Prufaid okeme 70/800 &) 4 3/20 YR Jer DELUBE-LP — epee SCOPE DELUBE-LP is a medium duty surfactants enriched degreasing chemical formulated to remove oil, lubricants and other contaminants from the surface of Iron and Steel ‘components. It is used by dip application preferably with slow air/mechanical agitation in the bath. BATH CONCENTRATION AND OPERATIONAL PARAMETERS DELUBE-LP is used normally at 3-5% concentration (w/v) in a tank containing tap water (preferably soft water), the operating temperature is maintain between 45-55°C by dipping time the components at recommended temperature time varies from 8-10 minutes for complete degreasing. TESTING & CONTROL OF BATH DELUBE -LP chemical concentration is controlled by simple volumetric titration of bath solution. 10 mls of the bath solution of 5% concentration titrated with N/10 Sulphuric Acid using Methyl Orange as indicator. will give 58-65 {nl reading which represents the alkaline pointage-of bath solution and is recommended to maintain as best as possible by regular additions. To raise the drop in pointage 0.9 kg of DELUBE-LP is added per 1000 Itrs. of bath for 1 point increase, OIL REMOVAL Oils and lubes removed from the surface of the components during treatment will float on the Surface of the bath in none operative. It is advised to remove oil as far as possible by manual or continuous oil separation arrangement for effective degreasing efficiency and thus reducing the contamination level of oil / lubes in the bath.DELUBE-SP_ ~ eyed . SCOPE DELUBE-SP is a very special heavy-duty alkali cleaner with efficient surfactants formulated to remove oil, lubricants and other contaminants from Iron and Steel components. It is used by dip application preferably with slow ait/mechanical agitation in the bath, BATH CONCENTRATION AND OPERATIONAL PARAMETERS DELUBE-SP is used normally at 4-5% concentration (w/v) in a tank containing tap water (preferably soft water), the operating temperature is maintained between 70-80°C of the components at recommended temperature vary from 8-10 minutes for complete degreasing. TESTING & CONTROL OF BATH DELUBE -SP chemical concentration is controlled by simple volumetric titration of bath solution. 10 ml of the bath solution of 5% concentration is titrated with N/10 sulphuric Acid using methyl Orange indicator 60-65 mls reading which represents the alkaline Pointage of bath solution and is recommended to maintain as best as possible by regular additions. To raise the drop in pointage 0.75 kg of DELUBE-SP is added per 1000 ltrs, of bath solution for one point increase, OIL REMOVAL ils and lubes removed from the surface of the components during treatment will float on the Surface of the bath in none operative. It is advised to remove oil as far as possible by manual or continuous oil separation arrangement for effective degreasing efficiency and thus reducing the contamination level of oil / lubes in the bath.DEOXID-140 - abe Revkiny 7 SCOPE ae DEOXID-140 is a blend of phosphoric & mixed inorganic acids derusting composition formulated, duly inhibited for low metal attack, to remove rust and oxide layer from the iron surfaces. This process is used by immersion only. BATH CONCENTRAION & OPERATIONAL PARAMETERS. DEOXID-140 is used at 20-30% concentration (v/v), in a tank suitably lined containing, water. The components are treated in the bath solution at temperature 40-50°C for 8-15 minutes depending upon the oxide and rust layer to be removed from the metal surface. TESTING & CONTROL The concentration of the chemical of DEOXID-140 bath is controlled by a simple volumetric titration of the bath solution for acid strength and Iron content. Acid strength is determined as follows 4) 10 ml of the bath sample is diluted with 90 mis of Distilled water in a measuring flask.10 ml of the diluted solution is titrated against N/10 Sodium Hydroxide using Methyl Orange indicator. The change of colour from pink to yellow is the end point. The quantity of N/10 Sodium Hydroxide used in the titration represents the pointage ‘of DEOXID 140 which at 20% concentration will give pointage 18-22 mls. For every one point lacking addition of 12.0 Kgs of DEOXID-140 per 1000 Itrs bath is added. The iron content of the bath solution is determined as under b) 10 ml bath solution is mixed with 10 ml of 50% Sulphuric acid and is titrated with titrated with N/10 Potassium Permanganate solution. No. of mls used to achieve the end point -colourless to pink represents the pointage. The iron percentage is calculated as No, of mls. consumed multiplied by 0.056. The recommended maximum permissible limit of iron Contents is 7% . Further increase the iron contents will reduce the efficiency of derusting drastically , hence advised for fresh bath preparation . EQUIPMENT. DEOXID -140 is used in a mild steel tank duly lined with lead, FRP or PVC/Rubber tanksKRISFINE-Z is conditioning rinse additive formulated with a complexing agent to ‘compensate for water hardness. It is used to activate steel and zine coated stee! prior to zinc phosfating. It eliminates the course, crystalline coatings sometimes obtained on zine surfaces and on steel surfaces which have been pickled with acid or cleaned with strong alkali, It promotes the formation of a dense, finely crystalline phosphate coating which is the preferred base for paint and which has superior corrosion resistance. BATH MAKE-UP Use 2.0 Kg of KRISFINE-Z per 1000 liters of bath. Disperse it in deionised water before adding to the bath BATH CONTROL POINTS Temperature : Ambient Dip Time : 1-15 minutes pH of working cone. 8.5-9.5 Titration 2 7.0-12 mls (for 100 ml) Titanium : Presence Indicated BATH CONTROL Titration: ‘Measure 100 mis of the bath solution into a flask. Add 5 drops of methyl orange indicator and titrate with 0.1N sulfuric acid until color change from yellow to red is obtained. ‘The number of mls of 0.11N sulfuric acid used is the pointage. TITANIUM PRESENCE To 30 mls of bath solution, add 5 ml of concentrated sulfurie acid & 5 ml of Phosphoric acid followed by 5 ml of (30%) hydrogen peroxide. If titanium is present, a yellow color will result. Two samples should be prepared from the bath , one from filtered liquid and other from liquid taken from the tank. These give levels of effective and total titanium: respectively.MAINTAINING LEVEL For best results the tank should be over flowed continuously. ‘The replenisher tank should be completely emptied every 4-8 hrs. ‘The replenisher tank should be stirred at al times. EQUIPMENT ‘The KRISFINE-Z rinse should be constructed of stainless steel or lined mild steel. ‘The replenisher tank should be similarly constructed, although for this tank, plastic is also suitable. HAZARD AND HANDLING PRECAUTIONS, KRISFINE-Z is a mildly alkaline liquid. Avoid breathing dust, wear rubber or PVC gloves when handling the liquid. Wash away any spills with plenty of water. FURTHER INFORMATION Users must satisfy themselves that there are no circumstances requiring additional information or safety precautions relating to details given herein and must not practise or use any patented invention or trademark without prior approval.KRISPAS-NC a “Peuivetsen £ TK SCOPE KRISPAS-NC is used in the final rinse after pretreatment either by immersion or spray process. KRISPAS-NC eliminates contaminants from the pretreated metal surface and thereby increases corrosion resistance and paint adhesion. Also counteracts the effects of hard water salts and acidifies the surface before painting. It thus reduces the risk of blistering under humid conditions. BATH CONCENTRATION ANI RATIONAL PARAMETER: KRISPAS-NC is used at 0.025-0.05% concentration (v/v), in a tank containing D.M. Water. The operating temperature is 70°-80°C also operative at room temperature and time varies between 30-60 sec. pH is maintained between 4.5-5.5. BATH MAINTENANCE If soluble salts carried over from previous rinses are allowed to accumulate, the PASSIVATE solution will deteriorate rapidly. It should therefore be made up a fresh regularly. Check the pH of rinse periodically, using universal pH paper. If it is over 5.5 add more KRISPAS; if it is below 4.5 discard part of the rinse and replenish with fresh water. TESTING AND CONTROL The bath is controlled by regular check of the pH. The pH should remain in the specified range and should not be allowed to drop or exceed much above the specified values. ‘TEST FOR CHROME PRESENCE: 10 ml bath sample + 50 mi distilled water. Then, add 20 ml 50 % Sulfuric acid solution. Now, add Ig of Potassium iodide and 1 ml of freshly prepared starch solution. There is occurrence of brownish yellow color, if chrome ions are present. No occurrence of the color indicates the absence of chrome ions.® KRISBOND-LT = Phosphoters - SCOPE KRISBOND-LT is a Nickel, Manganese modified Zine phosphate process operative at low temperature designed to treat steel surfaces for smooth, uniform Zine phosphate coating. The process is used by dip application. KRISBOND-LT coating is compatible which all types of organic finishes. BATH MAKE UP (PER 1000 LITRE OF BATH) Fill about three fourth of tank with water and add the following chemicals. 70 Kgs of KRISBOND-LT 500 g of T.C.2 Adjust the bath level to working volume and mix thoroughly. Maintain the operating ‘temperature, OPERATIONAL PARAMETERS Temperature: 35-45°C Time > 8:10min, Total Acid: 26-29 points Free Acid =: 1.2-1.5 points TC2 : 2-4 points SOLUTION CONTROL KRISBOND-LT bath is controlled by simple titration for total Acid, Free Acid and accelerator pointage. a) Total Acid : Pipette 10 ml of the solution in a conical flask and add few drops of Phenolphthalein indicator and titrate against 0.IN NaOH solution till a permanent faint pink colour is obtained. The ml. of the titrating solution used indicates the total acid points b) Free Acid : Pipette 10 ml of the bath solution in a conical flask and add few drops of Bromo- phenol blue indicator and titrate against 0.IN NaOH solution till the yellow colour of the solution just disappears to give blue violet colour. ‘The ml. of the titration solution used indicates the free acid point. TC-2-~- Tonnen Cher'ce/S \Batator: Fill the bath solution in the sachharometer and add 2-3 gms of. Sulphamic acid.Agitate the solution, and allow the sachharometer to stand undisturbed for two to three minutes. The extent of displacement of the solution due to generated gas indicates concentration of accelerator in bath. 4) Replenishing of the batl i) Total acid: To increase the total acid by 1 point, 2.3 Kgs of KRISBOND-LT. is added per 1000 ltrs. ii) Free acid: To decrease the free acid, Caustic soda is used to reduce free acid by 0.1 point,0.04 Kg Caustic soda is added per 1000 Ltr of bath. To increase free acid by 0.1 point, 1.2 ltr. of KRISBOND-LT is added per 1000 Itr. of bath. if)T.C2 : To increase the T.C.2 by I point, add 150 gms. of T.C.2 per 1000 ltrs. of bath. EALING. Zinc phosphate coating is an ideal surface for subsequent sealing by paint, lacquer or oil for longer protection of the steel surfaces. The sealing is done depending upon the requirement i.e. corrosion resistance or decorative/ aesthetic values of the surface. ‘ A Koi fF 1 Ce | poolr | sews Lh 1a “ , (O70 din - } Pees de, seal® RECOMMENDED PROCESS SEQUENCE s no [stace IcHEMICAL conc. Imme___|temp __|oscaro 1|DEGREASING |DELUBE-SP 15%, T.A:60-65ml. 10-12min. |50-60 Joil content Max-3000ppm_ 2{WareR RINSE PA79 so-a5sec_|Room [Running water | WATER RINSE PH = 6-7 0-assec [Room __ |Running water 4|DERUSTING IDEOXID - 140 120%, T.A:18-22ml |15-20 min. [40-50 jiron content Max. 7% 5| WATER RINSE pH=5-7 30-45 sec. {Room __|Running water 6|WaTER RINSE pH=5-7 30-45see_|Room _|Running water TIACTIVATION(OM WATER) KRISFINE - Z(air agitation) |0.2%PH =8.5-9.5. }1-1.5 min. [ROOM |Weekly PHOSPHATING(OM WaTeR) |kRISBOND-LT eat? eto min. [35-45 itera weekly A S|WATER RINSE(D M WATER) PH = 6-7. 130-45 sec. [ROOM (Running water 10]PASSIVATION(D M WATER) [KRISPAS -NC 10.025%, PH = 4.5-5.5 [30-45sec_ |ROOM - 70 |Weekly= RECOMMENDED PROCESS SEQUENCE 4 Q Aa se ae = ; 6h Vins ‘ prey -YAR> area TT! ip aes SR [STAGE CHEMICAL | CONC. | TIME] TEMP. DISCARD NO. : CC) 1 DEGREASING DELUBE-SP 5% 10-12 min ‘Oil content (ank made in TA: 60-65, TO- G0 | Max-3000 normal water) mi. 8 | ppm 2] WATER RINSE |= pHT9— | 30452 | ROOM] Running water (tank made in — normal water) 3] WATER RINSE] = paTs 3045 se | ROOM | Running water (ank made in normal water) a | DERUSTING DEOXID-140 | 20% | 1530min | 40-50 Tron conent (ank made in TA: 18-22 Max. 7% normal water) til 3] WATER RINSE] = pH 30a sec | ROOM | Running water (tank made in P = normal water) © | WATER RINSE |= pitas} 3045 ee | ROOM Running water (tank made in 3 normal water) > 7 [ACTIVATION | KRISFINEZ | 02% T-1S min, | ROOM Weekly (tank made in DM. (air agitation) PH: 8.5-9.5 water) 8 PHOSPHATING KRISBOND- 5% 8-10 min. 35-45 Filter weekly (tank made in DM | LT TA:26-29 water) ml FA:12- 1.sml | TC2: 2-4 ml 9} WATER RINSE | PHET | 30450. | ROOM] Running water (Cank made in DM _ water) 10” | PASSIVATION | KRISPASNC] 0025% | 30-45 see. | ROOM-T0 | Weekly (Cank made in DM ph 4S-55 water)CER Date: 30/0" TIPFICATE OF ANALYSI8 7/15 customer: 200AAP Order Number: Product Code: 170: Customer Item: Banner Name: Inte! colour: Batch Number: RF28\ Manufactured: 08/0: Shelf Life: 365 Re-test Date: Batch Qty: 16: Test Name Descripti SUBSTRATE BAKING TEMPERATURE (EM DEG. C BAKING TIME (AT EMT) MIN PARTICLE PARTICLE PARTICLE FLUIDITY aN srpon HYF Plus O6HA, 7/45 Days 93.0 KG Method on Referen DRY FILM THICKNESS | MICRONS COLOUR GLOSS. (60 DEG HEAD) PERCENT FLOW / FINTSH PENCIL HARDNESS FLEXIBILITY od ERICHSEN CUPPING od Impact KG. cM SIZE DIST(>83 PERCENT SIZE DIST(<32 PERCENT SIZE DIST(<10 PERCENT (R FACTOR) AKZO NOBEL INDIA LIMITED Plot # 62P 62A 628 43E HOSKOTE INDL AREA BANGALORE BANGALORE 562114, KA INDIA Specification co Range Test Result MILD STEEL MILD STEEL 200 200 10 AND 30 10 AND 30 70|90 a5 AS PER STD AS PER STD 275 76 COMPARABLE TO STD COMPARABLE T 2H 2H NA NA 2 a NA NA 5/10 8 26/30 29 5/20 7 170 ‘ated and needs no signature. 30/07/15