
14

14
17
26

Process
Cast
Cast and forged
Powder metallurgy
Blended elemental (P+S)
98
786

Blended elemental (HIP)


> 99
Realloyed (HIP)
100
880

P+S=pressed and sintered; HIP=hot isostatically pressed.


Source: After R.M. German

TABLE 11.4 Mechanical property comparison for Ti-6Al-4V titanium alloy.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

P/M Example: Bearing Caps

FIGURE 11.16 Powder-metal main bearing caps for 3.8- and 3.1-liter General Motors engines.
Source: Courtesy of Zenith Sintered Products, Inc., Milwaukee, WI.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Geometry for P/M Dies


Step requires up
to 12 taper to
assist ejection
0.250.50 mm parallel
surface to prevent
punch jamming
23 taper to
assist ejection
0.12 0.25 mm
parallel surface to
prevent powder
capture in die

Upper punch
Die
Workpiece

Maximum feasible taper


is 15 when bottom
compaction is employed
0.250.50 mm step
to prevent powder
capture in die
Lower punch

FIGURE 11.17 Die geometry and design features for powder-metal compaction.
Source: Metal Powder Industries Federation.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Poor

Poor

Good

Good
Fillet
radius

Sharp
radius

Design
Considerations

Fillet radius

Sharp radius
(a)

Sharp radius

(e)

Sharp
radius

Fillet radius

Fillet
radius

(b)

(f)

Acceptable
Die

Best

Punch

0.25 mm
(0.010 in.)
(min)

3045

Max 30
Can be
molded

Must be
machined

Workpiece
(g)

(c)

Upper
punch

0.25 mm
(0.010 in.)
(min)

Die

Acceptable, with additional operations

Feather edge
required on
punch
Flat
Hole must
be drilled

Workpiece
(d)

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Thread must be
machined
(h)

FIGURE 11.18 Examples of P/M parts,


showing various poor and good designs.
Note that sharp radii and reentry corners
should be avoided, and that threads and
transverse holes have to be produced
separately, by additional operations such
as machining or grinding. Source: Metal
Powder Industries Federation.

Design Considerations
Poor

Poor

Good

Good

Thicker flange

up to 12
r

Thin section

Taper to
assist ejection
Radius for ease
of ejection
Radius to reduce
likelihood of chipping

0.2H (max)
H

(a)

0.15H (max)
H

FIGURE 11.19 (a) Design features for


use with unsupported flanges. (b)
Design features for use with grooves.
Source: Metal Powder Industries
Federation.

(b)

Excessive
binder

Powder
build-up

Flow
direction

FIGURE 11.20 The use of abrupt transitions in molds


for powder injection molding causing non-uniform
metal-powder distribution within a part.
Manufacturing Processes for Engineering Materials, 5th ed.
Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Mold

Excessive
binder

Process Comparison
Process
Casting

Advantages Over P/M


Wide range of part shapes and sizes
produced; generally low mold and
setup cost.

Forging (hot)

High production rate of a wide range


of part sizes and shapes; high mechanical properties through control of
grain flow.
High production rate of long parts;
complex cross-sections may be produced.
Wide range of part shapes and sizes;
short lead time; flexibility; good dimensional control and surface finish;
simple tooling.

Extrusion (hot)
Machining

Limitations as Compared With P/M


Some waste of material in processing;
some finishing required; may not be
feasible for some high-temperature alloys.
Some finishing required; some waste
of material in processing; die wear;
relatively poor surface finish and dimensional control.
Only a constant cross-sectional shape
can be produced; die wear; poor dimensional control.
Waste of material in the form of chips;
relatively low productivity.

TABLE 11.5 Competitive features of P/M and some other manufacturing processes.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Type
Oxide Ceramics
Alumina

General Characteristics

Zirconia
Carbides
Tungsten carbide
Titanium carbide
Silicon carbide
Nitrides
Cubic boron nitride
Titanium nitride
Silicon nitride
Sialon
Cermets
Nanophase ceramics
Silica
Glasses
Glass ceramics
Graphite
Diamond

High hot hardness and abrasion resistance, moderate strength and toughness; most
widely used ceramic; used for cutting tools, abrasives, and electrical and thermal
insulation.
High strength and toughness; resistance to thermal shock, wear, and corrosion;
partially-stabilized zirconia and transformation-toughened zirconia have better
properties; suitable for heat-engine components.
High hardness, strength, toughness, and wear resistance, depending on cobalt binder
content; commonly used for dies and cutting tools.
Not as tough as tungsten carbide, but has a higher wear resistance; has nickel and
molybdenum as the binder; used as cutting tools.
High-temperature strength and wear resistance, used for engines components and
as abrasives.
Second hardest substance known, after diamond; high resistance to oxidation; used
as abrasives and cutting tools.
Used as coatings on tools, because of its low friction characteristics.
High resistance to creep and thermal shock; high toughness and hot hardness; used
in heat engines.
Consists of silicon nitrides and other oxides and carbides; used as cutting tools.
Consist of oxides, carbides, and nitrides; high chemical resistance but is somewhat
brittle and costly; used in high-temperature applications.
Stronger and easier to fabricate and machine than conventional ceramics; used in
automotive and jet-engine applications.
High temperature resistance; quartz exhibits piezoelectric effects; silicates containing various oxides are used in high-temperature, nonstructural applications.
Contain at least 50% silica; amorphous structure; several types available, with a
wide range of mechanical, physical, and optical properties.
High crystalline component to their structure; stronger than glass; good thermalshock resistance; used for cookware, heat exchangers, and electronics.
Crystalline form of carbon; high electrical and thermal conductivity; good thermalshock resistance; also available as fibers, foam, and buckyballs for solid lubrication;
used for molds and high-temperature components.
Hardest substance known; available as single-crystal or polycrystalline form; used
as cutting tools and abrasives and as die insert for fine wire drawing; also used as
coatings.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Types of
Ceramics
and
Glasses

TABLE 11.6 Types and general


characteristics of ceramics and
glasses.

Ceramic Structure
Silicon ions
Oxygen ions

Aluminum ions
OH ions

FIGURE 11.21 The crystal structure of kaolinite, commonly known as clay;


compare with Figs. 3.2-3.4 for metals.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Properties of Ceramics
Transverse
Rupture
Compressive
Elastic
Strength
Strength
Modulus
Material
Symbol
(MPa)
(MPa)
(GPa)
Aluminum oxide
Al2 O3
140240
10002900
310410
Cubic boron nitride
cBN
725
7000
850
Diamond

1400
7000
8301000
Silica, fused
SiO2

1300
70
Silicon carbide
SiC
100750
7003500
240480
Silicon nitride
Si3 N4
480600

300310
Titanium carbide
TiC
14001900
31003850
310410
Tungsten carbide
WC
10302600
41005900
520700
Partially stabilized zirconia
PSZ
620

200
Note: These properties vary widely, depending on the condition of the material.

Hardness
(HK)
20003000
40005000
70008000
550
21003000
20002500
18003200
18002400
1100

Poissons
Ratio
()
0.26

0.25
0.14
0.24

0.3

Density
(kg/m3 )
40004500
3480
3500

3100
3300
55005800
10,00015,000
5800

TABLE 11.7 Approximate range of properties of various ceramics at room temperature.

Strength:

Elastic modulus:

Thermal conductivity:

UTS UTSoenP

E Eo(1 1.9P + 0.9P2)

k = ko(1 P)

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Temperature Effects
1.8

Ni-base
superalloy

600

1.0

500

Polyethylene
Nylon

Al alloys
ZrSiO4
(zircon)

0.8
0.6

SiC

0.2

400

High-purity SiC
SiC

300

200 Sialon 116

0
20.2

Glass ceramic
Low-density SiC
0

200

400

FIGURE 11.22
Effect of
temperature on thermal
expansion for several ceramics,
metals, and plastics. Note that
the expansions for cast iron and
for partially stabilized zirconia
(PSZ) are within about 20%.

80
70

50
40

20
10

0
600 800 1000 1200 1400 1600
Temperature (C)

200 400 600 800 1000 1200 1400 1600


Temperature (C)

FIGURE 11.23
Effect of
temperature on the strength
of various engineering
ceramics. Note that much of
the strength is maintained at
high temperatures; compare
with Figs. 2.9 and 8.30.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

400

90

30

Silicon nitride (reaction bonded)

2400

60

60

Al2O3

100
Lithium aluminum silicate
Fused
SiO2

2500

High-purity silicon nitride

Si3N4
0.4

2000

High-purity silicon nitride


(Fine grain)
Tensile strength (MPa)

Linear thermal expansion (%)

1.2

1000

Al2O3

1.6
1.4

500

800

F
1600

SiC

50

TiC
Al2O3

40
MgO
30

300
Si3N4

ThO2

20

200

SrO2

MgAl2O4

10
0
0

400
800
1200
Temperature (C)

100

0
1600

FIGURE 11.24
Effect of
temperature on the modulus
of elasticity for various
ceramics; compare with Fig.
2.9. Source: After D.W.
Richerson.

GPa

F
1500

Modulus of elasticity (psi x 106)

2.0

F
800 1200 1600 2000 2400 2800 3200
Partially
stabilized
Cast iron and MgO
ZrO

psi x 10 3

400

Example: Ceramic Bearings

(a)

(b)

FIGURE 11.25 A selection of ceramic bearings and races. Source: Courtesy of Timken, Inc.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Processes & Particle Production


FIGURE 11.26 Methods of crushing ceramics
to obtain very fine particles: (a) roll crushing, (b)
ball milling, and (c) hammer milling.
(a)

(c)

(b)

Process
Slip casting
Extrusion
Dry pressing

TA B L E 1 1 . 8
characteristics of
processing methods.

General
ceramics

Advantages
Large parts; complex shapes; low equipment cost.
Hollow shapes and small diameters; high
production rate.
Close tolerances; high production rate
with automation.

Wet pressing

Complex shapes; high production rate.

Hot pressing

Strong, high-density parts.

Isostatic pressing
Jiggering

Uniform density distribution.


High production rate with automation;
low tooling cost.
Complex shapes; high production rate.

Injection molding

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Limitations
Low production rate; limited dimensional
accuracy.
Parts have constant cross-section; limited
thickness.
Density variation in parts with high
length-to-diameter ratios; dies require
high abrasive-wear resistance; equipment
can be costly.
Limited part size and dimensional accuracy; tooling costs can be high.
Protective atmospheres required; die life
can be short.
Equipment can be costly.
Limited to axisymmetric parts; limited dimensional accuracy.
Tooling costs can be high.

Slip Casting
Trimming
knife

(a)

(b)

(c)

(d)

FIGURE 11.27 Sequence of operations in slip casting a ceramic part. After the slip
has been poured, the part is dried and fired in an oven to give it strength and
hardness. The step in (d) is a trimming operation. Source: After F.H. Norton.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

(e)

Doctor-Blade Process
Air (filtered)
in
Ceramic tape
on carrier tape
Drying
chamber

Exhaust
out

Slurry chamber and


doctor blade

Ceramic
slurry

FIGURE 11.28 Production of ceramic sheets through the


doctor-blade process.

Take-up
spool
Controller
for take-up
spool

Carrier film

Doctor blade
Ceramic film

Carrier film

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Density Variation in Compacts


Punch

L
= 1.75
D
90

0
10

Die

65
50
54
40

L
20
10

Punch
D

FIGURE 11.29 Density variation in pressed compacts in a single-action press. Note that the
variation increases with increasing L/D ratio; see also Fig. 11.7e. Source: After W.D. Kingery.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Extruding and Joggering


Water
To vacuum

Bat former

Jigger tool

Deairing Clay
chamber slug

Formed
ware

FIGURE 11.30 (a) Extruding and (b) jiggering


operations in shaping ceramics. Source: After R.F.
Stoops.
Extruder
Mold return
(a)

(b)

FIGURE 11.31 Shrinkage of wet clay, caused by


removal of water during drying; shrinkage may be as
much as 20% by volume. Source: After F.H. Norton.
Interparticle
water
(a)
Manufacturing Processes for Engineering Materials, 5th ed.
Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Pore
water
(b)

Clay
particles

Dry
(c)

Glasses

Density
Strength
Resistance to thermal shock
Electrical resistivity
Hot workability
Heat treatability
Chemicals resistance
Impact abrasion resistance
Ultraviolet-light transmission
Relative cost

Soda-lime
Glass
High
Low
Low
Moderate
Good
Good
Poor
Fair
Poor
Lowest

Lead
Glass
Highest
Low
Low
Best
Best
Good
Fair
Poor
Poor
Low

Borosilicate
Glass
Medium
Moderate
Good
Good
Fair
Poor
Good
Good
Fair
Medium

TABLE 11.9 General characteristics of various types of glasses.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Fused
Low
High
Better
Good
Poor
None
Better
Good
Good
High

96% Silica
Glass
Lowest
Highest
Best
Good
Poorest
None
Best
Best
Good
Highest

Glass Sheet & Tubing


Controlled
Molten
atmosphere furnace
tin

Molten glass

Tube
Mandrel

Rollers
Furnace

Float bath

Lehr

FIGURE 11.32 The float method of


forming sheet glass. Source: Corning
Glass Works.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Rollers

FIGURE 11.33
Continuous manufacturing
process for glass tubing. Air is blown through the
mandrel to keep the tube from collapsing. Source:
Corning Glass Works.

Glass Bottles
Blow
head

Gob

Baffle

Air
Blank
mold

Neck
ring

Tip
Air

1. Gob falling into


blank mold

2. Gob in
blank mold

3. Blow down
in blank mold

4. Blow back in
blank mold

Air

Tongs

Blow
mold
Parison

5. Blank mold
reversed

6. Parison hanging on
neck ring, reheated
during transfer

7. Parison in
blow mold

8. Bottle blown,
cooling

9. Finished bottle
removed by tongs

FIGURE 11.34 Stages in manufacturing a common glass bottle. Source: After F.H. Norton.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Glass Pressing

1. Empty mold

2. Loaded mold

3. Glass pressed

4. Finished piece

FIGURE 11.35 Manufacturing steps for a glass item by pressing in a mold. Source: Corning Glass Works.

1. Empty mold

2. Loaded mold

3. Glass pressed

4. Finished
product

FIGURE 11.36 Pressing glass in a split mold. Note that the use of a split mold is essential to be
able to remove the part; see also Figs. 10.34, 10.35, and 10.36. Source: After E.B. Shand.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Residual Stresses in Glass


Step 1

Step 2

Step 3
Thickness

1. Hot glass,
no stresses.

2. Surface cools quickly,


surface contracts,
center adjusts, only
minor stresses.

3. Center cools,
center contracts,
surface is compressed,
center in tension.

(a)

Compression

Tension

Residual stresses
(b)

FIGURE 11.37 Stages in the development of residual stresses in tempered glass plate.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Metal-Matrix Composites
Fiber
Graphite

Boron
Alumina
Silicon carbide
Molybdenum, tungsten

Matrix
Aluminum
Magnesium
Lead
Copper
Aluminum
Magnesium
Titanium
Aluminum
Lead
Magnesium
Aluminum, titanium
Superalloy (cobalt base)
Superalloy

Typical Applications
Satellite, missile, and helicopter structures
Space and satellite structures
Storage-battery plates
Electrical contacts and bearings
Compressor blades and structural supports
Antenna structures
Jet-engine fan blades
Superconductor restraints in fusion power reactors
Storage-battery plates
Helicopter transmission structures
High-temperature structures
High-temperature engine components
High-temperature engine components

TABLE 11.10 Metal-matrix composite materials and typical applications.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Example: Brake Caliper

FIGURE 11.38 Aluminum-matrix composite brake caliper, using nanocrystalline alumina-fiber reinforcement.
Source: Courtesy of 3M Specialty Materials Division.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Powder-in-Tube Process

Superconducting
ceramic
powder

Hopper

High-purity
silver tube

Wire
1. Fill

2. Pack

3. Extrude/Draw

Strip
4. Roll

FIGURE 11.39 Schematic illustration of the steps involved in the powder-in-tube process. Source:
Courtesy of Concurrent Technologies Corporation.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

Case Study: Engine Valves


Steel shaft

Tungsten-carbide
wear face

Copper interlayer
Steel cap

FIGURE 11.40 A valve lifter for heavy-duty diesel engines, produced from a hot-isostatically-pressed
carbide cap on a steel shaft. Source: Courtesy of Metal Powder Industries Federation and Bodycote,
Inc.

Manufacturing Processes for Engineering Materials, 5th ed.


Kalpakjian Schmid
2008, Pearson Education
ISBN No. 0-13-227271-7

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