BAB IV

HASIL DAN PEMBAHASAN

4.1 Hasil Pengamatan

Tabel 1. Penentuan densitas dan viskositas larutan

Bobot Waktu (detik)

No. Piknometer Bobot
+ Larutan Larutan (g) Rata- Suhu
Larutan
(g) 1 2 Rata (C)
(detik)

1 Akuades 44,4364 24,7001 62 63 62,5 27

2 Gliserol 2 % 44,5855 24,8492 65 66 65,5 31

3 Gliserol 4 % 44,7311 24,9948 72 72 72 28

4 Gliserol 6 % 44,8657 25,1294 73 73 73 30

5 Gliserol 8 % 44,4700 25,7381 77 76 76,5 31

6 Gliserol 10 % 44,5986 25,8667 79 80 79,5 30

7 Gliserol X % 44,0275 25,2956 65 64 64,5 29

Keterangan:

Bobot piknometer kosong = 18,7319 g dan 19,7363 g

a (27oC) = 0,8937 cP

4.2 Penentuan Konsentrasi Gliserol X %

Tabel 2. Penentuan konsentrasi gliserol X %

No. Larutan Konsentrasi (%) (x) Viskositas (cP) (y)

1 Gliserol 2 % 2 0,9411

2 Gliserol 4 % 4 1,0411

3 Gliserol 6 % 6 1,0610
 4 Gliserol 8 % 8 1,1384

5 Gliserol 10 % 10 1,1894

6 Gliserol X % X 0,9439

Tabel 3. Perhitungan regresi manual

x Y xy x2 y2
2 0,9411 1,8822 4 0,8856
4 1,0411 4,1644 16 1,0838
6 1,0610 6,3660 36 1,1257
8 1,1384 9,1072 64 1,2959
10 1,1894 11,8940 100 1,4146
x = 30 y =5,3710 xy = 33,4138 x2 = 220 y2 = 5,8056
Lampiran 2.

Perhitungan

Perhitungan Densitas Larutan

a. Akuades

t bobot akuades 24,7001 g

Sg = = = 1,0000
bobot akuades 24,7001 g

dtaq (27 C) = 0,996512 g/cm3

a = Stg x dtaq (27 C)

= 1,0000 x 0,996512 g/cm3

= 0,9965 g/cm3

b. Gliserol 2 %

t bobot gliserol 2 % 24,8492 g

Sg = = = 1,0060
bobot akuades 24,7001 g

dtaq (31 C) = 0,995369 g/cm3

c = Stg x dtaq (31 C)

= 1,0060 x 0,995369 g/cm3

= 1,0013 g/cm3

c. Gliserol 4 %

t bobot gliserol 4 % 24,9948 g

Sg = = = 1,0119
bobot akuades 24,7001 g

dtaq (28 C) = 0,996232 g/cm3

c = Stg x dtaq (28 C)

= 1,0119 x 0,996232 g/cm3

= 1,0080 g/cm3

d. Gliserol 6 %

t bobot gliserol 6 % 25,1294 g

Sg = = = 1,0173
bobot akuades 24,7001 g

dtaq (30 C) = 0,995676 g/cm3

c = Stg x dtaq (30 C)

= 1,0173 x 0,995676 g/cm3

= 1,0129 g/cm3

e. Gliserol 8 %

t bobot gliserol 8 % 25,7381 g

Sg = = = 1,0420
bobot akuades 24,7001 g

dtaq (31 C) = 0,995369 g/cm3

c = Stg x dtaq (31 C)

= 1,0420 x 0,995369g/cm3

= 1,0371 g/cm3

f. Gliserol 10 %

t bobot gliserol 10 % 25,8667 g

Sg = = = 1,0472
bobot akuades 24,7001 g
dtaq (30 C) = 0,995676 g/cm3

c = Stg x dtaq (30 C)

= 1,0472 x 0,995676 g/cm3

= 1,0427 g/cm3

g. Gliserol X %

t bobot gliserol X % 25,2956 g

Sg = = = 1,0241
bobot akuades 24,7001 g

dtaq (29 C) = 0,995944 g/cm3

c = Stg x dtaq (29 C)

= 1,0241 x 0,995944 g/cm3

= 1,0199 g/cm3

Perhitungan Viskositas Larutan

a. Gliserol 2 %

c tc
c = x a
a ta

1,0013 g/cm3 x 65,5 s

= x 0,8937 cP
0,9965 g/cm3 x 62,5 s

= 0,9411 cP

b. Gliserol 4 %

c tc
c = a
a ta

1,0080 g/cm3 x 72 s
= 0,8937 cP
0,9965 g/cm3 x 62,5 s
 = 1,0414 cP

c. Gliserol 6 %

c tc
c = a
a ta

1,0129 g/cm3 x 73 s
= 0,8937 cP
0,9965 g/cm3 x 62,5 s

= 1,0610 cP

d. Gliserol 8 %

c tc
c = a
a ta

1,0371 g/cm3 x 76,5 s

= 0,8937 cP
0,9965 g/cm3 x 62,5 s

= 1,1384 cP

e. Gliserol 10 %

c tc
c = a
a ta

1,0427 g/cm3 x 79,5 s

= 0,8937 cP
0,9965 g/cm3 x 62,5 s

= 1,1894 cP

f. Gliserol X %

c tc
c = a
a ta

1,0199 g/cm3 x 64,5 s

= 0,8937 cP
0,9965 g/cm3 x 62,5 s
 = 0,9439 cP

Perhitungan Regresi Manual

y = ax + b

y.(x2 )(x)(xy)
b=
n(x2 ) (x)2

(5,3710) (220) - (30) (33,4138)

b=
5(220) - (30)2

= 0,8960
n(xy) (x)(y)
a =
n(x2 ) (x)2

5(33,4138) - (30) (5,3710)

=
5(220) - (30)2
= 0,0296

y = 0,0296x + 0,8960

2
((n.xy) (x.y))2
R =
((n.x2 )- (x)2 ) ((n.y2 )- (y)2 )
2
2 ((5 x 33,4138) (30 x 5,3710) )
R = 2 2
((5 x 220)(30) ) (5 x 5,8056) (5,3710) )
= 0,9775

R2 = 0,9775

a. Gliserol 2 %

y = 0,0296x + 0,8960

= 0,0296 (2) + 0,8960

= 0,9552

b. Gliserol 4 %

y = 0,0296x + 0,8960
 = 0,0296 (4) + 0,8960

= 1,0144

c. Gliserol 6 %

y = 0,0296x + 0,8960

= 0,0296 (6) + 0,8960

= 1,0736

d. Gliserol 8 %

y = 0,0296x + 0,8960

= 0,0296 (8) + 0,8960

= 1,1328

e. Gliserol 10 %

y = 0,0296x + 0,8960

= 0,0296 (10) + 0,8960

= 1,1920

Perhitungan Konsentrasi Gliserol X %

y = ax + b

y-b
x=
a

0,9439 - 0,8960
=
0,0296
 = 1,6182

Jadi, konsentrasi gliserol X % adalah 1,6182 %.