Analisis Kadar Gliserol Variable 1 : 6

T B S N W1 W2
t1 17.2 12.1 0.00934 1 4.1
t2 17.2 12.3 0.00934 1 4.7
t3 17.2 12.2 0.00934 1 4.8
t4 17.2 12 0.00934 1 4.8
t5 17.2 12.1 0.00934 1 5.0
t6 17.2 12.8 0.00934 1 4.8

Analisis asam awal 100C

(Vb Vt ) Nhcl
Ao t = 60
m

V blangko V HCL Ao

Analisis asam bebas 1:8

(VNaOH NNaOH )
Ab
m
 (VNaOH NNaOH )
Ab
m

V NaOH N NaOH Ab
10.5 0.67 7.035
9.1 0.67 6.097
8 0.67 5.36
8.4 0.67 5.628
8.2 0.67 5.494
9.4 0.67 6.298

suhu konversi
t1 = 99 74.6858
t2 = 98 78.7834
t3 = 98 78.8014
t4 = 109 77.9535
t5 = 110 79.2423
t6 = 110 81.3452

82
81.3452

80
78.7834 79.2423
78.8014
78 77.9535

76
Column D
74.6858
74

72

70
0 1 2 3 4 5 6 7
 Gb0 2,302 ( B S )( N )( 450 )(170 )
W 50 ( w )
bj

B = Volume titrasi Na2S2O3 untuk larutan blangko (mL)

S = Volume titrasi Na2S2O3 untuk larutan sampel (mL)
N = normalitas larutan Na2S2O3
W = berat sampel yang telah dilarutkan
w = berat sampel bahan baku

Gb0 = 82.497 %

Analisis Kadar Gliserol Variable 1 : 7

T B S N W1
t1 17.2 12.5 0.00934 1
t2 17.2 13.5 0.00934 1
t3 17.2 13 0.00934 1
t4 17.2 12.25 0.00934 1
t5 17.2 13 0.00934 1
t6 17.2 14 0.00934 1

Analisis Kadar Gliserol Variable 1 : 7

Gb % X% T B S N W1
24.0703 74.6858 t1 = 99 17.2 12.5 0.00934 1
20.1740 78.7834 t2 = 98 17.2 12.5 0.00934 1
20.1569 78.8014 t3 = 98 17.2 13 0.00934 1
20.9632 77.9535 t4 = 109 17.2 12.8 0.00934 1
19.7376 79.2423 t5 = 110 17.2 13 0.00934 1
17.7381 81.3452 t6 = 110 17.2 14 0.00934 1
Analisi asam awal 1:7
(Vb Vt ) Nhcl
Ao t = 60
m

V blangko V HCL Ao

Analisis asam bebas 1:7

(VNaOH NNaOH )
Ab
m
 V NaOH N NaOH Ab
21.5 0.72 15.48
23 0.72 16.56
28.5 0.72 20.52
24.1 0.72 17.352
29 0.72 20.88
24.2 0.72 17.424

suhu konversi
t1 = 99 79.99
t2 = 98 81.9532
88
t3 = 98 82.8712
t4 = 109 83.5701
86
t5 = 110 83.0074
t6 = 110 86.4046
84
82.
82 81.9532

80 79.99

78
81.3452

76
0 1 2 3

Column D

6 7
 82.49656
95.086

an blangko (mL)
an sampel (mL)

Analisis Kadar Gliserol Variable 1 : 8

W2 Gb % X% T B S N
4.78 19.0268 79.98995 t1 17.2 13.8 0.00934
4.92 14.5523 84.69566 t2 17.2 11.8 0.00934
4.99 16.2871 82.8712 t3 17.2 13 0.00934
4.55 21.0518 77.86029 t4 17.2 13.8 0.01152
5.03 16.1576 83.00742 t5 17.2 13.8 0.01152
4.79 12.9273 86.40458 t6 17.2 12.8 0.00934

Analisis Kadar Gliserol Variable 1 : 8

W2 Gb % X% T B S N
4.78 19.0268 79.9900 t1 = 96 17.2 12.5 0.00934
5.3 17.1600 81.9532 t2 = 96 17.2 12.7 0.00934
4.99 16.2871 82.8712 t3 = 100 17.2 13 0.00934
5.45 15.6225 83.5701 t4 = 100 17.2 13.8 0.01152
5.03 16.1576 83.0074 t5 = 101 17.2 13.8 0.01152
4.79 12.9273 86.4046 t6 = 104 17.2 12.8 0.00934
Analisis asam awal 1:8
(Vb Vt ) Nhcl
Ao
m

V blangko V HCL Ao
29 12.8 18.954

Analisis asam bebas 1:8

NaOH ) (VNaOH NNaOH )
Ab
m
 V NaOH N NaOH Ab
25.8 0.67 17.286
25.8 0.67 17.286
27 0.67 18.09
25.9 0.67 17.353
25.5 0.67 17.085
25.5 0.67 17.085

86.4046

83.5701
82.8712 83.0074
81.9532
Column N

79.99

1 2 3 4 5 6 7
 W1 W2 Gb % X%
1 5.2 12.6523 86.6938
1 5.4 19.3506 79.6494
1 5.2 15.6293 83.5629
1 5.1 15.9114 83.2663
1 5.1 15.9114 83.2663
1 5.1 16.6946 82.4426

W1 W2 Gb % X%
1 5.3 17.1600 81.9532
1 5.4 16.1255 83.0411
1 5.2 15.6293 83.5629
1 5.1 15.9114 83.2663
1 5.1 15.9114 83.2663
1 5.1 16.6946 82.4426

t = 60

H NNaOH )
m
suhu konversi
t1 = 96 81.9532 konversi
t2 = 96 83.0411
t3 = 98 83.5629 84
t4 = 109 83.2663 83.5 83.5629
t5 = 110 83.2663 83.2663
t6 = 110 82.4426 83 83.0411 83.2663

82.5 82.4426

82 81.9532

81.5

81
0 1 2 3 4 5 6 7
 83.2663

konversi
82.4426

5 6 7