Etude de spectres en RMN 13C

Spectre dcoupl

Spectre coupl

1. Spectres coupls / dcoupls

XB-ENCPB - 2011

2. Analyse de quelques spectres

57.79 1000

1-propanol

25.89 955

18.13 970

SDBS-13C NMR 25.16 MHz C2 H6 O 0.5 ml : 1.5 ml CDCl3 1-ethanol

ppm Int. Assign.

64.25 1000

SDBS-13C NMR 15.09 MHz C3 H8 O 0.25 ml : 0.75 ml CDCl3

13

ppm Int. Assign.

SDBS- C NMR 25.16 MHz C3 H6 O 0.5 ml : 1.5 ml CDCl3 acetone

1/10

10.28 820

ppm Int. Assign.

206.55 522

114.39 778

SDBS-13C NMR 25.16 MHz C5 H10 0.5 ml : 1.5 ml CDCl3

ppm Int. Assign.

139.00 798
1
13.66 864
5

128.36 1000

SDBS-13C NMR 25.16 MHz C6 H6 0.5 ml : 1.5 ml CDCl3

ppm Int. Assign.

30.81 1000
1-pentene

36.09 960

benzene

SDBS-13C NMR 25.16 MHz C7 H8 16.1 wt% in CDCl3 toluene

XB-ENCPB - 2011

22.26 1000

ppm Int. Assign.

137.83 214
1
125.38 517
4

129.09 910
21.41 209

2
5

136.47 211
128.98 976

4
1

2
6

136.92 1000
117.55 836

3
7

salicylaldehyde

134.43 423

benzaldehyde

128.28 1000

SDBS-13C NMR 15.09 MHz C7 H6 O 0.25 ml : 0.75 ml CDCl3

ppm Int. Assign.

192.28 463
5
129.68 1000
2

13

161.60 557
119.84 831

SDBS- C NMR 25.16 MHz C7 H6 O2 0.5 ml : 1.5 ml CDCl3

ppm Int. Assign.

196.54 438
1
120.72 398
5

2/10

133.73 846

XB-ENCPB - 2011

33.09 271

2
6

36.32 975

ethyl butyrate

30.05 609

SDBS-13C NMR 25.16 MHz C9 H18 0.5 ml : 1.5 ml CDCl3 isopropylcyclohexane

ppm Int. Assign.

44.32 275
5
19.77 754
1

60.13 1000
13.70 670

SDBS-13C NMR 25.16 MHz C6 H12 O2 0.5 ml : 1.5 ml CDCl3

1
5

ppm Int. Assign.

173.61 670
14.32 735

3/10

18.57 900

26.88 1000