1400

PDF 00-064-0738 Ca10 ( P O4 )6 ( O H )2 Hydroxylapatite, syn

1300
1200
1100
1000
900

Counts

800
700
600
500
400
300
200
100
0
10

20

30

40

50

2Theta (Coupled TwoTheta/Theta) WL=1.54060

60

70

80

Ca10 ( P O4 )6 ( O H )2
Calcium Phosphate Hydroxide
Hydroxylapatite, syn

8.1586
8
5.2595
3
4.7105
0

Hexagonal
P63/m (176)

1004.64
528.83

1.00000
0.73028

999.9 (0.0002,30)

51.272 114

1.7544
7

52.087 120

52.127

3.8867
9

22.862

85

1.7200
0

53.211 154

3.5088
9

25.363

14

1.6830
1

54.477

10

1.6441
4

55.876

56

1.6430
9

55.914

1.6317
7

56.337

56.949

25.880 613
28.129

90

28.931 164

0
0
1

0
1
2

2.8139
9

31.774 999

1.6156
6

2.7780
6

32.196 548

1.6107
3

57.140

36

2.7196
4

32.907 613

1.5877
1

58.046

15

2.6297
9

34.065 237

1.5848
9

58.160

1.5811
7

58.310

10

1.5701
8

58.758

1.5418
7

59.946

44

60.424

26

2.3552
7
2.2961
9

35.464
38.180
39.202

43
1
60

0
2
1

3
2
2

2.2628
4

39.804 230

1.5308
1

2.2282
8

40.448

15

1.5045
5

61.592

26

2.2078
0

40.840

1.5021
3

61.702

38

1.4743
1

62.998

72

1.4653
7

63.427

15

1.4536
6

63.998

69

64.175

60

41.998
42.331
43.873

59
10
50

1
0
1

3
3
1

2.0396
8

44.377

10

1.4500
8

1.9990
7

45.328

40

1.4332
2

65.022

68

1.9555
5

46.395

1.4283
9

65.269

10

1.4070
0

66.388

20

1.4063
5

66.423

1.3693
3

68.463

1.3598
0

69.010

1.9433
7
1.8905
1
1.8717
5
1.8402
2

1.54060

2.0619
4

50.490 152

1.7804
0

2.1334
1

CuK1

1.8061
3

2.1495
6

Primary Reference
Publication: J. Appl. Crystallogr.
Detail: volume 43, page 320 (2010)
Authors: Veselinovic, L., Karanovic, L., Stojanovic, Z., Bracko, I.,
Markovic, S., Ignjatovic, N., Uskokovic, D.

63

2.5291
8

Analysis: ICP and Rietveld analyses: ''Ca10 ( P O4 )6 ( O H )2''

General Comments: I/Io <0.3% have been omitted
Sample Preparation: Prepared by adding a filtered
supersaturated alkaline solution of ''Ca ( N O3 )2'' dropwise into
a mixture of ''H3 P O4'' and ammonia water at 323 K under
constant stirring. In a stainless steel Parr reactor the mixture was
hydrothermally treated at 473 K
Temperature of Data Collection: Pattern taken at 295 K

20

21.769

3.0837
3

18.824

33

1.7531
9

3.1698
0

6.88000

16.843

82

4.0794
1

3.4399
5

9.42100

10.835

46.703 285
48.090 115
48.603

22

49.491 307

2
1
2
1

2
3
3
2

1.3568
4
1.3481
4
1.3413
0
1.3295
5

69.182
69.693
70.100
70.812

1
18
2
2

0
1
3
0

1
5
4
5

1.1578
1

1.1491
7

1.1481
0

1.1466
6

84.953

83.412
84.182
84.278
84.409

23
2
27
13

3
0
2
0

1.0030
9

100.33
6

17

0.9995
5

100.82
4

12

0.9967
6

101.21
3

0.9864
6

102.68
2

0.9848
8

102.91
1

21

4
7
4
0

1.3208
0

71.353

1.1407
0

1.3165
1

71.621

28

1.1355
1

85.433

15

0.9777
7

103.96
3

32

1.3149
0

71.722

1.1164
3

87.255

0.9777
7

103.96
3

32

1.1154
4

0.9775
7

103.99
4

1.1141
4

0.9717
0

104.88
4

23

1.1141
4

0.9648
8

105.94
4

1.1086
6

0.9640
3

106.07
8

88.502

53

0.9621
3

106.37
8

0.9474
4

108.78
7

1.3064
5
1.3038
3
1.2956
0
1.2835
1

72.259
72.427
72.961
73.761

26
2
2
20

2
0
3
2

5
2
3
5

87.352
87.480
87.480
88.023

26
33
33
27

1
1
4
2

5
1
4
3

1.2795
6

74.027

28

1.1038
9

1.2664
8

74.922

16

1.0936
2

89.555

1.2645
9

75.053

1.0887
3

90.067

1.0806
6

90.927

17

1.0747
7

91.567

11

1.0675
7

92.364

93.483

1.2565
8
1.2496
6
1.2442
1

75.615
76.109
76.502

45
20
12

1
3
1

2
4
6

1.2370
3

77.027

47

1.0577
1

1.2348
1

77.191

21

1.0403
6

95.534

1.2243
4

77.976

1.0390
5

95.693

1.0348
6

96.207

1.0327
9

96.463

12

1.0309
8

96.689

29

97.073

1.2213
4
1.1880
9
1.1837
9

78.204
80.835
81.190

42
3
5

2
2
0

5
2
5

1.1776
3

81.704

16

1.0279
2

1.1757
0

81.867

1.0266
4

97.235

1.1700
3

82.350

1.0228
4

97.719

15

1.1655
5

82.736

1.0198
5

98.104

1.0166
3

98.524

17

1.0081
0

99.656

18

1.1607
4
1.1596
3

83.154
83.252

1
11

4
3

4
3