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500-001 (Liquified Gas Handbook) PDF
500-001 (Liquified Gas Handbook) PDF
Section: 500
Effective: December 2008
Replaces: March 2008
Liquefied Gas
Handbook
Practical suggestions on the
design and installation of
handling systems for propane,
butane, anhydrous ammonia
and similar liquefied gases
Process
Energy
Transport
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past models, is available at our website. Specification
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Table of Contents
About Blackmer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Compressors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Propane Installations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Delivery Systems on Bobtail Trucks . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Delivery Systems on Transports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Stationary Motor-Driven Pumps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Vaporizer/Standby Plant Applications . . . . . . . . . . . . . . . . . . . . . . . . 29
Appendix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
About Blackmer
Blackmer has become a global company, supplying
markets around the world with expert flow-technology
applications. Blackmer is quick to respond to the industrys
rapid advances, through constantly reengineering its
products to include new innovations.
Mission Statement
Experts in the field are continuously providing one-onone product training throughout the world. Blackmer
believes strongly in its team, whose purpose is to service
its customers needs through years of experience and
longevity in the workforce.
Products
LB Compressors for LPG and NH3 Transfer
These ductile iron compressors are available in four sizes
to meet any application. Compressors are especially wellsuited for unloading rail cars, evacuating cylinders and
tanks and anywhere vapor recovery is required.
In addition to products available for the transfer of liquefied gases, Blackmer manufactures a wide range of products for use
in many industries and markets worldwide:
Sliding Vane
Pumps
Centrifugal
Pumps
HD Industrial Process
Compressors
HR Gear Reducers
Hand Pumps
Properties of LPG
The following properties of LPG should be understood
for the purpose of promoting safety in usage and for
intelligent action in handling this fuel:
10. Liquid drawn from the storage tank will cause freeze
burns on contact. This is due to the rapid absorption
of heat by the liquid upon vaporization in the open.
Figure 1
Figure 2
Compressors
A piston type compressor is classified as a reciprocating
positive displacement compressor. Other positive
displacement compressor types are screw, sliding vane,
wobble plate, diaphragm or lobe.
General
Blackmer compressors are quite specialized among the
many types of compressors offered in the market. They
are a positive displacement, vertical, reciprocating design
and are available in single or two-stage models. All models
have two cylinders and some are available with either
air-cooling or water-cooling. Most models have singleacting cylinders, although the largest have double-acting
cylinders. Oil-free ductile iron cylinders with PTFE piston
rings are standard.
Applications
Blackmer compressors may be used in many industries and
in many situations. In general, most LPG applications will
fall into two categories:
Compressors
Figure 3
In any of these situations, a liquid pump would be useless
in trying to empty the vessel. Compressors, on the other
hand, can easily handle all of these situations, while the
very best that a pump can do is to empty a vessel of liquid
but still leave it full of vapor.
LPG Transfer
A liquid pump cannot completely empty a LPG vessel
of all its product. A small amount of liquid (the liquid
heel) will always remain. Even if all of the liquid could be
pumped out, the vessel would still be full of vapor at vapor
pressure. This remaining vapor can equal approximately
3% of the tanks total capacity. This means that if a plant
were to receive its product via transport, 97 transports
unloaded with a compressor would be the same amount
of product as 100 transports unloaded with a liquid pump.
Also, if a vessel needs to be opened to atmosphere for
service or repair work, venting the vapor to atmosphere
can be expensive and may pose a safety hazard. Using a
compressor to recover these vapors before opening the
tank to atmosphere can minimize both of these problems.
Vapor Recovery
Compressor Components
Figure 5
Figure 4
Compressors
Typical Compressor Packages
Figure 6 illustrates the various components that make up
a typical LPG liquid transfer and vapor recovery package.
The mounting arrangement consists of the compressor,
complete with pressure gauges, a baseplate, the belt guard
and the belt drive system. It also includes the four-way
valve, liquid trap, inlet strainer, relief valve and possibly a
liquid level switch.
Figure 6
Four-Way Valve
One advantage of using a compressor is that both the
liquid and the vapor may be recovered from the vessel.
The four-way valve makes this process both practical and
easy. The four-way valve reverses the flow of gas through
the system without changing the direction of compressor
rotation.
Figure 7
Liquid Traps
Figure 8
10
Compressors
installations, the optional ASME trap will provide sufficient
volume, although in some cases, an even larger vessel may
be required.
Figure 10
Figure 9
Installation Guidelines
Figure 11 shows a typical compressor installation. Since
Blackmer compressors are reciprocating rather than a
rotating devices, a proper foundation for the compressor
and support for the piping is very important. A 8-10-inch
(20 to 25 cm) foundation depth is recommended.
The compressor baseplate must be well supported, along
with its entire length, and be firmly bolted to the concrete
foundation. Pipes leading to and from the compressor
should be well supported as near to the compressor as
feasible. Flex connectors may be used to help dampen
any vibration induced by the compressor.
Figure 11
11
The vapor return line from the top of the receiving tank to
the supply tank helps to keep the pressure up in the supply
tank and reduces the amount of boiling. Also, relieving
vapor pressure in the receiving tank as the liquid rises in
the tank equalizes pressures in both tanks and reduces the
differential pressure across the pump. Consequently, the
pump can deliver more product at the lower differential
pressures.
Figure 12
Set the bypass valve at least 25 psi (1.7 bar) lower than
the pumps internal relief valve setting. This will ensure
the bypass valve opens first. The pumps internal relief
valve should open only as a final system protection device.
The pumps internal relief valve routes discharge fluid back
to the pump inlet, which will quickly cause wear and tear
on the pump if used excessively.
Figure 13
12
Figure 14
Figure 16
Figure 15
Figure 17
13
Figure 18
14
Pump Drive
Pumps on bobtails are commonly driven by the power
take-off through a jackshaft connected by universal joints.
A well lubricated, splined slip joint is recommended for
the drive shaft. Also note that the PTO and pumps shafts
must always be parallel, that the universal yokes at the
ends of the jackshaft must be parallel and in phase, and
thatthe angularity between two adjacent shafts must not
exceed 15 degrees. Failure to heed these suggestions will
result in a gallup or uneven turning of the pump rotor,
which will result in a premature bearing, shaft or seal
failure. Figure 19 illustrates the correct mounting of the
driveline when universal joints are used.
Figure 20
Hydraulic driven units are becoming more prevalent.
They increase pump service life by eliminating the external
loading on the pump shaft, which is inherent with a power
take-off. They also provide, for more consistent speed
control and soft starting of the pump.
Required
guards not shown.
Figure 19
15
Pump Mounting
There are several methods of mounting and piping pumps
on bobtails. Figures 21 and 22 show the arrangements most
common, both of which use an internal tank valve with
excess flow capability. An internal valve is mandatory.
NFPA Pamphlet No. 58 requires that liquid unloading
connections on tank trucks be equipped with remotely
controlled internal shut-off valves. They are either flanged
to the tank, as shown in Figure 21, or threaded, as in
Figure 22. The valve can be actuated in any of several
ways: hydraulic, using pump discharge pressure or an oil
hydraulic system, cable control or pneumatic power.
INTERNAL VALVE
WITH STRAINER
REMOTE
SAFETY RELEASE
VALVE CONTROL
Figure 21
Figure 22
The Foot-Mounted Pump (Figure 22) can be mounted on
a pad welded to the tank when an internal valve with a
sided outlet is used. This eliminates the need for a flexible
pipe connector, which is usually necessary on pumps
attached to the chassis. The foot-mounting arrangement
requires the use of flanged connectors. The internal
valve is equipped with a strainer which must be cleaned
periodically.
16
Flexible Connector
12 Clutch Control
Vapor Eliminator
Meter
Differential Regulator
15 Thermometer
Bypass Valve
Tachometer
18 Pressure Gage
Throttle Control
22 Filler Valve
15
Figure 23
17
19
20
5
6
16
5 21
12
22
Figure 24
17
15
6
7
10
8
9
11
Figure 25
18
13
14
Excess-Flow Valves
Excess-Flow Valves are still in use in the liquid unloading
connections of many older trucks. Delivery rates from
these older trucks are usually lower than from new ones
because their intake piping design and excess flow valves
offer significantly greater restriction to flow.
FILL
CONNECTION
SIGHT GLASS
BYPASS
VALVE
FROM
PUMP
TO METER AND
DELIVERY HOSE
Figure 26
19
Figure 27
Figure 27 illustrates the vapor formation when fluid is
recirculating through the pumps internal relief valve.
It rapidly transforms to vapor because of turbulence within
the valve, the heating of the liquid and the sharp pressure
drop between pump discharge and inlet. The recirculation
results in noise, vibration and excessive wear within the
pump. Consequently, a back-to-tank bypass valve is critical
to longer, trouble-free pump operation.
To set the bypass valve, first check the pressure setting
of the pumps internal relief valve. Shut off the separate
bypass line, then gradually shut off flow through the
delivery line while watching a pressure gauge on the
pump discharge. The pumps internal relief valve setting
is the peak pressure which shows on this gauge. (After
recirculation starts through the pumps internal relief
valve, vaporization will cause the pressure to fall quickly).
Figure 27
20
Troubleshooting
No Product Delivery
On trucks equipped with lever-operated internal valves,
when the lever is moved to the open position, the excessflow valve may remain closed if the pressure on the pump
side is lower than in the tank. A leak in the piping system
will lower pressure. Also, putting the pump in gear before
opening the valve sometimes will keep the excess flow
valve from opening. In this case, the driver must wait until
the pressure equalizes. This is accomplished by an orifice
hole in the valve, which allows the fluid to slowly bleed
through the valve. Manually trying to actuate the valve
to the open position will also help the situation.
Figure 29
The regulator also serves as one more safety device since it
opens only when the pump is running. There have been
accidents when the delivery hose was pulled off a moving
truck. However, the differential regulator blocked the flow
since the pump was not running.
Low Capacity
If the pumping rate is not as fast as it should be, the operator
will usually suspect something is wrong with the pump.
All too often, he will attempt to compensate by overspeeding, which only causes more liquid to bypass. Instead
of boosting the delivery rate, it will only damage the pump.
21
A possible cause of low delivery is loss through the backto-tank bypass line, either because the separate bypass valve
is set too low or the bypass valve is leaking. To determine
if this is the problem, close the manual valve in the bypass
line while delivering. If pressure and flow rate increases,
the bypass valve is at fault.
Occasionally, a driver forgets to disengage the power takeoff and drives away with the pump in gear. This is a very
severe operating condition for the pump and will result in
melting the vanes. The other reason for rapid vane wear is
pumping excessive vapors, usually the result of a restricted
inlet caused by:
Pump Troubleshooting
Excess Vane Wear
The life of pump vanes can vary widely, depending on
operating conditions. Unusually rapid vane wear is an
indicator of poor system design, improper bypass valve
adjustment, sticking bypass valve, pump overspeeding or
severe operational abuse.
22
23
Figure 20
Pump Drives
Traditionally, transport pumps have been driven by a
PTO shaft from the tractor and mounted near or between
the landing gear brackets or just ahead of the rear wheels.
More recently, hydraulic drive systems have become
more popular as they allow more flexibility with pump
placement, greater speed control and increased pump
service life.
A typical hydraulic drive system includes a PTO, hydraulic
pump, Hydrive cooler/controller, speed control valve,
hydraulic motor and mounting adaptor. Hydraulic drives
make use of hydraulic oil to power rotating equipment.
The Hydrive cooler protects the system during cold startup, allows for system on/off control and provides both
controlled system cooling and oil filtration monitoring.
The speed control valve provides overspeed protection,
and Hydraulic motor adapters provide close-coupled
connections between the pump and hydraulic motor.
Hydraulic motor adapter kits are also available to easily
mount on Blackmer pumps.
24
Bypass Valve
AUXILLARY INLET
LOADING CONNECTION
(or vapor return line)
STRAINER
BYPASS VALVE
DELIVERY HOSE
Figure 30
25
Pump Drive
Refer to Figure 31 and follow these simple rules to avoid
problems when using jackshafts and universal joints to
drive the pump from the power takeoff:
Salt Corrosion
Salt water can seep into the propane from poorly serviced
calcium chloride dehydrators or underground storage
domes. LPG pumps were never designed to pump brine.
They have little corrosion resistance. If the slightest trace
of salt water corrosion turns up on pumps or other system
equipment, investigate at once. Find the source of the brine
and correct it immediately. Then clean out the complete
pumping system and repair any damage. Obviously, an
extremely dangerous condition would exist if for example,
relief valves should freeze up from this salt water corrosion.
Required
guards not shown.
Figure 31
26
BYPASS LINE
VAPOR RETURN
LINE
TO LOAD TANK
VEHICLES
TO UNLOAD TANK
VEHICLES
Figure 32
BYPASS VALVE
DELIVERY
Figure 33
27
Figure 34
Bottle Filling
Cylinders or bottles are usually filled by weight. Scales
with automatic trip-valves, such as those shown in Figure
34, are widely used for this service. When selecting pumps
for filling bottles, use this rule of thumb; it takes about 1 12
minutes to fill a 100-pound (45 kg) cylinder at 85 psi
(5.9 bar) differential pressure. To fill one bottle at a time,
a motor-mounted pump should do the job. For larger
operations, the pump size depends on the number of
bottles to be filled at any one time. One man can handle
three filling points by moving from one scale to another
in turn. A 2 inch, 50 gpm (189 L/min) pump has proven
most popular for a three-station setup.
BYPASS LINE
Figure 35
28
Vaporizers
Commercial applications using large size burners such as
grain dryers, tobacco dryers or industrial furnaces require
large quantities of vapor. Vaporizers employ heat to
accelerate the normal vaporization rate and are used
to meet this high demand.
29
Pump Selection
Because of the critical function of the standby plant in
providing an uninterrupted fuel supply, the sizing of its
components should be governed by the maximum peak
demand of the system at the coldest temperature, even
though the standby plant will normally operate at somewhat
less than this demand.
Most vaporizer manufacturers make general recommendations
on the gpm rating of the supply pump. A common rule of
thumb is to specify a pump with a flow rating 3 to 4 times
the rating of the vaporizer. Manufacturers have suggested
that factors might differ. There are two principle factors
which make this oversize rating necessary.
A vaporizer operating at full rated output will have its heat
exchange chamber nearly full of liquid propane. This is
necessary to maintain maximum contact area between
the liquid and the heating surface. If the vapor demand
is suddenly reduced to near zero, as will happen when
the using furnace is shut down or modulating, the liquid
continues to boil. Accumulating vapor drives liquid from
the chamber back through the piping toward the pump.
Renewed vapor demand requires a rapid refilling of the
vaporizer and the pump must have enough capacity to
provide the necessary surge in addition to the normal
liquid flow rate. If the total flow is insufficient to maintain
proper pressure at the vaporizer, automatic controls should
shut down the system.
The second consideration in sizing a pump for vaporizer
service is the range of anticipated operating temperatures
for the system. Standby plants usually operate in very cold
weather when the demand for natural gas is highest or
premium rates are in effect. As shown in Figure 18, page
14, pump efficiencies are significantly lower in a cold
environment. This reduced efficiency is a thermodynamic
property of the liquid propane.
30
Appendix
Appendix
Description
Page
Appendix A
Appendix B
Appendix C
Appendix D
Appendix E
Appendix F
Appendix G
31
Appendix A
Properties of Liquefied Gases*
English
ANHYDROUS
AMMONIA
PROPANE
BUTANE
Formula
NH3
C3H8
C4H10
Boiling Point, F
-28
-44
32
0.596
1.50
2.01
0.616
0.504
0.582
5.14
4.20
4.81
91,502
102,032
21,548
21,221
2,488
3,280
36.38
31.26
2.75
8.66
6.51
3,027
773
808
920 1,120
900 1,000
3,595
3,615
At Lower Limit %
2.15
1.55
At Upper Limit %
9.60
8.60
Over 100
92
Metric
ANHYDROUS
AMMONIA
PROPANE
BUTANE
Formula
NH3
C3H8
C4H10
Boiling Point, C
-33
-42
0.596
1.50
2.01
0.616
0.504
0.582
616
504
582
121,280
92,430
49,920
49,140
25,140
28,100
0.105
0.271
0.235
0.171
0.539
0.410
846
32
216
226
493 549
482 538
1,980
2,008
2.15
9.60
1.55
8.60
Over 100
92
Appendixes B and C
Appendix B
Vapor Pressure of Liquefied Gases
Appendix C
Saturated Propane Vapor in 10,000
Gallon Tank
33
Appendixes D and E
Appendix D
Friction Loss in LPG Hose
Hose Friction loss in psi for 100 ft. smooth
bore rubber hose with inside diameters
as shown, for propane. (These values will
vary because of manufacturing tolerances
on hose diameters.)
For Butane:
Multiply friction loss values by 1.15
For Anhydrous Ammonia:
Multiply friction loss values by 1.21
Appendix E
Friction Loss in Pipe
Pipe Friction loss in psi for 100 ft. new,
clean extra strong schedule 80 pipe for
propane
For Butane:
Multiply friction loss values by 1.15
For Anhydrous Ammonia:
Multiply friction loss values by 1.21
34
Appendixes F and G
Appendix F
Resistance of Valves & Fittings in Equivalent Feet of Pipe
PIPE SIZE
1
1.25
1.5
2.5
Elbow 90
4.5
11
Elbow 45
2.5
12
14
17
22
25
25
25
42
42
42
60
16
16
16
16
14
20
Globe valve
28
35
45
60
65
85
120
Angle valve
15
19
22
28
35
42
57
Ball valve
0.5
0.5
0.5
0.5
0.5
0.5
0.5
Quick-closing gate
Above values are approximate and will vary from one manufacturer to another.
Appendix G
Other Reference Materials From Blackmer
500-002
500-003
CB254
CB047
CB048
LBLTRAN
CB296
35
Notes
36
Notes
37
Notes
38
Manager of
Repair Center
Customer Care
Regional Sales
Manager
Manufacturing
Application
Engineer
Design
Engineering
Distributed by:
World Headquarters
12/08
2008 Blackmer
www.blackmer.com