Professional Documents
Culture Documents
hướng dẫn phân tích nhiệt PDF
hướng dẫn phân tích nhiệt PDF
TI LIU HNG DN
PHNG PHP PHN TCH NHIT
H Ni, 09 / 2015
MC LC
1. Phn tch nhit l g? .................................................................................. 3
2. Mt s ng cong c trng ca phn tch nhit ..................................... 4
3. Phn tch nhit ng thi ........................................................................... 6
3.1. TG (Phn tch nhit trng)................................................................... 6
3.2. Phn tch nhit vi sai DTA (Differential Thermal Analysis) .............. 8
3.3. Mt s ng cong in hnh ca TG-DTA ..................................... 11
4. DSC (Differential Scanning Calorimetry) ............................................... 12
4.1. S nguyn l ................................................................................. 12
Nguyn l ca loi b nng lng. ............................................... 12
c trng m hc Thermoacoustic
Thu vo Ta nhit
Mt i Thu nhit
Loi s dng cm bin vi sai theo phng ngang l k thut phn tch chnh
thng c s dng v s tri nhit do thay i khi lng biu kin khi tng nhit
l tng i nh so vi cc phng php khc.
H thng ThremoPlus EVO2 ca Rigaku l mt thit b p dng cm bin vi
sai theo phng ngang.
Mu o
iu khin
Bn mu PID
ca cn cn Mch o
nhit trng
Cun dy dn Cun
Cundy
dydn
S2
ng S1 ng S2
D liu
ra
Tm kim loi
mang mu
(cm bin, Pt)
B kt ni
Cp nhit in ng alumin
Mi ni Mi ni
Cp nhit in Mi ni Cp nhit in (mu so snh) (mu o)
vi sai
in p
in p
in p
L t
Nhit mu o
Mch b tr nhit
Thi gian
Ta nhit
Mch DTA
Nhit mu o
Thu nhit
Tn hiu ra
ng c s
xy ha, Hp ph Bin i t
4.1. S nguyn l
Tm kim loi
(cm bin)
Cp nhit in
Cp nhit in
Si t
Cp nhit in Si t
: Gi tr l thuyt, n v tnh J
E: Gi tr nng lng
Thng hoa,
Kh nc
Phng php ti nn
Cun dy
Nam chm
H thng cn
in t
Mch iu khin
ti trng
Qu cn chun Ti nn
B chuyn
i vi sai Mch pht hin
chuyn di
Que d
Thanh t
Cp nhit in
ng
Mch iu khin
nhit
Mu so snh Mu o
Li
Cun th cp S1
S2
Cun s cp P
B chuyn i
vi sai
Chuyn ng
theo phng Y
Cun dy
Nam chm
H thng cn
in t Mch iu khin
ti trng
Qu cn chun Ti ko
B chuyn
i vi sai
Mch pht hin
Thc trc vi chuyn di
ng Que d
Mu
Thanh t Mch iu khin
nhit
Cp nhit in
Ngm kp
kim loi
Cun dy
Nam chm
H thng cn
in t
Mch iu khin
ti trng
Qu cn chun
Ti nn
B chuyn
i vi sai Mch pht hin
chuyn di
Que d
Thanh t
Mi nhn
Mu
Cp nhit in Mch iu khin
nhit
ng
S chy do
S chuyn pha thy tinh
S nung kt