TLC Rf TLC Rf TLC Rf TLC Rf TLC Rf

Acetophenone 2min 4min 6min 10min 15min AVG Rf GC peaks

Starting Material 0.68 0.72 0.73 0.76 0.78 0.734
co-spot (SM) 0.68 0.72 0.73 0.76 0.78 0.734
co-spot (product) 0.53 0.53 0.56 0.58 0.58 0.556 inconclusive
Product 0.68 0.72 0.73 0.76 0.78 0.734
SM in product lane 0.53 0.53 0.56 0.58 0.58 0.556
4-methoxy-
acetophenone
Starting Material 0.69 0.8 0.78 0.67 0.69 0.726
co-spot (SM) 0.69 0.78 0.78 0.67 0.69 0.722
co-spot (product) 0.53 0.62 0.62 0.5 0.52 0.558 Ret. Time =
3.95; area =
Product 0.51 0.62 0.62 0.5 0.52 0.554 1176; conc. =
SM in product lane 0.67 0.78 0.78 0.73 0.69 0.73 10.785
4-methyl-
acetophenone
Starting Material 0.58 0.56 0.56 0.58 0.64 0.584
co-spot (SM) 0.58 0.56 0.56 0.58 0.64 0.584
co-spot (product) 0.42 0.44 0.42 0.5 0.48 0.452 ret. Time =
2.641; area =
Product 0.58 0.56 0.56 0.58 0.64 0.584 2406; conc. =
SM in product lane 0.42 0.44 0.42 0.5 0.48 0.452 18.223
4-chloro-
acetophenone
Starting Material 0.88 0.9 0.95 0.93 0.93 0.918
co-spot (SM) 0.88 0.9 0.95 0.93 0.93 0.918 Ret. Time =
3.311; area =
co-spot (product) 0.63 0.65 0.68 0.68 0.65 0.658 2154; conc. =
Product 0.63 0.65 0.68 0.68 0.65 0.658 24.239
 IR

alcohol O-H ~ 3343.09

cm^-1; Aromatic C-H
~3062 cm^-1; alkane C-
H ~2972.36 cm^-1

inconclusive

inconclusive

alcohol O-H ~ 3329

cm^-1; Aromatic C-H
~3087 cm^-1; aromatic
C=C ~1492 cm^-1