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Distilassiiiiiiiiiii
Distilassiiiiiiiiiii
BUTANE-PENTANE SPLITTER
i di li=di/(i-1) vi=li+di
C3 5 5.0 1.3 6.3
iC4 2.6 15.0 9.4 24.4
10.6 30.6
i bi v'i=ibi/(LK-i) l'i=v'i+bi
nC5 0.845 35.0 25.6 60.6
25.6 60.6
Le 101.875 kmol
Ve 126.875 kmol
V'e 131.893939 kmol
L'e 151.893939 kmol
komposisi
xf 0.5
xd 0.96
xb 0.05
2
garis kesetimbangan y=x/(1+(-1)x)
Page 1
Sheet1
y=2x/(1+x)
1.20
1.00 i fi di/bi di bi
C3 5 5 40000 5.00 0.00
0.80 iC4 2.6 10 150 y=x 9.93 0.07
nC4 (LK) 2 20 21
y kes19.09 0.91
0.60iC5 (HK) 1 20 0.053 1.01 18.99
nC5 0.845 35 0.011 q line 0.38 34.62
0.40 y op atas
i fi di
y op bawah
bi
0.20
C3 5 5 5.0 0.0
0.00 iC4 2.6 10 9.9 0.1
nC4 (LK) 2 20 19.1 0.9
0.00 0.20
iC5 (HK)
0.40 10.60 0.80 1.00
20
1.20 1.0 19.0
nC5 0.845 35 0.4 34.6
90 35.4 54.6
Nm 8.6301812529
Mencari nilai
xi,f i i.xi,f 1.50 1.20 1.35
C3 0.05 5 0.25 0.07 0.07 0.07
iC4 0.1 2.6 0.26 0.24 0.19 0.21
nC4 (LK) 0.2 2 0.4 0.80 0.50 0.62
iC5 (HK) 0.2 1 0.2 -0.40 -1.00 -0.57
nC5 0.35 0.845 0.29575 -0.45 -0.83 -0.58
0.26 -1.08 -0.26
Mencari Rm
xi,d i i.xi,d i.xi,d/(i-)
C3 0.14 5 0.71 0.19
iC4 0.28 2.6 0.73 0.58
nC4 (LK) 0.54 2 1.08 1.66
iC5 (HK) 0.03 1 0.03 -0.08
nC5 0.01 0.845 0.01 -0.02
2.34
Rm+1 2.34
Rm 1.34
Rm/(Rm+1) 0.57 1.4765079697
R/(R+1) 0.67 2.0134199586
Page 2
Sheet1
Figure 11.11
Nm/N 0.6
N 14.3836354
R R/(R+1) Nm/N N
1.5 0.6 0.3 28.8
1.6 0.6 0.4 21.6
1.7 0.6 0.5 18.4
1.8 0.6 0.5 16.6
1.9 0.7 0.6 14.9
2.0 0.7 0.6 14.4
Page 3
Sheet3
Page 4
Sheet3
Le 154.4629441845
Ve 175.4629441845
V'e 236.4492600423
L'e 265.4492600423
komposisi
Page 5
Sheet3
xf 0.4
xd 0.9047619048
xb 0.0344827586
2.1224137931
Component i fi di/bi di
C3 10.21 5.00 600000.00 5.00
iC4 4.99 10.00 3950.00 10.00
nC4 4.24 15.00 3100.00 15.00
iC5 2.30 20.00 19.00 19.00
Page 6
Sheet3
Component i fi di bi
C3 10.21 5.00 5.00 0.00
iC4 4.99 10.00 10.00 0.00
nC4 4.24 15.00 15.00 0.00
iC5 2.30 20.00 19.00 1.00
nC5 (LK) 2.12 20.00 18.75 1.25
C6 (HK) 1.00 30.00 1.15 28.85
C7 0.49 40.00 0.12 39.88
Nm 7.875748249
Mencari nilai
Mencari Rm
Rm+1 1.8146396092
Rm 0.8146396092
Rm/(Rm+1) 0.4489263902
R/(R+1) 0.7142857143
Page 7
Sheet3
N 9.3758907724
diambil N 10
Flow-rates
Feed 11130 kg/jam
Number of stage 10
slope of bottom 1.122647878
slope of top 0.8803166099
reflux ratio 2.5
Physical properties
column eficiency 0.6
Number of real stage 16.6666666667
17
column pressure drop 100 mmH2O/plate
column pressure drop 16677 Pa
Top pressure, 8 bar 800000 Pa
bottom pressure 783323 Pa
Page 8
Sheet3
Column diameter
slope atas 0.8803166099
slope bawah 1.122647878
K bottom 0.098
K top 0.075
Plate spacing 1m
bottom diameter 1.4705735268 m
top diameter 1.1503880914 m
Standard pipe size BS 1600
OD 1.68 m
ID 1.54 m
Page 9
Sheet3
Ad/Ac 0.12
lw/Dc 0.76 (Fig 11.31)
lw 1.1704 m
Take
Weir height, hw 100 mm
Hole diameter, dh 7 mm
Plate thickness 10 mm
Check weeping
Max liquid rate 16.8606882305 kg/s
Min liquid rate 11.8024817613 kg/s (70 per cent TD)
Page 10
Sheet3
hd 2.7302471289 mm liquid
residual head
hr 18.6266913036 mm liquid
Check entraintment
uv 19.1494869783 m/s
percent flooding 3174.466181625
Trial layout
use cartridge type layout
50 mm unperforated strip round plate edge
50 mm wide calming zone
Page 11
Sheet3
Perforated area
lw/Dc 0.76
Fig 11.32, tetta 99 degree
Number of hole
Area of one hole 3.8484510E-005 m^2
Number of hole 3678.4
Plate specification
Plate no 1
Plate I.D. 0,79 m
Hole size 7 mm
Hole pitch 17,5 mm
Active hole 978
Turn down 70 per cent max rate
Plate material Mild steel
Downcomer material Mild steel
Plate spacing 0,5 m
Plate thickness 5 mm
Plate pressure drop 147 mm liquid = 1,36 kPa
Page 12
Sheet3
V/K
1.39
5.71
10.00
25.97
29.41
0.58
73.07
Page 13
Sheet3
1.2
0.8
Page 14
0.6
y
0.4
1.2
1
Sheet3
0.8
0.6
y
0.4
0.2
0
0 0.2 0.4 0.6
x
bi
0.00
0.00
0.00
1.00
Page 15
Sheet3
1.25
28.85
39.88
Page 16
Sheet3
Page 17
Sheet3
Page 18
Sheet3
Page 19
Sheet3
Page 20
Sheet3
Page 21
Sheet3
Page 22
Sheet3
Page 23
Sheet3
Page 24
Sheet3
Page 25
Sheet3
Page 26
Sheet3
Page 27
Sheet3
Page 28
Sheet3
Page 29
Sheet3
Page 30
Sheet2
garis kesetimbangan
0.5 0.590640394
0.55 0.630788177
0.6 0.670935961
0.65 0.711083744
0.7 0.751231527
0.75 0.79137931
0.8 0.831527094
0.85 0.871674877
0.9 0.91182266
0.96 0.96
Page 31
Sheet2
q line
x y
0.56 0.56
0.56 0.6
0.56 0.6
0.56 0.735
1 cum
mp Heat of fussion
SbCl5 4 2400
H2O 0 1440 80 1 80
H2O2 -2 2520 74.11764706 1.45 107.4705882
H3PO2 17.4 2310
Icl(alpha) 17.2 2660
MoF6 17 2500
OsO4(yellow) 56 4060
SO3 17 2060
SnBr4 30 3000
Page 32
Sheet5
Design Menara Distilasi
Component Feed (kmol) di bi
C3 5 5 0
iC4 10 10 0
nC4 15 15 0
iC5 20 20 0
nC5 (LK) 20 19 1
C6 (HK) 30 2 28
C7 40 0 40
140 71 69
Page 33
Sheet5
iC5 2.6551724138 1.95 2.3025862069
nC5 (LK) 2.3448275862 1.9 2.1224137931
C6 (HK) 1 1 1
C7 0.4827586207 0.5 0.4913793103
Le 154.4629441845
Ve 175.4629441845
V'e 236.4492600423
L'e 265.4492600423
komposisi
xf 0.4
xd 0.9047619048
xb 0.0344827586
2.1224137931
1.2
0.8
0.6
Page 34
0.4
1
0.8
Sheet5
0.6
0.4
0.2
0
0 0.2 0.4 0.6 0.8 1 1.2
Component 0 0 0 0 bi
C3 10.2068965517 5 600000 4.9999916667 8.3333194E-006
iC4 4.9922413793 10 3950 9.9974689952 0.0025310048
nC4 4.2362068966 15 3100 14.9951628507 0.0048371493
iC5 2.3025862069 20 19 19 1
nC5 (LK) 2.1224137931 20 15 18.75 1.25
C6 (HK) 1 30 0.04 1.1538461538 28.8461538462
C7 0.4913793103 40 0.003 0.1196410768 39.8803589232
Component i fi di bi rho Mr
C3 10.2068965517 5 4.9999916667 8.3333194E-006 590 44
iC4 4.9922413793 10 9.9974689952 0.0025310048 600 58
nC4 4.2362068966 15 14.9951628507 0.0048371493 600 58
iC5 2.3025862069 20 19 1 630 72
nC5 (LK) 2.1224137931 20 18.75 1.25 630 72
C6 (HK) 1 30 1.1538461538 28.8461538462 660 86
C7 0.4913793103 40 0.1196410768 39.8803589232 680 100
Nm 7.875748249
rho top v 618.72
rho bottom v 671.09
Mencari nilai
Mencari Rm
Component 0 0 0 0
Page 35
Sheet5
C3 0.0724467318 10.2068965517 0.7394562973 0.0827419556
iC4 0.1448570325 4.9922413793 0.7231612716 0.1942811328
nC4 0.2172704705 4.2362068966 0.9204026654 0.3102961788
iC5 0.2752980398 2.3025862069 0.6338974692 0.6138930241
nC5 (LK) 0.2716756971 2.1224137931 0.5766082469 0.6764417135
C6 (HK) 0.0167185044 1 0.0167185044 -0.0619203868
C7 0.0017335239 0.4913793103 0.0008518178 -0.0010940087
1 1.8146396092
Rm+1 1.8146396092
Rm 0.8146396092
Rm/(Rm+1) 0.4489263902
R/(R+1) 0.7142857143
Nm/N 0.84 (Fig 11.11)
N 9.3758907724
diambil N 10
Flow-rates
Feed 11130 kg/jam
Number of stage 10
slope of bottom 1.122647878
slope of top 0.8803166099
reflux ratio 2.5
Physical properties
column eficiency 0.6
Number of real stage 16.6666666667
17
column pressure drop 100 mmH2O/plate
column pressure drop 16677 Pa
Top pressure, 8 bar 800000 Pa 7.8953861337
bottom pressure 783323 Pa 7.7307969405
Page 36
Sheet5
rho l 671.08
Mr bottom Err:501
Column diameter
slope atas 0.8803166099
slope bawah 1.122647878
K bottom 0.093
K top 0.092
Page 37
Sheet5
Page 38
Sheet5
Page 39
Sheet5
1.2
Ptop 7.8953861337
T top 363.7055555556
P bottom 7.7307969405
T bottom 422.0388888889
rho 671.0853320729
17.256
24.731
24.7311359301
Page 40
Sheet5
Page 41
Sheet5
Page 42
Sheet4
x yeq y x
0 0 0 0
0.05 0.100481593 0.05 0.05
0.1 0.190823128 0.1 0.1
0.15 0.272485797 0.15 0.15
0.2 0.346662912 0.2 0.2
0.25 0.414338607 0.25 0.25
0.3 0.476331743 0.3 y=x 0.3
0.35 0.533329207 0.35 y equilibrium 0.35
0.4 0.585911471 0.4 0.4
0.45 0.634572427 0.45 0.45
0.5 0.679734953 0.5 0.5
0.55 0.721763232 0.55 0.55
0.6 0.760972594 0.6 0.6
0.65 0.797637442 0.65 0.65
0.7 0.831997683 0.7 0.7
0.75 0.864263983 0.75 0.75
0.8 0.894622093 0.8 0.8
0.85 0.923236423 0.85 0.85
0.9 0.950253023 0.9 0.9
0.95 0.975802078 0.95 0.95
1 1 1 1
0.35 0.416395785
0.4 0.460411616 0.034482759 0.034482759
0.45 0.504427446 0.05 0.051903157
0.5 0.548443277 0.1 0.108035551
0.55 0.592459107 0.15 0.164167945
0.6 0.636474938 0.2 0.220300338
0.65 0.680490768 0.25 0.276432732
0.7 0.724506599 0.3 0.332565126
0.75 0.768522429 0.35 0.38869752
0.8 0.81253826 0.4 0.444829914
0.85 0.85655409 0.45 0.500962308
0.904761905 0.904761905
Page 43
Sheet4
Page 44
Sheet4
xf 0.4
xd 0.904761905
xb 0.034482759
xf y
0.4 0 0.4 0.4
0.4 0.4 0.4 0.585911471
xd y
0.904761905 0
0.904761905 0.904761905
xb y
0.034482759 0
0.034482759 0.034482759
Component i fi di bi msdds
C3 10.20689655 5 4.999991667 8.3333E-006 219.9996333 0.000366666
iC4 4.992241379 10 9.997468995 0.002531005 579.8532017 0.146798279
nC4 4.236206897 15 14.99516285 0.004837149 869.7194453 0.28055466
iC5 2.302586207 20 19 1 1368 72
nC5 (LK) 2.122413793 20 18.75 1.25 1350 90
C6 (HK) 1 30 1.153846154 28.84615385 99.23076923 2480.769231
C7 0.49137931 40 0.119641077 39.88035892 11.96410768 3988.035892
65.1843042 93.41884352
Component
C3
iC4
nC4
Page 45
Sheet4
iC5
nC5 (LK)
C6 (HK)
C7
Page 46